CN103976920A - Shinyleaf pricklyash root extracting solution as well as preparation method and application thereof - Google Patents
Shinyleaf pricklyash root extracting solution as well as preparation method and application thereof Download PDFInfo
- Publication number
- CN103976920A CN103976920A CN201410242058.7A CN201410242058A CN103976920A CN 103976920 A CN103976920 A CN 103976920A CN 201410242058 A CN201410242058 A CN 201410242058A CN 103976920 A CN103976920 A CN 103976920A
- Authority
- CN
- China
- Prior art keywords
- extracting solution
- radix zanthoxyli
- preparation
- extract
- essence
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Abstract
The invention discloses a shinyleaf pricklyash root extracting solution as well as a preparation method and application thereof. The shinyleaf pricklyash root extracting solution prepared in a water extraction manner has an anti-oxidative effect. The shinyleaf pricklyash root extracting solution has the effects of removing damage to cell membrane caused by free radicals in a cell and preventing the moisture of the cell from losing. The problems of dull yellow skin, blackhead, stains, pachulosis and the like can be improved when the shinyleaf pricklyash root extracting solution is applied to cosmetics.
Description
Technical field
The present invention relates to cosmetic field, particularly relate to a kind of Radix Zanthoxyli extracting solution and its preparation method and application.
Background technology
Along with the raising of people's living standard, cosmetics have become necessary article in people's life.But people are but very high for the prescription of cosmetics, not only require effectively, and require to be free from side effects.Along with the development of cosmetics industry, natural plants series products due to use safety, action temperature and, the advantage such as successful welcome.Be generally to obtain by corresponding processing the plant extract that contains effective ingredient, and add in cosmetics.
At present the plant extract in cosmetics, mostly adopts the methods such as water extraction, alcohol extraction, ultrasonic extraction, microwave extraction to extract gained, and extraction process is complicated, through operations such as concentrate dryings, also to add antiseptic so that the shelf-life of extract more permanent.The drawback of bringing like this, one is waste resource, and in leaching process, solution is concentrated, generally only gets concentrated fraction elite out, and most solutions is thrown away.This part solution still can contain active component in fact, can also again utilize, and directly throw away the waste that has just caused resource.Another drawback is in extract, add antiseptic no doubt can make extract obtain the longer shelf-life, but the while to be also for skin brings sensitization source.
Meanwhile, extraneous ultraviolet, radiation, the destruction of airborne harmful substance to keratodermatitis, epidermis and hypodermal cell metabolism produce more free radical, and cellulose is damaged, and cause the loss of moisture, and Here it is, and skin is oxidized.And the loss of moisture causes secreting more oils and fats, soil is more difficult to be washed off, causes in the course of time the colour of skin dark yellow, blackhead, mottle, the problems such as pachylosis.
Therefore, select which kind of plant, how simple, safety, effectively this plant extract is carried out, and by being applied in cosmetics of its safety, protection skin is not oxidized, is problem demanding prompt solution.
Summary of the invention
Based on this, the object of the invention is to provide a kind of Radix Zanthoxyli extracting solution and its preparation method and application.
The concrete technical scheme solving the problems of the technologies described above is as follows:
A preparation method for Radix Zanthoxyli extracting solution, comprises the following steps:
By Radix Zanthoxyli drying and crushing, with the 800-1000 order gauze bag of sterilizing, install, be placed in vacuum emulsifying pot, by the weight of Radix Zanthoxyli, the deionized water that adds 8-12 doubly to measure, in 90-100 ℃ of extraction, can make Radix Zanthoxyli extracting solution.
In some embodiment, the time of described extraction is 20-50min therein.
In some embodiment, by Radix Zanthoxyli drying and crushing, with the 800-1000 order gauze bag of sterilizing, install therein, be placed in vacuum emulsifying pot, after having extracted, directly gauze bag is taken out, remaining solution is Radix Zanthoxyli extracting solution.In the method, owing to adopting vacuum emulsifying pot, it can directly add other cosmetics adjuvants after extraction completes, and carries out Cosmetic Manufacture, and does not need to extract with special herbal extraction equipment, has saved cost; In addition, adopt gauze bag dress Radix Zanthoxyli powder, extracted and directly gauze bag has been taken out afterwards, need not filter, simplification extraction process, raises the efficiency.
