CN103989187A - High-density fast-decomposition edible cellulose tablet and preparation method thereof - Google Patents

High-density fast-decomposition edible cellulose tablet and preparation method thereof Download PDF

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Publication number
CN103989187A
CN103989187A CN201410008734.4A CN201410008734A CN103989187A CN 103989187 A CN103989187 A CN 103989187A CN 201410008734 A CN201410008734 A CN 201410008734A CN 103989187 A CN103989187 A CN 103989187A
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tablet
cellulose
label
acid
plant fiber
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CN103989187B (en
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杨如会
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HANGZHOU HIBIO TECH Co Ltd
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HANGZHOU HIBIO TECH Co Ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/20Reducing nutritive value; Dietetic products with reduced nutritive value
    • A23L33/21Addition of substantially indigestible substances, e.g. dietary fibres
    • A23L33/24Cellulose or derivatives thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23PSHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
    • A23P20/00Coating of foodstuffs; Coatings therefor; Making laminated, multi-layered, stuffed or hollow foodstuffs
    • A23P20/20Making of laminated, multi-layered, stuffed or hollow foodstuffs, e.g. by wrapping in preformed edible dough sheets or in edible food containers
    • A23P20/25Filling or stuffing cored food pieces, e.g. combined with coring or making cavities
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Mycology (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Medicinal Preparation (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

The invention relates to a cellulose tablet, especially to a high-density fast-decomposition edible cellulose tablet and a preparation method thereof. The high-density fast-decomposition edible cellulose tablet is composed of a tablet core and a coating out of the tablet core. The tablet is characterized in that the tablet core comprises the following components by weight: 28 to 42% of a soluble edible vegetable fiber, 55 to 70% of a non-soluble edible vegetable fiber and 1 to 4% of an effervescing agent. The cellulose tablet is prepared through high pressure compression, has the characteristics of high density and high fiber content and overcomes the disadvantages of low density and low fiber content of cellulose product on the market at present; since the cellulose tablet provided by the invention contains the effervescing agent, the cellulose tablet can be rapidly cracked in the stomach; cellulose components in the tablet are soluble and non-soluble edible cellulose which are both originated from edible plants and prepared by using a purely physical method (high pressure compaction).

