CN104010971B - 分子筛前体和分子筛的合成 - Google Patents

分子筛前体和分子筛的合成 Download PDF

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Publication number
CN104010971B
CN104010971B CN201280052903.3A CN201280052903A CN104010971B CN 104010971 B CN104010971 B CN 104010971B CN 201280052903 A CN201280052903 A CN 201280052903A CN 104010971 B CN104010971 B CN 104010971B
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China
Prior art keywords
zeolite
directing agent
colloidal solution
structure directing
colloidal
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Expired - Fee Related
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CN201280052903.3A
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English (en)
Chinese (zh)
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CN104010971A (zh
Inventor
A·莫伊尼
S·阿莱拉苏
S·普拉萨德
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BASF Corp
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BASF Corp
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/86—Catalytic processes
    • B01D53/8621—Removing nitrogen compounds
    • B01D53/8625—Nitrogen oxides
    • B01D53/8628—Processes characterised by a specific catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/92—Chemical or biological purification of waste gases of engine exhaust gases
    • B01D53/94—Chemical or biological purification of waste gases of engine exhaust gases by catalytic processes
    • B01D53/9404—Removing only nitrogen compounds
    • B01D53/9409—Nitrogen oxides
    • B01D53/9413—Processes characterised by a specific catalyst
    • B01D53/9418—Processes characterised by a specific catalyst for removing nitrogen oxides by selective catalytic reduction [SCR] using a reducing agent in a lean exhaust gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7015—CHA-type, e.g. Chabazite, LZ-218
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/04—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof using at least one organic template directing agent, e.g. an ionic quaternary ammonium compound or an aminated compound
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2255/00—Catalysts
    • B01D2255/50—Zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/30—Erionite or offretite type, e.g. zeolite T
    • C01B39/305—Erionite or offretite type, e.g. zeolite T using at least one organic template directing agent

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Environmental & Geological Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Combustion & Propulsion (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Catalysts (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Exhaust Gas Treatment By Means Of Catalyst (AREA)
CN201280052903.3A 2011-08-25 2012-08-24 分子筛前体和分子筛的合成 Expired - Fee Related CN104010971B (zh)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US201161527312P 2011-08-25 2011-08-25
US61/527,312 2011-08-25
US13/592,726 US9174849B2 (en) 2011-08-25 2012-08-23 Molecular sieve precursors and synthesis of molecular sieves
US13/592,726 2012-08-23
PCT/US2012/052228 WO2013028958A1 (en) 2011-08-25 2012-08-24 Molecular sieve precursors and synthesis of molecular sieves

Publications (2)

Publication Number Publication Date
CN104010971A CN104010971A (zh) 2014-08-27
CN104010971B true CN104010971B (zh) 2016-11-09

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CN201280052903.3A Expired - Fee Related CN104010971B (zh) 2011-08-25 2012-08-24 分子筛前体和分子筛的合成

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US (2) US9174849B2 (enExample)
EP (1) EP2748109B1 (enExample)
JP (1) JP6112568B2 (enExample)
KR (1) KR101991529B1 (enExample)
CN (1) CN104010971B (enExample)
ES (1) ES2812508T3 (enExample)
PL (1) PL2748109T3 (enExample)
WO (1) WO2013028958A1 (enExample)

