CN104107216A - Traditional Chinese medicine compound preparation and its preparation method and use - Google Patents
Traditional Chinese medicine compound preparation and its preparation method and use Download PDFInfo
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Abstract
The invention discloses a traditional Chinese medicine compound preparation and its preparation method and use. The traditional Chinese medicine compound preparation comprises active components and pharmaceutically acceptable accessory materials. The active components comprises, by weight, 1-25 parts of honeysuckle flower extract, 6-18 parts of radix scutellariae extract and 1-9 parts of licorice root extract. Through compatibility of honeysuckle flower, radix scutellariae and licorice root, the traditional Chinese medicine compound preparation has effects of clearing heat and removing toxins, eliminating phlegm and stopping cough, resisting viruses and bacteria, diminishing inflammation, relieving fever and adjusting immunity, and can be used for treating pig wind-heat type common cold. The traditional Chinese medicine compound preparation has synergism and good effects, produces effects fast and does not produce antibiotic residue and resistance to drug. The preparation method has simple processes, a low cost and good market competitiveness. The preparation method utilizes traditional Chinese medicines having abundant sources, has a moderate price and is suitable for industrial production and application.
Description
Technical field
The present invention relates to field of veterinary, relate in particular to a kind of compound Chinese medicinal preparation for the treatment of pig anemopyretic cold and preparation method thereof.
Background technology
The traditional Chinese medical science is thought: wind is " first of six climate exopathogens ", " length of all kinds of diseases and ailments ", in Various Seasonal, often press from both sides to tremble with fear or press from both sides heat and invade simultaneously, surmount organism adaptation ability, exopathogen is taken advantage of in imperial evil scarce capacity, and invasion and attack lung is defended, can cause morbidity (list of references: what is built up. how Chinese veterinarian treats piglet is caught a cold [J]. Chinese animal health, 2013,15(1): 49-50.).As pig health body, yang deficiency person easily has a cold, and deficiency of YIN person is subject to wind heat.Due to the above cause of disease, therefore syndrome performance is different, face card with anemofrigid cold, the large class of anemopyretic cold two.
The sick pig of anemopyretic cold, it shows as down in spirits, initial stage poor appetite, heat is burnt on the whole body, and aversion to wind is trembled, eyes red and nasal obstruction, tachypnea, muzzle is xeothermic, and nose antiperspirant cuts in and out, and two is just normal, and the appetite that continues subtracts greatly or does not eat, happiness is sleeping lazy moving, and breathing is urged, argol yellowish urine, and mouthful color is red, thin fur.
The Therapeutic Principle of pig anemopyretic cold is relieving the exterior syndrome with drugs of pungent in flavor and cool in nature, heat-clearing and toxic substances removing.
At present clinically for pig anemopyretic cold, mainly with antibiotics, treat, the shortcoming of existence has: effect is single, only antibacterial is infected effectively the respiratory tract disease weak curative effect that viral infection is caused; There is the risk of bacterial resistance; After use, easily in poultry body, have residually, produce toxic and side effects healthy the bring potential safety hazard of the antibiotic remains by livestock products food to people, easily human body forms drug resistance, drug resistance body constitution, causes body immunity to decline.
Summary of the invention
In order to overcome the weak point of the prior art of above-mentioned indication, the invention provides a kind of good effect, have no drug resistance, can be used for compound Chinese medicinal preparation for the treatment of pig anemopyretic cold and preparation method thereof.
The present invention is achieved by the following technical solutions:
A compound Chinese medicinal preparation, is comprised of effective ingredient and pharmaceutically acceptable adjuvant, and described effective ingredient is comprised of the material of following parts by weight proportioning: 1～25 part of Flos Lonicerae extract, 6～18 parts of Radix Scutellariae extracts, 1～9 part of Radix Glycyrrhizae extract.
Preferably, described effective ingredient is comprised of the material of following parts by weight proportioning: 5～25 parts of Flos Lonicerae extracts, 10～18 parts of Radix Scutellariae extracts, 5～9 parts of Radix Glycyrrhizae extracts.
