CN1041414C - 制备3-(甲硫基)丙醛的方法 - Google Patents

制备3-(甲硫基)丙醛的方法 Download PDF

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Publication number
CN1041414C
CN1041414C CN93118591A CN93118591A CN1041414C CN 1041414 C CN1041414 C CN 1041414C CN 93118591 A CN93118591 A CN 93118591A CN 93118591 A CN93118591 A CN 93118591A CN 1041414 C CN1041414 C CN 1041414C
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CN
China
Prior art keywords
gas
liquid
acrolein
methylthio
reaction
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Expired - Fee Related
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CN93118591A
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English (en)
Chinese (zh)
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CN1096779A (zh
Inventor
Y·C·徐
D·A·鲁思特
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Novus International Inc
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Novus International Inc
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Publication of CN1096779A publication Critical patent/CN1096779A/zh
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Publication of CN1041414C publication Critical patent/CN1041414C/zh
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C07C319/18—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by addition of thiols to unsaturated compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
    • C07C45/34—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds
    • C07C45/35—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds in propene or isobutene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/783—Separation; Purification; Stabilisation; Use of additives by gas-liquid treatment, e.g. by gas-liquid absorption
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00716—Means for reactor start-up

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN93118591A 1993-06-08 1993-10-09 制备3-(甲硫基)丙醛的方法 Expired - Fee Related CN1041414C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/073,763 1993-06-08
US08/073,763 US5352837A (en) 1993-06-08 1993-06-08 Process for the preparation of 3-(methylthio)propanal

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CN 98115072 Division CN1222507A (zh) 1993-06-08 1998-06-24 制备3－(甲硫基)丙醛的方法

Publications (2)

Publication Number Publication Date
CN1096779A CN1096779A (zh) 1994-12-28
CN1041414C true CN1041414C (zh) 1998-12-30

Family

ID=22115663

Family Applications (1)

Application Number Title Priority Date Filing Date
CN93118591A Expired - Fee Related CN1041414C (zh) 1993-06-08 1993-10-09 制备3-(甲硫基)丙醛的方法

Country Status (15)

Country Link
US (1) US5352837A (enExample)
EP (2) EP0889029A3 (enExample)
JP (1) JPH09501145A (enExample)
KR (1) KR100274685B1 (enExample)
CN (1) CN1041414C (enExample)
AT (1) ATE178594T1 (enExample)
BR (1) BR9307864A (enExample)
DE (1) DE69324380T2 (enExample)
DK (1) DK0703890T3 (enExample)
ES (1) ES2131120T3 (enExample)
RU (1) RU2118314C1 (enExample)
SG (1) SG43158A1 (enExample)
TW (1) TW270925B (enExample)
WO (1) WO1994029254A1 (enExample)
ZA (1) ZA935850B (enExample)

