CN103172406A - Gold spot temmoku glaze and preparation technology thereof - Google Patents
Gold spot temmoku glaze and preparation technology thereof Download PDFInfo
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- CN103172406A CN103172406A CN2013101257920A CN201310125792A CN103172406A CN 103172406 A CN103172406 A CN 103172406A CN 2013101257920 A CN2013101257920 A CN 2013101257920A CN 201310125792 A CN201310125792 A CN 201310125792A CN 103172406 A CN103172406 A CN 103172406A
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Abstract
The invention relates to a gold spot temmoku glaze and a preparation technology thereof. The preparation technology is characterized by comprising the steps of processing gold spot temmoku glaze ceramic glaze and a green body raw material, glazing, sintering and checking. The gold spot temmoku glaze provided by the invention fills the gap that temmoku glaze ceramic has no golden flow liners or spots, a new variety is added to the temmoku glaze ceramic, and the gold spot temmoku glaze prepared by utilizing the preparation technology provided by the invention is mainly characterized by taking black as a substrate, flow liners or spots on the surface of the gold spot temmoku glaze are gold, and the colour of the gold spot temmoku glaze is gorgeous, so that the gold spot temmoku glaze has a good decorative effect; and the preparation technology of the gold spot temmoku glaze is simple, the flow is scientific and reasonable, the preparation efficiency is higher, the energy is saved and the environment is protected, so that the preparation technology provided by the invention is applicable to large-scale development and application.
Description
Technical field
The invention belongs to pottery with the preparation technology field of glaze, relate in particular to a kind of golden spot temmoku glaze and preparation technology thereof.
Background technology
Temmoku glaze is porcelain glaze color name, and it is to present the color glaze of strip or grivelle on a kind of chocolate or dark brown background color.It is documented, 12-13 century Japan Buddhist monk takes back black glaze porcelain so gain the name from Tianmu Mountains of Zhejiang Province.The temmoku glaze kind is more, and famous and precious have oil droplet, the writing brush made of rabbit's hair, francolin spot, a hawksbill turtle etc.Simultaneously, temmoku glaze is again the common name of iron black crystalline glaze of Song dynasty.
Since ancient times, successively there are countless ceramic famous experts and ceramist all temmoku glaze to be copied and studied, countless ceramics personnel think to burn out on the surface of pottery golden color, even the gold of part is also the target that the ceramics personnel pursue, golden glaze, spot and flow liner are the glaze decorating effects dreamed of of porcelain making people since ancient times, but nearly one thousand years ceramics personnel never find suitable formula and firing process.
Summary of the invention
The present invention designed a kind of golden spot temmoku glaze and preparation technology thereof, and its ceramics personnel for thousands of years of having solved can't prepare the problem of the temmoku glaze with golden spot and golden flow liner glaze.
In order to solve the technical problem of above-mentioned existence, the present invention has adopted following scheme:
The present invention has provided a kind of feed composition formula of golden spot temmoku glaze, gold spot temmoku glaze enamel comprises following feed composition according to the massfraction meter: feldspar 30%-55%, kaolin 2%-6%, high iron ore soil 4%-9%, quartzy 20%-30%, titanium dioxide 1%-5%, Linan glaze soil 2%-10%, Wingdale 3%-8%, talcum 2%-10%; Gold spot temmoku glaze base substrate comprises following feed composition according to the massfraction meter: feldspar 10%-25%, Zijin soil 20%-40%, porcelain stone 35%-50%, quartzy 16%-26%, high iron ore soil 2%-10%.
The present invention gives a kind of feed composition formula of this gold spot temmoku glaze, gold spot temmoku glaze enamel comprises following feed composition according to the massfraction meter: feldspar 40%-48%, kaolin 3%-5%, high iron ore soil 6%-8%, quartzy 23%-27.5%, titanium dioxide 1%-2%, Linan glaze soil 5%-8%, Wingdale 5%-7%, talcum 3%-8%; Gold spot temmoku glaze base substrate comprises following feed composition according to the massfraction meter: feldspar 12%-18%, Zijin soil 23%-35%, porcelain stone 38%-45%, quartzy 18%-24%, high iron ore soil 4%-8%.
