CN103961270B - Antifouling stealth protection liquid of a kind of net carbon and preparation method thereof - Google Patents
Antifouling stealth protection liquid of a kind of net carbon and preparation method thereof Download PDFInfo
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- CN103961270B CN103961270B CN201310034339.9A CN201310034339A CN103961270B CN 103961270 B CN103961270 B CN 103961270B CN 201310034339 A CN201310034339 A CN 201310034339A CN 103961270 B CN103961270 B CN 103961270B
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Abstract
The invention discloses antifouling stealth protection liquid of a kind of net carbon and preparation method thereof, the percentage by weight of this protective liquid prescription is：Surfactant：0.5~1.5%, hydrophilic natural macromolecule active material：0.1~0.5%, poly- hexamethyl biguanides 0.05~0.1%, water-soluble silicon oil 1.0~5.0%, edible alcohol 5~10%, humectants and emollients 10~15%, citric acid 0~0.5%, essence 0.1~0.3%, deionized water is surplus；This product has prepared a kind of barriers function not only with common stealth protection liquid in view of the deficiencies of the prior art, also has the function that gentle decontamination, nursing skin, has easy to use, the advantages such as effect is notable.
Description
Technical field
The present invention relates to a kind of protective liquid, refers in particular to antifouling stealth protection liquid of a kind of net carbon and preparation method thereof.
Background technology
Among routine work, exposed skin is often subject to various dirts, dust and the pollution of bacterium and invades people
Enter, particularly the practitioner of the industry such as colliery, finance, medical treatment, machinery.Because of work taken up feature, skin often in contact with
The easy skin permeation texture deep layer of the spots such as powder, greasy dirt, germ, it is difficult to pass through general cleaning method and traditional cleaning skin
Articles for use wash these spots, meanwhile, frequently cleaning can also damage skin.Such as：Mechanic's contact machine oil,
The organic solvents such as kerosene, paint, have skin different degrees of stimulation, and the skin part of the person that can make Long Term Contact exposure goes out
The symptoms such as now dry, decortication, breach and allergy.The number of also China's coal-mine worker is very huge, and coal miner is in underground
In mining environment, carbon black powders granularity is small, it is easy to stick on the skin, be sticked to fine carbon black mix with sweat and sebum,
Adhesion strength is high, is difficult to wash off with common articles for washing, it is necessary to frequently higher using alkalescence with the higher articles for washing of alkalescence
Articles for washing, not only washes rear uncomfortable, and excessive degreasing can make dry skin, coarse, wrinkle is more, is easy to conceal dirt, at the same time also
Easily cause irritable inflammation, seriously affect beauty and the health of miner.The practitioner of financial industry counting at work daily
When, various bacteria and virus have been infected with, has been unfavorable for health.These occupational hazards in order to prevent, the method usually prevented are to wear
Mask and protective gloves, but it is inconvenient at work, work efficiency is influenced, does not also reach preferable protection effect, in addition, near several
Also there is the Protection Product of similar liquid gloves effect in the market over year（Also stealthy liquid gloves are）Although have certain
Antifouling, dust-proof, bacteriological protection and other effects, but there is also many problems, such as the film company property of formation are poor, it is not wear-resisting, the shelf-life is short,
Function is single etc., makes practical effect unobvious.
The content of the invention
The technical problem to be solved in the present invention is to provide one kind not only to have barriers function, also with gentle decontamination, nursing
The effect of skin, has easy to use, antifouling stealth protection liquid of net carbon of advantage such as effect is notable and preparation method thereof.
The present invention solves the technical solution that above-mentioned technical problem uses：
A kind of antifouling stealth protection liquid of net carbon, the percentage by weight of the protective liquid prescription are：
Surfactant：0.5~1.5%；
Hydrophilic natural macromolecule active material：0.1~0.5%；
Poly- hexamethyl biguanides 0.05~0.1%；
Water-soluble silicon oil 1.0~5.0%；
Edible alcohol 5~10%；
Humectants and emollients 10~15%；
Citric acid 0~0.5%；
Essence 0.1~0.3%；
Deionized water is surplus；
The surfactant is alkyl glycosides APG0814, anion and amphoteric amino acids class surfactant, cocoyl
One or both of glycine betaine；
The humectants and emollients are one kind in the polyethylene glycols of glycerine, propane diols, sorbierite, molecular weight 200~800
Or two kinds.