Said method is simple to operation, and the Radix Zanthoxyli extract use of can now withdrawing deposit, does not need to add antiseptic, significantly reduces the sensitization source to skin.In cosmetic formulations, itself is just added with antiseptic, and extract of the present invention is now carried and being added, and has avoided producing spoilage problems because of placement.
The prepared Radix Zanthoxyli extracting solution of said method improves the application in the cosmetics of the problems such as skin is dark yellow, blackhead, mottle, pachylosis in preparation.
In some embodiment, in described cosmetics, the content of Radix Zanthoxyli extracting solution is 58-95wt% therein.
In some embodiment, described cosmetics are essence therein.
The present invention also provides a kind of essence, and described essence comprises the component of following weight percentage ratio:
Chelating agen: 0.01-0.1wt%,
Wetting agent: 5-18wt%,
Antiinflammatory: 0.05-2.5wt%,
Antiseptic: 0.3-0.66wt%,
The Radix Zanthoxyli extract that above-mentioned preparation method makes: surplus;
Described chelating agen is at least one in EDTA-disodium or Etidronic Acid;
Described wetting agent is at least one in glycerol, propylene glycol, Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate, Aloe vulgaris leaf extract or PEG400;
Described antiinflammatory is at least one in allantoin, Hamamelis virginiana extract, glycyrrhizic acid dipotassium or Flos Inulae extract;
Described antiseptic is at least one in methyl hydroxybenzoate, phenoxyethanol/Sensiva SC50 or Kazon.
In some embodiment, described essence comprises the component of following weight percentage ratio therein:
Chelating agen: 0.01-0.025wt%,
Wetting agent: 10-15.5wt%,
Antiinflammatory: 1.9-2.4wt%,
Antiseptic: 0.54-0.66wt%,
The Radix Zanthoxyli extract that above-mentioned preparation method makes: surplus;
Described chelating agen is EDTA-disodium;
Described wetting agent is at least one in glycerol, propylene glycol, Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate or Aloe vulgaris leaf extract;
Described antiinflammatory is at least one in allantoin, Hamamelis virginiana extract or glycyrrhizic acid dipotassium;
Described antiseptic is at least one in methyl hydroxybenzoate or phenoxyethanol/Sensiva SC50.
In some embodiment, described essence comprises the component of following weight percentage ratio therein:
EDTA-disodium: 0.018-0.022wt%,
Glycerol: 4-6wt%,
Propylene glycol: 4-6wt%,
Allantoin: 0.09-0.11wt%,
Methyl hydroxybenzoate: 0.09-0.11wt%,
Hamamelis virginiana extract: 1.8-2.2wt%,
Glycyrrhizic acid dipotassium: 0.045-0.055wt%,
Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate: 0.9-1.1wt%,
Aloe vulgaris leaf extract: 1.8-2.2wt%,
Phenoxyethanol/Sensiva SC50: 0.45-0.55,
Above-mentioned Radix Zanthoxyli extracting solution: surplus.
A kind of Radix Zanthoxyli extracting solution of the present invention and its preparation method and application has the following advantages and beneficial effect:
The present invention is through a large amount of experiment of inventor and research; draw at optimum process---prepared Radix Zanthoxyli extracting solution under water extraction; it has antioxidative effect; this specific character makes Radix Zanthoxyli extracting solution possess the effect that the destruction of radical pair cellulose in scavenger cell and the moisture of Cell protection do not run off, and is applied to can improve the problems such as skin is dark yellow, blackhead, mottle, pachylosis in cosmetics.
The specific embodiment
Radix Zanthoxyli of the present invention is is root or the branch and leaf of rutaceae Radix Zanthoxyli.Can adopt the whole year, cleans, and section, dries.Be born in the bushes of haugh hillside fields more.The ground such as distribution Guangdong, Guangxi, Fujian, Taiwan, Yunnan, Hunan.The present invention makes Radix Zanthoxyli extracting solution by Radix Zanthoxyli through water extraction, uses it for preparation and has in the cosmetics of problems such as improving skin is dark yellow, blackhead, mottle, pachylosis.