The present invention gives a kind of preparation technology of golden spot temmoku glaze, comprises the steps: step 1 to golden spot temmoku glaze enamel and blank raw material is processed, step 2 glazing, step 3 are burnt till, step 4 is checked.The step 1 Raw material processing comprises the grinding screening successively, proportioning, and dehydration, old, manual assembly, repaired biscuit and drying process.Grind in screening process the long 10%-25% of time that described golden spot temmoku glaze base substrate mud grinds that is compared to for the milling time of golden spot temmoku glaze enamel glaze water; Dehydration procedure is to adopt pressure filter to dewater, and after described dehydration, the water ratio of raw material is 20%-24%; The old time is 15-30 days; Drying temperature is 50 ℃-90 ℃, and dry humidity is 30%-40%, and be 20h-40h time of drying.The step 2 glazing is that described golden spot temmoku glaze enamel glaze water concentration is transferred to water ratio is 35%-40%, again golden spot temmoku glaze enamel glaze water is positioned over than in the large container of the golden spot temmoku glaze base substrate of want glazing, the mode that employing is oozed and soaked, make golden spot temmoku glaze enamel glaze water adhesion in the surface of described golden spot temmoku glaze base substrate, and make glaze water thickness reach 0.9mm-1.2mm; If one time glazing thickness can't reach 0.9mm-1.2mm, with the dry 8h-10h under the condition of 50 ℃-80 ℃ of golden spot temmoku glaze base substrate after a glazing, make its water ratio at 8%-10%, then adopt spray gun, make the water ratio of the golden spot temmoku glaze base substrate after glazing reach 6%-8%.Spray gun adopts air compressor machine pressurized air as power, and the pressure range of spray gun air compressor machine is 0.1MP-0.2MP.It is to burn to 1260 ℃-1290 ℃ after the product loading of kiln after the step 2 glazing, then to cool the temperature to 1230 ℃-1240 ℃ that step 3 is burnt till, and after insulation 60min, is cooled to below 100 ℃ and gets final product kiln discharge, and the required time of firing is 12h-15h.Step 3 is burnt till middle employing drawer kiln and is utilized oil liquefied gas to burn till as fuel; Heat-up rate in sintering process is 2-3 ℃/min.The project of step 4 check is for having obvious golden spot or flow liner to require simultaneously finished product device deformation form quotient less than 5%.Simultaneously also need to check the glaze surface imperfection, such as situations such as: pin hole, contracting glaze, scarce glaze, glaze are smooth.
This gold spot temmoku glaze and preparation technology thereof have following beneficial effect:
1, the present invention gold spot temmoku glaze has been filled up the blank that the temmoku glaze pottery does not have golden flow liner and spot, for the temmoku vitreous enamel has increased a new kind.
2, the golden spot temmoku glaze that utilizes preparation technology of the present invention to prepare mainly refers to it with the black substrate, and it is golden that its surperficial flow liner or spot are, and its color is gorgeous, and very well decorative effect is arranged.
3, the preparation technology of the present invention's gold spot temmoku glaze is simple, and flow process is scientific and reasonable, the application of proper scale.
4, the higher and energy-conserving and environment-protective of the preparation efficiency of the present invention gold spot temmoku glaze.
Embodiment
Below in conjunction with specific embodiment, the present invention will be further described:
Embodiment 1
The feed composition formula of gold spot temmoku glaze, golden spot temmoku glaze enamel comprises following feed composition according to the massfraction meter: feldspar 40%, kaolin 4%, high iron ore soil 6%, quartz 25%, titanium dioxide 2%, Linan glaze soil 8%, Wingdale 7%, talcum 8%; Gold spot temmoku glaze base substrate comprises following feed composition according to the massfraction meter: feldspar 12%, Zijin soil 23%, porcelain stone 38%, quartz 22%, high iron ore soil 5%.
Need to carry out field trip in the process of carrying out material choice, gather raw material and raw material is carried out physico-chemical analysis, begin raw material is processed through screening with after eluriating.