Description

The fast edible cellulose tablet and preparation method thereof that decomposes of a kind of high density
Technical field
The present invention relates to a kind of cellulose tablet, particularly the fast edible cellulose tablet and preparation method thereof that decomposes of a kind of high density.
Background technology
Edible cellulose claims again dietary fiber, be mainly derive from vegetables, fruit and cereal be generally difficult for digested nutrient for plants, mainly contain the summation of vegetalitas composition, carbohydrate and similar material thereof, comprise polysaccharide, oligosaccharides, lignin.Can be divided into solubility and insolubility two classes.Insoluble fibers is mainly present in wheat bran, nut, vegetables, mainly improves large intestine function, comprises the time of passing through, the increase defecation frequency that shorten slaking residue, plays the effect of Constipation and intestinal cancer.Barley, beans, carrot, oranges and tangerines, oat etc. all contain abundant Soluble Fiber, can slow down the digestion rate of food, reduce consumption and the absorption of lipid food, make postprandial blood sugar steady, reduce the health-care effects such as blood norcholesterol level.Along with the variation of people's dietary structure, the role that cellulose is being played the part of in health is more and more important, and absorbing enough fibers can angiocardiopathy preventing, intestines problem, cancer, diabetes etc.
Cellulose is due to can not be by pipe intestinal digesting and absorption, need certain input quantity just can reach its physiological action, and along with the rising of people's living standard, the food trend that becomes more meticulous is obvious, cellulosic content continuous decrease in food, has become one of major reason of metabolism class disease.Current commercially available edible fiber element product mainly exists that volume is large, product density is little, average external volume content is low, solubility and the feature such as non-solubility proportioning is unreasonable.Therefore, develop a kind of pure natural food source, the preparation of pure physical method, unit volume inner cellulose content is high, and reasonable mixture ratio, oral formulations that can fast decoupled are significant.
Application number: the Chinese invention patent of 98810293.5, the applying date: 1998-08-21 discloses a kind of quickly disintegrated methylcellulose tablets, this tablet comprises intragranular component and the outer component of grain, wherein intragranular component comprise have viscosity > 1000 in the least pascal seconds methylcellulose, be selected from the starch of microcrystalline cellulose, cornstarch, pregelatinized and the diluent of their mixture; The outer component of grain comprises wetting agent, lubricant and the outer disintegrant of grain, wherein the ratio of methylcellulose and microcrystalline cellulose is 2: 1-14: 1, the ratio of methylcellulose and cornstarch is 7.5-15: 1, the ratio of methylcellulose and starch,pregelatinized is 2: 1-5: 1, and described tablet has the structure of intragranular component and the outer component of grain.There is following defect in this patent: 1. methylcellulose is industrial products, needs acid-base reaction in preparation process, is not pure natural source, has unsafe factor on material source.2. in this formula, starch proportion is too high, and starch belongs to can absorb low value nutrient, has increased user's energy source, does not meet modern nutrient balance requirement.3. density is low, and cellulose has the large feature of unit mass volume, and the cellulosic products unit volume intensive amount of common compacting is few, and commodity value is low.4. the methylcellulose in main component is not obvious to fat absorption intervention, there is no non-solubility cellulose components, there is no enteron aisle regulating action.
Summary of the invention
The invention provides a kind of high density, decompose edible cellulose tablet soon.
The present invention also provides a kind of preparation method of described cellulose tablet.
The technical solution adopted for the present invention to solve the technical problems is:
The edible cellulose tablet of the fast decomposition of high density, this tablet is comprised of label and the dressing being wrapped in outside label, it is characterized in that the label of this tablet comprises following component by weight percentage:
Solubility food plant fiber 28 ~ 42%,
Non-solubility food plant fiber 55 ~ 70%,
Effervescent agent 1 ~ 4%.
Cellulose tablet of the present invention adopts high pressure compressed to form, and has that density is high, the high feature of fiber content, has avoided low, the poor feature of cellulose products density on the market; Contain effervescent agent, under one's belt the feature of cracking fast simultaneously.Cellulose components in tablet is solubility and non-solubility edible cellulose, and its source is consumption plant, pure physical method preparation (high pressure compacting).
Solubility food plant fiber (yet claiming water-soluble dietary fiber) is not digested by human body digestive ferment, but water soluble, be mainly some gelatin substances, as pectin etc., the content in the foods such as konjaku, oat, barley, beans, carrot, oranges and tangerines, apple, grape, apricot of take, as many, have Weight-reducing and lipid-lowering, controls the effects such as blood sugar, prevention of cardiac.
