CN104041908B - Preparation method of peony pollen effervescent tablet - Google Patents
Preparation method of peony pollen effervescent tablet Download PDFInfo
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- CN104041908B CN104041908B CN201410311348.2A CN201410311348A CN104041908B CN 104041908 B CN104041908 B CN 104041908B CN 201410311348 A CN201410311348 A CN 201410311348A CN 104041908 B CN104041908 B CN 104041908B
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- Prior art keywords
- peony pollen
- pvp
- peony
- pollen
- use amount
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- 241000736199 Paeonia Species 0.000 title claims abstract description 70
- 235000006484 Paeonia officinalis Nutrition 0.000 title claims abstract description 70
- 239000007938 effervescent tablet Substances 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 55
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 33
- 239000000284 extract Substances 0.000 claims description 25
- 239000012141 concentrate Substances 0.000 claims description 20
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 16
- 239000011122 softwood Substances 0.000 claims description 16
- 239000003795 chemical substances by application Substances 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 15
- 108090000623 proteins and genes Proteins 0.000 claims description 15
- 102000004169 proteins and genes Human genes 0.000 claims description 15
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 claims description 14
- 239000008101 lactose Substances 0.000 claims description 12
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 11
- 239000003513 alkali Substances 0.000 claims description 11
- 235000003599 food sweetener Nutrition 0.000 claims description 11
- 239000000314 lubricant Substances 0.000 claims description 11
- 239000003765 sweetening agent Substances 0.000 claims description 11
- 239000003085 diluting agent Substances 0.000 claims description 10
- -1 requirement Substances 0.000 claims description 10
- 239000008118 PEG 6000 Substances 0.000 claims description 8
- 229920002584 Polyethylene Glycol 6000 Polymers 0.000 claims description 8
- 239000000853 adhesive Substances 0.000 claims description 8
- 230000001070 adhesive effect Effects 0.000 claims description 8
- 239000003826 tablet Substances 0.000 claims description 7
- 239000000706 filtrate Substances 0.000 claims description 4
- 238000004064 recycling Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 3
- 239000000047 product Substances 0.000 claims description 3
- 239000007787 solid Substances 0.000 abstract description 7
- 239000000463 material Substances 0.000 abstract description 4
- 238000000605 extraction Methods 0.000 abstract description 2
- 239000002075 main ingredient Substances 0.000 abstract 2
- 238000004062 sedimentation Methods 0.000 abstract 1
- 239000003205 fragrance Substances 0.000 description 10
- 244000269722 Thea sinensis Species 0.000 description 7
- 240000005001 Paeonia suffruticosa Species 0.000 description 6
- 235000003889 Paeonia suffruticosa Nutrition 0.000 description 6
- 235000013361 beverage Nutrition 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 230000000694 effects Effects 0.000 description 4
- 235000016709 nutrition Nutrition 0.000 description 4
- FTLYMKDSHNWQKD-UHFFFAOYSA-N (2,4,5-trichlorophenyl)boronic acid Chemical compound OB(O)C1=CC(Cl)=C(Cl)C=C1Cl FTLYMKDSHNWQKD-UHFFFAOYSA-N 0.000 description 3
- FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical compound C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 description 3
- UDIPTWFVPPPURJ-UHFFFAOYSA-M Cyclamate Chemical compound [Na+].[O-]S(=O)(=O)NC1CCCCC1 UDIPTWFVPPPURJ-UHFFFAOYSA-M 0.000 description 3
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 3
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 239000008103 glucose Substances 0.000 description 3
- 230000036541 health Effects 0.000 description 3
- 230000035764 nutrition Effects 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 238000001556 precipitation Methods 0.000 description 3
- 229940085605 saccharin sodium Drugs 0.000 description 3
- RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical compound CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 description 2
- 108010011485 Aspartame Proteins 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 229920002134 Carboxymethyl cellulose Polymers 0.000 description 2
