ATE178594T1 - Verfahren zur herstellung von 3-(methylthio) propanal - Google Patents
Verfahren zur herstellung von 3-(methylthio) propanalInfo
- Publication number
- ATE178594T1 ATE178594T1 AT93922171T AT93922171T ATE178594T1 AT E178594 T1 ATE178594 T1 AT E178594T1 AT 93922171 T AT93922171 T AT 93922171T AT 93922171 T AT93922171 T AT 93922171T AT E178594 T1 ATE178594 T1 AT E178594T1
- Authority
- AT
- Austria
- Prior art keywords
- acrolein
- propanal
- methylthio
- gas
- feed stream
- Prior art date
Links
- CLUWOWRTHNNBBU-UHFFFAOYSA-N 3-methylthiopropanal Chemical compound CSCCC=O CLUWOWRTHNNBBU-UHFFFAOYSA-N 0.000 title abstract 4
- 238000004519 manufacturing process Methods 0.000 title 1
- HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 abstract 12
- LSDPWZHWYPCBBB-UHFFFAOYSA-N Methanethiol Chemical compound SC LSDPWZHWYPCBBB-UHFFFAOYSA-N 0.000 abstract 6
- 239000007788 liquid Substances 0.000 abstract 5
- 239000007795 chemical reaction product Substances 0.000 abstract 3
- 239000012429 reaction media Substances 0.000 abstract 3
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
- C07C319/18—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by addition of thiols to unsaturated compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
- C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
- C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
- C07C45/34—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds
- C07C45/35—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds in propene or isobutene
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/783—Separation; Purification; Stabilisation; Use of additives by gas-liquid treatment, e.g. by gas-liquid absorption
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00716—Means for reactor start-up
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/073,763 US5352837A (en) | 1993-06-08 | 1993-06-08 | Process for the preparation of 3-(methylthio)propanal |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE178594T1 true ATE178594T1 (de) | 1999-04-15 |
Family
ID=22115663
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT93922171T ATE178594T1 (de) | 1993-06-08 | 1993-09-09 | Verfahren zur herstellung von 3-(methylthio) propanal |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US5352837A (de) |
| EP (2) | EP0889029A3 (de) |
| JP (1) | JPH09501145A (de) |
| KR (1) | KR100274685B1 (de) |
| CN (1) | CN1041414C (de) |
| AT (1) | ATE178594T1 (de) |
| BR (1) | BR9307864A (de) |
| DE (1) | DE69324380T2 (de) |
| DK (1) | DK0703890T3 (de) |
| ES (1) | ES2131120T3 (de) |
| RU (1) | RU2118314C1 (de) |
| SG (1) | SG43158A1 (de) |
| TW (1) | TW270925B (de) |
| WO (1) | WO1994029254A1 (de) |
| ZA (1) | ZA935850B (de) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5905171A (en) * | 1995-06-22 | 1999-05-18 | Novus International, Inc. | Process for the preparation of 3-(methylthio)propanal |
| US5925794A (en) * | 1993-06-08 | 1999-07-20 | Novus International, Inc. | Process for the preparation of 3-(methylthio)propanal |
| US5637766A (en) * | 1993-06-08 | 1997-06-10 | Novus International, Inc. | Process for the preparation of 3-(methylthio) propanal |
| RU2149159C1 (ru) * | 1994-07-11 | 2000-05-20 | Новус Интернэшнл, Инк. | Способ непрерывного получения 3-(метилтио)-пропаналя (варианты) |
| ES2164244T3 (es) * | 1995-06-07 | 2002-02-16 | Novus Int Inc | Procedimiento de hidrolisis en continuo para la preparacion de acido 2-hidroxi-4-metiltiobutanoico y sales del mismo. |
| US5663409A (en) * | 1995-06-07 | 1997-09-02 | Novus International, Inc. | Process for the preparation of 3-(methylthio) propanal and 2-hydroxy-4-(methylthio) butanenitrile |