The preparation method is as follows：
【1】, film forming agent preparation：Humectants and emollients are added in the stainless steel emulsion tank of 50L first, add hydrophily
High molecular reactive material, unlatching high-shear emulsion machine stir after ten minutes, stop stirring, standby use when standing thawing 2 is small；
【2】, by formula ratio deionized water is added in material-compound tank, be warming up to 50~60 DEG C, open stirring, add surface
Activating agent, stirs 10~20 minutes, is completely dissolved it；
【3】, open cooling water, the feed liquid in material-compound tank is cooled to 30~35 DEG C, add step【1】The film forming of preparation
Agent, is stirred 20~30 minutes, and untill solution is transparent, pH value is adjusted to 6.5~7.0 with citric acid；
【4】, add water-soluble silicon oil, poly hexamethylene biguanide, edible alcohol, essence, stir 10 minutes, stop stirring
30 minutes are stood afterwards, discharging detection, pH value 6.5~7.0 obtains this protective liquid.
The technological progress obtained using the above-mentioned technical proposal present invention is：
The present invention is multiple using natural green surfactant, hydrophilic natural macromolecule active material and humectants and emollients etc.
With into skin hinder protection cleaning solution, with the addition of natural green surfactant, ring on the basis of formula system is obstructed
Guarantor's type fungicide, emollient, not only play the barrier action of the harmful substances such as isolation dirt, and finish or be infected with work
Easily cleaned up after dirt with clear water, there are the multiple functions such as protection, cleaning, moisturizing, sterilization, also comply with people to product work(
Imitate diversified, natural, environmentally friendly, gentle, nontoxic non-stimulated demand.
The surfactant that the present invention uses is alkyl glycosides APG0814, anion and amphoteric amino acids class surface-active
One or both of agent, Cocoamidopropyl betaine, raw material sources belong to green surfactant in natural, biology
Degraded is complete, nontoxic to human body, gentle non-stimulated, has preferable broad spectrum antibiotic activity；Surface tension is low, gentle decontamination, bubble
Foam is fine and smooth, and stability is good, and pH value is in alkalescent, there is certain neutralization to acidic materials.
The poly hexamethylene biguanide that the present invention uses, belongs to nontoxic level, is a kind of water miscible fungicide, stingless to skin
Swash.
The hydrophilic natural macromolecule active material that the present invention uses：It is a kind of crosslinked acrylate copolymer (water
I types of dissolubility resin of thickening CBP-), pH value is in acid, and the gene in molecule is through in alkaline matter and after ionization, having hydrophilic
Property, negative electrical charge is mutually exclusive, stretches strand disperse, significantly expands, and forms transparent hydrophilic gel, and a kind of pH value tune
Save agent.
The water-soluble silicon oil that the present invention uses, not only can deep layer moisturizing, can also play grease proofing, waterproof action.
The humectants and emollients that the present invention uses are glycerine, propane diols, sorbierite, the polyethylene glycols of molecular weight 200~800
One or both of.Auxiliary element：Edible alcohol, not only makees disinfectant, but also makees film adjuvants.
In addition, the protrusion effect of the present invention is as follows：
1. the characteristics of this product is the neutral transparent shape aqueous solution that pH value is 7, non-stimulated to skin, environmentally safe,
Barrier propterty is excellent, not only has fabulous buffer action to dirt, harmful dust, but also has shielding action to bacterium, virus, also
There is antibacterial, sterilize, prevent dry skin etc..
Before 2. the characteristics of this product is work, this product is uniformly rubbed and is applied to skin surface, it is slightly dry, in skin surface shape
The stealthy protective film being invisible to the naked eye into one layer simultaneously can more securely keep on the skin, preventing the dirts such as dust, greasy dirt from oozing
Enter dermatoglyph, after operation, easily rinsed well with clear water, due to containing surfactant in film, and with fine
Hydrophily, conveniently and efficiently film and subsidiary Fouling Cleaning can be fallen, realize cleaning and prevent dirt deposition in skin
Function.Contain skin care ingredient in this product, after film is retained and is cleaned, the effect of skin care moisturizing can be played, have very to skin
Good moist nursing role, and protection, decontamination, antibacterial, skin care multiple efficacies can be made once to complete.
3. the product belongs to environmental type product, liquid is hindered in traditional skin（Stealthy liquid gloves）On the basis of add
Natural green surfactant and hydrophilic natural macromolecule active material, make a variety of work(such as antifouling, decontamination, antibacterial, skin care
It can roll into one, wide market was both convenient and efficient, had environmentally protective.
