CN1879593A - A liquid-state protective hands mask and preparation method thereof - Google Patents
A liquid-state protective hands mask and preparation method thereof Download PDFInfo
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- CN1879593A CN1879593A CN 200610078037 CN200610078037A CN1879593A CN 1879593 A CN1879593 A CN 1879593A CN 200610078037 CN200610078037 CN 200610078037 CN 200610078037 A CN200610078037 A CN 200610078037A CN 1879593 A CN1879593 A CN 1879593A
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Abstract
The invention relates to a liquid protection hand film and method for making same, wherein the raw material comprises the following constituents (by weight ratio): film-forming agent 10-15, film-forming adjuvant 8-14, emollient 1-4, auxiliary solvent 1-2, solvent 38-82, and preservative agent 0.01-0.05.
Description
Technical field
The present invention relates to the liquid-state protective hands mask that a kind of labor protection is used, relate in particular to a kind of liquid-state protective hands mask that machinery, vehicle maintenance, paint, spraying and contact organic solvent operator use and preparation method thereof that is used to be engaged in.
Background technology
The operator of industries such as machining maintenance, spraying, printing, hands is often polluted by various oils and fatss, paint, printing ink, organic solvent, directly the contact infiltration is attached in fingerprint and the fingernail seam, be difficult to wash off these stupid stains with general cleaning method, and when some organic solvent of contact, skin can be subjected to the stimulation of organic solvent, and skin allergy, defat, drying even dry and cracked take place.On the market common to be that some prevent xerodermatic hand cream and the cleaning agent of removing dirts such as machine oil, pigment, dyestuff, paint; be main component or mainly with the protective agent of preparations such as zinc oxide, starch, Pulvis Talci, vegetable oil, vaseline with kaolin, Testa Tritici skin, weak property alkali; the common ground of its effect is to wash dirt and skin moistening nursing; handle but all belong to afterwards; it is not contaminated fundamentally not stop hand skin, accomplishes advance preventing and protection.
The present invention is exactly the skin health from the protection operator, and preparation a kind of is used for the convenient and swift effective protection hands film smeared before the work
Summary of the invention
The purpose of this invention is to provide the liquid-state protective hands mask that a kind of labor protection is used, a kind of liquid-state protective hands mask that machinery, vehicle maintenance, paint, spraying and contact organic solvent operator use and preparation method thereof that is used to be engaged in especially is provided, has overcome the shortcoming of above-mentioned traditional protective agent.
The objective of the invention is to be achieved through the following technical solutions:
A kind of liquid-state protective hands mask is made up of following weight portion raw material components: film forming matter 10-15, coalescents 8-14, emollient 1-4, cosolvent 1-2, solvent 38-82, antiseptic 0.01-0.05.
Described film forming matter is a kind of or its combination in gelatin, casein, methylcellulose, the polyvinyl alcohol;
Described coalescents is a kind of or its combination in diethylene glycol, propylene glycol, the glycerol;
Described emollient is a kind of in dibutyl adipate, dioctyl cyclohexane extraction, isopropyl palmitate, the olive oil;
Described cosolvent be a kind of in sodium carbonate, sodium bicarbonate, aqua ammonia, the triethanolamine or or its combination;
Described solvent is two kinds or its combination in deionized water, methanol, ethanol, the isopropyl alcohol, but wherein a kind of deionized water that is necessary for;
Bronopol), 5-chloro-2-methyl-4-isothiazoline-3-ketone (trade name: a kind of KF-88) described antiseptic is sodium benzoate, 2-bromo-2-nitro-1, ammediol (trade name:.
Described raw material preferably is made up of following weight portion raw material components: film forming matter 10.2-12, coalescents 9-14, emollient 1-4, cosolvent 1-2, solvent 38-40, antiseptic 0.01-0.04;
The present invention also provides a kind of preparation method of liquid-state protective hands mask, may further comprise the steps:
(1) get above-mentioned raw materials respectively, film forming matter, coalescents are put into reactor, heating, 60-80 ℃ is incubated 1-3 hour.
(2) cosolvent and solvent are put into another reactor and fully stir evenly, slowly pour in the material that (1) prepare, heating keeps temperature in the kettle at 60-80 ℃, and constant temperature stirs, and adds emollient simultaneously, stirs evenly, and stops heat tracing;
When (3) treating that temperature of charge is reduced to 40 ℃ of left and right sides in the still, add antiseptic, stirring gets product.
