CN104085144A - Macromolecular-adhesive-film self-adhered waterproofing coiled material and preparation method thereof - Google Patents
Macromolecular-adhesive-film self-adhered waterproofing coiled material and preparation method thereof Download PDFInfo
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- CN104085144A CN104085144A CN201410322850.3A CN201410322850A CN104085144A CN 104085144 A CN104085144 A CN 104085144A CN 201410322850 A CN201410322850 A CN 201410322850A CN 104085144 A CN104085144 A CN 104085144A
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Abstract
The invention relates to a macromolecular-adhesive-film self-adhered waterproofing coiled material and a preparation method thereof and belongs to the technical field of building waterproofing coiled materials. The macromolecular-adhesive-film self-adhered waterproofing coiled material comprises an adhesive film and an asphalt layer which is formed on the adhesive film in a dip-coating manner, wherein the asphalt layer is prepared from the following components in parts by weight: 0.5-2.5 parts of asphalt 100#, 0.1-1.2 parts of asphalt 10#, 0.1-0.6 part of SBS (Styrene Butadiene Styrene block polymer), 0.05-0.25 part of SBR (Styrene Butadiene Rubber), 0.05-0.25 part of hydrogenated petroleum resin and 0.1-2 parts of rock flour. The macromolecular-adhesive-film self-adhered waterproofing coiled material has the advantages of good waterproof performance, ageing resistance, high tensile strength, good extensibility and excellent low-temperature flexibility and heat resistance.
Description
Technical field
The invention belongs to building waterproof coil technical field, be specifically related to a kind of polymeric laminate adhesive waterproof coil and preparation method thereof.
Background technology
Waterproof roll is mainly used for construction wall, roofing and tunnel, highway, refuse landfill etc. and locates, play a kind of flexible building material product that is curled into web-like of resisting extraneous rainwater, ground water seepage, be connected as ne-leakage between engineering foundation and building, be the first barrier of whole engineering waterproofing, whole engineering is played to vital effect.Product mainly contains asphalt water-proof coiled material and polymer membranes.
Application number be 2007101208098 Chinese invention patent " a kind of low-temperature resistant self-adhesive rubber asphalt waterproofing coiled material " disclose a kind of by asphalt, subtract the waterproof roll that bitumen layer that third fractional oil, thermoplastic styrene butadiene rubber, powder styrene butadiene rubber, coumarone indene resin, Petropols, terpene resin, little molecular weight polyisoprene isobutene, ultra-violet absorber, antioxidant, calcium carbonate make is made.This waterproof roll exists the shortcomings such as non-refractory.
Application number is that 2009100663136 Chinese invention patent " a kind of preparation method of polymer membranes " discloses the polymer membranes of being made up of pitch, rubber, carbon black and antiaging agent.The shortcomings such as this waterproof roll also exists non-refractory, and the scope of application is little.
Because extreme weather is outstanding now, the performance of existing waterproof roll can not satisfy the demands, has become therefore improve the performance of waterproof roll the technical problem of needing solution badly.
Summary of the invention
The object of this invention is to provide a kind of high temperature-resistant polymer glued membrane adhesive waterproof coil.
The technical solution used in the present invention is a kind of polymeric laminate adhesive waterproof coil, comprises glued membrane and the dip-coating bitumen layer on glued membrane, and described bitumen layer is made up of the component of following parts by weight: 100
#0.5～2.5 part of pitch, 10
#0.1～1.2 part of pitch, SBS0.1～0.6 part, SBR0.05～0.25 part, 0.05～0.25 part of hydrogenated petroleum resin, 0.1～2 part of stone flour.
Preferably, described bitumen layer is made up of the component of following parts by weight: 100
#1～2 part of pitch, 10
#0.4～0.8 part of pitch, SBS0.2～0.4 part, SBR0.1～0.2 part, 0.1～0.2 part of hydrogenated petroleum resin, 0.5～1.5 part of stone flour.
Preferably, described bitumen layer is made up of the component of following parts by weight: 100
#1.5 parts of pitches, 10
#0.6 part of pitch, SBS0.3 part, SBR0.15 part, 0.15 part of hydrogenated petroleum resin, 1 part of stone flour.
