CN104138027A - Tobacco moisturizing agent and preparation method and application thereof - Google Patents

Tobacco moisturizing agent and preparation method and application thereof Download PDF

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Publication number
CN104138027A
CN104138027A CN201410320056.5A CN201410320056A CN104138027A CN 104138027 A CN104138027 A CN 104138027A CN 201410320056 A CN201410320056 A CN 201410320056A CN 104138027 A CN104138027 A CN 104138027A
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China
Prior art keywords
tobacco
levan
maltotriose
humectant
cigarette
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CN201410320056.5A
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Chinese (zh)
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CN104138027B (en
Inventor
张磊
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Shandong Meichen Ecology & Environment Co ltd
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Jin Mei Bio Tech Ltd Shandong
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Abstract

The invention discloses a tobacco moisturizing agent and a preparation method and application thereof. The tobacco moisturizing agent consists of water solution of levan and maltotriose, wherein the mass concentration of levan is 1.5-15 percent (W/V) and the mass concentration of maltotriose is 0.5-15 percent (W/V). During cigarette processing, the tobacco moisturizing agent is uniformly mixed with tobacco feed liquid and is directly sprayed onto tobacco leaves or cut tobacco, and then cigarettes are made through cut tobacco processing, flavoring and cigarette making processes. In the invention, the levan has the ability of bonding free water, the price is low, the viscosity is lower and the adaptability to cigarette flavor and aftertaste is very good; the maltotriose has an excellent moisturizing performance, the viscosity is low, the product after burning is carbon dioxide and water which do no harm to body health, and a very light burnt fragrance is obtained. The moisturizing agent is suitable for various tobacco products, including tobacco leaves and cut tobacco, the existing process equipment do not need to be changed and the operation is simple and convenient to conduct.