Described method also further comprises:
Step (1) is put into the rustless steel still with film forming matter, coalescents, soaks 2 hours under 60-80 ℃ of temperature;
When step (3) treats that temperature of charge is reduced to 30-50 ℃ in the still, add antiseptic, stirring gets product.
Raw material of the present invention all can obtain quality raw materials from market.
The using method of liquid-state protective hands mask of the present invention: with the labor protection is a kind of liquid hands film of purpose preparation, before the work it is evenly spread upon on hand, can be solidified into the thin film of one deck light flexible after a few minutes at skin surface, work finishes and can rinse well soon with tap water, suds or a small amount of handwashing liquid.
The present invention has the following advantages:
1, the skin of watch face is isolated with the pollutant that contact, consumption is few, and fast drying is easy to use.
2, compare with traditional protective agent, have isolation well, thin film easily solidifies, and the toughness height uses up the convenient advantage of washing in back.
For proving above-mentioned advantage, the present invention has carried out following test:
The liquid-state protective hands mask outward appearance of embodiment 1 to embodiment 7 preparation is the translucent colloid solution of milky, and pH value is 8-9.Getting an amount of (2ml-3ml) liquid-state protective hands mask evenly spreads upon on the both hands, generally in spring, winter, autumn during dry weather, relative humidity is below 60%, during 16 ℃-25 ℃ of room temperatures, the 1min-3min film-forming, summer, relative humidity was more than 60%, 3min-5min film-forming during 25 ℃-30 ℃ of room temperatures.Finger bends and stretches the limbs freely after the film forming.Film and skin attachment are good, and be flexible, do not break, face is smooth glossy, during the clean glass surface of finger touch, does not have finger mark on the glass face, respectively with No. 30 an amount of machinery oil, No. 3 calcium-base grease, alkyd ready-mixed paint, tinol, greasy filth on the lathe arbitrarily sticks on the intact hand skin of film forming and rubs back and forth, the hands film does not have damage, and with suds or handwashing liquid, tap water is easy to wash these dirts afterwards.Observe hand skin and do not have contaminated vestige.State protective hands mask is evenly coated on 8 clean Glass rods or the 8 blocks of clean sheet glass, treat film-forming after, be immersed in kerosene, gasoline, machinery oil, synthetic thinner respectively, nitro-thinner, trichloroethane, toluene, the no abnormal variation of rete more than 30 hours in the butyl acetate.More than test shows that liquid-state protective hands mask of the present invention and skin attachment are good, fast drying, and good toughness, solvent resistance is strong, and fine labor protection characteristic is arranged.
The specific embodiment
Embodiment 1
Liquid-state protective hands mask
Get following raw material (kg): methylcellulose 4, polyvinyl alcohol 7, diethylene glycol 9, caproic acid dibutyl ester 1.2, sodium carbonate 1, sodium benzoate 0.04, methanol 40, add deionized water surplus to 100.
Preparation method: film forming matter, coalescents are put into the rustless steel still, and heating and insulation were soaked 2 hours under this temperature at 60-80 ℃.After after a while cosolvent and solvent being put into another rustless steel still and stirring, slowly pour in the above-mentioned material for preparing, heating keeps temperature in the kettle at 60-80 ℃, turn on agitator is carried out constant temperature and is stirred, add emollient simultaneously, be stirred to evenly, can stop heat tracing.When treating that temperature of charge is reduced to 40 ℃ in the still, add antiseptic, stirring gets product.
Embodiment 2
Liquid-state protective hands mask
Get following raw material (kg): gelatin 0.4, casein 11, propylene glycol 11.5, isopropyl palmitate 1, triethanolamine 0.5, sodium bicarbonate 1, Bronopol 0.02, isopropyl alcohol 10, methanol 28, add water surplus to 100.