Below with reference to specific embodiment, the present invention will be further described.
In following embodiment, described Hamamelis virginiana extract purchased from Xi'an Sen Ran biological engineering company limited, Aloe vulgaris leaf extract purchased from Tianfeng Biological Science & Technology Co., Ltd., Xi'an, the equal commercially available prod of other raw materials.
In following examples, composition title used is international cosmetic raw material name (InternationalNomenclatureCosmeticIngredient, INCI) title of defined, for example phenoxyethanol/Sensiva SC50, Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate.
Embodiment 1 essence
Described in the present embodiment, in essence, contain Radix Zanthoxyli extracting solution, the preparation method of described Radix Zanthoxyli extracting solution comprises the following steps: 1 kilogram of Herba Zornia Diphyllae is cleaned, dry, drying and crushing to 80 order, installs with 800 order gauze bags of sterilizing, is placed in vacuum emulsifying pot, the deionized water that adds 10 kilograms, in 90 ℃ of extraction 20min, filter, obtain Herba Zornia Diphyllae extracting solution.
The component of described essence and content are in Table 1:
The component of table 1 essence and content
| Composition | Percentage by weight (wt%) |
| Radix Zanthoxyli extracting solution | Surplus |
| EDTA-disodium | 0.02 |
| Glycerol | 5 |
| Allantoin | 0.1 |
| Methyl hydroxybenzoate | 0.1 |
| Hamamelis virginiana extract | 2 |
| Glycyrrhizic acid dipotassium | 0.05 |
| Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate | 1 |
| Aloe vulgaris leaf extract | 2 |
| Phenoxyethanol/Sensiva SC50 | 0.5 |
| Add up to | 100 |
Comparative example 1 essence
The component of described essence and content are in Table 2:
The component of table 2 essence and content
| Composition | Percentage by weight (wt%) |
| Deionized water | Surplus |
| EDTA-disodium | 0.02 |
| Glycerol | 5 |
| Allantoin | 0.1 |
| Methyl hydroxybenzoate | 0.1 |
| Hamamelis virginiana extract | 2 |
| Glycyrrhizic acid dipotassium | 0.05 |
| Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate | 1 |
| Aloe vulgaris leaf extract | 2 |
| Phenoxyethanol/Sensiva SC50 | 0.5 |
| Add up to | 100 |
Embodiment 2 effect evaluations
One, experiment purpose
By relative analysis, evaluate the antioxidant effect of prepared cosmetics in the various embodiments described above.
Two, experimental technique
This experiment is divided into experimental group and matched group, and wherein, experiment component is: embodiment 1-essence; Matched group is comparative example 1-essence, a certain commercially available antioxidative essence that has.
Collect 200 volunteers of oxidized skin above-mentioned each product on probation after 28 days, observed result.Wherein, women 120 people, male 80 people, maximum 30 years old age, minimal ages 15 years old, 22 years old mean age.
Described sensitive-skinned showing as: skin is dark yellow, mottle, pachylosis, skin oil and fat secretion.
Experimental result
Result is referring to table 3.
The efficacy outcomes table of table 3 experimental group and matched group
As known from Table 3: each product of matched group is that comparative example 1-essence, a certain commercially available essence and each product embodiments of experimental group 1-essence are dark yellow to skin, mottle, pachylosis, skin oil and fat secretion all have improvement in various degree, from experimental data, can find out, each product, mottle dark yellow to skin in experimental group, pachylosis, skin oil and fat secretion improvement degree are obviously high than the improvement degree of each product in matched group, hence one can see that, and the cosmetics that contain Radix Zanthoxyli extracting solution have significant antioxidative effect.
The above embodiment has only expressed several embodiment of the present invention, and it describes comparatively concrete and detailed, but can not therefore be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that for the person of ordinary skill of the art, without departing from the inventive concept of the premise, can also make some distortion and improvement, these all belong to protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (6)
1. a preparation method for Radix Zanthoxyli extracting solution, is characterized in that, comprises the following steps:
Radix Zanthoxyli be dry, pulverize, pack the 800-1000 order gauze bag of sterilizing into, be placed in vacuum emulsifying pot, by the weight of Radix Zanthoxyli, the deionized water that adds 8-12 doubly to measure, in 90-100 ℃ of extraction.