Non-solubility food plant fiber (also claiming Water insoluble dietary fiber) is not by human body alimentary canal enzymic digestion and water insoluble, be mainly the part of plant cell wall, comprise cellulose, lignin and part hemicellulose, main from the wheat bran in food, corn bran, celery, pericarp and rhizome vegetables.There is prevention intestinal cancer, reduce cholesterol, prevent gall stone, treat the effects such as constipation.
As preferably, for there is organic acid, carbonate or the bicarbonate of acid-base reaction in water in effervescent agent, organic acid is selected from citric acid, tartaric acid, fumaric acid, malic acid or butanedioic acid, and carbonate or bicarbonate are selected from potash, saleratus, sodium carbonate or sodium acid carbonate.
As preferably, described dressing comprises that adhesive, the flavoring of with weight ratio 0.1 ~ 1:0.1 ~ 1:0.1 ~ 1, mixing rectify toner and lubricant.Further, described dressing comprises the strong toner of adhesive, flavoring and the lubricant mixing with weight ratio 0.5:1:1.
As preferably, adhesive is selected from PEG 4000, PEG 6000, PVP K53, PVP K15 or HPMC E5.
As preferably, flavoring is rectified toner and is selected from one or more in bata-carotene, Steviosin, Sucralose or fruity flavor.Flavoring is rectified mouthfeel and the color and luster that toner has had tablet.
As preferably, lubricant is selected from leucine, PEG 6000, hydrogenated vegetable oil, stearic acid or stearate.
A preparation method for described cellulose tablet, the method comprises the steps: a, each component of label is dry mixed according to proportioning, after stirring, obtains compound, by compound compressed tablets on tablet press machine, pressure > 25kg/cm 2, the tablet obtaining is as label; B, each component raw material of dressing is mixed by proportioning, be controlled at≤100 orders of the particle diameter of each raw material, the mixture obtaining is usingd 75% ethanol (volume fraction) as solvent, makes the coating solution of tablet by every 20 ~ 25mg solute and 100ml solvent; C, the label suppressing is placed in coating pan, coating solution is evenly sprayed to sheet wicking surface, at sheet wicking surface, form dressing; Control the 2.5-3% that dressing accounts for tablet total weight amount.Adopt super-pressure compressed preparation, density is high, adopts High Voltage method to compress in compression process, and its pressure is higher than common tablet press machine more than 2 times.
As preferably, in each component of label, particle diameter≤30 order of solubility food plant fiber, particle diameter≤20 order of non-solubility food plant fiber, particle diameter≤80 order of effervescent agent.
The invention has the beneficial effects as follows: under equal volume tablet, cellulose tablet of the present invention is 2g/ sheet, and existing cellulose tablet product is 0.2 ~ 0.4g/ sheet.Under simulation gastric acid environment, tablet of the present invention decomposes completely in 30s.Tablet a slice of the present invention is equivalent to the 5-10 sheet of general fibre element product tablet, and density is greater than 1g/mm 3.Therefore, advantage of the present invention is:
1. pure natural is originated, and pure physical method compacting, has security guarantee on source;
2. density is high, and because cellulose exists, volume is large, the low feature of density, and the present invention takes high compression, and in unit volume, active principle is high;
3. solubility and non-solubility cellulose reasonable mixture ratio, soluble cellulose can be intervened fat absorption, and non-solubility cellulose can increase feeling of repletion, condition function of intestinal canal, without other exogenous energy, increases.
The specific embodiment
Below by specific embodiment, technical scheme of the present invention is described in further detail.Should be appreciated that enforcement of the present invention is not limited to the following examples, any pro forma accommodation that the present invention is made and/or change all will fall into protection domain of the present invention.
In the present invention, if not refer in particular to, all part, percentages are unit of weight, and the equipment adopting and raw material etc. all can be buied from market or this area is conventional.Method in following embodiment, if no special instructions, is the conventional method of this area.
In the present invention, solubility food plant fiber and non-solubility food plant fiber just extracting method are common process, at this, do not do tired stating.
Embodiment 1:
1) by solubility food plant fiber, non-solubility food plant fiber, sodium acid carbonate by weight the ratio of 32:64:4 be dry mixed, after stirring, obtain compound.Solubility food plant fiber 30 orders wherein, non-solubility food plant fiber is 20 orders, sodium acid carbonate 80 orders.
2) by above-mentioned compound compressed tablets on tablet press machine, pressure > 25kg/cm 2, the present embodiment is selected compound to be pressed into oval tablet, the surface area 0.5cm of tablet 2, volume 0.25cm 3, hardness > 10kg/cm 2, density is greater than 1g/mm 3, the tablet obtaining is as label.
3) adhesive (PEG 4000), the strong toner (bata-carotene) of flavoring and lubricant (leucine) are mixed with weight ratio 0.5:1:1, filter order number and be 100 orders, the mixture obtaining is usingd 75% ethanol (volume fraction) as solvent, makes the coating solution (solution of this concentration the most easily forms dressing) of tablet by every 25mg solute and 100ml solvent.