Described Flos Lonicerae extract, Radix Scutellariae extract, Radix Glycyrrhizae extract are basis physicochemical properties separately, through extracting, concentrated, dry making.Chlorogenic acid weight content in described Flos Lonicerae extract is 6%～18%, and the baicalin weight content in Radix Scutellariae extract is 20%～60%, and the glycyrrhizic acid weight content in Radix Glycyrrhizae extract is 6%～20%.
The present invention selects the effect of Chinese medicine to be summarized as follows:
Flos Lonicerae is cold in nature, and sweet in the mouth enters lung, the heart, stomach warp, has the effect of heat-clearing and toxic substances removing, antiinflammatory, tonify deficiency treatment wind.Flos Lonicerae is described as the good medicine of heat-clearing and toxic substances removing from ancient times.The sweet cold of its property fragrance, clearing away heat with drugs sweet in flavor and cold in nature and not injuring one's stomach, fragrance thoroughly reaches and can be eliminating evil.Flos Lonicerae can dispelling wind-heat, and kind removing summer-heat blood poison also, for various febrile diseases, as fever of the body, dermexanthesis, send out the diseases such as speckle, pyretic toxicity carbuncle sore, laryngopharynx swelling and pain.It is dispelling wind-heat that the present invention adds the object of Flos Lonicerae, induce sweat, removing summer-heat blood poison.
Radix Scutellariae is cold in nature, and bitter in the mouth is returned lung, gallbladder, spleen, stomach, large intestine, small intestine meridian.Energy heat clearing and damp drying, eliminating fire and detoxication.Cure mainly the diseases such as epidemic febrile disease, upper respiratory tract infection, cough due to lung-heat, hyperpyrexia and infantile convulsion, headache nasal sinusitis.Radix Scutellariae is good at treating the diseases such as cough due to lung-heat, and Radix Scutellariae is partial to clear part of the body cavity above the diaphragm housing the heart and lungs fire.It is heat clearing away, eliminating fire and detoxication that the present invention adds the object of Radix Scutellariae, and can be for the complication cough due to lung-heat of pig heating flu.
Radix Glycyrrhizae sweet in the mouth, property is flat.GUIXIN, lung, spleen, stomach warp.The effect that has QI invigorating invigorating middle warmer, heat-clearing and toxic substances removing, expelling phlegm for arresting cough, relieving spasm to stop pain, the mediation property of medicine.Be applicable to weakness of the spleen and stomach, the card of deficiency of QI in middle-JIAO; Cough and asthma.It is QI invigorating invigorating middle warmer, heat-clearing and toxic substances removing, the mediation property of medicine that the present invention adds the object of Radix Glycyrrhizae.
In the present invention, Flos Lonicerae, Radix Scutellariae, Radix Glycyrrhizae compatibility, can strengthen dispel the wind, the effect of heat-clearing and toxic substances removing, preventing phlegm from forming and stopping coughing.From the angle of modern pharmacology, can strengthen antiviral, antibacterial, antiinflammatory, antipyretic, immunoregulatory effect.
In the present invention, preferably, described pharmaceutically acceptable adjuvant is the one or more kinds of combinations in Icing Sugar, starch, dextrin, lactose.
Preferably, the dosage form of described compound Chinese medicinal preparation is granule.Described compound Chinese medicinal preparation is to take after each Chinese medicine extract, adds appropriate amount of auxiliary materials, mixes, and granulates, the dry granule making.