Embodiment
Embodiment 1:
Surfactant A PG0814 1g,
Hydrophilic natural macromolecule active material 0.3g,
Poly- hexamethyl biguanides 0.08g,
Water-soluble silicon oil 3g,
Edible alcohol 8g,
Polyethylene glycol 400 10g,
Citric acid 0.1g,
Essence 0.1g,
Deionized water 77.42g.
Preparation method：
The preparation method of the antifouling stealth protection liquid of net carbon, the preparation method are as follows：
【1】, film forming agent preparation：Humectants and emollients polyethylene glycol 400 is added to the stainless steel emulsion tank of 50L first
In, hydrophilic macromolecule active material is added, the stirring of unlatching high-shear emulsion machine after ten minutes, stops stirring, it is small to stand thawing 2
Shi Houbei is used；
【2】, by formula ratio deionized water is added in material-compound tank, be warming up to 50 DEG C, open stirring, add surface-active
Agent APG0814, stirs 15 minutes, is completely dissolved it；
【3】, open cooling water, the feed liquid in material-compound tank is cooled to 35 DEG C, add step【1】The film forming agent of preparation, is stirred
Mix 25 minutes, untill solution is transparent, pH value is adjusted to 6.5~7.0 with citric acid；
【4】, add water-soluble silicon oil, poly hexamethylene biguanide, edible alcohol, essence, stir 10 minutes, stop stirring
30 minutes are stood afterwards, discharging detection, pH value 6.5~7.0 obtains this protective liquid.
Embodiment 2:
N- cocoyl Sodium Glycinate 1.2g,
Hydrophilic natural macromolecule active material 0.2g,
Poly- hexamethyl biguanides 0.1g,
Water-soluble silicon oil 2.5g,
Edible alcohol 6g,
Propane diols 12g,
Citric acid 0.2g,
Essence 0.1g,
Deionized water 77.7g.
Preparation method：
The preparation method of the antifouling stealth protection liquid of net carbon, the preparation method are as follows：
【1】, film forming agent preparation：Humectants and emollients propane diols is added in the stainless steel emulsion tank of 50L first, is added
Hydrophilic macromolecule active material, the stirring of unlatching high-shear emulsion machine after ten minutes, stop stirring, standby when standing thawing 2 is small
With；
【2】, by formula ratio deionized water is added in material-compound tank, be warming up to 55 DEG C, open stirring, add surface-active
Agent N- cocoyl Sodium Glycinates, stir 10 minutes, are completely dissolved it；
【3】, open cooling water, the feed liquid in material-compound tank is cooled to 30 DEG C, add step【1】The film forming agent of preparation, is stirred
Mix 30 minutes, untill solution is transparent, pH value is adjusted to 6.5~7.0 with citric acid；
【4】, add water-soluble silicon oil, poly hexamethylene biguanide, edible alcohol, essence, stir 10 minutes, stop stirring
30 minutes are stood afterwards, discharging detection, pH value 6.5~7.0 obtains this protective liquid.
Embodiment 3:
Cocoamidopropyl betaine 1g,
Hydrophilic natural macromolecule active material 0.2g,
Poly- hexamethyl biguanides 0.08g,
Water-soluble silicon oil 4g,
Edible alcohol 6g,
Glycerine 12g,
Citric acid 0.1g,
Essence 0.2g,
Deionized water 76.42g;
Preparation method
The preparation method of the antifouling stealth protection liquid of net carbon, the preparation method are as follows：
【1】, film forming agent preparation：Humectants and emollients glycerine is added in the stainless steel emulsion tank of 50L first, adds parent
Aqueous high molecular active material, unlatching high-shear emulsion machine stir after ten minutes, stop stirring, standby use when standing thawing 2 is small；
【2】, by formula ratio deionized water is added in material-compound tank, be warming up to 55 DEG C, open stirring, add surface-active
Agent Cocoamidopropyl betaine, stirs 10 minutes, is completely dissolved it；
【3】, open cooling water, the feed liquid in material-compound tank is cooled to 30 DEG C, add step【1】The film forming agent of preparation, is stirred
Mix 25 minutes, untill solution is transparent, pH value is adjusted to 6.5~7.0 with citric acid；
【4】, add water-soluble silicon oil, poly hexamethylene biguanide, edible alcohol, essence, stir 10 minutes, stop stirring
30 minutes are stood afterwards, discharging detection, pH value 6.5~7.0 obtains this protective liquid.