| FR2735989B1 (fr) * | 1995-06-29 | 1997-08-14 | Rhone Poulenc Nutrition Animal | Procede et installation de purification d'un flux gazeux contenant de l'acroleine |
| CN1042742C (zh) * | 1995-11-02 | 1999-03-31 | 中国石化兰州炼油化工总厂 | 一种润滑油添加剂的制备方法 |
| US5825369A (en) * | 1996-01-16 | 1998-10-20 | International Business Machines Corporation | Compression of simple geometric models using spanning trees |
| US6057481A (en) * | 1996-04-01 | 2000-05-02 | Union Carbide Chemicals & Plastics Technology Corporation | Processes for the manufacture of methylmercaptopropanal |
| US6187963B1 (en) | 1997-03-27 | 2001-02-13 | Union Carbide Chemicals & Plastics Technology Corporation | Processes for the manufacture of acrolein derivatives |
| US6166263A (en) * | 1997-03-27 | 2000-12-26 | Union Carbide Chemicals & Plastics Technology Corporation | Processes for the manufacture of acrolein |
| NL1007442C2 (nl) * | 1997-11-04 | 1998-12-07 | Josephus Johannes Petrus Maria | Batch-Continue tegenstroomapparatuur met superieure performance. |
| US6342651B1 (en) | 1999-08-05 | 2002-01-29 | Novus International, Inc. | Reductive combustion of ammonium salts of sulfuric acid |
| FR2835831B1 (fr) * | 2002-02-12 | 2006-09-01 | Aventis Animal Nutrition Sa | Procede de purification de l'acroleine |
| JP4186572B2 (ja) * | 2002-09-27 | 2008-11-26 | 住友化学株式会社 | ３−メチルチオプロパナールの製造方法 |
| DE102004038053A1 (de) | 2004-08-05 | 2006-04-27 | Degussa Ag | Verfahren zur Herstellung von 3-(Methylthio)propanal |
| DE102005003990A1 (de) * | 2005-01-28 | 2006-08-03 | Degussa Ag | Herstellung von 3-(Alkylthio)propanal |
| JP2010111642A (ja) * | 2008-11-07 | 2010-05-20 | Sumitomo Chemical Co Ltd | メチオニンの製造方法 |
| FR2938535B1 (fr) | 2008-11-20 | 2012-08-17 | Arkema France | Procede de fabrication de methylmercaptopropionaldehyde et de methionine a partir de matieres renouvelables |
| JP5182198B2 (ja) | 2009-04-06 | 2013-04-10 | 住友化学株式会社 | ３−メチルチオプロパナールの製造方法 |
| JP5402864B2 (ja) | 2010-07-20 | 2014-01-29 | 住友化学株式会社 | ３−メチルチオプロパナールの製造方法 |
| DE102010064250A1 (de) * | 2010-12-28 | 2012-06-28 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Methylmercaptopropionaldehyd |
| EP2679579A1 (de) | 2012-06-27 | 2014-01-01 | Evonik Industries AG | Integriertes Verfahren zur Herstellung von Acrolein und 3-Methylmercaptopropionaldehyd |
| EP3205643A1 (de) * | 2016-02-15 | 2017-08-16 | Evonik Degussa GmbH | Verfahren zur herstellung von 3-methylthiopropionaldehyd |
| CN111116437B (zh) * | 2018-11-01 | 2021-02-05 | 山东新和成氨基酸有限公司 | 制备2-羟基-4-甲硫基丁酸及其中间体的方法和装置 |
| WO2023118974A1 (en) * | 2021-12-24 | 2023-06-29 | Vinati Organics Limited | An agitator reactor for synthesis of acrylamido tertiary butyl sulfonic acid and process implemented thereon |
Family Cites Families (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA797873A (en) * | 1968-10-29 | Sumitomo Chemical Company | PROCESS FOR PRODUCING .beta.-METHYLMERCAPTOPROPIONALDEHYDE | |
| CA820968A (en) * | 1969-08-19 | Shima Takesaburo | PROCESS FOR PRODUCING HIGH PURITY .beta.-METHYLMERCAPTOPROPIONALDEHYDE | |
| US2542768A (en) * | 1945-10-24 | 1951-02-20 | Du Pont | Hydroxy-methylmercaptobutyronitrile |
| US2564105A (en) * | 1949-08-03 | 1951-08-14 | Du Pont | Aqueous methionine nitrile sulfate |
| US2626282A (en) * | 1949-10-05 | 1953-01-20 | Standard Oil Dev Co | Vapor phase production of betamethylmercaptopropionaldehyde |
| US2676190A (en) * | 1951-10-23 | 1954-04-20 | Du Pont | Process for the manufacture of beta-methylmercapto-propionaldehyde |
| US2776996A (en) * | 1955-12-22 | 1957-01-08 | Du Pont | Manufacture of beta-methylmercaptopropionaldehyde |
| NL6705426A (de) * | 1966-04-18 | 1967-10-19 | ||
| DE1618884B1 (de) * | 1966-04-25 | 1971-09-16 | Sumitomo Chemical Co | Verfahren zur Herstellung von 3-Methylmercaptoproionaldehyd |