The present invention also provides the preparation method of above-mentioned compound Chinese medicinal preparation, comprises the following steps:
A, prepare Flos Lonicerae extract: take Flos Lonicerae, add 8～14 times of water gagings to decoct 3 times, decocting time is respectively 0.5～1 hour, filter, merging filtrate is also concentrated into thick paste shape, preferably, the extractum that while being concentrated into 70 ℃, relative density is 1.10～1.20, adds adjuvant dry;
B, prepare Radix Scutellariae extract: take Radix Scutellariae, add 8～14 times of water gagings to decoct 2 times, decocting time is respectively 1 hour, merging filtrate concentrated after filtering, gained concentrated solution salt adding acid for adjusting pH value to 1.0～2.0, insulation at 80 ℃～90 ℃, standing, after filtration, gained precipitate being added to water stirs evenly, with 40% sodium hydroxide solution, regulate pH value to 7.0 again, add equivalent 95% ethanol, stir evenly and dissolve and filter, gained filtrate is used salt acid for adjusting pH value to 1.0～2.0, insulation at 60 ℃～80 ℃, standing, after filtration, gained precipitate successively water and 95% alcohol flushing makes pH value be adjusted to 6.0～7.0, ethanol is volatilized and be dried,
C, prepare Radix Glycyrrhizae extract: take Radix Glycyrrhizae, section, adds 8～14 times of water gagings to decoct 3 times, and decocting time is respectively 2～3 hours, merging filtrate after filtering, makes, after filtrate precipitation, to get supernatant concentration to thick paste shape for standing 10 hours, is dried to fine powder;
D, be prepared into granule: take respectively Flos Lonicerae extract, Radix Scutellariae extract, the Radix Glycyrrhizae extract of parts by weight proportioning, add adjuvant, mix granulation after being ground into powdery, and following dry at 60 ℃.
The present invention also provides the application of described compound Chinese medicinal preparation in the medicine of preparation control pig anemopyretic cold, can be used for the medicine of preparation control pig anemopyretic cold.In medication process, can be according to practical situation, every pig consumption is 10～20g every day.
Compared with prior art, beneficial effect of the present invention comprises:
(1) combined effect of performance compound Chinese medicinal preparation, good effect, instant effect, has broad-spectrum antiseptic and antivirus action, can stop toxin to absorb, and strengthens immunologic function, and expelling phlegm for arresting cough, can be used for treating pig anemopyretic cold;
(2) the residual and drug resistance of antibiotic-free;
(3) preparation technology is simple, cost is low, has the stronger market competitiveness;
(4) Chinese medicine source is abundant, and moderate cost is applicable to suitability for industrialized production and application.
The specific embodiment
For the ease of those skilled in the art's understanding, below the invention will be further described.
Embodiment 1
A compound Chinese medicinal preparation, is comprised of effective ingredient and pharmaceutically acceptable appropriate amount of auxiliary materials, and described effective ingredient is comprised of the material of following parts by weight proportioning: 1 part of Flos Lonicerae extract, 6 parts of Radix Scutellariae extracts, 1 part of Radix Glycyrrhizae extract.Specifically, in every part of 100g, by the material of following parts by weight proportioning, formed:
Flos Lonicerae extract (chlorogenic acid content: 6%) 100g
Radix Scutellariae extract (content of baicalin: 20%) 600g
Radix Glycyrrhizae extract (glycyrrhizic acid content: 6%) 100g
Icing Sugar 500g
The preparation method of above-mentioned compound Chinese medicinal preparation, comprises the following steps:
A, prepare Flos Lonicerae extract: take Flos Lonicerae, add 8～14 times of water gagings to decoct 3 times, decocting time is respectively 0.5～1 hour, filters, and merging filtrate is also concentrated into thick paste shape, preferably, the extractum that while being concentrated into 70 ℃, relative density is 1.10～1.20, adds Icing Sugar dry, takes out appropriate, measure chlorogenic acid content and also regulate and make it up to specification, obtain;
B, prepare Radix Scutellariae extract: take Radix Scutellariae, add 8～14 times of water gagings to decoct 2 times, decocting time is respectively 1 hour, merging filtrate concentrated after filtering, gained concentrated solution salt adding acid for adjusting pH value to 1.0～2.0, insulation at 80 ℃～90 ℃, standing, after filtration, gained precipitate being added to water stirs evenly, with 40% sodium hydroxide solution, regulate pH value to 7.0 again, add equivalent 95% ethanol, stir evenly and dissolve and filter, gained filtrate is used salt acid for adjusting pH value to 1.0～2.0, insulation at 60 ℃～80 ℃, standing, after filtration, gained precipitate successively water and 95% alcohol flushing makes pH value be adjusted to 6.0～7.0, ethanol is volatilized and be dried, take out appropriate, measure content of baicalin and regulate and make it up to specification, obtain,
C, prepare Radix Glycyrrhizae extract: take Radix Glycyrrhizae, section, adds 8～14 times of water gagings to decoct 3 times, and decocting time is respectively 2～3 hours, merging filtrate after filtering, within standing 10 hours, make, after filtrate precipitation, to get supernatant concentration to thick paste shape, take out appropriate, measure glycyrrhizic acid content, it is up to specification that adjusting makes it, and is dried to fine powder, obtains;
D, be prepared into granule: take respectively Flos Lonicerae extract, Radix Scutellariae extract, the Radix Glycyrrhizae extract of parts by weight proportioning, add appropriate Icing Sugar, mix granulation after being ground into powdery, and following dry at 60 ℃.