- 229920001353 Dextrin Polymers 0.000 description 2
- 239000004375 Dextrin Substances 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 2
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 2
- 229930006000 Sucrose Natural products 0.000 description 2
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 description 2
- 239000002671 adjuvant Substances 0.000 description 2
- 239000000605 aspartame Substances 0.000 description 2
- 235000010357 aspartame Nutrition 0.000 description 2
- IAOZJIPTCAWIRG-QWRGUYRKSA-N aspartame Chemical compound OC(=O)C[C@H](N)C(=O)N[C@H](C(=O)OC)CC1=CC=CC=C1 IAOZJIPTCAWIRG-QWRGUYRKSA-N 0.000 description 2
- 229960003438 aspartame Drugs 0.000 description 2
- 235000010948 carboxy methyl cellulose Nutrition 0.000 description 2
- 229920006184 cellulose methylcellulose Polymers 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 235000019425 dextrin Nutrition 0.000 description 2
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 description 2
- 235000012907 honey Nutrition 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000008107 starch Substances 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- 229960004793 sucrose Drugs 0.000 description 2
- 239000000811 xylitol Substances 0.000 description 2
- 235000010447 xylitol Nutrition 0.000 description 2
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 2
- 229960002675 xylitol Drugs 0.000 description 2
- YYGNTYWPHWGJRM-UHFFFAOYSA-N (6E,10E,14E,18E)-2,6,10,15,19,23-hexamethyltetracosa-2,6,10,14,18,22-hexaene Chemical compound CC(C)=CCCC(C)=CCCC(C)=CCCC=C(C)CCC=C(C)CCC=C(C)C YYGNTYWPHWGJRM-UHFFFAOYSA-N 0.000 description 1
- 108010010803 Gelatin Proteins 0.000 description 1
- 206010020880 Hypertrophy Diseases 0.000 description 1
- BHEOSNUKNHRBNM-UHFFFAOYSA-N Tetramethylsqualene Natural products CC(=C)C(C)CCC(=C)C(C)CCC(C)=CCCC=C(C)CCC(C)C(=C)CCC(C)C(C)=C BHEOSNUKNHRBNM-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000010009 beating Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N dodecahydrosqualene Natural products CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 229920000159 gelatin Polymers 0.000 description 1
- 239000008273 gelatin Substances 0.000 description 1
- 235000019322 gelatine Nutrition 0.000 description 1
- 235000011852 gelatine desserts Nutrition 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 238000001802 infusion Methods 0.000 description 1
- 238000002372 labelling Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 210000005075 mammary gland Anatomy 0.000 description 1
- GBCAVSYHPPARHX-UHFFFAOYSA-M n'-cyclohexyl-n-[2-(4-methylmorpholin-4-ium-4-yl)ethyl]methanediimine;4-methylbenzenesulfonate Chemical compound CC1=CC=C(S([O-])(=O)=O)C=C1.C1CCCCC1N=C=NCC[N+]1(C)CCOCC1 GBCAVSYHPPARHX-UHFFFAOYSA-M 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000035755 proliferation Effects 0.000 description 1
- 210000002307 prostate Anatomy 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 229940031439 squalene Drugs 0.000 description 1
- TUHBEKDERLKLEC-UHFFFAOYSA-N squalene Natural products CC(=CCCC(=CCCC(=CCCC=C(/C)CCC=C(/C)CC=C(C)C)C)C)C TUHBEKDERLKLEC-UHFFFAOYSA-N 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 230000005760 tumorsuppression Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/40—Effervescence-generating compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
- A23L2/395—Dry compositions in a particular shape or form
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Medicinal Preparation (AREA)
- Medicines Containing Plant Substances (AREA)
- Non-Alcoholic Beverages (AREA)
- Confectionery (AREA)
Abstract
The invention discloses a preparation method of a peony pollen effervescent tablet. According to the preparation method, specific to an alcohol extraction technology of peony pollen, water-soluble auxiliary materials are completely adopted in a formula, and a concentrated solution is directly added in main ingredients so that the main ingredients are granulated, and thus a step of preparing a solid by adopting the concentrated solution is saved. The prepared peony pollen effervescent tablet solves the problem of sedimentation of the peony pollen, is transparent and bright during use, and has peony taste and good taste.
Description
Technical field
The present invention relates to method for preparing solid beverage thereof technical field, particularly relate to a kind of preparation method of peony pollen effervescent tablet.