4) label suppressing is placed in coating pan, the coating solution that coating material is made is evenly sprayed at sheet wicking surface, dry low temperature blowing, and after solvent evaporates, coating material just forms dressing at sheet wicking surface.
5) part by weight of label and dressing is 97:3.
The external disintegration time < of tablet 10 minutes (general tablet requires 15 ~ 30 minutes) obtaining.
In the present embodiment, the source of solubility food plant fiber is oat, and the source of non-solubility food plant fiber is corn bran.
Embodiment 2:
1) by solubility food plant fiber, non-solubility food plant fiber, sodium carbonate by weight the ratio of 28:70:2 be dry mixed, after stirring, obtain compound.Solubility food plant fiber 30 orders wherein, non-solubility food plant fiber is 20 orders, sodium carbonate 80 orders.
2) by above-mentioned compound compressed tablets on tablet press machine, pressure > 25kg/cm 2, the present embodiment is selected compound to be pressed into oval tablet, the surface area 0.5cm of tablet 2, volume 0.25cm 3, hardness > 10kg/cm 2, density is greater than 1g/mm 3, the tablet obtaining is as label.
3) adhesive (PVP K15), the strong toner (Sucralose) of flavoring and lubricant (hydrogenated vegetable oil) are mixed with weight ratio 1:1:1, filter order number and be 100 orders, the mixture obtaining is usingd 75% ethanol (volume fraction) as solvent, makes the coating solution (solution of this concentration the most easily forms dressing) of tablet by every 20mg solute and 100ml solvent.
4) label suppressing is placed in coating pan, the coating solution that coating material is made is evenly sprayed at sheet wicking surface, dry low temperature blowing, and after solvent evaporates, coating material just forms dressing at sheet wicking surface, controls dressing and accounts for 2.5% of tablet total weight amount.
The external disintegration time < of tablet 10 minutes (general tablet requires 15 ~ 30 minutes) obtaining.In the present embodiment, the source of solubility food plant fiber is konjaku, and the source of non-solubility food plant fiber is celery.
Embodiment 3:
1) by solubility food plant fiber, non-solubility food plant fiber, citric acid by weight the ratio of 42:55:3 be dry mixed, after stirring, obtain compound.Solubility food plant fiber 30 orders wherein, non-solubility food plant fiber is 20 orders, sodium carbonate 80 orders.
2) by above-mentioned compound compressed tablets on tablet press machine, pressure > 25kg/cm 2, the present embodiment is selected compound to be pressed into oval tablet, the surface area 0.5cm of tablet 2, volume 0.25cm 3, hardness > 10kg/cm 2, density is greater than 1g/mm 3, the tablet obtaining is as label.
3) adhesive (HPMC E5), the strong toner (Steviosin) of flavoring and lubricant (hydrogenated vegetable oil) are mixed with weight ratio 0.5:1:1, filter order number and be 100 orders, the mixture obtaining is usingd 75% ethanol (volume fraction) as solvent, makes the coating solution (solution of this concentration the most easily forms dressing) of tablet by every 20mg solute and 100ml solvent.
4) label suppressing is placed in coating pan, the coating solution that coating material is made is evenly sprayed at sheet wicking surface, dry low temperature blowing, and after solvent evaporates, coating material just forms dressing at sheet wicking surface, controls dressing and accounts for 3% of tablet total weight amount.
The external disintegration time < of tablet 10 minutes (general tablet requires 15 ~ 30 minutes) obtaining.In the present embodiment, the source of solubility food plant fiber is konjaku, and the source of non-solubility food plant fiber is celery.
Embodiment 4:
1) by solubility food plant fiber, non-solubility food plant fiber, butanedioic acid by weight the ratio of 31:68:1 be dry mixed, after stirring, obtain compound.Solubility food plant fiber 30 orders wherein, non-solubility food plant fiber is 20 orders, sodium carbonate 80 orders.
2) by above-mentioned compound compressed tablets on tablet press machine, pressure > 25kg/cm 2, the present embodiment is selected compound to be pressed into oval tablet, the surface area 0.5cm of tablet 2, volume 0.25cm 3, hardness > 10kg/cm 2, density is greater than 1g/mm 3, the tablet obtaining is as label.
3) adhesive (PVP K15), flavoring being rectified to toner (Steviosin and fruity flavor mix with weight ratio 1:1) and lubricant (stearic acid) mixes with weight ratio 0.5:1:1, filter order number and be 100 orders, the mixture obtaining is usingd 75% ethanol (volume fraction) as solvent, makes the coating solution (solution of this concentration the most easily forms dressing) of tablet by every 20mg solute and 100ml solvent.
4) label suppressing is placed in coating pan, the coating solution that coating material is made is evenly sprayed at sheet wicking surface, dry low temperature blowing, and after solvent evaporates, coating material just forms dressing at sheet wicking surface, controls dressing and accounts for 3% of tablet total weight amount.
The external disintegration time < of tablet 10 minutes (general tablet requires 15 ~ 30 minutes) obtaining.In the present embodiment, the source of solubility food plant fiber is carrot, and the source of non-solubility food plant fiber is oranges and tangerines.
Above-described embodiment is a kind of preferably scheme of the present invention, not the present invention is done to any pro forma restriction, also has other variant and remodeling under the prerequisite that does not exceed the technical scheme that claim records.

