CN104010713B - 制造氢气分离复合膜的方法 - Google Patents

制造氢气分离复合膜的方法 Download PDF

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Publication number
CN104010713B
CN104010713B CN201280062973.7A CN201280062973A CN104010713B CN 104010713 B CN104010713 B CN 104010713B CN 201280062973 A CN201280062973 A CN 201280062973A CN 104010713 B CN104010713 B CN 104010713B
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CN
China
Prior art keywords
support
gas
coated
particulate material
particle size
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Expired - Fee Related
Application number
CN201280062973.7A
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English (en)
Chinese (zh)
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CN104010713A (zh
Inventor
J·C·索凯蒂斯
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Shell Internationale Research Maatschappij BV
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Shell Internationale Research Maatschappij BV
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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/10—Supported membranes; Membrane supports
    • B01D69/108—Inorganic support material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/22—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by diffusion
    • B01D53/228—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by diffusion characterised by specific membranes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0039—Inorganic membrane manufacture
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0039—Inorganic membrane manufacture
    • B01D67/0046—Inorganic membrane manufacture by slurry techniques, e.g. die or slip-casting
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0039—Inorganic membrane manufacture
    • B01D67/0069—Inorganic membrane manufacture by deposition from the liquid phase, e.g. electrochemical deposition
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0039—Inorganic membrane manufacture
    • B01D67/0076—Pretreatment of inorganic membrane material prior to membrane formation, e.g. coating of metal powder
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0081—After-treatment of organic or inorganic membranes
    • B01D67/0095—Drying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/02—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor characterised by their properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/10—Supported membranes; Membrane supports
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/12—Composite membranes; Ultra-thin membranes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/12—Composite membranes; Ultra-thin membranes
    • B01D69/1213—Laminated layers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/02—Inorganic material
    • B01D71/022—Metals
    • B01D71/0223—Group 8, 9 or 10 metals
    • B01D71/02231—Palladium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen; Reversible storage of hydrogen
    • C01B3/50—Separation of hydrogen or hydrogen-containing gases from gaseous mixtures, e.g. purification
    • C01B3/501—Separation of hydrogen or hydrogen-containing gases from gaseous mixtures, e.g. purification by diffusion
    • C01B3/503—Separation of hydrogen or hydrogen-containing gases from gaseous mixtures, e.g. purification by diffusion characterised by membranes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/16—Hydrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2323/00—Details relating to membrane preparation
    • B01D2323/08—Specific temperatures applied
    • B01D2323/081—Heating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2323/00—Details relating to membrane preparation
    • B01D2323/10—Specific pressure applied
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2325/00—Details relating to properties of membranes
    • B01D2325/02—Details relating to pores or porosity of the membranes
    • B01D2325/0283—Pore size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2325/00—Details relating to properties of membranes
    • B01D2325/06—Surface irregularities
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2325/00—Details relating to properties of membranes
    • B01D2325/22—Thermal or heat-resistance properties

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Electrochemistry (AREA)
  • Combustion & Propulsion (AREA)
  • Analytical Chemistry (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Hydrogen, Water And Hydrids (AREA)
CN201280062973.7A 2011-12-19 2012-12-17 制造氢气分离复合膜的方法 Expired - Fee Related CN104010713B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201161577479P 2011-12-19 2011-12-19
US61/577,479 2011-12-19
PCT/US2012/070064 WO2013096183A1 (en) 2011-12-19 2012-12-17 A method of making a hydrogen separation composite membrane

Publications (2)

Publication Number Publication Date
CN104010713A CN104010713A (zh) 2014-08-27
CN104010713B true CN104010713B (zh) 2016-06-01

Family

ID=47505346

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201280062973.7A Expired - Fee Related CN104010713B (zh) 2011-12-19 2012-12-17 制造氢气分离复合膜的方法

Country Status (8)