Preparation method: film forming matter, coalescents are put into reactor, and heating and insulation were soaked 1 hour under this temperature at 60-80 ℃.After after a while cosolvent and solvent being put into another reactor and stirring, slowly pour in the above-mentioned material for preparing, heating keeps temperature in the kettle at 60-80 ℃, turn on agitator is carried out constant temperature and is stirred, add emollient simultaneously, be stirred to evenly, can stop heat tracing.When treating that temperature of charge is reduced to 30 ℃ in the still, add antiseptic, stirring gets product.
Embodiment 3
Liquid-state protective hands mask
Get following raw material (kg): polyvinyl alcohol 10, gelatin 0.2, glycerol 14, dioctyl cyclohexane extraction 4, ethanol 20, methanol 20, sodium carbonate 0.5, aqua ammonia 0.7, KF-88 0.01, add deionized water surplus to 100.
Preparation method: film forming matter, coalescents are put into reactor, and heating and insulation were soaked 3 hours under this temperature at 60-80 ℃.After after a while cosolvent and solvent being put into another reactor and stirring, slowly pour in the above-mentioned material for preparing, heating keeps temperature in the kettle at 60-80 ℃, turn on agitator is carried out constant temperature and is stirred, add emollient simultaneously, be stirred to evenly, can stop heat tracing.When treating that temperature of charge is reduced to 50 ℃ in the still, add antiseptic, stirring gets product.
Embodiment 4
Get following raw material (kg): casein 4, polyvinyl alcohol 8, glycerol 6, propylene glycol 6, olive oil 1, ethanol 30, isopropyl alcohol 10, triethanolamine 2, KF-88 0.01, deionized water surplus to 100.
Preparation method: add with embodiment 1.
Embodiment 5
Get following raw material (kg): methylcellulose 10, diethylene glycol 8, caproic acid dibutyl ester 1, sodium carbonate 1, methanol 38, sodium benzoate 0.01, add deionized water surplus to 100.
Preparation method: with embodiment 1.
Embodiment 6
Liquid-state protective hands mask
Get following raw material (kg): gelatin 15, propylene glycol 14, isopropyl palmitate 4, triethanolamine 2,, isopropyl alcohol 82, Bronopol 0.05, add deionized water surplus to 100.
Preparation method: with embodiment 2.
Embodiment 6
Liquid-state protective hands mask
Get following raw material (kg): polyvinyl alcohol 12, glycerol 20, olive oil 1, isopropyl palmitate 2, triethanolamine 1.5, ethanol 68, KF-88 0.01, add water surplus to 100.
Preparation method: with embodiment 2.
Claims (4)
1, a kind of liquid-state protective hands mask is made up of following weight portion raw material components: film forming matter 10-15, coalescents 8-14, emollient 1-4, cosolvent 1-2, solvent 38-82, antiseptic 0.01-0.05.
Described film forming matter is a kind of or its combination in gelatin, casein, methylcellulose, the polyvinyl alcohol;
Described coalescents is a kind of or its combination in diethylene glycol, propylene glycol, the glycerol;
Described emollient is a kind of in dibutyl adipate, dioctyl cyclohexane extraction, isopropyl palmitate, the olive oil;
Described cosolvent be a kind of in sodium carbonate, sodium bicarbonate, aqua ammonia, the triethanolamine or or its combination;
Described solvent is two kinds or its combination in water, methanol, ethanol, the isopropyl alcohol, but wherein a kind of water that is necessary for;
Described antiseptic is sodium benzoate, 2-bromo-2-nitro-1, a kind of in ammediol, the 5-chloro-2-methyl-4-isothiazoline-3-ketone.
2, according to the liquid-state protective hands mask of claim 1, form: film forming matter 10.2-12, coalescents 9-14, emollient 1-4, cosolvent 1-2, solvent 38-40, antiseptic 0.01-0.04 by following weight portion raw material components;
3, a kind of preparation method of liquid-state protective hands mask may further comprise the steps:
(1) the weighting profit requires 1 or 2 raw material respectively, and film forming matter, coalescents are put into reactor, heating, and 60-80 ℃ is incubated 1-3 hour.
(2) cosolvent and solvent are put into another reactor and fully stir evenly, slowly pour in the material that (1) prepare, heating keeps temperature in the kettle at 60-80 ℃, and constant temperature stirs, and adds emollient simultaneously, stirs evenly, and stops heat tracing;
When (3) treating that temperature of charge is reduced to 40 ℃ of left and right sides in the still, add antiseptic, stirring gets product.