To golden spot temmoku glaze enamel with blank raw material is processed, Raw material processing comprises successively and grinds screening, proportioning, dehydration, old, manual assembly, repaired biscuit and drying process.Grind in screening process the time long 10% that described golden spot temmoku glaze base substrate mud grinds that is compared to for the milling time of golden spot temmoku glaze enamel glaze water; Dehydration procedure is to adopt pressure filter to dewater, and after dehydration, the water ratio of raw material is 20%; The old time is 15 days; Drying temperature is 650 ℃, and dry humidity is 34%, and be 25h time of drying.Glazing is that described golden spot temmoku glaze enamel glaze water concentration is transferred to water ratio is 36%, again golden spot temmoku glaze enamel glaze water is positioned over than in the large container of the golden spot temmoku glaze base substrate of want glazing, the mode that employing is oozed and soaked, make golden spot temmoku glaze enamel glaze water adhesion in the surface of described golden spot temmoku glaze base substrate, and make glaze water thickness reach 0.9mm; If one time glazing thickness can't reach 0.9mm, with golden spot temmoku glaze base substrate dry 10h under the condition of 65 ℃ after a glazing, make its water ratio 8%, then adopt spray gun, make the water ratio of the golden spot temmoku glaze base substrate after glazing reach 6%.Spray gun adopts air compressor machine pressurized air as power, and the pressure range of spray gun air compressor machine is 0.1MP-0.2MP.Burning till is to burn to 1260 ℃ after the product loading of kiln after glazing, then to cool the temperature to 1230 ℃, after insulation 60min, is cooled to 90 ℃ and gets final product kiln discharge, and the required time of firing is 12h.Adopt the drawer kiln in sintering process and utilize oil liquefied gas to burn till as fuel; Heat-up rate in sintering process is 2 ℃/min.Through this product of check have obvious golden spot or flow liner simultaneously this finished product device deformation form quotient be 0.85%.The situations such as free of pinholes, contracting glaze, scarce glaze, glaze is smooth.
Embodiment 2
The feed composition formula of gold spot temmoku glaze, golden spot temmoku glaze enamel comprises following feed composition according to the massfraction meter: feldspar 46%, kaolin 5%, high iron ore soil 8%, quartz 27%, titanium dioxide 1%, Linan glaze soil 5%, Wingdale 5%, talcum 3%; Gold spot temmoku glaze base substrate comprises following feed composition according to the massfraction meter: feldspar 14%, Zijin soil 24%, porcelain stone 40%, quartz 18%, high iron ore soil 4%.
To golden spot temmoku glaze enamel with blank raw material is processed, Raw material processing comprises successively and grinds screening, proportioning, dehydration, old, manual assembly, repaired biscuit and drying process.Grind in screening process the time long 25% that described golden spot temmoku glaze base substrate mud grinds that is compared to for the milling time of golden spot temmoku glaze enamel glaze water; Dehydration procedure is to adopt pressure filter to dewater, and after dehydration, the water ratio of raw material is 24%; The old time is 28 days; Drying temperature is 85 ℃, and dry humidity is 38%, and be 40h time of drying.Glazing is that described golden spot temmoku glaze enamel glaze water concentration is transferred to water ratio is 40%, again golden spot temmoku glaze enamel glaze water is positioned over than in the large container of the golden spot temmoku glaze base substrate of want glazing, the mode that employing is oozed and soaked, make golden spot temmoku glaze enamel glaze water adhesion in the surface of described golden spot temmoku glaze base substrate, and make glaze water thickness reach 1.2mm; If one time glazing thickness can't reach 1.2mm, with golden spot temmoku glaze base substrate dry 8h under the condition of 75 ℃ after a glazing, make its water ratio 10%, then adopt spray gun, make the water ratio of the golden spot temmoku glaze base substrate after glazing reach 8%.Spray gun adopts air compressor machine pressurized air as power, and the pressure range of spray gun air compressor machine is 0.1MP-0.2MP.Burning till is to burn to 1290 ℃ after the product loading of kiln after glazing, then to cool the temperature to 1240 ℃, after insulation 60min, is cooled to 80 ℃ and gets final product kiln discharge, and the required time of firing is 14h.Burn till middle employing drawer kiln and utilize oil liquefied gas to burn till as fuel; Heat-up rate in sintering process is 3 ℃/min.Through this product of check, obvious golden spot or flow liner this finished product device deformation form quotient 1.05% is simultaneously arranged.Check simultaneously the glaze surface imperfection there is no the feelings such as pin hole, contracting glaze, scarce glaze, glaze is smooth.
