CN104114491B - 制备沉淀二氧化硅的方法 - Google Patents

制备沉淀二氧化硅的方法 Download PDF

Info

Publication number
CN104114491B
CN104114491B CN201280069767.9A CN201280069767A CN104114491B CN 104114491 B CN104114491 B CN 104114491B CN 201280069767 A CN201280069767 A CN 201280069767A CN 104114491 B CN104114491 B CN 104114491B
Authority
CN
China
Prior art keywords
acid
concentration
weight
silicate
concentrated
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201280069767.9A
Other languages
English (en)
Chinese (zh)
Other versions
CN104114491A (zh
Inventor
M.克卢安
S.内沃
J.拉西努
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rhodia Operations SAS
Original Assignee
Rhodia Operations SAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rhodia Operations SAS filed Critical Rhodia Operations SAS
Publication of CN104114491A publication Critical patent/CN104114491A/zh
Application granted granted Critical
Publication of CN104114491B publication Critical patent/CN104114491B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/126—Preparation of silica of undetermined type
    • C01B33/128—Preparation of silica of undetermined type by acidic treatment of aqueous silicate solutions
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
    • C01B33/193—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/50—Agglomerated particles

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Silicon Compounds (AREA)
CN201280069767.9A 2011-12-23 2012-12-19 制备沉淀二氧化硅的方法 Expired - Fee Related CN104114491B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR1104090A FR2984870B1 (fr) 2011-12-23 2011-12-23 Nouveau procede de preparation de silices precipitees.
FR1104090 2011-12-23
PCT/EP2012/076213 WO2013092749A1 (fr) 2011-12-23 2012-12-19 Procédé de préparation de silices précipitées

Publications (2)

Publication Number Publication Date
CN104114491A CN104114491A (zh) 2014-10-22
CN104114491B true CN104114491B (zh) 2017-03-08

Family

ID=47504953

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201280069767.9A Expired - Fee Related CN104114491B (zh) 2011-12-23 2012-12-19 制备沉淀二氧化硅的方法

Country Status (14)

Country Link
US (1) US9725325B2 (enExample)
EP (1) EP2794480B1 (enExample)
JP (1) JP5844480B2 (enExample)
KR (1) KR20140111296A (enExample)
CN (1) CN104114491B (enExample)
AU (1) AU2012357116A1 (enExample)
BR (1) BR112014015270A8 (enExample)
CA (1) CA2859542C (enExample)
FR (1) FR2984870B1 (enExample)
IN (1) IN2014CN04719A (enExample)
MX (1) MX363346B (enExample)
MY (1) MY180099A (enExample)
RU (1) RU2605709C2 (enExample)
WO (1) WO2013092749A1 (enExample)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2607741C2 (ru) 2011-12-23 2017-01-10 Родиа Операсьон Новый способ получения диоксидов кремния
FR2985990B1 (fr) 2012-01-25 2014-11-28 Rhodia Operations Nouveau procede de preparation de silices precipitees a morphologie, granulometrie et porosite particulieres
FR2985993B1 (fr) 2012-01-25 2014-11-28 Rhodia Operations Nouveau procede de preparation de silices precipitees
FR2985992B1 (fr) 2012-01-25 2015-03-06 Rhodia Operations Nouveau procede de preparation de silices precitees
FR2985991B1 (fr) 2012-01-25 2014-11-28 Rhodia Operations Nouveau procede de preparation de silices precipitees
CN105712361A (zh) * 2016-03-24 2016-06-29 通化双龙化工股份有限公司 一种食品添加剂白炭黑的生产方法
CN106241822B (zh) * 2016-08-27 2018-08-28 安徽龙泉硅材料有限公司 一种干粉农药载体用沉淀二氧化硅的制备方法
CN106315599B (zh) * 2016-08-27 2018-08-28 安徽龙泉硅材料有限公司 一种工业胶辊橡胶补强用沉淀二氧化硅的制备方法
JP7069604B2 (ja) * 2017-08-28 2022-05-18 味の素株式会社 沈降シリカの製造法
EP3894354A1 (en) * 2018-12-11 2021-10-20 Rhodia Operations Precipitated silica for battery separator
CN109607555B (zh) * 2019-01-02 2019-08-09 广州市飞雪材料科技有限公司 一种高磨擦高透明牙膏用二氧化硅及其制备方法
CN113200551A (zh) * 2021-04-29 2021-08-03 武汉理工大学 一种改性白炭黑的制备方法
CN117800342A (zh) * 2023-12-29 2024-04-02 中南大学 改性硅基活性材料及其制备和应用
WO2025147104A1 (ko) * 2024-01-02 2025-07-10 선진뷰티사이언스(주) 고 비표면적을 가지는 나노 프리 실리카 입자 및 그의 제조방법

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4094771A (en) * 1976-01-13 1978-06-13 Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler Process for preparation of a sprayable precipitated silicic acid suspension
CN1069244A (zh) * 1991-06-26 1993-02-24 罗纳·布朗克化学公司 沉淀二氧化硅新制备方法，新沉淀二氧化硅及其在弹性体增强过程中的应用
CN101094808A (zh) * 2004-12-30 2007-12-26 科学与工业研究委员会 从金伯利岩尾矿制备非晶二氧化硅的方法
CN102137813A (zh) * 2008-09-01 2011-07-27 赢创德固赛有限责任公司 制备沉淀二氧化硅的方法、沉淀二氧化硅及其用途