4, according to the preparation method of a kind of liquid-state protective hands mask of claim 3, also comprise:
Step (1) is put into the rustless steel still with film forming matter, coalescents, soaks 2 hours under 60-g0 ℃ of temperature; When step (3) treats that temperature of charge is reduced to 30-50 ℃ in the still, add antiseptic, stirring gets product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100780371A CN100475185C (en) | 2006-04-30 | 2006-04-30 | A liquid-state protective hands mask and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100780371A CN100475185C (en) | 2006-04-30 | 2006-04-30 | A liquid-state protective hands mask and preparation method thereof |
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| CN1879593A true CN1879593A (en) | 2006-12-20 |
| CN100475185C CN100475185C (en) | 2009-04-08 |
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| CNB2006100780371A Active CN100475185C (en) | 2006-04-30 | 2006-04-30 | A liquid-state protective hands mask and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102961266A (en) * | 2012-12-07 | 2013-03-13 | 纳润（厦门）科技有限公司 | Skin surface paint and greasy dirt isolation film and preparation method thereof |
| CN103074791A (en) * | 2013-01-22 | 2013-05-01 | 陕西科技大学 | Non-wood fiber raw material cooking auxiliary agent and preparation process thereof |
| CN103784338A (en) * | 2012-11-02 | 2014-05-14 | 贾全禄 | Oil-proof hand protection mask |
| CN103784360A (en) * | 2012-11-02 | 2014-05-14 | 贾全禄 | Hand guard film |
| CN103961270A (en) * | 2013-01-30 | 2014-08-06 | 石家庄菠莉亚日用化工有限公司 | Carbon-removing antifouling transparent protection liquid and preparation method thereof |
| CN111053707A (en) * | 2020-03-16 | 2020-04-24 | 广州康健医学科技有限公司 | Liquid film protective agent for disinfection protection and preparation method and application thereof |
-
2006
- 2006-04-30 CN CNB2006100780371A patent/CN100475185C/en active Active
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103784338A (en) * | 2012-11-02 | 2014-05-14 | 贾全禄 | Oil-proof hand protection mask |
| CN103784360A (en) * | 2012-11-02 | 2014-05-14 | 贾全禄 | Hand guard film |
| CN102961266A (en) * | 2012-12-07 | 2013-03-13 | 纳润（厦门）科技有限公司 | Skin surface paint and greasy dirt isolation film and preparation method thereof |
| CN102961266B (en) * | 2012-12-07 | 2014-07-02 | 纳润（厦门）科技有限公司 | Skin surface paint and greasy dirt isolation film and preparation method thereof |
| CN103074791A (en) * | 2013-01-22 | 2013-05-01 | 陕西科技大学 | Non-wood fiber raw material cooking auxiliary agent and preparation process thereof |
| CN103074791B (en) * | 2013-01-22 | 2015-05-20 | 陕西科技大学 | Non-wood fiber raw material cooking auxiliary agent and preparation process thereof |
| CN103961270A (en) * | 2013-01-30 | 2014-08-06 | 石家庄菠莉亚日用化工有限公司 | Carbon-removing antifouling transparent protection liquid and preparation method thereof |
| CN103961270B (en) * | 2013-01-30 | 2018-05-08 | 石家庄菠莉亚日用化工有限公司 | Antifouling stealth protection liquid of a kind of net carbon and preparation method thereof |
| CN111053707A (en) * | 2020-03-16 | 2020-04-24 | 广州康健医学科技有限公司 | Liquid film protective agent for disinfection protection and preparation method and application thereof |
| CN111053707B (en) * | 2020-03-16 | 2020-06-19 | 广州康健医学科技有限公司 | Liquid film protective agent for disinfection protection and preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN100475185C (en) | 2009-04-08 |
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Owner name: BEIJING XINLI MACHINERY CO., LTD. Free format text: FORMER NAME: XINLI MACHINERY FACTORY (STATE-OWNED FACTORY 699), BEIJING |
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Address after: 100039 box 103, box 132, Beijing Patentee after: Beijing Xinli Machinery Co.,Ltd. Address before: 100039 box 103, box 132, Beijing Patentee before: Beijing Xinli Machinery Works (State-owned 699 Works) |