CN103992140B - A kind of copper iron look sunlight becomes gold ring temmoku glaze and makes the method for household china of it - Google Patents
A kind of copper iron look sunlight becomes gold ring temmoku glaze and makes the method for household china of it Download PDFInfo
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- CN103992140B CN103992140B CN201410262647.1A CN201410262647A CN103992140B CN 103992140 B CN103992140 B CN 103992140B CN 201410262647 A CN201410262647 A CN 201410262647A CN 103992140 B CN103992140 B CN 103992140B
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- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical group [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 title claims abstract description 19
- IYRDVAUFQZOLSB-UHFFFAOYSA-N copper iron Chemical compound [Fe].[Cu] IYRDVAUFQZOLSB-UHFFFAOYSA-N 0.000 title claims abstract description 17
- 238000000034 method Methods 0.000 title claims abstract description 15
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims abstract description 13
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 12
- NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical compound O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229940036811 bone meal Drugs 0.000 claims abstract description 8
- 239000002374 bone meal Substances 0.000 claims abstract description 8
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims abstract description 8
- -1 4 ~ 6 parts Inorganic materials 0.000 claims abstract description 7
- 229910021532 Calcite Inorganic materials 0.000 claims abstract description 7
- 239000004927 clay Substances 0.000 claims abstract description 7
- 239000010433 feldspar Substances 0.000 claims abstract description 7
- 239000010453 quartz Substances 0.000 claims abstract description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000000454 talc Substances 0.000 claims abstract description 7
- 235000012222 talc Nutrition 0.000 claims abstract description 7
- 229910052623 talc Inorganic materials 0.000 claims abstract description 7
- 238000010304 firing Methods 0.000 claims description 10
- 238000000227 grinding Methods 0.000 claims description 7
- 239000002994 raw material Substances 0.000 claims description 7
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 6
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 6
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 6
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 6
- 238000002386 leaching Methods 0.000 claims description 6
- 238000005507 spraying Methods 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 238000009413 insulation Methods 0.000 claims 1
- 238000002425 crystallisation Methods 0.000 abstract description 8
- 230000008025 crystallization Effects 0.000 abstract description 8
- 239000000126 substance Substances 0.000 abstract description 7
- 239000003973 paint Substances 0.000 abstract description 4
- FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical compound C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 abstract description 3
- 230000035807 sensation Effects 0.000 abstract description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 10
- 229910052573 porcelain Inorganic materials 0.000 description 6
- 238000005245 sintering Methods 0.000 description 6
- 230000015572 biosynthetic process Effects 0.000 description 5
- 229910052742 iron Inorganic materials 0.000 description 5
- 238000002791 soaking Methods 0.000 description 5
- 239000013078 crystal Substances 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 239000000919 ceramic Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 2
- 239000000292 calcium oxide Substances 0.000 description 2
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- GNTDGMZSJNCJKK-UHFFFAOYSA-N divanadium pentaoxide Chemical compound O=[V](=O)O[V](=O)=O GNTDGMZSJNCJKK-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 230000004927 fusion Effects 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 239000000395 magnesium oxide Substances 0.000 description 2
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 2
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
- 238000005191 phase separation Methods 0.000 description 2
- 239000004408 titanium dioxide Substances 0.000 description 2
- 241001125671 Eretmochelys imbricata Species 0.000 description 1
- 241001165859 Perdicinae Species 0.000 description 1
- 241001122767 Theaceae Species 0.000 description 1
- 241001300078 Vitrea Species 0.000 description 1
- 239000001506 calcium phosphate Substances 0.000 description 1
- 229910000389 calcium phosphate Inorganic materials 0.000 description 1
- 235000011010 calcium phosphates Nutrition 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 239000010437 gem Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- YOBAEOGBNPPUQV-UHFFFAOYSA-N iron;trihydrate Chemical compound O.O.O.[Fe].[Fe] YOBAEOGBNPPUQV-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000009377 nuclear transmutation Methods 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 229910001112 rose gold Inorganic materials 0.000 description 1
- 238000010583 slow cooling Methods 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 1
Abstract
The present invention relates to a kind of copper iron look sunlight and become gold ring temmoku glaze, this glaze comprises following component and weight proportion number: 14 ~ 28 parts, quartz, clay 3 ~ 8 parts, burn 6 ~ 12 parts, talcum, 4 ~ 6 parts, calcite, bone meal 6 ~ 15 parts, feldspar 40 ~ 55 parts, ferric oxide 8 ~ 15 parts, burns titanium oxide 0 ~ 3 part, ferric metasilicate 0.05 ~ 0.15 part; The present invention also provides a kind of copper iron look sunlight to become the method for gold ring temmoku glaze making household china, the copper iron look sunlight that the method obtains becomes gold ring temmoku glaze household china crystalline substance flower and is of moderate size, flower shape rounding, crystallization is evenly distributed, and crystalline substance is spent golden yellow, and level is changeable, stereoscopic sensation is strong, product quality is more stable, and glossiness is good, and glaze paint is smoothly gentle.