Description

Tobacco humectant and preparation method thereof and application
Technical field
The present invention relates to tobacco additive agent field, relate in particular to a kind of for maintaining the tobacco humectant and preparation method thereof and application of tobacco moisture content.
Background technology
The humidity of tobacco is controlled most important to tobacco business, if cigarette becomes dry in storage, transportation, sucking process, can make fragrance scatter and disappear gradually, smoke components changes, cause nicotine and other compositions (aldehyde, ketone, phenol, pyrazine) increase in flue gas, flue gas becomes the bitter excitement enhancing of peppery change, and the harmful components, increase flue gas moisture feeling, the reduction stimulation that therefore retain moisture in cut tobacco, reduce in flue gas become tobacco business problem demanding prompt solution.
NMF is the material with moistening effect, can improve the physical property of blade or pipe tobacco, thereby reach, increase cigarette product toughness, elasticity and water holding capacity, conventional tobacco humectant mainly contains glycerine, propane diols, sorbierite etc., these are chemical industry synthetic, to health, may have a negative impact, conventional tobacco humectant has the NMFs such as hyaluronic acid in addition, because its cost is too high, cannot realize large-scale application.
Levan is the polymer of beta-D-fructofuranose, in molecule, contain a large amount of β-(2,6) glycosidic bond and a small amount of β-(2,1) fructose glycosidic bond, the molecular mass of levan is conventionally between several ten thousand to 1,000,000, levan wide material sources, the plants such as wheat, rye grass and orchardgrass can produce the levan of low molecular mass, the levan of high molecule mass is mainly produced by microorganism fermentation, levan has different physiological roles and biologically active, and there is the moistening effect the same with hyaluronic acid, but price is only hyaluronic 1/10th.
Maltotriose is a kind of trisaccharide, by three glucose molecules, formed, and with α-1,4 glycosidic bonds are linked, and have very high hygroscopicity and moisture retention, and viscosity is lower than the compound sugar product viscosity of same concentrations, at acidity and high temperatures, be difficult for Maillard reaction occurs, there is good color-protecting function, there is research to claim the cake of making as glycogen of sucrose, the distortion of will drying up after a couple of days, and utilize the cake of maltotriose processing, quality is soft, storage is for a long time not dry, and fresh keeping property is good.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of natural safe, nontoxic, has the tobacco humectant of good moisture retention energy.
For solving the problems of the technologies described above, technical scheme of the present invention is: tobacco humectant, by the aqueous solution of levan and maltotriose, formed, wherein, the mass concentration of levan is 0.5~15%(W/V), the mass concentration of maltotriose is 0.5~15%(W/V).
Preferably, described levan is plant origin or microbe-derived levulan, and molecular mass is 10000~2000000Da.
Preferably, described maltotriose is food stage, and being calculated in mass percent purity is 75~99%.
The present invention also provides the preparation method of above-mentioned tobacco humectant, and method is as follows: by described levan and maltotriose ultra-pure water stirring and dissolving 0.5~2h under 40~60 ℃ of conditions, can make described tobacco humectant.
The present invention also provides the application of above-mentioned tobacco humectant in reconstituted tobacoo preparation, in the reinforced process of Cigarette processing technique, after described tobacco humectant is mixed with tobacco feed liquid, be sprayed directly on tobacco leaf or pipe tobacco, cigarette process routinely again, through throwing, perfuming, cigarette technique, roll into cigarette, without changing existing process equipment, easy and simple to handle.
Preferably, the consumption of described tobacco humectant is 0.1~10 ‰ of tobacco leaf or pipe tobacco weight.
Owing to having adopted technique scheme, tobacco humectant, is comprised of the aqueous solution of levan and maltotriose, and wherein, the mass concentration of levan is 0.5~15%(W/V), the mass concentration of maltotriose is 0.5~15%(W/V); In the reinforced process of Cigarette processing technique, after described tobacco humectant is mixed with tobacco feed liquid, be sprayed directly on tobacco leaf or pipe tobacco, then cigarette process routinely, through throwing, perfuming, cigarette technique, roll into cigarette; The present invention has following beneficial effect: Levan and has the ability in conjunction with Free water, performance of keeping humidity and hyaluronic acid are very nearly the same, but price is cheaper, are hyaluronic 1/10th, the viscosity of levan is less, in water not swelling, do not form gel, there is the characteristics such as pseudoplastic behavior; Burning afterproduct is carbon dioxide and water, nontoxic to health, has slight burnt odor taste, and the fragrance of cigarette and mouthfeel pleasant impression are had to good adaptability; Maltotriose has remarkable performance of keeping humidity, is the best compound sugar of performance of keeping humidity, and has low viscosity, preferably heat-resisting, acid resistance and have good color-protecting function; Can improve the flexibility of pipe tobacco, reduce the waste of single case pipe tobacco; Maltotriose burning afterproduct is carbon dioxide and water, is harmful to human health, and has very slight burnt odor taste.Tobacco humectant of the present invention is applicable to each tobacco articles, comprises tobacco leaf, pipe tobacco, reconstituted tobacco etc., without changing existing process equipment, easy and simple to handle.
accompanying drawing explanation:
fig. 1 is the tobacco and the performance of keeping humidity comparison that does not add NMF (contrasting tobacco) that adds NMF in embodiment 1.
The specific embodiment
Below in conjunction with the drawings and specific embodiments, the present invention is described further.
embodiment 1
Take levan 2g, maltotriose 2g, is dissolved in 100mL ultra-pure water, and 40 ℃ add thermal agitation 0.5h, after mixed dissolution is even, obtains tobacco humectant.
Get the tobacco humectant solution 30g preparing, be mixed in the feed liquid preparing, shake up and with high pressure nozzle, evenly spray application on 100kg tobacco leaf afterwards, then cigarette process routinely, rolls into cigarette through throwing, perfuming, wraparound technique.
As shown in Figure 1, add the tobacco of NMF and compare with the tobacco (contrasting tobacco) of not adding NMF, along with the prolongation of time, from experimental data (assay method GB/T 23357-2009), moisture reduces slower, and performance of keeping humidity is good.
embodiment 2
Take levan 4g, maltotriose 8g, is dissolved in 100mL ultra-pure water, and 50 ℃ add thermal agitation 50min, after mixed dissolution is even, obtains tobacco humectant.
Get the tobacco humectant solution 50g preparing, shake up and with high pressure nozzle, evenly spray application on 100kg tobacco leaf afterwards, then cigarette process routinely, rolls into cigarette through throwing, perfuming, wraparound technique.
embodiment 3
Take levan 10g, maltotriose 3g, is dissolved in 100mL ultra-pure water, and 60 ℃ add thermal agitation 1h, after mixed dissolution is even, obtains tobacco humectant.
Get the tobacco humectant solution 50g preparing, be mixed in the feed liquid preparing, shake up and with high pressure nozzle, evenly spray application on 150kg tobacco leaf afterwards, then cigarette process routinely, rolls into cigarette through throwing, perfuming, wraparound technique.
embodiment 4
Take levan3g, maltotriose 10g is dissolved in 100mL ultra-pure water, and 55 ℃ add thermal agitation 0.5h, after mixed dissolution is even, obtains tobacco humectant.
Get the tobacco humectant solution 12g preparing, be mixed in the feed liquid preparing, shake up and with high pressure nozzle, evenly spray application on 120kg tobacco leaf afterwards, then cigarette process routinely, rolls into cigarette through throwing, perfuming, wraparound technique.
The foregoing is only the schematic specific embodiment of the present invention, not in order to limit scope of the present invention.Any those skilled in the art, not departing from equivalent variations and the modification of having done under the prerequisite of design of the present invention and principle, all should belong to the scope of protection of the invention.