The present invention also provides a kind of preparation method of described polymeric laminate adhesive waterproof coil, comprises the following steps:
A, preparation bitumen layer: get 100
#pitch and 10
#pitch is warming up to 185 DEG C～195 DEG C after mixing, and adds SBS oxidation 0.5～1.5 hour, grind again 0.5～1.5 hour, be cooled to 165 DEG C～175 DEG C, then add SBR oxidation 0.5～1.5 hour, again grind 0.5～1.5 hour, add subsequently hydrogenated petroleum resin oxidation 0.5～1.5 hour, be warming up to 175 DEG C～185 DEG C, then add stone flour, stir 0.5～1.5 hour, be cooled to 115 DEG C～125 DEG C, the bitumen layer that must prepare;
B, by the above-mentioned bitumen layer preparing uniform fold on glued membrane.
In the present invention, the abbreviation that SBS is s-B-S; SBR is the abbreviation of butadiene-styrene rubber.
Beneficial effect of the present invention is: water resistance is good, ageing-resistant, and hot strength is high, and good extending performance has good low-temperature tenderness and heat resistance.The waterproof, seepage control of the engineerings such as industry and civil building roof covering, body of wall, kitchen and toilet, basement, swimming pool and bridge, subway, reservoir be can be applicable to, canister and pipeline corrosion protection protection are also applicable to.Be specially adapted to employ the engineering waterproofing construction of naked light, be also applicable to moist basal plane construction.
Detailed description of the invention
For making those skilled in the art understand in detail production technology of the present invention and technique effect, further introduce application of the present invention and technique effect with concrete production instance below.
Embodiment 1:
A, preparation bitumen layer: get 1.5 ton 100
#pitch and 0.6 ton 10
#pitch is warming up to 190 DEG C after mixing, and adds 0.3 ton of SBS oxidation 1 hour, being placed in colloid mill grinds 1 hour, be cooled to 170 DEG C, then add 0.15 ton of SBR oxidation 1 hour, be again placed in colloid mill and grind 1 hour, add subsequently 0.15 ton of hydrogenated petroleum resin oxidation 1 hour, be warming up to 180 DEG C, then add 1 ton of stone flour, stir 1 hour, be cooled to 120 DEG C, the bitumen layer that must prepare;
B, by the above-mentioned bitumen layer preparing uniform fold on glued membrane.
Embodiment 2:
A, preparation bitumen layer: get 2.5 ton 100
#pitch and 0.1 ton 10
#pitch is warming up to 195 DEG C after mixing, and adds 0.1 ton of SBS oxidation 1.5 hours, being placed in colloid mill grinds 0.5 hour, be cooled to 175 DEG C, then add 0.05 ton of SBR oxidation 0.5 hour, be again placed in colloid mill and grind 1.5 hours, add subsequently 0.25 ton of hydrogenated petroleum resin oxidation 0.5 hour, be warming up to 175 DEG C, then add 0.1 ton of stone flour, stir 1.5 hours, be cooled to 115 DEG C, the bitumen layer that must prepare;
B, by the above-mentioned bitumen layer preparing uniform fold on glued membrane.
Embodiment 3:
A, preparation bitumen layer: get 0.5 ton 100
#pitch and 1.2 ton 10
#pitch is warming up to 185 DEG C after mixing, and adds 0.6 ton of SBS oxidation 0.5 hour, being placed in colloid mill grinds 1.5 hours, be cooled to 165 DEG C, then add 0.25 ton of SBR oxidation 1.5 hours, be again placed in colloid mill and grind 0.5 hour, add subsequently 0.05 ton of hydrogenated petroleum resin oxidation 1.5 hours, be warming up to 185 DEG C, then add 2 tons of stone flours, stir 0.5 hour, be cooled to 125 DEG C, the bitumen layer that must prepare;
B, by the above-mentioned bitumen layer preparing uniform fold on glued membrane.