Above-mentioned compound Chinese medicinal preparation is used for the treatment of pig anemopyretic cold, can be according to practical situation, and every pig consumption is 10～20g every day.
Embodiment 2
A compound Chinese medicinal preparation, is comprised of effective ingredient and pharmaceutically acceptable appropriate amount of auxiliary materials, and described effective ingredient is comprised of the material of following parts by weight proportioning: 5 parts of Flos Lonicerae extracts, 6 parts of Radix Scutellariae extracts, 5 parts of Radix Glycyrrhizae extracts.Specifically, in every part of 100g, by the material of following parts by weight proportioning, formed:
Flos Lonicerae extract (chlorogenic acid content: 12%) 500g
Radix Scutellariae extract (content of baicalin: 40%) 600g
Radix Glycyrrhizae extract (glycyrrhizic acid content: 10%) 500g
Dextrin 200g
The preparation method of above-mentioned compound Chinese medicinal preparation and to be applied to treat pig anemopyretic cold similar or identical with embodiment mono-, does not launch to repeat at this.
Embodiment 3
A compound Chinese medicinal preparation, is comprised of effective ingredient and pharmaceutically acceptable appropriate amount of auxiliary materials, and described effective ingredient is comprised of the material of following parts by weight proportioning: 10 parts of Flos Lonicerae extracts, 15 parts of Radix Scutellariae extracts, 6 parts of Radix Glycyrrhizae extracts.Specifically, in every part of 100g, by the material of following parts by weight proportioning, formed:
Flos Lonicerae extract (chlorogenic acid content: 12%) 1000g
Radix Scutellariae extract (content of baicalin: 40%) 1500g
Radix Glycyrrhizae extract (glycyrrhizic acid content: 20%) 600g
Lactose 100g
The preparation method of above-mentioned compound Chinese medicinal preparation and be applied to treat pig anemopyretic cold and catch similarly or identical with embodiment mono-, does not launch to repeat at this.
Embodiment 4
A compound Chinese medicinal preparation, is comprised of effective ingredient and pharmaceutically acceptable appropriate amount of auxiliary materials, and described effective ingredient is comprised of the material of following parts by weight proportioning: 15 parts of Flos Lonicerae extracts, 10 parts of Radix Scutellariae extracts, 9 parts of Radix Glycyrrhizae extracts.Specifically, in every part of 100g, by the material of following parts by weight proportioning, formed:
Flos Lonicerae extract (chlorogenic acid content: 12%) 1500g
Radix Scutellariae extract (content of baicalin: 40%) 1000g
Radix Glycyrrhizae extract (glycyrrhizic acid content: 20%) 900g
Lactose 100g
The preparation method of above-mentioned compound Chinese medicinal preparation and to be applied to treat pig anemopyretic cold similar or identical with embodiment mono-, does not launch to repeat at this.
Embodiment 5
A compound Chinese medicinal preparation, is comprised of effective ingredient and pharmaceutically acceptable appropriate amount of auxiliary materials, and described effective ingredient is comprised of the material of following parts by weight proportioning: 20 parts of Flos Lonicerae extracts, 15 parts of Radix Scutellariae extracts, 6 parts of Radix Glycyrrhizae extracts.Specifically, in every part of 100g, by the material of following parts by weight proportioning, formed:
Flos Lonicerae extract (chlorogenic acid content: 12%) 2000g
Radix Scutellariae extract (content of baicalin: 40%) 1500g
Radix Glycyrrhizae extract (glycyrrhizic acid content: 20%) 600g
Lactose 100g
The preparation method of above-mentioned compound Chinese medicinal preparation and to be applied to treat pig anemopyretic cold similar or identical with embodiment mono-, does not launch to repeat at this.