2. the Radix Zanthoxyli extracting solution that preparation method as claimed in claim 1 makes.
3. Radix Zanthoxyli extracting solution as prepared in claim 2 improves the application in the cosmetics of the problems such as skin is dark yellow, blackhead, mottle, pachylosis in preparation.
4. application according to claim 3, is characterized in that, in described cosmetics, the content of Radix Zanthoxyli extracting solution is 58-95wt%.
5. according to the application described in claim 3 or 4, it is characterized in that, described cosmetics are essence.
6. an essence, is characterized in that, described essence comprises the component of following weight percentage ratio:
Chelating agen: 0.01-0.1wt%,
Wetting agent: 5-18wt%,
Antiinflammatory: 0.05-2.5wt%,
Antiseptic: 0.3-0.66wt%,
Radix Zanthoxyli extract as claimed in claim 2: surplus;
Described chelating agen is at least one in EDTA-disodium or Etidronic Acid;
Described wetting agent is at least one in glycerol, propylene glycol, Fructus Hordei Germinatus oligose base glucosides/hydrogenated starch hydrolysate, Aloe vulgaris leaf extract or PEG400;
Described antiinflammatory is at least one in allantoin, Hamamelis virginiana extract, glycyrrhizic acid dipotassium or Flos Inulae extract;
Described antiseptic is at least one in methyl hydroxybenzoate, phenoxyethanol/Sensiva SC50 or Kazon.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410242058.7A CN103976920B (en) | 2014-05-31 | 2014-05-31 | A kind of Radix Zanthoxyli extracting solution and its preparation method and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410242058.7A CN103976920B (en) | 2014-05-31 | 2014-05-31 | A kind of Radix Zanthoxyli extracting solution and its preparation method and application |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103976920A true CN103976920A (en) | 2014-08-13 |
| CN103976920B CN103976920B (en) | 2016-08-24 |
Family
ID=51269252
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410242058.7A Active CN103976920B (en) | 2014-05-31 | 2014-05-31 | A kind of Radix Zanthoxyli extracting solution and its preparation method and application |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103976920B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105534829A (en) * | 2016-03-02 | 2016-05-04 | 广州丹奇日用化工厂有限公司 | Anti-aging plant extract composition and application thereof to cosmetics |
| CN105662971A (en) * | 2016-03-04 | 2016-06-15 | 佛山市聚成生化技术研发有限公司 | Chinese herbal medicine composition and application thereof |
| CN108030755A (en) * | 2017-12-05 | 2018-05-15 | 广州赛莱拉干细胞科技股份有限公司 | It is a kind of to dispel blackhead skin care item and preparation method thereof containing Chinese wolfberry fruit dry cell extract |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1148489A (en) * | 1996-08-20 | 1997-04-30 | 江西江中绿世界日化厂 | Liangmianzhen face-washing cream |
| CN103599036A (en) * | 2013-10-25 | 2014-02-26 | 张亚丽 | Moisture supplementing pockmark fading mask |
| CN103784388A (en) * | 2014-01-15 | 2014-05-14 | 孙亚男 | Chinese herb extract for facial care and preparation method thereof |
-
2014
- 2014-05-31 CN CN201410242058.7A patent/CN103976920B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1148489A (en) * | 1996-08-20 | 1997-04-30 | 江西江中绿世界日化厂 | Liangmianzhen face-washing cream |
| CN103599036A (en) * | 2013-10-25 | 2014-02-26 | 张亚丽 | Moisture supplementing pockmark fading mask |
| CN103784388A (en) * | 2014-01-15 | 2014-05-14 | 孙亚男 | Chinese herb extract for facial care and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 李东光 主编: "《日用化学品配方与制备手册》", 28 February 2010, 中国纺织出版社 * |
| 胡莹 等: "广东地产药材入地金牛的药理作用及临床应用研究进展", 《今日药学》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105534829A (en) * | 2016-03-02 | 2016-05-04 | 广州丹奇日用化工厂有限公司 | Anti-aging plant extract composition and application thereof to cosmetics |
| CN105662971A (en) * | 2016-03-04 | 2016-06-15 | 佛山市聚成生化技术研发有限公司 | Chinese herbal medicine composition and application thereof |