Background technology
The alcohol extract of peony pollen is through detecting containing 35 kinds of active components, wherein it should be noted that content of phytosterol is 20%, squalene 5%, wherein phytosterol in reduction blood cholesterol concentration, prevent and treat in hypertrophy of the prostate, Tumor suppression, the suppression proliferation of mammary gland, immunity moderation etc. and have remarkable effect.By being concentrated through alcohol extract by peony pollen, obtain concentrate, concentrate darker in color is popular in bright, and remains the original fragrance of peony pollen, and stable in properties after placing a few days.But existing peony flower tea or other peonies or peony pollen beverage, food etc. fully by the active principle stripping in peony pollen, can not be unfavorable for absorption of human body, in addition, are not easy to transport and deposit.
Effervescent tablet is the tablet obtained with sour agent and effervescent agent mixing, meets water and disperses rapidly, release carbon dioxide.Publication number is 101336711, publication date is the Chinese patent application of 2009-01-07, disclose the technical scheme of " the flowers effervescent tablet prepared with edible flower or floral extract and smart sheet ", effervescent tablet prepared by the floral extract and the auxiliary material (sodium acid carbonate, citric acid, cane sugar powder, honey, Aspartame, xylitol, CMC, starch, gelatin, dextrin, dolomol, edible talcum powder) that relate to peony or peony, has the advantages such as instant, healthy nutritive value is high, mouthfeel is good.In the technical scheme of this patent application, the auxiliary material such as CMC, starch, dextrin, dolomol, use talcum powder is water-insoluble auxiliary material, and effervescent tablet produces muddy and precipitation when brewing, affect outward appearance; The sugarinesses such as sweetener cane sugar powder, honey, Aspartame, xylitol are little, and use amount is larger; Direct for peony defibrination, making beating are made tablet by the embodiment 4 of this patent application, easily occur suspension floccule in use, affect outward appearance and acceptance.The preparation of peony pollen effervescent tablet is not disclosed in prior art in addition.
Summary of the invention
Object of the present invention is exactly defect for above-mentioned existence and provides a kind of preparation method of peony pollen effervescent tablet.The present invention, to the alcohol-extracting technology of peony pollen, all adopts water soluble adjuvant in prescription, and adding of main component adopts concentrate directly to add granulation, eliminates the step being prepared into solid by concentrate.Obtained product solves the problem of peony pollen precipitation, and during use, color is transparent vivid, has the taste of the tree peony fragrance of a flower, and mouthfeel is good.
Preparation method's technical scheme of a kind of peony pollen effervescent tablet of the present invention is, by peony pollen alcohol extract, filter, extract is evaporated to without ethanol smell for subsequent use; Take effervescent agent, filler, flavouring, extract concentrate and 20%PVP with pollen
k30ethanolic solution is that sour grain alkali grain prepared respectively by adhesive; Merge sour grain and alkali grain after dry, add lubricant; Compressing tablet.
The preparation method of described a kind of peony pollen effervescent tablet, concrete steps are:
(1) by peony pollen and the mixing of 95% ethanol, mix and blend 100-150min under normal temperature, filters, and collects filtrate;
(2) repeat step (1) 3-4 time, extracting concentrate by concentrated for filter vacuum without obtaining peony pollen till ethanol smell, reclaiming ethanol recycling;
(3) supplementary material is selected: effervescent agent, diluent, sweetener, and peony pollen extracts concentrate, PVP
k30, lubricant; Take PVP
k3020 grams are dissolved in 100ml 50% ethanolic solution and prepare 20%PVP
k30ethanolic solution;
(4) prepare sour grain: the lactose of citric acid, 1/2 use amount, the protein sugar of 1/2 use amount are mixed, add peony pollen extract and the 20%PVP of 1/2 use amount
k30ethanolic solution, wherein, 20%PVP
k30the percentage by weight of ethanolic solution in sour grain is 12%, and prepare softwood, requirement, softwood is held agglomerating, and namely flicking falls apart; Dry, temperature 45 ± 5 DEG C, moisture≤7%;
(5) prepare alkali grain: the lactose of sodium acid carbonate, 1/2 use amount, the protein sugar of 1/2 use amount are mixed, add peony pollen extract and the 20%PVP of 1/2 use amount
k30ethanolic solution, wherein, 20%PVP
k30the percentage by weight of ethanolic solution in alkali grain is 18%, and prepare softwood, requirement, softwood is held agglomerating, and namely flicking falls apart; Dry, temperature 45 ± 5 DEG C, moisture≤7%;
(6) product in step (4), (5) and PEG6000 are merged, mix, compressing tablet, control strip is 0.5g heavily about.