Detect through instrument, all in certain scope, its scope sees following table for details for the base substrate of the golden spot temmoku glaze for preparing according to composition of raw materials and the preparation technology of the present invention's gold spot temmoku glaze and the chemical composition in glaze:
The chemical composition range of table one gold spot temmoku vitreous enamel base substrate and glaze
The above has carried out exemplary description to the present invention in conjunction with specific embodiments; obvious realization of the present invention is not subject to the restrictions described above; as long as the various improvement of having adopted method design of the present invention and technical scheme to carry out; or without improving, design of the present invention and technical scheme are directly applied to other occasion, all in protection scope of the present invention.
Claims (10)
1. golden spot temmoku glaze, it is characterized in that: described golden spot temmoku glaze enamel comprises following feed composition according to the massfraction meter: feldspar 30%-55%, kaolin 2%-6%, high iron ore soil 4%-9%, quartzy 20%-30%, titanium dioxide 1%-5%, Linan glaze soil 2%-10%, Wingdale 3%-8%, talcum 2%-10%; Described golden spot temmoku glaze base substrate comprises following feed composition according to the massfraction meter: feldspar 10%-25%, Zijin soil 20%-40%, porcelain stone 35%-50%, quartzy 16%-26%, high iron ore soil 2%-10%.
2. golden spot temmoku glaze according to claim 1, it is characterized in that: described golden spot temmoku glaze enamel comprises following feed composition according to the massfraction meter: feldspar 40%-48%, kaolin 3%-5%, high iron ore soil 6%-8%, quartzy 23%-27.5%, titanium dioxide 1%-2%, Linan glaze soil 5%-8%, Wingdale 5%-7%, talcum 3%-8%; Described golden spot temmoku glaze base substrate comprises following feed composition according to the massfraction meter: feldspar 12%-18%, Zijin soil 23%-35%, porcelain stone 38%-45%, quartzy 18%-24%, high iron ore soil 4%-8%.
3. the preparation technology of golden spot temmoku glaze as claimed in claim 1 or 2, is characterized in that comprising the steps:
Step 1 is processed golden spot temmoku glaze enamel and blank raw material;
The step 2 glazing;
Step 3 is burnt till;
The step 4 check.
4. the preparation technology of golden spot temmoku glaze according to claim 3 is characterized in that: described step 1 Raw material processing comprises successively and grinds screening, proportioning, and dehydration, old, manual assembly, repaired biscuit and drying process.
5. the preparation technology of golden spot temmoku glaze according to claim 4 is characterized in that:
The long 10%-25% of time that grinds for the described golden spot temmoku glaze base substrate mud of being compared to of the milling time of golden spot temmoku glaze enamel glaze water in described grinding screening process;
Described dehydration procedure is to adopt pressure filter to dewater, and after described dehydration, the water ratio of raw material is 20%-24%;
The described old time is 15-30 days; Described drying temperature is 50 ℃-90 ℃, and dry humidity is 30%-40%, and be 20h-40h time of drying.
6. the preparation technology of golden spot temmoku glaze according to claim 3, it is characterized in that: described step 2 glazing is that described golden spot temmoku glaze enamel glaze water concentration is transferred to water ratio is 35%-40%, again described golden spot temmoku glaze enamel glaze water is positioned over than in the large container of the described golden spot temmoku glaze base substrate of want glazing, the mode that employing is oozed and soaked, make described golden spot temmoku glaze enamel glaze water adhesion in the surface of described golden spot temmoku glaze base substrate, and make glaze water thickness reach 0.9mm-1.2mm; If one time glazing thickness can't reach 0.9mm-1.2mm, with the dry 8h-10h under the condition of 50 ℃-80 ℃ of golden spot temmoku glaze base substrate after a glazing, make its water ratio at 8%-10%, then adopt spray gun, make the water ratio of the golden spot temmoku glaze base substrate after glazing reach 6%-8%.
7. the preparation technology of golden spot temmoku glaze according to claim 6, it is characterized in that: described spray gun adopts air compressor machine pressurized air as power, and the pressure range of described spray gun air compressor machine is 0.1MP-0.2MP.