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WO2015112660A1 (en) 2014-01-22 2015-07-30 California Institute Of Technology Novel methods for producing crystalline microporous solids and compositions derived from the same
BR112016029733B8 (pt) * 2014-06-18 2022-09-27 Basf Corp Catalisador scr, método para reduzir seletivamente óxidos de nitrogênio (nox) e sistema de tratamento de gás de exaustão
US9889437B2 (en) 2015-04-15 2018-02-13 Basf Corporation Isomorphously substituted catalyst
CA2952435C (en) * 2014-06-18 2023-10-03 Basf Corporation Molecular sieve catalyst compositions, catalyst composites, systems, and methods
US10850265B2 (en) 2014-06-18 2020-12-01 Basf Corporation Molecular sieve catalyst compositions, catalytic composites, systems, and methods
US9764313B2 (en) 2014-06-18 2017-09-19 Basf Corporation Molecular sieve catalyst compositions, catalyst composites, systems, and methods
EP3261751A4 (en) * 2015-02-27 2018-11-14 BASF Corporation Exhaust gas treatment system
JP6599637B2 (ja) * 2015-05-13 2019-10-30 イビデン株式会社 ゼオライト、該ゼオライトの製造方法、該ゼオライトを使用したハニカム触媒及び排ガス浄化装置
JP6616101B2 (ja) * 2015-05-15 2019-12-04 イビデン株式会社 ゼオライト、該ゼオライトの製造方法、該ゼオライトを使用したハニカム触媒及び排ガス浄化装置
US9708193B2 (en) * 2015-08-20 2017-07-18 Chevron U.S.A. Inc. Synthesis of aluminosilicate LEV framework type zeolites
CN107922206B (zh) * 2015-09-01 2021-07-20 东曹株式会社 Aei型沸石的制造方法
JP2018531208A (ja) * 2015-10-26 2018-10-25 エコラブ ユーエスエイ インク 高度に均質なゼオライトの前駆体
CN108290144B (zh) 2015-11-25 2021-04-02 三菱化学株式会社 沸石催化剂及低级烯烃的制造方法
US20170158520A1 (en) * 2015-12-04 2017-06-08 Chevron U.S.A. Inc. Synthesis of aluminosilicate zeolites having the offretite structure
CN106145137B (zh) * 2016-06-27 2018-06-05 杨晓波 一种直接水热合成中硅铝比菱沸石的方法
JP7362478B2 (ja) * 2016-10-03 2023-10-17 ビーエーエスエフ コーポレーション アルミニウム傾斜アルミノシリケートゼオライト組成物
WO2018102555A1 (en) * 2016-12-02 2018-06-07 Ecolab USA, Inc. Polyaluminum salts and their uses in preparation of high-purity colloidal aluminum-silica composite particles and zeolites
EP3551581A4 (en) * 2016-12-08 2020-09-16 BASF Corporation ACCELERATED ZEOLITE ALUMINOSILICATE CRYSTALLIZATION
WO2018110998A2 (ko) * 2016-12-14 2018-06-21 서강대학교산학협력단 마이크로다공성 및 메조다공성 계층적 구조의 mfi 제올라이트, 이의 제조방법 및 이의 촉매 용도
CN107233914A (zh) * 2017-05-27 2017-10-10 清华大学 一种Cu‑SAPO‑47分子筛脱硝催化剂的制备方法及其脱硝应用
WO2019154071A1 (en) * 2018-02-06 2019-08-15 Basf Se A process for preparing a zeolitic material having a framework structure type RTH
EP3768638A4 (en) * 2018-03-21 2021-12-29 BASF Corporation Cha zeolite material and related method of synthesis
US20210101801A1 (en) * 2018-04-20 2021-04-08 Basf Se A process for preparing a porous oxidic material which comprises micropores and mesopores and which comprises a zeolitic material having a framework type aei
CN113039157A (zh) * 2018-09-11 2021-06-25 巴斯夫公司 制备具有骨架类型aei的沸石材料的方法
KR102239941B1 (ko) * 2019-05-16 2021-04-13 한국화학연구원 메탄올로부터 경질올레핀의 전환을 위한 고활성 ssz-13 제올라이트 합성방법
JP7370194B2 (ja) * 2019-08-27 2023-10-27 東ソー株式会社 ゼオライト製造用有機構造指向剤、及びこれを用いたゼオライトの製造方法
JP2023502595A (ja) * 2019-11-19 2023-01-25 ビーエーエスエフ コーポレーション ゼオライト合成
CN111017950A (zh) * 2019-12-31 2020-04-17 山东齐鲁华信高科有限公司 一种低成本ssz-13分子筛的制备方法及应用
CN115178231B (zh) * 2021-04-01 2024-05-07 中国科学院大连化学物理研究所 一种吸附剂及其制备方法、应用

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Also Published As

Publication number Publication date
WO2013028958A1 (en) 2013-02-28
JP2014527017A (ja) 2014-10-09
CN104010971A (zh) 2014-08-27
JP6112568B2 (ja) 2017-04-12
EP2748109B1 (en) 2020-06-03
EP2748109A1 (en) 2014-07-02
US20150343375A1 (en) 2015-12-03
ES2812508T3 (es) 2021-03-17
PL2748109T3 (pl) 2020-11-16
US20130052125A1 (en) 2013-02-28
KR101991529B1 (ko) 2019-06-20
EP2748109A4 (en) 2015-05-27
KR20140057616A (ko) 2014-05-13
US9174849B2 (en) 2015-11-03

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Granted publication date: 20161109