In step (1), peony pollen and 95% ethanol weight ratio are 1:3-5.
Preferably, in step (1), peony pollen and 95% ethanol weight ratio are 1:4.
In step (3), effervescent agent is citric acid by weight: sodium acid carbonate=1-2:1.
Preferably, in step (3), effervescent agent is citric acid by weight: sodium acid carbonate=1.4:1.
In step (3), diluent is lactose, and sweetener is protein sugar, and lubricant is PEG6000.
Protein sugar composition of the present invention: sodium cyclohexyl sulfamate, saccharin sodium, glucose.Manufacturer: Ke Dun bio tech ltd, Tianjin.
In step (3), supplementary material is by weight percentage: effervescent agent 20-30%, diluent 40-60%, sweetener 8-15%, and peony pollen extracts concentrate 10-15%, adhesive PVP
k300.5-1.5%, lubricant 1-3%.
Preferably, in step (3), supplementary material is by weight percentage: effervescent agent 25%, diluent 50%, sweetener 10%, and peony pollen extracts concentrate 12%, adhesive 1%, lubricant 2%.
Beneficial effect of the present invention is:
(1) present invention process is to the alcohol-extracting technology of peony pollen, peony pollen alcohol extract 3-4 time, and the concentrated vacuum and low temperature that adopts concentrates, and production efficiency is high, maintains the smell of the tree peony fragrance of a flower, and the concentrated requirement terminated is without ethanol smell.Employing for raw material adds effervescent tablet, can avoid effervescent tablet to occur sediment with peony pollen alcohol extract in passes during brewing.
(2) all water soluble adjuvant is adopted in prescription, to ensure effervescent tablet after infusion for transparence liquid.
(3) peony pollen extraction concentrate adds in the mode of adhesive, decreases the operating procedure being become powder from concentrate.
(4) employing acid, alkali are granulated, respectively to ensure not react in production process.
(5) adopt low temperature drying, do not change to keep the taste of peony pollen.
(6) solving with pollen is the problem that raw material prepares that solid beverage produces precipitation, and ensure that the reservation of the nutritional labeling of pollen.During use, color is transparent vivid, has the taste of the tree peony fragrance of a flower, and mouthfeel is good.
Peony pollen adds in effervescent tablet by the present invention, as a kind of solid beverage, can be dispersed in tea rapidly after putting into water tumbler.Easy to use, every glass brews a slice, and after brewing effervescent tablet dispersion, tea is bright, in golden yellow, distributes peony fragrance.People can be allowed to realize the taste of the tree peony fragrance of a flower, play again the effect of nutrition and health care.
detailed description of the invention:
In order to understand the present invention better, describe technical scheme of the present invention in detail with instantiation below, but the present invention is not limited thereto.
Embodiment 1
A preparation method for peony pollen effervescent tablet, comprises following step:
(1) peony pollen side and 95% ethanol are mixed (mass ratio) with 1:4, mix and blend 120min under normal temperature, filter, collect filtrate.
(2) repeat step (1) 4 time, extracting concentrate by concentrated for filter vacuum without obtaining peony pollen till ethanol smell, reclaiming ethanol recycling.
(3) supplementary material is selected: effervescent agent 25% (citric acid: sodium acid carbonate=1.4:1), diluent 50%(lactose), sweetener 10%(protein sugar), peony pollen extracts concentrate 12%, adhesive 1%(PVP
k30), lubricant 2% (PEG6000).Protein sugar composition of the present invention: sodium cyclohexyl sulfamate, saccharin sodium, glucose.Manufacturer: Ke Dun bio tech ltd, Tianjin.
