CN103923769A - Ecological detergent and preparation method thereof - Google Patents
Ecological detergent and preparation method thereof Download PDFInfo
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- CN103923769A CN103923769A CN201410180441.4A CN201410180441A CN103923769A CN 103923769 A CN103923769 A CN 103923769A CN 201410180441 A CN201410180441 A CN 201410180441A CN 103923769 A CN103923769 A CN 103923769A
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Abstract
The invention discloses an ecological detergent prepared from pure natural plant raw materials, and belongs to the field of washing products. The ecological detergent disclosed by the invention is prepared from the following raw materials in parts by weight: 8-57 parts of plant raw materials, 2-5 parts of plant thickener, 0.05-0.35 part of leavening agent and 27-180 parts of water, wherein the plant raw materials comprise one or more of citrus peels, pomelo peels, orange peels and citrus limon, longan leaves, stems or leaves of banana trees, carambola leaves and sour carambola fruit. The ecological detergent is unique in formula and wide in sources of the materials and has a relatively strong decontamination effect as well as multiple functions of sterilization, bacteria removal, protection, skin nourishment and the like.
Description
Technical field
The present invention relates to articles for washing field, especially relate to a kind of ecological washing composition of making raw material with plant and preparation method thereof.
Background technology
Washing composition is the requisite in daily life, and people clean various vessel, tableware, clothing and be unable to do without washing composition.According to incompletely statistics, the annual soapless soap consumption of China is 30～400,000 tons of left and right, and has the trend rising year by year.These soapless soaps often contain toxic substance, and the abuse of washing composition can cause the problem such as harden of pollution, the soil of tap water, farm crop and vegetables, even cause cancer, serious threat people's health.Research shows, the soapless soap toxin that enters human body can make calcium ion concn in blood decline, and acidification of blood, makes people easily tired; These toxin also can make the functions of expelling toxin of liver reduce, immunity degradation, and liver cell lesion aggravation, has stronger bringing out property of cancer.According to investigations, the chemical pollution that household detergent causes has made hemopathic patient's showed increased, also causes children's cancer morbidity to increase simultaneously.
In view of this, developing the washing composition of more ecological safer environmental protection, is a problem anxious to be resolved.At present, some domestic technician have done relevant research to this: the Chinese patent that application publication number is CN101451093 discloses a kind of cool leaf, Chinese honey locust washing composition, comprise: cool leaf, Chinese honey locust, its weight percentages is: cool leaf is 10-50% or 50-90%, and Chinese honey locust is 50-90% or 10-50%.Its advantage is nontoxic, pollution-free, and to the person, without any harm, but the raw material of this technology employing is cool leaf, Chinese honey locust, the current quantity of this bi-material is fewer, and raw material sources are wideless, makes formula too simple, do not possess the fresh-keeping effect of self, easily corrupt, be difficult to apply.Granted publication number is that the Chinese patent of CN1318554C discloses a kind of gramineae plant washing composition and compound method thereof, this washing composition is taking straw or straw as raw material, is burned and made extracting solution that plant ash, water raise from plant ash and add the washing composition of auxiliary material preparation as main body composition by control, and auxiliary material comprises zymin, tensio-active agent, thickening material, salt.This invention additive used is many, and is all Chemicals, and making processes cannot ensure the natural environmental-protective of washing composition 100%.
Therefore, existing ecological washing composition still have that starting material are difficult for obtaining, fresh-keeping difficulty or can not ensure the defects such as 100% pure natural.Taking the stem of peel of Citrus reticulata Blanco, pomelo peel, Pericarpium citri sinensis, longan leaf, plantain tree or leaf, carambola leaf, sour Carambola fruit, Lemon fruit as plant material, the technology of producing washing composition as thickening material with plant amylum also has no report in addition.
Summary of the invention
Goal of the invention of the present invention is: for the problem of above-mentioned existence; it is the ecological washing composition of raw material that a kind of natural plant that adopts is provided, and formula is unique, and material source is extensive; when thering is stronger clean effect, also there is the several functions such as sterilization, degerming, protection and skin nutrition.The present invention also provides the making method of described ecological washing composition.
The technical solution used in the present invention is as follows:
A kind of ecological washing composition, raw material by following weight part is made: 8～57 parts of plant materials, 27～180 parts, 2～5 parts of plant thickening materials, 0.05～0.35 part of starter and water are made, described plant material comprises one or more in peel of Citrus reticulata Blanco, pomelo peel, Pericarpium citri sinensis, Lemon fruit, also comprises the stem of longan leaf, plantain tree or leaf, carambola leaf, sour Carambola fruit.