Embodiment 4:
A, preparation bitumen layer: get 2 ton 100
#pitch and 0.4 ton 10
#pitch is warming up to 185 DEG C after mixing, and adds 0.4 ton of SBS oxidation 1 hour, being placed in colloid mill grinds 1 hour, be cooled to 165 DEG C, then add 0.2 ton of SBR oxidation 1.5 hours, be again placed in colloid mill and grind 0.5 hour, add subsequently 0.1 ton of hydrogenated petroleum resin oxidation 1.5 hours, be warming up to 185 DEG C, then add 0.5 ton of stone flour, stir 0.5 hour, be cooled to 125 DEG C, the bitumen layer that must prepare;
B, by the above-mentioned bitumen layer preparing uniform fold on glued membrane.
Embodiment 5:
A, preparation bitumen layer: get 1 ton 100
#pitch and 0.8 ton 10
#pitch is warming up to 190 DEG C after mixing, and adds 0.2 ton of SBS oxidation 1 hour, being placed in colloid mill grinds 1 hour, be cooled to 165 DEG C, then add 0.1 ton of SBR oxidation 1 hour, be again placed in colloid mill and grind 0.5 hour, add subsequently 0.2 ton of hydrogenated petroleum resin oxidation 1 hour, be warming up to 185 DEG C, then add 1.5 tons of stone flours, stir 0.5 hour, be cooled to 120 DEG C, the bitumen layer that must prepare;
B, by the above-mentioned bitumen layer preparing uniform fold on glued membrane.
Comparative example 1:
Hydrogenated petroleum resin is replaced by Petropols, and all the other are implemented by the method for embodiment 1 completely, obtain comparative example 1.
Comparative example 2-5:
The consumption of SBS is changed to 0.02 ton, 0.04 ton, 0.26 ton and 0.28 ton, and all the other are implemented by the method for embodiment 1 completely, obtain comparative example 2-5.
For verifying technique effect of the present invention, inspection below special work:
Above-described embodiment gained waterproof roll water resistance is good, ageing-resistant, and hot strength is high, and good extending performance has good low-temperature tenderness and heat resistance.The waterproof, seepage control of the engineerings such as industry and civil building roof covering, body of wall, kitchen and toilet, basement, swimming pool and bridge, subway, reservoir be can be applicable to, canister and pipeline corrosion protection protection are also applicable to.Be specially adapted to employ the engineering waterproofing construction of naked light, be also applicable to moist basal plane construction.
Finally it should be noted that, above embodiment is the unrestricted technical scheme of the present invention in order to explanation only, although the present invention is had been described in detail with reference to above-described embodiment, those skilled in the art are to be understood that, still can modify or be equal to replacement the present invention, and not departing from any modification or partial replacement of the spirit and scope of the present invention, it all should be encompassed in claim scope of the present invention.
Claims (4)
1. a polymeric laminate adhesive waterproof coil, comprises glued membrane and the dip-coating bitumen layer on glued membrane, it is characterized in that, described bitumen layer is made up of the component of following parts by weight: 100
#0.5～2.5 part of pitch, 10
#0.1～1.2 part of pitch, SBS0.1～0.6 part, SBR0.05～0.25 part, 0.05～0.25 part of hydrogenated petroleum resin, 0.1～2 part of stone flour.
2. polymeric laminate adhesive waterproof coil according to claim 1, is characterized in that, described bitumen layer is made up of the component of following parts by weight: 100
#1～2 part of pitch, 10
#0.4～0.8 part of pitch, SBS0.2～0.4 part, SBR0.1～0.2 part, 0.1～0.2 part of hydrogenated petroleum resin, 0.5～1.5 part of stone flour.
3. polymeric laminate adhesive waterproof coil according to claim 2, is characterized in that, described bitumen layer is made up of the component of following parts by weight: 100
#1.5 parts of pitches, 10
#0.6 part of pitch, SBS0.3 part, SBR0.15 part, 0.15 part of hydrogenated petroleum resin, 1 part of stone flour.
4. the preparation method based on polymeric laminate adhesive waterproof coil described in claim 1-3, is characterized in that, comprises the following steps:
A, preparation bitumen layer: get 100
#pitch and 10
#pitch is warming up to 185 DEG C～195 DEG C after mixing, and adds SBS oxidation 0.5～1.5 hour, grind again 0.5～1.5 hour, be cooled to 165 DEG C～175 DEG C, then add SBR oxidation 0.5～1.5 hour, again grind 0.5～1.5 hour, add subsequently hydrogenated petroleum resin oxidation 0.5～1.5 hour, be warming up to 175 DEG C～185 DEG C, then add stone flour, stir 0.5～1.5 hour, be cooled to 115 DEG C～125 DEG C, the bitumen layer that must prepare;
B, by the above-mentioned bitumen layer preparing uniform fold on glued membrane.