(4) prepare sour grain: the lactose of citric acid, 1/2 use amount, the protein sugar of 1/2 use amount are mixed, add peony pollen extract and the 20%PVP of 1/2 use amount
k30ethanolic solution, wherein, 20%PVP
k30the percentage by weight of ethanolic solution in sour grain is 12%, and prepare softwood, requirement, softwood is held agglomerating, and namely flicking falls apart; Dry, temperature 45 ± 5 DEG C, moisture≤7%;
(5) prepare alkali grain: the lactose of sodium acid carbonate, 1/2 use amount, the protein sugar of 1/2 use amount are mixed, add peony pollen extract and the 20%PVP of 1/2 use amount
k30ethanolic solution, wherein, 20%PVP
k30the percentage by weight of ethanolic solution in alkali grain is 18%, and prepare softwood, requirement, softwood is held agglomerating, and namely flicking falls apart; Dry, temperature 45 ± 5 DEG C, moisture≤7%;
(6) (4), (5), PEG6000 are merged, mix, compressing tablet, control strip is 0.5g heavily about.
Peony pollen adds in effervescent tablet by the present invention, as a kind of solid beverage, can be dispersed in tea rapidly after putting into water tumbler.Easy to use, every glass brews a slice, and after brewing effervescent tablet dispersion, tea is bright, in golden yellow, distributes peony fragrance.People can be allowed to realize the taste of the tree peony fragrance of a flower, play again the effect of nutrition and health care.
Embodiment 2
A preparation method for peony pollen effervescent tablet, comprises following step:
(1) peony pollen side and 95% ethanol are mixed (mass ratio) with 1:4, mix and blend 150min under normal temperature, filter, collect filtrate.
(2) repeat step (1) 3 time, extracting concentrate by concentrated for filter vacuum without obtaining peony pollen till ethanol smell, reclaiming ethanol recycling.
(3) supplementary material is selected: effervescent agent 28% (citric acid: sodium acid carbonate=1.5:1), diluent 45%(lactose), sweetener 12%(protein sugar), peony pollen extracts concentrate 13%, adhesive 0.5%(PVP
k30), lubricant 1.5% (PEG6000).Protein sugar composition of the present invention: sodium cyclohexyl sulfamate, saccharin sodium, glucose.Manufacturer: Ke Dun bio tech ltd, Tianjin.
(4) prepare sour grain: the lactose of citric acid, 1/2 use amount, the protein sugar of 1/2 use amount are mixed, add peony pollen extract and the 20%PVP of 1/2 use amount
k30ethanolic solution, wherein, 20%PVP
k30the percentage by weight of ethanolic solution in sour grain is 12%, and prepare softwood, requirement, softwood is held agglomerating, and namely flicking falls apart; Dry, temperature 45 ± 5 DEG C, moisture≤7%;
(5) prepare alkali grain: the lactose of sodium acid carbonate, 1/2 use amount, the protein sugar of 1/2 use amount are mixed, add peony pollen extract and the 20%PVP of 1/2 use amount
k30ethanolic solution, wherein, 20%PVP
k30the percentage by weight of ethanolic solution in alkali grain is 18%, and prepare softwood, requirement, softwood is held agglomerating, and namely flicking falls apart; Dry, temperature 45 ± 5 DEG C, moisture≤7%;
(6) (4), (5), PEG6000 are merged, mix, compressing tablet, control strip is 0.5g heavily about.
Peony pollen adds in effervescent tablet by the present invention, as a kind of solid beverage, can be dispersed in tea rapidly after putting into water tumbler.Easy to use, every glass brews a slice, and after brewing effervescent tablet dispersion, tea is bright, in golden yellow, distributes peony fragrance.People can be allowed to realize the taste of the tree peony fragrance of a flower, play again the effect of nutrition and health care.