Embodiment 6
A compound Chinese medicinal preparation, is comprised of effective ingredient and pharmaceutically acceptable appropriate amount of auxiliary materials, and described effective ingredient is comprised of the material of following parts by weight proportioning: 25 parts of Flos Lonicerae extracts, 18 parts of Radix Scutellariae extracts, 9 parts of Radix Glycyrrhizae extracts.Specifically, in every part of 100g, by the material of following parts by weight proportioning, formed:
Flos Lonicerae extract (chlorogenic acid content: 18%) 2500g
Radix Scutellariae extract (content of baicalin: 60%) 1800g
Radix Glycyrrhizae extract (glycyrrhizic acid content: 14%) 900g
Starch 100g
The preparation method of above-mentioned compound Chinese medicinal preparation and to be applied to treat pig anemopyretic cold similar or identical with embodiment mono-, does not launch to repeat at this.
In order to show the therapeutic effect of compound Chinese medicinal preparation of the present invention to pig anemopyretic cold, medicine of the present invention is carried out to clinical observation on the therapeutic effect test, below by test example, further set forth the beneficial effect of medicine of the present invention:
(1) subjects: pig farm, Qingyuan City Qingxin County, pig farm, Fugang County, pig farm, Yangshan County diagnosis anemopyretic cold piglet be totally 420 examples.Male earner pig 220 examples wherein, female piglet 200 examples, the monthly age is 0.5～1.5.
(2) test method: at random 420 examples are divided into 7 groups.Test group 1～6 is respectively according to the prepared compound Chinese medicinal preparation administration of embodiment, the corresponding embodiment 1 of test group 1 wherein, the corresponding embodiment 2 of test group 2, the corresponding embodiment 3 of test group 3, the corresponding embodiment 4 of test group 4, the corresponding embodiment 5 of test group 5, the corresponding embodiment 6 of test group 6, blank group does not give any medicine.
(3) curative effect judging standard: in effective-treatment 3 days, body temperature is normal, and symptom and sign disappears substantially; Effectively-treatment 3～5 days, body temperature is normal, and symptom and sign disappears substantially; Invalid-above symptom for the treatment of 5 days is without improvement.Wherein, total effective rate=(effective number+effective number)/number of cases * 100%.
(4) statistical method: application SPSS14.0 software data processing, adopts X 2 test.
(5) result of the test:
The curative effect comparison of table 1 different tests group
(6) conclusion: 4 test group of medicine of the present invention and blank group total effective rate all have significant difference (
p<0.05).
Above content is in conjunction with concrete optimal way further description made for the present invention, should not assert that specific embodiment of the invention is confined to above explanation.For those skilled in the art, without departing from the inventive concept of the premise, can also make some simple deduction or replace, within the definite protection domain of the claim that all should be considered as being submitted to by the present invention.
Claims (7)
1. a compound Chinese medicinal preparation, it is characterized in that, effective ingredient and pharmaceutically acceptable adjuvant, consist of, described effective ingredient is comprised of the material of following parts by weight proportioning: 1～25 part of Flos Lonicerae extract, 6～18 parts of Radix Scutellariae extracts, 1～9 part of Radix Glycyrrhizae extract.
2. compound Chinese medicinal preparation according to claim 1, is characterized in that, described effective ingredient is comprised of the material of following parts by weight proportioning: 5～25 parts of Flos Lonicerae extracts, 10～18 parts of Radix Scutellariae extracts, 5～9 parts of Radix Glycyrrhizae extracts.
3. compound Chinese medicinal preparation according to claim 2, is characterized in that: described pharmaceutically acceptable adjuvant is the one or more kinds of combinations in Icing Sugar, starch, dextrin, lactose.
4. compound Chinese medicinal preparation according to claim 3, it is characterized in that: the chlorogenic acid weight content in described Flos Lonicerae extract is 6%～18%, baicalin weight content in Radix Scutellariae extract is 20%～60%, and the glycyrrhizic acid weight content in Radix Glycyrrhizae extract is 6%～20%.