Claims (8)

1. tobacco humectant, is characterized in that: the aqueous solution by levan and maltotriose forms, and wherein, the mass concentration of levan is 0.5~15%(W/V), the mass concentration of maltotriose is 0.5~15%(W/V).
2. tobacco humectant as claimed in claim 1, is characterized in that: described levan is plant origin or microbe-derived levulan, and molecular mass is 10000~2000000Da.
3. tobacco humectant as claimed in claim 1, is characterized in that: described maltotriose is food stage, and being calculated in mass percent purity is 75~99%.
4. the preparation method of the tobacco humectant as described in claim 1,2 or 3, is characterized in that: by described levan and maltotriose ultra-pure water stirring and dissolving 0.5~2h under 40~60 ℃ of conditions, make described tobacco humectant.
5. the preparation method of tobacco humectant as claimed in claim 4, is characterized in that: described levan is plant origin or microbe-derived levulan, and molecular mass is 10000~2000000Da.
6. the preparation method of tobacco humectant as claimed in claim 4, is characterized in that: described maltotriose is food stage, and being calculated in mass percent purity is 75~99%.
7. the application of the tobacco humectant as described in claim 1,2 or 3 in tobacco preparation, it is characterized in that: in the reinforced process of Cigarette processing technique, after described tobacco humectant is mixed with tobacco feed liquid, be sprayed directly on tobacco leaf or pipe tobacco, then roll into cigarette through throwing, perfuming, cigarette technique.
8. the application of tobacco humectant as claimed in claim 7 in tobacco preparation, is characterized in that: the consumption of described tobacco humectant is 0.1~10 ‰ of tobacco leaf or pipe tobacco weight.
CN201410320056.5A 2014-07-08 2014-07-08 tobacco humectant Expired - Fee Related CN104138027B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105661626A (en) * 2016-03-25 2016-06-15 河南中烟工业有限责任公司 Composite biological agent microcapsule capable of improving sensory quality of tobacco
CN108887727A (en) * 2018-07-26 2018-11-27 上海烟草集团有限责任公司 A kind of heating of paper process is not burnt reconstituted tobacoo and its coating fluid, coating method and preparation method

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61139374A (en) * 1984-12-10 1986-06-26 日本たばこ産業株式会社 Humectant of tobacco
CN102964462A (en) * 2012-11-26 2013-03-13 浙江中烟工业有限责任公司 Wedelia prostrate polysaccharide as well as preparation method and application of wedelia prostrate polysaccharide
CN103099310A (en) * 2013-02-04 2013-05-15 红云红河烟草(集团)有限责任公司 Tobacco humectant and application thereof
CN103126063A (en) * 2011-11-23 2013-06-05 福建中烟工业有限责任公司 Novel tobacco sense organ humectant and using method thereof in tobacco
CN103504463A (en) * 2013-09-27 2014-01-15 广东中烟工业有限责任公司 Application of shaddock ped polysaccharide to tobacco leaf moisturizing
CN103637398A (en) * 2013-12-06 2014-03-19 川渝中烟工业有限责任公司 Tobacco humectant
CN103859575A (en) * 2014-01-26 2014-06-18 广西中烟工业有限责任公司 Novel tobacco humectant and novel tobacco humectant application

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61139374A (en) * 1984-12-10 1986-06-26 日本たばこ産業株式会社 Humectant of tobacco
CN103126063A (en) * 2011-11-23 2013-06-05 福建中烟工业有限责任公司 Novel tobacco sense organ humectant and using method thereof in tobacco
CN102964462A (en) * 2012-11-26 2013-03-13 浙江中烟工业有限责任公司 Wedelia prostrate polysaccharide as well as preparation method and application of wedelia prostrate polysaccharide
CN103099310A (en) * 2013-02-04 2013-05-15 红云红河烟草(集团)有限责任公司 Tobacco humectant and application thereof
CN103504463A (en) * 2013-09-27 2014-01-15 广东中烟工业有限责任公司 Application of shaddock ped polysaccharide to tobacco leaf moisturizing
CN103637398A (en) * 2013-12-06 2014-03-19 川渝中烟工业有限责任公司 Tobacco humectant
CN103859575A (en) * 2014-01-26 2014-06-18 广西中烟工业有限责任公司 Novel tobacco humectant and novel tobacco humectant application

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105661626A (en) * 2016-03-25 2016-06-15 河南中烟工业有限责任公司 Composite biological agent microcapsule capable of improving sensory quality of tobacco
CN108887727A (en) * 2018-07-26 2018-11-27 上海烟草集团有限责任公司 A kind of heating of paper process is not burnt reconstituted tobacoo and its coating fluid, coating method and preparation method
CN108887727B (en) * 2018-07-26 2021-10-22 上海烟草集团有限责任公司 Papermaking-method heating non-combustible tobacco sheet and coating liquid, coating method and preparation method thereof

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Effective date of registration: 20201020

Address after: No.12001, Mizhou East Road, Zhucheng City, Weifang City, Shandong Province

Patentee after: SHANDONG MEICHEN ECOLOGY & ENVIRONMENT Co.,Ltd.

Address before: Ten, Zhucheng City four village 262200 Missouri street in Shandong province Weifang City No. 600

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Granted publication date: 20160113