Claims (4)
1. a preparation method for peony pollen effervescent tablet, is characterized in that, concrete steps are:
(1) by peony pollen and the mixing of 95% ethanol, mix and blend 100-150min under normal temperature, filters, and collects filtrate;
(2) repeat step (1) 3-4 time, extracting concentrate by concentrated for filter vacuum without obtaining peony pollen till ethanol smell, reclaiming ethanol recycling;
(3) supplementary material is selected: effervescent agent, diluent, sweetener, and peony pollen extracts concentrate, PVP
k30, lubricant; Take PVP
k3020 grams are dissolved in 100ml 50% ethanolic solution and prepare 20%PVP
k30ethanolic solution;
(4) prepare sour grain: the lactose of citric acid, 1/2 use amount, the protein sugar of 1/2 use amount are mixed, add peony pollen extract and the 20%PVP of 1/2 use amount
k30ethanolic solution, wherein, 20%PVP
k30the percentage by weight of ethanolic solution in sour grain is 12%, and prepare softwood, requirement, softwood is held agglomerating, and namely flicking falls apart; Dry, temperature 45 ± 5 DEG C, moisture≤7%;
(5) prepare alkali grain: the lactose of sodium acid carbonate, 1/2 use amount, the protein sugar of 1/2 use amount are mixed, add peony pollen extract and the 20%PVP of 1/2 use amount
k30ethanolic solution, wherein, 20%PVP
k30the percentage by weight of ethanolic solution in alkali grain is 18%, and prepare softwood, requirement, softwood is held agglomerating, and namely flicking falls apart; Dry, temperature 45 ± 5 DEG C, moisture≤7%;
(6) product in step (4), (5) and PEG6000 are merged, mix, compressing tablet;
In step (1), peony pollen and 95% ethanol weight ratio are 1:3-5;
In step (3), effervescent agent is citric acid by weight: sodium acid carbonate=1-2:1;
In step (3), diluent is lactose, and sweetener is protein sugar, and lubricant is PEG6000;
In step (3), supplementary material is by weight percentage: effervescent agent 20-30%, diluent 40-60%, sweetener 8-15%, and peony pollen extracts concentrate 10-15%, adhesive PVP
k300.5-1.5%, lubricant 1-3%.
2. the preparation method of a kind of peony pollen effervescent tablet according to claim 1, is characterized in that, in step (1), peony pollen and 95% ethanol weight ratio are 1:4.
3. the preparation method of a kind of peony pollen effervescent tablet according to claim 1, is characterized in that, in step (3), effervescent agent is citric acid by weight: sodium acid carbonate=1.4:1.
4. the preparation method of a kind of peony pollen effervescent tablet according to claim 1, is characterized in that, in step (3), supplementary material is by weight percentage: effervescent agent 25%, diluent 50%, sweetener 10%, peony pollen extracts concentrate 12%, adhesive 1%, lubricant 2%.
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| CN104664385B (en) * | 2015-03-17 | 2016-07-06 | 菏泽瑞璞牡丹产业科技发展有限公司 | A kind of Paeonia suffruticosa nutrient tablet and preparation method thereof |
| CN107048295A (en) * | 2017-04-18 | 2017-08-18 | 甘肃省医学科学研究院 | A kind of peony pollen buccal tablet and preparation method thereof |
| CN112410158A (en) * | 2020-12-22 | 2021-02-26 | 和田昆玉中科生物科技有限公司 | Peony health care wine capable of improving chronic prostate diseases and preparation method thereof |
| CN113367264A (en) * | 2021-05-28 | 2021-09-10 | 山东省科学院菏泽分院 | Full-nutrient peony pistil effervescent tablet |
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| CN1823843A (en) * | 2005-12-23 | 2006-08-30 | 刘春� | Child ammonia phenol alkyl amine affervescent tablet and its preparation method |
| CN101336711A (en) * | 2008-06-23 | 2009-01-07 | 昆明七彩云花生物科技有限公司 | Flower effervescent tablets and concentrated tablet prepared by edible flower or flower extract |
| CN101647871B (en) * | 2009-09-07 | 2011-09-14 | 甘肃中川牡丹研究所 | Peony pollen oral liquid and preparation method thereof |
| CN101756338A (en) * | 2010-01-17 | 2010-06-30 | 苏星 | Pollen effervescent solid beverage and preparing method thereof |
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