Performance test（This product compared with similar products compared with）
| Project kind | This product | Market 1# products | Market 2# products |
| Appearance | Water white transparency | Colorless viscous shape liquid | Milky thick liquid |
| Dry film forming speed（Dosage 3g） | 5s | 20s | 30s |
| Cleaning effect | It is good | Generally | Generally |
| Irritation | Nothing | Nothing | Have |
| PH value | 7.0 | 8.2 | 8.7 |
Claims (2)
1. a kind of net antifouling stealth protection liquid of carbon, it is characterised in that the percentage by weight of the protective liquid prescription is：
The hydrophilic natural macromolecule active material：It is a kind of crosslinked acrylate copolymer, its pH value is in acidity,
Gene in molecule is through in alkaline matter and after ionization, having hydrophily, negative electrical charge is mutually exclusive, stretches strand disperse
Exhibition, significantly expands, and forms transparent hydrophilic gel, can be used as pH value conditioning agents；
The surfactant is alkyl glycosides APG0814, anion and amphoteric amino acids class surfactant, cocoyl beet
One or both of alkali；
The humectants and emollients are one kind or two in the polyethylene glycols of glycerine, propane diols, sorbierite, molecular weight 200~800
Kind.
2. the preparation method of the antifouling stealth protection liquid of net carbon according to claim 1, it is characterised in that the preparation method is such as
Under：
【1】, film forming agent preparation：Humectants and emollients are added in the stainless steel emulsion tank of 50L first, add hydrophily high score
Sub- active material, unlatching high-shear emulsion machine stir after ten minutes, stop stirring, standby use when standing thawing 2 is small；
【2】, by formula ratio deionized water is added in material-compound tank, be warming up to 50~60 DEG C, open stirring, add surface-active
Agent, stirs 10~20 minutes, is completely dissolved it；
【3】, open cooling water, the feed liquid in material-compound tank is cooled to 30~35 DEG C, add step【1】The film forming agent of preparation, is stirred
Mix 20~30 minutes, untill solution is transparent, with lemon acid for adjusting pH value to 6.5~7.0；
【4】, add water-soluble silicon oil, poly hexamethylene biguanide, edible alcohol, essence, stir 10 minutes, after stopping stirring
30 minutes are stood, discharging detection, pH values 6.5~7.0 obtain this protective liquid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310034339.9A CN103961270B (en) | 2013-01-30 | 2013-01-30 | Antifouling stealth protection liquid of a kind of net carbon and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310034339.9A CN103961270B (en) | 2013-01-30 | 2013-01-30 | Antifouling stealth protection liquid of a kind of net carbon and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103961270A CN103961270A (en) | 2014-08-06 |
| CN103961270B true CN103961270B (en) | 2018-05-08 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201310034339.9A Active CN103961270B (en) | 2013-01-30 | 2013-01-30 | Antifouling stealth protection liquid of a kind of net carbon and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104398410A (en) * | 2014-10-29 | 2015-03-11 | 石家庄新华能源环保科技股份有限公司 | Cleaning and skin whitening mask, preparation method and application |
| CN116285900B (en) * | 2023-03-17 | 2023-12-05 | 麦岩智能科技(北京)有限公司 | Electrostatic dust pulling agent and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1114182A (en) * | 1994-05-23 | 1996-01-03 | 湖南大学 | Multifunctional skin care composition |
| CN1457764A (en) * | 2003-06-10 | 2003-11-26 | 汪瑜 | Liquid composition and its preparing method and use |
| CN1879593A (en) * | 2006-04-30 | 2006-12-20 | 北京市航天焊接材料厂 | Liquid protective hand mask and preparation method thereof |
| CN102732154A (en) * | 2012-06-20 | 2012-10-17 | 康绍光 | Invisible protective agent and preparation method thereof |
-
2013
- 2013-01-30 CN CN201310034339.9A patent/CN103961270B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1114182A (en) * | 1994-05-23 | 1996-01-03 | 湖南大学 | Multifunctional skin care composition |
| CN1457764A (en) * | 2003-06-10 | 2003-11-26 | 汪瑜 | Liquid composition and its preparing method and use |
| CN1879593A (en) * | 2006-04-30 | 2006-12-20 | 北京市航天焊接材料厂 | Liquid protective hand mask and preparation method thereof |
| CN102732154A (en) * | 2012-06-20 | 2012-10-17 | 康绍光 | Invisible protective agent and preparation method thereof |
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| CN103961270A (en) | 2014-08-06 |
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