Description
Technical field
The present invention relates to a kind of method that copper iron look sunlight becomes gold ring temmoku glaze and makes household china of it.
Background technology
Namely temmoku glaze puts up a kiln the black small cup the fired call in Japan.Put up a kiln with Jianyang, Fujian Province's today for representative, kiln site in Shui Ji town, Jianyang, to produce black porcelain and famous.The Tang Dynasty firstly appears burning, is hemera to the Song dynasty especially Southern Song Dynasty, the end to the Qing Dynasty.Among the ceramic artistic glaze kind of China, " temmoku glaze " comes from the Song dynasty, refers to that Fujian puts up a kiln and the tea small cup of Jiangxi Chien ware the earliest.Porcelain common name " temmoku " of its Fan Shihei glaze, as the francolin spot, hawksbill turtle, oil droplet, iron embroidery, sunlight change etc. that are commonly called as.And yohen Tenmoku Ze Shi China wherein one of precious transmutation crystalline glaze of inventing the earliest period of the Southern Song Dynasty in history, treasure handed down from ancient times is lost centuries already.Its burning techniques is called as " masterstroke ", and masterstroke " god " is executing a kind of glaze colours, and namely one firedly present colorful, and change unpredictably, the xln that feature is different is that the pure natural that people's will not can be is formed.This porcelain has its very important status in China's porcelain developing history, is considered to the higher boundary of pottery collection.
Yohen Tenmoku is special because filling a prescription, and fires difficulty, and many experts of China, scholar is also concentrating on studies.As far back as 20 century 70s, existing ceramic colour glaze Senior Expert, inventor Zhang Yuchun is first born with and carries out theoretic discussion to iron system crystalline glaze (i.e. temmoku glaze) at " artistic glaze " of his work in book, and tries to have burnt the temmoku bowl that crystal formation exactly likes treasure in practice.1981, " iron oxide red gold ring crystalline glaze " porcelain works of crystalline glaze study group of Tangshan ceramics institute exploitation, being regarded as by existing famous ancient pottery and porcelain expert Mr. Ye Hongming and have " sunlight change " feature, through the expert statement of State Scientific and Technological Commission, was a domestic initiation gem of art.
Yohen Tenmoku and serial new lines iron tying crystalline substance, based on the liquid phase separation of high temperature fusibility, oxydizing flame or reducing flame once-firing, usually leaded.And due to the composition of glaze and sintering technology complex, the mobility of glaze is very large, and firing range is extremely narrow, occurs that the effect of brilliant flower is completely different in different situations of firing.The compound that sunlight becomes crystallization iron is in kiln in high-temperature fusion, first the glaze layer surface of thickness is gone out, again in localized clusters, growth, stagnation, fusion, this is the change that people cannot estimate and control, if brilliant flower can not normal development and precipitation or produce diffusion, or trickle change occurs some condition, or in sintering procedure, be difficult to the duration and degree of heating controlled, usually cause yield rate low, and quality is unstable.
Summary of the invention
The object of the present invention is to provide a kind of copper iron look sunlight to become gold ring temmoku glaze and make the method for household china of it, to solve Problems existing and defect in above-mentioned technology, producing a kind of red with more macrocrystalline temmoku glaze.
For achieving the above object, the present invention by the following technical solutions:
A kind of copper iron look sunlight becomes gold ring temmoku glaze, comprises following component and weight proportion number: 14 ~ 28 parts, quartz, clay 3 ~ 8 parts, burns 6 ~ 12 parts, talcum, 4 ~ 6 parts, calcite, bone meal 6 ~ 15 parts, feldspar 40 ~ 55 parts, ferric oxide 8 ~ 15 parts, burns titanium oxide 0 ~ 3 part, ferric metasilicate 0.05 ~ 0.15 part.
The present invention also provides a kind of copper iron look sunlight to become the preparation method of gold ring temmoku glaze household china, comprises the following steps:
Step 1: get raw material by above-mentioned weight proportion number and enter mill, take total mass as benchmark, add the water that mass percent is 45-48%, grinding 18-20 hour, fineness control 250 mesh sieves tail over≤0.1%, add 0.1% carboxymethyl cellulose grinding 2 hours, cross 200 mesh sieves;
Step 2: add ferric metasilicate 0.05-0.15% and mix;
Step 3: the technique glazing adopting leaching glaze or glaze spraying, glazed thickness controls at 0.3-0.4mm thickness, klining is entered after oven dry, firing temperature controls at 1250 DEG C-1260 DEG C, and be then incubated, soaking time is short, control at 5-10min, be slow cooling to 900 DEG C with the speed of 120-180 DEG C/h again, be convenient to the formation of brilliant flower and grow up, then naturally cooling to room temperature.