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3639845A1 (de) 1986-11-21 1988-06-01 Degussa Faellungskieselsaeuren, verfahren zu ihrer herstellung und verwendung
FR2646673B1 (fr) * 1989-05-02 1991-09-06 Rhone Poulenc Chimie Silice sous forme de bille, procede de preparation et son utilisation au renforcement des elastomeres
FR2732331B1 (fr) * 1995-03-29 1997-06-20 Rhone Poulenc Chimie Nouveau procede de preparation de silice precipitee, nouvelles silices precipitees contenant du zinc et leur utilisation au renforcement des elastomeres
DE19526476A1 (de) 1995-07-20 1997-01-23 Degussa Fällungskieselsäure
FR2763581B1 (fr) * 1997-05-26 1999-07-23 Rhodia Chimie Sa Silice precipitee utilisable comme charge renforcante pour elastomeres
FR2763593B1 (fr) * 1997-05-26 1999-07-09 Michelin & Cie Composition de caoutchouc a base de silice destinee a la fabrication d'enveloppes de pneumatiques routiers ayant une resistance au roulement amelioree
AU2002211736A1 (en) 2000-10-13 2002-04-22 University Of Cincinnati Methods for synthesizing precipitated silica and use thereof
DE10061680A1 (de) * 2000-12-11 2002-06-20 Solarworld Ag Verfahren zur Herstellung von Silan
ES2610590T3 (es) * 2001-08-13 2017-04-28 Rhodia Chimie Procedimiento de preparación de sílices con distribución granulométrica y/o reparto de poros particulares
FR2902781B1 (fr) * 2006-06-27 2008-09-05 Rhodia Recherches Et Technologies Sas Silice precipitee pour application papier
RU2329950C1 (ru) * 2006-11-07 2008-07-27 Николай Алексеевич Дежов Способ получения композиции, содержащей соединения осажденного диоксида кремния и алюминия
FR2928363B1 (fr) * 2008-03-10 2012-08-31 Rhodia Operations Nouveau procede de preparation de silices precipitees, silices precipitees a morphologie, granulometrie et porosite particulieres et leurs utilisations, notamment pour le renforcement de polymeres
FR2962996B1 (fr) 2010-07-23 2012-07-27 Rhodia Operations Nouveau procede de preparation de silices precipitees
RU2607741C2 (ru) 2011-12-23 2017-01-10 Родиа Операсьон Новый способ получения диоксидов кремния
FR2985993B1 (fr) 2012-01-25 2014-11-28 Rhodia Operations Nouveau procede de preparation de silices precipitees
FR2985991B1 (fr) 2012-01-25 2014-11-28 Rhodia Operations Nouveau procede de preparation de silices precipitees
FR2985990B1 (fr) 2012-01-25 2014-11-28 Rhodia Operations Nouveau procede de preparation de silices precipitees a morphologie, granulometrie et porosite particulieres
FR2985992B1 (fr) 2012-01-25 2015-03-06 Rhodia Operations Nouveau procede de preparation de silices precitees

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4094771A (en) * 1976-01-13 1978-06-13 Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler Process for preparation of a sprayable precipitated silicic acid suspension
CN1069244A (zh) * 1991-06-26 1993-02-24 罗纳·布朗克化学公司 沉淀二氧化硅新制备方法，新沉淀二氧化硅及其在弹性体增强过程中的应用
CN101094808A (zh) * 2004-12-30 2007-12-26 科学与工业研究委员会 从金伯利岩尾矿制备非晶二氧化硅的方法
CN102137813A (zh) * 2008-09-01 2011-07-27 赢创德固赛有限责任公司 制备沉淀二氧化硅的方法、沉淀二氧化硅及其用途

Also Published As

Publication number Publication date
WO2013092749A1 (fr) 2013-06-27
KR20140111296A (ko) 2014-09-18
JP5844480B2 (ja) 2016-01-20
JP2015502324A (ja) 2015-01-22
CN104114491A (zh) 2014-10-22
US20150210555A1 (en) 2015-07-30
EP2794480A1 (fr) 2014-10-29
US9725325B2 (en) 2017-08-08
FR2984870B1 (fr) 2014-03-21
IN2014CN04719A (enExample) 2015-09-18
MY180099A (en) 2020-11-22
CA2859542C (fr) 2017-05-09
CA2859542A1 (fr) 2013-06-27
BR112014015270A2 (pt) 2017-06-13
MX2014007592A (es) 2015-03-19
FR2984870A1 (fr) 2013-06-28
RU2605709C2 (ru) 2016-12-27
EP2794480B1 (fr) 2020-04-08
AU2012357116A1 (en) 2014-07-10
RU2014130210A (ru) 2016-02-10
MX363346B (es) 2019-03-20
BR112014015270A8 (pt) 2017-06-13

Similar Documents

Publication Publication Date Title
CN104114491B (zh) 制备沉淀二氧化硅的方法
US9334169B2 (en) Method for preparing precipitated silicas containing aluminium
US9938154B2 (en) Precipitated silica production process
US11975978B2 (en) Preparation of precipitated silicas useful as fillers in silicon matrices
JP2799773B2 (ja) 沈降シリカ
AU708040B2 (en) New process for the preparation of precipitated silica, new precipitated silicas containing aluminium and their use for the reinforcement of elastomers
JP3325029B2 (ja) エラストマー補強充填剤用沈降シリカ
JP4463474B2 (ja) アルミニウムを含有する沈降シリカの製造法
US5846311A (en) Process for the preparation of precipitated silica, new precipitated silicas containing zinc and their use for the reinforcement of elastomers
CN101605725A (zh) 使用快速混合机制备沉淀二氧化硅的新方法
WO1998050305A1 (en) Improved silicas for use in rubber
MXPA96005925A (es) Nuevo proceso para la preparacion de silice precipitado, nuevo silices precipitados que contienenzinc y su uso para reforzar elastomeros

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170308

Termination date: 20211219

CF01 Termination of patent right due to non-payment of annual fee