8. the preparation technology of golden spot temmoku glaze according to claim 3, it is characterized in that: it is to burn to 1260 ℃-1290 ℃ after the product loading of kiln after the step 2 glazing that described step 3 is burnt till, then cool the temperature to 1230 ℃-1240 ℃, after insulation 60min, be cooled to below 100 ℃ and get final product kiln discharge, the required time of firing is 12h-15h.
9. the preparation technology of according to claim 3 or 8 described golden spot temmoku glazes, it is characterized in that: described step 3 is burnt till middle employing drawer kiln and is utilized oil liquefied gas to burn till as fuel; Heat-up rate in described sintering process is 2-3 ℃/min.
10. the preparation technology of the described golden spot temmoku glaze of according to claim 3-9 any one is characterized in that: the project of described step 4 check is for having obvious golden spot or flow liner to require simultaneously finished product device deformation form quotient less than 5%.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103992140A (en) * | 2014-06-13 | 2014-08-20 | 广东松发陶瓷股份有限公司 | Novel copper-iron-colored yohen golden-ring temmoku glaze and method for making household porcelain from same |
| CN104496558A (en) * | 2014-12-04 | 2015-04-08 | 王泽彬 | Black oil-drop temmoku glaze |
| CN104649715A (en) * | 2014-12-31 | 2015-05-27 | 路今铧 | Novel temmoku glazed porcelain and firing method thereof |
| CN107021626A (en) * | 2017-05-24 | 2017-08-08 | 禹州市神器钧窑有限公司 | A kind of blue glaze of golden spot |
| CN107098677A (en) * | 2017-05-31 | 2017-08-29 | 福建德化陶知然陶瓷文化创意有限公司 | Black matrix erythema droplet temmoku glaze ceramics and its preparation technology |
| CN111454079A (en) * | 2020-04-09 | 2020-07-28 | 广东皓明陶瓷科技有限公司 | Method for forming black substrate golden wafer ceramic product in glaze firing process |
| CN112374909A (en) * | 2020-11-23 | 2021-02-19 | 王建勋 | Firing process of black gold bowl |
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Patent Citations (3)
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| JPH02283680A (en) * | 1989-04-25 | 1990-11-21 | Toto Ltd | Production of decorative ceramic ware |
| CN1548397A (en) * | 2003-05-09 | 2004-11-24 | 郭森镇 | Ceramic baking process |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103992140A (en) * | 2014-06-13 | 2014-08-20 | 广东松发陶瓷股份有限公司 | Novel copper-iron-colored yohen golden-ring temmoku glaze and method for making household porcelain from same |
| CN103992140B (en) * | 2014-06-13 | 2016-01-06 | 广东松发陶瓷股份有限公司 | A kind of copper iron look sunlight becomes gold ring temmoku glaze and makes the method for household china of it |
| CN104496558A (en) * | 2014-12-04 | 2015-04-08 | 王泽彬 | Black oil-drop temmoku glaze |
| CN104649715A (en) * | 2014-12-31 | 2015-05-27 | 路今铧 | Novel temmoku glazed porcelain and firing method thereof |
| CN104649715B (en) * | 2014-12-31 | 2016-08-24 | 路今铧 | Temmoku vitreous enamel and method for cooking thereof |
| CN107021626A (en) * | 2017-05-24 | 2017-08-08 | 禹州市神器钧窑有限公司 | A kind of blue glaze of golden spot |
| CN107098677A (en) * | 2017-05-31 | 2017-08-29 | 福建德化陶知然陶瓷文化创意有限公司 | Black matrix erythema droplet temmoku glaze ceramics and its preparation technology |
| CN107098677B (en) * | 2017-05-31 | 2020-07-21 | 福建德化陶知然陶瓷文化创意有限公司 | Black-bottom red-spot oil-drop temmoku glaze ceramic and preparation process thereof |
| CN111454079A (en) * | 2020-04-09 | 2020-07-28 | 广东皓明陶瓷科技有限公司 | Method for forming black substrate golden wafer ceramic product in glaze firing process |
| CN112374909A (en) * | 2020-11-23 | 2021-02-19 | 王建勋 | Firing process of black gold bowl |
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