Burn titanium oxide in the product, mainly with titanium dioxide generation effect, titanium dioxide contributes to Vitrea phase-splitting, reduces viscosity of vitreous, promotes crystallization; Calcium oxide, aluminum oxide, magnesium oxide are introduced with quartzy form, and calcium oxide contributes to increasing vitreum to the solubleness of ferric oxide, reduces maturing temperature and the viscosity of vitreous of glaze, contributes to crystallization; The high temperature viscosity of content on glaze of aluminum oxide has larger impact, plays an important role to the formation of crystallization and crystal growth; Magnesium oxide it can promote to present the growth of pleonast(e) and brown glaze paint, and be conducive to the formation of crystal.Calcium phosphate affects the colour generation of iron crystalline glaze, introduces with bone meal form, and when its content reaches 8%-15%, there will be bright-coloured redness crystalline substance flower, it is suitable for adding 10%-15%, because the Vanadium Pentoxide in FLAKES in formula is one of composition making the easy liquid phase separation of iron-red glaze crystallization; When ferric oxide in filling a prescription content lower than 8% time, glaze paint presents brown instead of red, and along with the increase of iron oxide content, glaze towards red transition, and has golden yellow brilliant flower; The introducing of ferric metasilicate, plays crystal seed, is beneficial to brilliant flower and is uniformly distributed, simplify the technology difficulty that size controls.
Compared with prior art, the present invention has following beneficial effect:
1. improve leadless glaze glaze firing yield rate, the product of production is not leaded, and stay in grade, quality is significantly better than there being plumbous product;
2. crystalline substance has the bright crystallization of more gold to occur in spending, and greatly meets the requirement of decoration.
Embodiment
Below in conjunction with embodiment, the present invention is further illustrated.
Embodiment 1
Present embodiment discloses a kind of copper iron look sunlight and become gold ring temmoku glaze, comprise component and weight proportion number is 14 parts, quartz, clay 3 parts, burns 10 parts, talcum, 6 parts, calcite, bone meal 12 parts, feldspar 45 parts, ferric oxide 12 parts, burns titanium oxide 1 part, ferric metasilicate 0.1 part.
Above-mentioned raw materials is entered mill, and be benchmark with total mass, add the water that mass percent is 45%, grind 18 hours, fineness controls to tail over 0.1% at 250 mesh sieves, adds 0.1% carboxymethyl cellulose grinding 2 hours, crosses 200 mesh sieves; Add ferric metasilicate 0.1% to mix; Adopt the technique glazing of leaching glaze or glaze spraying, glazed thickness controls at 0.3mm thickness, klining is entered after oven dry, firing temperature controls at 1250 DEG C, when close to maximum sintering temperature, be rapidly heated, soaking time controls at 5min, cool to 900 DEG C with the speed of 120 DEG C/h again, then naturally cool to room temperature.
Copper iron look sunlight prepared by the present embodiment becomes gold ring temmoku glaze household china product, and the colored shape of crystalline substance is of moderate size, flower shape rounding, and crystallization is evenly distributed, and crystalline substance is spent golden yellow, and level is changeable, and stereoscopic sensation is strong, and product quality is more stable, and glossiness, good brightness, glaze paint is smoothly gentle.
Embodiment 2
Present embodiment discloses a kind of copper iron look sunlight and become gold ring temmoku glaze, comprise component and weight proportion number is 14 parts, quartz, clay 5 parts, burns 12 parts, talcum, 2 parts, calcite, bone meal 11 parts, feldspar 49 parts, ferric oxide 11 parts, burns titanium oxide 1 part, ferric metasilicate 0.1.
Above-mentioned raw materials is entered mill, and be benchmark with total mass, add the water that mass percent is 48%, grind 20 hours, fineness controls to tail over 0.05% at 250 mesh sieves, adds 0.1% carboxymethyl cellulose grinding 2 hours, crosses 200 mesh sieves; Add ferric metasilicate 0.1% to mix; Adopt the technique glazing of leaching glaze or glaze spraying, glazed thickness controls at 0.4mm thickness, klining is entered after oven dry, firing temperature controls, at 1260 DEG C, when close to maximum sintering temperature, to be rapidly heated, soaking time controls at 10min, cool to 900 DEG C with the speed of 150 DEG C/h again, be convenient to the formation of brilliant flower and grow up, then naturally cooling to room temperature.
Embodiment 3
Present embodiment discloses a kind of copper iron look sunlight and become gold ring temmoku glaze, comprise component and weight proportion number is 16 parts, quartz, clay 7 parts, burns 12 parts, talcum, 3 parts, calcite, bone meal 11 parts, feldspar 49 parts, ferric oxide 11 parts, burns titanium oxide 1 part, ferric metasilicate 0.1 part.