Country Link
US (1) US20130156945A1 (https=)
EP (1) EP2794066B1 (https=)
JP (1) JP2015507533A (https=)
KR (1) KR20140108642A (https=)
CN (1) CN104010713B (https=)
CA (1) CA2858403A1 (https=)
TW (1) TW201336577A (https=)
WO (1) WO2013096183A1 (https=)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101475679B1 (ko) * 2012-12-14 2014-12-23 한국에너지기술연구원 이산화탄소 포집용 수소 분리막 모듈
WO2015157414A1 (en) * 2014-04-10 2015-10-15 Shell Oil Company A method of making a supported gas separation membrane
JP6787790B2 (ja) * 2014-04-10 2020-11-18 シエル・インターナシヨナル・リサーチ・マートスハツペイ・ベー・ヴエー 担持されたガス分離膜を作製する方法
US20210308630A1 (en) * 2020-04-07 2021-10-07 Ralph Aaron Bauer Support for Nano-Thickness Membranes
CN111686586B (zh) * 2020-06-29 2022-06-07 山东理工大学 一种用于在氧化铝中空纤维膜内表面制备钯膜的真空流动化学镀法

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU2003221816A1 (en) * 2002-04-03 2003-10-20 Colorado School Of Mines Process for preparing palladium alloy composite membranes for use in hydrogen separation, palladium alloy composite membranes and products incorporating or made from the membranes
CA2519774A1 (en) 2003-03-21 2004-10-07 Worcester Polytechnic Institute Method for fabricating composite gas separation modules
JP4379684B2 (ja) * 2003-07-09 2009-12-09 株式会社豊田中央研究所 流体分離フィルタおよびその製造方法と燃料電池システム
EP1723999B1 (en) * 2004-03-12 2017-06-07 NGK Insulators, Ltd. Carbon film laminate and method for production thereof, and voc removing device
JP2005262082A (ja) * 2004-03-18 2005-09-29 National Institute Of Advanced Industrial & Technology 水素分離膜、その製造方法並びに水素の分離方法
US7727596B2 (en) 2004-07-21 2010-06-01 Worcester Polytechnic Institute Method for fabricating a composite gas separation module
JP2008513337A (ja) * 2004-09-21 2008-05-01 ウスター ポリテクニック インスティチュート 膜増強反応器
JP2007000858A (ja) * 2005-05-23 2007-01-11 Kobe Steel Ltd 水素透過部材およびその製造方法
CN101351263B (zh) * 2006-07-20 2012-09-05 日本碍子株式会社 陶瓷过滤器
US7744675B2 (en) 2006-11-08 2010-06-29 Shell Oil Company Gas separation membrane comprising a substrate with a layer of coated inorganic oxide particles and an overlayer of a gas-selective material, and its manufacture and use
US7959711B2 (en) 2006-11-08 2011-06-14 Shell Oil Company Gas separation membrane system and method of making thereof using nanoscale metal material
ES2476801T3 (es) 2007-02-20 2014-07-15 Shell Internationale Research Maatschappij B.V. Un método para reacondicionar una membrana de separación de gases
US8048199B2 (en) * 2007-02-20 2011-11-01 Shell Oil Company Method of making a leak stable gas separation membrane system
US20080255811A1 (en) * 2007-04-13 2008-10-16 Zi Qiang Sheng System and Method for Determining Surface Roughness
US20090277331A1 (en) * 2008-05-09 2009-11-12 Membrane Reactor Technologies Ltd. Hydrogen separation composite membrane module and the method of production thereof
JP5354516B2 (ja) * 2008-08-15 2013-11-27 日本碍子株式会社 水素分離体
JP5526387B2 (ja) * 2010-03-29 2014-06-18 独立行政法人産業技術総合研究所 無欠陥化水素分離膜、無欠陥化水素分離膜の製造方法及び水素分離方法

Also Published As

Publication number Publication date
JP2015507533A (ja) 2015-03-12
CN104010713A (zh) 2014-08-27
TW201336577A (zh) 2013-09-16
CA2858403A1 (en) 2013-06-27
US20130156945A1 (en) 2013-06-20
KR20140108642A (ko) 2014-09-12
EP2794066B1 (en) 2019-08-14
WO2013096183A1 (en) 2013-06-27
EP2794066A1 (en) 2014-10-29

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Granted publication date: 20160601

Termination date: 20211217