Families Citing this family (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5925794A (en) * 1993-06-08 1999-07-20 Novus International, Inc. Process for the preparation of 3-(methylthio)propanal
US5905171A (en) 1995-06-22 1999-05-18 Novus International, Inc. Process for the preparation of 3-(methylthio)propanal
US5637766A (en) * 1993-06-08 1997-06-10 Novus International, Inc. Process for the preparation of 3-(methylthio) propanal
AU699841B2 (en) * 1994-07-11 1998-12-17 Novus International Inc Process for the preparation of 3-(methylthio)propanal
US5663409A (en) * 1995-06-07 1997-09-02 Novus International, Inc. Process for the preparation of 3-(methylthio) propanal and 2-hydroxy-4-(methylthio) butanenitrile
DE69615183T2 (de) * 1995-06-07 2002-05-29 Novus International, Inc. Kontinuerliches hydrolyse-verfahren zur herstellung von 2-hydroxy-4-methylthiobutansäure oder salze davon
FR2735989B1 (fr) * 1995-06-29 1997-08-14 Rhone Poulenc Nutrition Animal Procede et installation de purification d'un flux gazeux contenant de l'acroleine
CN1042742C (zh) * 1995-11-02 1999-03-31 中国石化兰州炼油化工总厂 一种润滑油添加剂的制备方法
US5825369A (en) * 1996-01-16 1998-10-20 International Business Machines Corporation Compression of simple geometric models using spanning trees
DE69722195T2 (de) * 1996-04-01 2004-04-01 Union Carbide Chemicals & Plastics Technology Corp., Danbury Verfahren zur herstellung von methylmercatopropanal
US6166263A (en) * 1997-03-27 2000-12-26 Union Carbide Chemicals & Plastics Technology Corporation Processes for the manufacture of acrolein
US6187963B1 (en) 1997-03-27 2001-02-13 Union Carbide Chemicals & Plastics Technology Corporation Processes for the manufacture of acrolein derivatives
NL1007442C2 (nl) * 1997-11-04 1998-12-07 Josephus Johannes Petrus Maria Batch-Continue tegenstroomapparatuur met superieure performance.
US6342651B1 (en) 1999-08-05 2002-01-29 Novus International, Inc. Reductive combustion of ammonium salts of sulfuric acid
FR2835831B1 (fr) * 2002-02-12 2006-09-01 Aventis Animal Nutrition Sa Procede de purification de l'acroleine
RU2223814C2 (ru) * 2002-04-23 2004-02-20 Московский государственный университет инженерной экологии Аппарат для контактирования газа и жидкости
JP4186572B2 (ja) * 2002-09-27 2008-11-26 住友化学株式会社 ３−メチルチオプロパナールの製造方法
DE102004038053A1 (de) 2004-08-05 2006-04-27 Degussa Ag Verfahren zur Herstellung von 3-(Methylthio)propanal
DE102005003990A1 (de) * 2005-01-28 2006-08-03 Degussa Ag Herstellung von 3-(Alkylthio)propanal
JP2010111642A (ja) * 2008-11-07 2010-05-20 Sumitomo Chemical Co Ltd メチオニンの製造方法
FR2938535B1 (fr) 2008-11-20 2012-08-17 Arkema France Procede de fabrication de methylmercaptopropionaldehyde et de methionine a partir de matieres renouvelables
JP5182198B2 (ja) * 2009-04-06 2013-04-10 住友化学株式会社 ３−メチルチオプロパナールの製造方法
JP5402864B2 (ja) 2010-07-20 2014-01-29 住友化学株式会社 ３−メチルチオプロパナールの製造方法
DE102010064250A1 (de) * 2010-12-28 2012-06-28 Evonik Degussa Gmbh Verfahren zur Herstellung von Methylmercaptopropionaldehyd
EP2679579A1 (de) 2012-06-27 2014-01-01 Evonik Industries AG Integriertes Verfahren zur Herstellung von Acrolein und 3-Methylmercaptopropionaldehyd
EP3205643A1 (de) * 2016-02-15 2017-08-16 Evonik Degussa GmbH Verfahren zur herstellung von 3-methylthiopropionaldehyd
CN111116437B (zh) * 2018-11-01 2021-02-05 山东新和成氨基酸有限公司 制备2-羟基-4-甲硫基丁酸及其中间体的方法和装置
EP4178944B1 (en) * 2020-07-08 2024-06-26 Evonik Operations GmbH Process for preparing 3-methylthiopropionaldehyde
WO2023118974A1 (en) * 2021-12-24 2023-06-29 Vinati Organics Limited An agitator reactor for synthesis of acrylamido tertiary butyl sulfonic acid and process implemented thereon

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4048232A (en) * 1973-04-21 1977-09-13 Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler Process for the production of 3-methylmercaptopropionaldehyde
US4225516A (en) * 1975-06-20 1980-09-30 Rhone-Poulenc Industries Process for the manufacture of beta-methylthiopropionaldehyde