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| CN201410322850.3A CN104085144B (en) | 2014-07-08 | 2014-07-08 | Polymeric laminate adhesive waterproof coil and preparation method thereof |
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| CN201410322850.3A CN104085144B (en) | 2014-07-08 | 2014-07-08 | Polymeric laminate adhesive waterproof coil and preparation method thereof |
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| CN104085144B CN104085144B (en) | 2016-02-17 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105419364A (en) * | 2016-01-05 | 2016-03-23 | 四川杨氏达防水材料有限公司 | Preparation method and application of SBS/rubber compound modification asphalt |
| CN109849452A (en) * | 2018-11-20 | 2019-06-07 | 苏州卓宝科技有限公司 | A kind of modified asphalt waterproof coiled material and preparation method thereof |
| CN110001174A (en) * | 2019-03-27 | 2019-07-12 | 四川环图材料科技有限公司 | Anti-low-temperature cracking self-adhesive modified asphalt waterproof rolling material and preparation method |
| CN114106574A (en) * | 2021-12-30 | 2022-03-01 | 四川蜀羊防水材料有限公司 | Anti-stripping self-adhesive asphalt waterproof coiled material and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101481931A (en) * | 2009-01-20 | 2009-07-15 | 北京市建国伟业防水材料有限公司 | Sticking modified asphalt waterproof coiled material and adhesive, as well as preparation method and application thereof |
| CN102559135A (en) * | 2012-02-09 | 2012-07-11 | 深圳市卓宝科技股份有限公司 | Asphalt self-adhesive and high-polymer self-adhesion rubber waterproof coiled material prepared from asphalt self-adhesive |
| CN103612429A (en) * | 2013-11-30 | 2014-03-05 | 郑恩成 | Dry-and-wet neutral detergent fiber (NDF) macromolecular self-adhesive waterproof coiled material, as well as production process and equipment thereof |
| CN103740122A (en) * | 2014-01-24 | 2014-04-23 | 郑家玉 | Waterproof coiled material of self-adhesive polymer modified asphalt polyester tire and preparation method for waterproof coiled material |
-
2014
- 2014-07-08 CN CN201410322850.3A patent/CN104085144B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101481931A (en) * | 2009-01-20 | 2009-07-15 | 北京市建国伟业防水材料有限公司 | Sticking modified asphalt waterproof coiled material and adhesive, as well as preparation method and application thereof |
| CN102559135A (en) * | 2012-02-09 | 2012-07-11 | 深圳市卓宝科技股份有限公司 | Asphalt self-adhesive and high-polymer self-adhesion rubber waterproof coiled material prepared from asphalt self-adhesive |
| CN103612429A (en) * | 2013-11-30 | 2014-03-05 | 郑恩成 | Dry-and-wet neutral detergent fiber (NDF) macromolecular self-adhesive waterproof coiled material, as well as production process and equipment thereof |
| CN103740122A (en) * | 2014-01-24 | 2014-04-23 | 郑家玉 | Waterproof coiled material of self-adhesive polymer modified asphalt polyester tire and preparation method for waterproof coiled material |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105419364A (en) * | 2016-01-05 | 2016-03-23 | 四川杨氏达防水材料有限公司 | Preparation method and application of SBS/rubber compound modification asphalt |
| CN109849452A (en) * | 2018-11-20 | 2019-06-07 | 苏州卓宝科技有限公司 | A kind of modified asphalt waterproof coiled material and preparation method thereof |
| CN110001174A (en) * | 2019-03-27 | 2019-07-12 | 四川环图材料科技有限公司 | Anti-low-temperature cracking self-adhesive modified asphalt waterproof rolling material and preparation method |
| CN114106574A (en) * | 2021-12-30 | 2022-03-01 | 四川蜀羊防水材料有限公司 | Anti-stripping self-adhesive asphalt waterproof coiled material and preparation method thereof |
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| CN104085144B (en) | 2016-02-17 |
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