5. according to the compound Chinese medicinal preparation described in any one in claim 1～4, it is characterized in that: the dosage form of described compound Chinese medicinal preparation is granule.
6. according to the preparation method of the compound Chinese medicinal preparation described in any one in claim 1～4, it is characterized in that, comprise the following steps:
A, prepare Flos Lonicerae extract: take Flos Lonicerae, add 8～14 times of water gagings to decoct 3 times, decocting time is respectively 0.5～1 hour, filters, and merging filtrate is also concentrated into thick paste shape, adds adjuvant dry;
B, prepare Radix Scutellariae extract: take Radix Scutellariae, add 8～14 times of water gagings to decoct 2 times, decocting time is respectively 0.5～1 hour, merging filtrate concentrated after filtering, gained concentrated solution salt adding acid for adjusting pH value to 1.0～2.0, insulation at 80 ℃～90 ℃, standing, after filtration, gained precipitate being added to water stirs evenly, with 40% sodium hydroxide solution, regulate pH value to 7.0 again, add equivalent 95% ethanol, stir evenly and dissolve and filter, gained filtrate is used salt acid for adjusting pH value to 1.0～2.0, insulation at 60 ℃～80 ℃, standing, after filtration, gained precipitate successively water and 95% alcohol flushing makes pH value be adjusted to 6.0～7.0, ethanol is volatilized and be dried,
C, prepare Radix Glycyrrhizae extract: take Radix Glycyrrhizae, section, adds 8～14 times of water gagings to decoct 3 times, and decocting time is respectively 2～3 hours, merging filtrate after filtering, makes, after filtrate precipitation, to get supernatant concentration to thick paste shape for standing 10 hours, is dried to fine powder;
D, be prepared into granule: take respectively Flos Lonicerae extract, Radix Scutellariae extract, the Radix Glycyrrhizae extract of parts by weight proportioning, add adjuvant, mix granulation after being ground into powdery, and following dry at 60 ℃.
7. the application in the medicine of preparation control pig anemopyretic cold according to the compound Chinese medicinal preparation described in any one in claim 1～4.
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Cited By (5)
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| CN106943454A (en) * | 2017-03-30 | 2017-07-14 | 黑龙江童医生儿童生物制药有限公司 | A kind of disposable antibacterial spraying of plant type and preparation method thereof |
| CN107412511A (en) * | 2017-05-08 | 2017-12-01 | 河南省中兽医药研究院有限公司 | It is a kind of to be used to improve pig body immunity, the Chinese medicine composition for preventing and treating virus diseases of pigs and products thereof and feeding method |
| CN109549973A (en) * | 2017-09-26 | 2019-04-02 | 洛阳惠中兽药有限公司 | It is a kind of with treat and prevent livestock and poultry Chinese medicine composition, and its preparation method and application |
| CN111588750A (en) * | 2020-06-28 | 2020-08-28 | 广东容大生物股份有限公司 | Preparation method of traditional Chinese medicine granules for treating wind-heat type common cold of pigs |
| CN116211925A (en) * | 2023-02-13 | 2023-06-06 | 青岛和美生物科技有限公司 | A veterinary pharmaceutical composition containing flos Lonicerae and radix astragali |
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| CN116211925A (en) * | 2023-02-13 | 2023-06-06 | 青岛和美生物科技有限公司 | A veterinary pharmaceutical composition containing flos Lonicerae and radix astragali |
| CN116211925B (en) * | 2023-02-13 | 2024-03-15 | 青岛和美生物科技有限公司 | A veterinary composition containing flos Lonicerae and radix astragali with antioxidant and immunity enhancing effects |
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Address after: 511517 construction two, No. 31, Qingyuan hi tech Industrial Development Zone, Guangdong Applicant after: GUANGDONG RONGDA BIOLOGICAL CO., LTD. Address before: 511517 bio pharmaceutical City, Qingyuan hi tech Industrial Development Zone, Guangdong Applicant before: Qingyuan Contain Bioengineering Co., Ltd. |
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Application publication date: 20141022 |
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