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA797873A (en) * 1968-10-29 Sumitomo Chemical Company PROCESS FOR PRODUCING .beta.-METHYLMERCAPTOPROPIONALDEHYDE
CA820968A (en) * 1969-08-19 Shima Takesaburo PROCESS FOR PRODUCING HIGH PURITY .beta.-METHYLMERCAPTOPROPIONALDEHYDE
US2542768A (en) * 1945-10-24 1951-02-20 Du Pont Hydroxy-methylmercaptobutyronitrile
US2564105A (en) * 1949-08-03 1951-08-14 Du Pont Aqueous methionine nitrile sulfate
US2626282A (en) * 1949-10-05 1953-01-20 Standard Oil Dev Co Vapor phase production of betamethylmercaptopropionaldehyde
US2676190A (en) * 1951-10-23 1954-04-20 Du Pont Process for the manufacture of beta-methylmercapto-propionaldehyde
US2776996A (en) * 1955-12-22 1957-01-08 Du Pont Manufacture of beta-methylmercaptopropionaldehyde
NL6705426A (enExample) * 1966-04-18 1967-10-19
US3529940A (en) * 1966-04-25 1970-09-22 Sumitomo Chemical Co Apparatus for two-stage production of beta-methylmercaptopropionaldehyde
DE1618884B1 (de) * 1966-04-25 1971-09-16 Sumitomo Chemical Co Verfahren zur Herstellung von 3-Methylmercaptoproionaldehyd
ES339942A1 (es) * 1966-04-30 1968-05-16 Sumitomo Chemical Co Un procedimiento para producir betametilmercaptopropional- dehido.
NL132124C (enExample) * 1966-09-02
CH491882A (de) * 1967-10-13 1970-06-15 Glanzstoff Ag Verfahren zur Herstellung von B-Methylmercaptopropionaldehyd
NL6809647A (enExample) * 1968-07-09 1970-01-13
JPS49818B1 (enExample) * 1970-08-12 1974-01-10
JPS4856144A (enExample) * 1971-11-12 1973-08-07
BE791831A (fr) * 1971-11-26 1973-03-16 Degussa Procede d'obtention de 3-methylmercaptopropionaldehyde pur
FR2460925A1 (fr) * 1979-07-10 1981-01-30 Rhone Poulenc Ind Procede de preparation directe d'aldehyde beta-methylthiopropionique
US5198578A (en) * 1986-07-17 1993-03-30 Union Carbide Chemicals Anhydrous diluents for the propylene oxidation reaction to acrolein and acrolein oxidation to acrylic acid
US5183936A (en) * 1986-08-21 1993-02-02 Union Carbide Chemicals & Plastics Technology Corporation Anhydrous diluent process for the propylene oxidation reaction to acrolein and acrolein oxidation to acrylic acid
US5155262A (en) * 1988-09-26 1992-10-13 Union Carbide Chemicals & Plastics Technology Corporation Anhydrous diluents for the isobutylene oxidation reaction to methacrolein and methacrolein oxidation to methacrylic acid

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4048232A (en) * 1973-04-21 1977-09-13 Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler Process for the production of 3-methylmercaptopropionaldehyde
US4225516A (en) * 1975-06-20 1980-09-30 Rhone-Poulenc Industries Process for the manufacture of beta-methylthiopropionaldehyde

Also Published As

Publication number Publication date
AU673856B2 (en) 1996-11-28
EP0889029A2 (en) 1999-01-07
ES2131120T3 (es) 1999-07-16
JPH09501145A (ja) 1997-02-04
US5352837A (en) 1994-10-04
EP0703890A1 (en) 1996-04-03
SG43158A1 (en) 1997-10-17
TW270925B (enExample) 1996-02-21
CN1096779A (zh) 1994-12-28
ATE178594T1 (de) 1999-04-15
ZA935850B (en) 1994-05-25
EP0703890B1 (en) 1999-04-07
AU5126893A (en) 1995-01-03
DK0703890T3 (da) 1999-10-18
RU2118314C1 (ru) 1998-08-27
DE69324380T2 (de) 1999-08-26
KR100274685B1 (ko) 2000-12-15
EP0889029A3 (en) 2002-03-13
BR9307864A (pt) 1996-01-23
DE69324380D1 (de) 1999-05-12
EP0703890A4 (en) 1996-10-30
WO1994029254A1 (en) 1994-12-22

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