| CN108030755A (en) * | 2017-12-05 | 2018-05-15 | 广州赛莱拉干细胞科技股份有限公司 | It is a kind of to dispel blackhead skin care item and preparation method thereof containing Chinese wolfberry fruit dry cell extract |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103976920B (en) | 2016-08-24 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103961289B (en) | A kind of Radix Talini Paniculati's extracting solution and its preparation method and application | |
| CN103976916B (en) | Berberis julianae schneid extracting solution and preparation method and application thereof | |
| CN103976919B (en) | A kind of Caulis Seu Folium Lespedezae Bicoloris extracting solution and its preparation method and application | |
| CN103961292B (en) | A kind of fourth grass in last of the ten Heavenly stems extract and its preparation method and application | |
| CN106667837A (en) | Camellia oleifera component based body lotion and preparation method thereof | |
| CN103976909B (en) | A kind of Herba Leibnitziae extracting solution and its preparation method and application | |
| CN101912432A (en) | Antioxidant substance extracted from branches, barks and leaves of eucommia bark leaved forest and extraction method thereof | |
| EP3146961A1 (en) | A method for preparing bioactive botanical compositions and the compositions made from said method using an electromagnetic field of greater than 3 ghz | |
| CN102113987A (en) | Cosmetic containing natural plant extractives and preparation method thereof | |
| CN103976923A (en) | Japanese saussurea herb extracting solution as well as preparation method and application thereof | |
| CN103976914A (en) | China creeper root extracting solution as well as preparation method and application thereof | |
| CN103961293A (en) | Sword bean extraction solution, as well as preparation method and application thereof | |
| CN104069036A (en) | Anti-aging cosmetic composition and preparation method thereof | |
| CN104027285A (en) | Skin whitening cosmetic composition and manufacturing method thereof | |
| CN103976920A (en) | Shinyleaf pricklyash root extracting solution as well as preparation method and application thereof | |
| CN103961291B (en) | A kind of Herba Origani extracting solution and its preparation method and application | |
| CN105007988B (en) | Bioactivity plant composition and application thereof | |
| CN113893209A (en) | Acne-removing repairing functional composition, application of composition in cosmetics, gel and preparation method | |
| KR20200060168A (en) | Care Pack after Brazilian Waxing and Manufacturing Method of it | |
| KR101955261B1 (en) | Cosmetic composition and method thereof | |
| CN103976917B (en) | A kind of hispid arthraxon extract and its preparation method and application | |
| CN106806176A (en) | Tea bran extract and preparation method thereof | |
| CN105496935A (en) | Cosmetic composition with acne removing function as well as preparation method and application thereof | |
| CN103976921B (en) | A kind of Herba Moslae Cavaleriei extracting solution and its preparation method and application | |
| CN104257565A (en) | Moisturizing and restoring hand cream and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20161205 Address after: 528051 K, room, 2, 08-14, 127 Zhangcha Road, Chancheng District, Guangdong, Foshan Patentee after: FOSHAN JUCHENG BIOCHEMISTRY TECHNOLOGY R&D CO., LTD. Address before: 510370 Guangdong province Guangzhou City Creek Road in Panlong industrial zone of Liwan District dragon two friends of a 6 storey industrial building Patentee before: Guangzhou Danqi Daily Chemical Factory Co., Ltd. |
|
| CB03 | Change of inventor or designer information |
Inventor after: Zhu Jianuo Inventor before: Yang Guangqun Inventor before: Li Su |
|
| CB03 | Change of inventor or designer information | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20170323 Address after: 510800 Guangdong city in Guangzhou Province, Xinhua Street, Huadu District, Xinhua Industrial Zone Yongxiang road building 32-2 (plant to use) Patentee after: Guangzhou zuoduozi Cosmetics Co. Ltd. Address before: 528051 K, room, 2, 08-14, 127 Zhangcha Road, Chancheng District, Guangdong, Foshan Patentee before: FOSHAN JUCHENG BIOCHEMISTRY TECHNOLOGY R&D CO., LTD. |
|
| TR01 | Transfer of patent right |