| US3529940A (en) * | 1966-04-25 | 1970-09-22 | Sumitomo Chemical Co | Apparatus for two-stage production of beta-methylmercaptopropionaldehyde |
| ES339942A1 (es) * | 1966-04-30 | 1968-05-16 | Sumitomo Chemical Co | Un procedimiento para producir betametilmercaptopropional- dehido. |
| NL132124C (de) * | 1966-09-02 | |||
| CH491882A (de) * | 1967-10-13 | 1970-06-15 | Glanzstoff Ag | Verfahren zur Herstellung von B-Methylmercaptopropionaldehyd |
| NL6809647A (de) * | 1968-07-09 | 1970-01-13 | ||
| JPS49818B1 (de) * | 1970-08-12 | 1974-01-10 | ||
| JPS4856144A (de) * | 1971-11-12 | 1973-08-07 | ||
| BE791831A (fr) * | 1971-11-26 | 1973-03-16 | Degussa | Procede d'obtention de 3-methylmercaptopropionaldehyde pur |
| DE2320544C2 (de) * | 1973-04-21 | 1975-06-05 | Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt | Verfahren zur Herstellung von 3-Methylmercaptopropionaldehyd |
| FR2314917A1 (fr) * | 1975-06-20 | 1977-01-14 | Rhone Poulenc Ind | Procede de fabrication de l'aldehyde beta-methylthiopropionique |
| FR2460925A1 (fr) * | 1979-07-10 | 1981-01-30 | Rhone Poulenc Ind | Procede de preparation directe d'aldehyde beta-methylthiopropionique |
| US5198578A (en) * | 1986-07-17 | 1993-03-30 | Union Carbide Chemicals | Anhydrous diluents for the propylene oxidation reaction to acrolein and acrolein oxidation to acrylic acid |
| US5183936A (en) * | 1986-08-21 | 1993-02-02 | Union Carbide Chemicals & Plastics Technology Corporation | Anhydrous diluent process for the propylene oxidation reaction to acrolein and acrolein oxidation to acrylic acid |
| US5155262A (en) * | 1988-09-26 | 1992-10-13 | Union Carbide Chemicals & Plastics Technology Corporation | Anhydrous diluents for the isobutylene oxidation reaction to methacrolein and methacrolein oxidation to methacrylic acid |
-
1993
- 1993-06-08 US US08/073,763 patent/US5352837A/en not_active Expired - Fee Related
- 1993-08-11 ZA ZA935850A patent/ZA935850B/xx unknown
- 1993-09-09 DE DE69324380T patent/DE69324380T2/de not_active Expired - Fee Related
- 1993-09-09 EP EP98114518A patent/EP0889029A3/de not_active Withdrawn
- 1993-09-09 RU RU96100238/04A patent/RU2118314C1/ru not_active IP Right Cessation
- 1993-09-09 EP EP93922171A patent/EP0703890B1/de not_active Expired - Lifetime
- 1993-09-09 WO PCT/US1993/008552 patent/WO1994029254A1/en active IP Right Grant
- 1993-09-09 BR BR9307864A patent/BR9307864A/pt not_active Application Discontinuation
- 1993-09-09 DK DK93922171T patent/DK0703890T3/da active
- 1993-09-09 SG SG1996004573A patent/SG43158A1/en unknown
- 1993-09-09 KR KR1019950705025A patent/KR100274685B1/ko not_active IP Right Cessation
- 1993-09-09 AT AT93922171T patent/ATE178594T1/de active
- 1993-09-09 JP JP7501709A patent/JPH09501145A/ja not_active Ceased
- 1993-09-09 ES ES93922171T patent/ES2131120T3/es not_active Expired - Lifetime
- 1993-10-05 TW TW082108204A patent/TW270925B/zh active
- 1993-10-09 CN CN93118591A patent/CN1041414C/zh not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| JPH09501145A (ja) | 1997-02-04 |
| EP0703890A4 (de) | 1996-10-30 |
| SG43158A1 (en) | 1997-10-17 |
| ES2131120T3 (es) | 1999-07-16 |
| KR100274685B1 (ko) | 2000-12-15 |
| EP0703890A1 (de) | 1996-04-03 |
| BR9307864A (pt) | 1996-01-23 |
| EP0889029A3 (de) | 2002-03-13 |
| CN1041414C (zh) | 1998-12-30 |
| WO1994029254A1 (en) | 1994-12-22 |
| EP0889029A2 (de) | 1999-01-07 |
| AU673856B2 (en) | 1996-11-28 |
| US5352837A (en) | 1994-10-04 |
| EP0703890B1 (de) | 1999-04-07 |
| DE69324380D1 (de) | 1999-05-12 |
| DE69324380T2 (de) | 1999-08-26 |
| AU5126893A (en) | 1995-01-03 |
| RU2118314C1 (ru) | 1998-08-27 |
| DK0703890T3 (da) | 1999-10-18 |
| ZA935850B (en) | 1994-05-25 |
| TW270925B (de) | 1996-02-21 |
| CN1096779A (zh) | 1994-12-28 |
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