Above-mentioned raw materials is entered mill, and be benchmark with total mass, add the water that mass percent is 47%, grind 19 hours, fineness controls to tail over 0.08% at 250 mesh sieves, adds 0.1% carboxymethyl cellulose grinding 2 hours, crosses 200 mesh sieves; Add ferric metasilicate 0.1% to mix; Adopt the technique glazing of leaching glaze or glaze spraying, glazed thickness controls at 0.35mm thickness, klining is entered after oven dry, firing temperature controls at 1255 DEG C, when close to maximum sintering temperature, be rapidly heated, soaking time controls at 8min, cool to 900 DEG C with the speed of 180 DEG C/h again, then naturally cool to room temperature.
Embodiment 4
Present embodiment discloses a kind of copper iron look sunlight and become gold ring temmoku glaze, comprise component and weight proportion number is 14 parts, quartz, clay 4 parts, burns 12 parts, talcum, 5 parts, calcite, bone meal 11 parts, feldspar 49 parts, ferric oxide 11 parts, burns titanium oxide 0.08 part, ferric metasilicate 0.08 part.
Above-mentioned raw materials is entered mill, and be benchmark with total mass, add the water that mass percent is 45%, grind 18 hours, fineness controls to tail over 0.05% at 250 mesh sieves, adds 0.1% carboxymethyl cellulose grinding 2 hours, crosses 200 mesh sieves; Add ferric metasilicate 0.08% to mix; Adopt the technique glazing of leaching glaze or glaze spraying, glazed thickness controls at 0.4mm thickness, klining is entered after oven dry, firing temperature controls at 1260 DEG C, when close to maximum sintering temperature, be rapidly heated, soaking time controls at 8min, cool to 900 DEG C with the speed of 160 DEG C/h again, then naturally cool to room temperature.
Claims (2)
1. a copper iron look sunlight becomes gold ring temmoku glaze, it is characterized in that, comprise following component and weight proportion number: 14 ~ 28 parts, quartz, clay 3 ~ 8 parts, burn 6 ~ 12 parts, talcum, 4 ~ 6 parts, calcite, bone meal 6 ~ 15 parts, feldspar 40 ~ 55 parts, ferric oxide 8 ~ 15 parts, burn titanium oxide 0 ~ 3 part, ferric metasilicate 0.05 ~ 0.15 part.
2. become with copper iron look sunlight according to claim 1 the method that gold ring temmoku glaze makes household china, it is characterized in that, comprise the following steps:
Step 1: become the raw material of gold ring temmoku glaze and proportioning by described copper iron look sunlight and take desired raw material and enter mill, take total mass as benchmark, add the water that mass percent is 45-48%, grinding 18-20 hour, fineness control 250 mesh sieves tail over≤0.1%, add 0.1% carboxymethyl cellulose and grind 2 hours again, cross 200 mesh sieves;
Step 2: add ferric metasilicate 0.05-0.15% and mix;
Step 3: the technique glazing adopting leaching glaze or glaze spraying, glazed thickness controls at 0.3-0.4mm, enters klining after oven dry, firing temperature controls at 1250 DEG C-1260 DEG C, insulation 5-10min, then cool to 900 DEG C with the speed of 120-180 DEG C/h, then naturally cool to room temperature.
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CN105272376B (en) * | 2015-11-09 | 2017-04-05 | 醴陵陶润实业发展有限公司 | Transmutation temmoku glaze and preparation method thereof |
CN107265863A (en) * | 2017-08-02 | 2017-10-20 | 宜兴市金鱼陶瓷有限公司 | A kind of celadon with iron oxide red gold ring glaze layer and preparation method thereof |
CN109052944A (en) * | 2018-09-14 | 2018-12-21 | 湖南高峰陶瓷制造有限公司 | Temmoku glaze and preparation method thereof |
CN113912293B (en) * | 2021-08-24 | 2023-07-04 | 福建良瓷科技有限公司 | Formula of Tianmu glaze special for sanitary ceramic and glazing method |
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CN103172406A (en) * | 2013-04-12 | 2013-06-26 | 徐维茂 | Gold spot temmoku glaze and preparation technology thereof |
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临安天目兔毫釉的研究与探讨;高晟等;《山东陶瓷》;20131031;第36卷(第5期);13-17 * |
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Denomination of invention: A copper iron obsidian gold ring Tianmu glaze and a method for making daily porcelain using it Effective date of registration: 20231214 Granted publication date: 20160106 Pledgee: China Co. truction Bank Corp Chaozhou branch Pledgor: Guangdong Songfa Ceramics Co.,Ltd. Registration number: Y2023980071819 |
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