Claims (8)

1. high density is decomposed an edible cellulose tablet soon, and this tablet is comprised of label and the dressing being wrapped in outside label, it is characterized in that the label of this tablet comprises following component by weight percentage:
Solubility food plant fiber 28 ~ 42%,
Non-solubility food plant fiber 55 ~ 70%,
Effervescent agent 1 ~ 4%.
2. cellulose tablet according to claim 1, it is characterized in that: effervescent agent is for organic acid, carbonate or the bicarbonate of acid-base reaction occur in water, organic acid is selected from citric acid, tartaric acid, fumaric acid, malic acid or butanedioic acid, and carbonate or bicarbonate are selected from potash, saleratus, sodium carbonate or sodium acid carbonate.
3. cellulose tablet according to claim 1, is characterized in that: described dressing comprises the strong toner of adhesive, flavoring and the lubricant mixing with weight ratio 0.1 ~ 1:0.1 ~ 1:0.1 ~ 1.
4. cellulose tablet according to claim 1, is characterized in that: adhesive is selected from PEG 4000, PEG 6000, PVP K53, PVP K15 or HPMC E5.
5. cellulose tablet according to claim 1, is characterized in that: the strong toner of flavoring is selected from one or more in bata-carotene, Steviosin, Sucralose or fruity flavor.
6. cellulose tablet according to claim 1, is characterized in that: lubricant is selected from leucine, PEG 6000, hydrogenated vegetable oil, stearic acid or stearate.
7. a preparation method for cellulose tablet claimed in claim 1, is characterized in that the method comprises the steps:
A, each component of label is dry mixed according to proportioning, after stirring, obtains compound, by compound compressed tablets on tablet press machine, pressure > 25kg/cm 2, the tablet obtaining is as label;
B, each component raw material of dressing is mixed by proportioning, be controlled at≤100 orders of the particle diameter of each raw material, the mixture obtaining is usingd 75% ethanol (volume fraction) as solvent, makes the coating solution of tablet by every 20 ~ 25mg solute and 100ml solvent;
C, the label suppressing is placed in coating pan, coating solution is evenly sprayed to sheet wicking surface, at sheet wicking surface, form dressing; Control the 2.5-3% that dressing accounts for tablet total weight amount.
8. preparation method according to claim 7, is characterized in that: in each component of label, and particle diameter≤30 order of solubility food plant fiber, particle diameter≤20 order of non-solubility food plant fiber, particle diameter≤80 order of effervescent agent.
CN201410008734.4A 2014-01-09 2014-01-09 High-density fast-decomposition edible cellulose tablet and preparation method thereof Active CN103989187B (en)

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CN109330987A (en) * 2018-11-16 2019-02-15 深圳市阳光之路生物材料科技有限公司 A kind of chitosan piece of fater disintegration and dissolution
CN110506779A (en) * 2019-09-27 2019-11-29 河南景珍生物科技有限公司 A kind of artificial synthesized collagen high tenacity casing and preparation method thereof

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CN109330987A (en) * 2018-11-16 2019-02-15 深圳市阳光之路生物材料科技有限公司 A kind of chitosan piece of fater disintegration and dissolution
CN110506779A (en) * 2019-09-27 2019-11-29 河南景珍生物科技有限公司 A kind of artificial synthesized collagen high tenacity casing and preparation method thereof
CN110506779B (en) * 2019-09-27 2021-08-24 河南景珍生物科技有限公司 Artificially synthesized collagen high-toughness casing and preparation method thereof

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