Preferably, in described plant material, each component is the stem of 1～10 part of peel of Citrus reticulata Blanco, 1～10 part of pomelo peel, 1～10 part of Pericarpium citri sinensis, Lemon fruit, 1～10 part of skin, 1～10 part of longan leaf, plantain tree or 1～10 part, leaf, 1～10 part of carambola leaf, 1～10 part of sour Carambola fruit by weight.
Further, described plant material is plant material dry products or fresh goods.
Further, described plant thickening material is yam starch or tapioca (flour).
Further, described starter is distiller's yeast.
Further, the weight of described water is plant material and plant thickening material gross weight 3 times.
Preferably, described ecological washing composition is made up of the raw material of following weight part:
(1) plant material: 7 parts, 7 parts of pomelo peels, 3 parts of peel of Citrus reticulata Blanco, 7 parts of Pericarpium citri sinensiss, 10 parts of Lemon fruits, 7 parts of longan leaves, 6 parts of carambola leaves, 10 parts of sour Carambola fruits, bajiao banana tree root, stem or leaf.
(2) plant thickening material: 3 parts of potato or tapioca (flour)s;
(3) starter: 0.25 part, distiller's yeast;
(4) water: 180 parts.
Preferably, the form of described ecological washing composition is any one in liquid, solid-state, powdery, paste, pasty state.
The making method that a kind of ecological washing composition is provided, comprises the following steps:
(1) will be described mix by weight after plant material chopping, put the infusion 30-60 minute that adds water in pot into, then pour out and put paste roller mill into and fully stir, until described plant material all becomes soup compound.
(2) described soup compound is poured in pot and heated, then add plant thickening material to carry out thickening, when heating, constantly stir, until described soup compound becomes mashed prod.
(3) described mashed prod is poured out to nature and cool to 25～35 DEG C, add powdered starter to mix thoroughly, then tinning sealing, is placed on temperature and is in the environment of 20～30 DEG C and ferment.
(4) after fully fermenting under the effect at distiller's yeast until the each composition in described plant material, can use.
(5) the ecological washing composition being made into seals preservation in shady and cool environment, and the quality guaranteed period can reach about 36 months.
Plant material pomelo peel in above-mentioned formula, peel of Citrus reticulata Blanco, Pericarpium citri sinensis, Lemon fruit belong to Rutaceae Citrus in phytology, for thering is the hesperidium aurantium of keratin pericarp, infusion through step (1) can obtain its natural citrus extracts, wherein comprise the Multiple components such as sad, Palmitic acid, limonene, myrcene, phantol oxide compound, germacrene, wherein main component is limonene, myrcene etc.Step of the present invention (1) gained citrus extracts is a kind of natural vegetalitas solvent, and greasy dirt is had to extremely strong solvency power; Wherein limonene is all effective to the cleaning of ink, grease, paint, tar, bubble gum and pitch, add containing enzyme agent and can remove bloodstain, add lower concentration acids can removing rust, coffee & tea stain, D-limonene can substitute the various chemical solventss of current use in industry cleaning link, changes this present situation of heavy chemicals poisonous and harmful.
The part natural component that the natural citrus extracts of step of the present invention (1) gained contains also has the effect that suppresses microorganism growth, can reach natural antibacterial, bacteriostasis efficacy.The test-results that applicant carries out shows, this extract has the bacteriostatic action of wide spectrum to common bacterial classification, especially the strongest to the bacteriostatic action of intestinal bacteria and streptococcus aureus.
In addition, the natural citrus extracts of step of the present invention (1) gained, limonene, the myrcene itself having has acid and fresh aromatic odour, not only can expel intense strain and pressure, improve the caused insomnia of anxiety, and without extra essence and the pigment of adding, its light orange perfumed ribbon carrys out pure and fresh and spiritual releive happy as sunlight.
In the present invention, by using thickening material can effectively maintain the effective concentration of washing composition, improve the stability of product, prevent that effective constituent runs off, wherein thickening material used is plant thickening material, is preferably tapioca (flour) or yam starch, makes washing composition have excellent dispersion suspension and thickening properties, after disperseing in water, granularity is tiny and be evenly distributed, and has effectively strengthened the soil removability of product.Potato or tapioca (flour) are all the raw materials of food grade, have ensured the ecological, environmental protective of washing composition.
Carambola leaf, the stem of longan leaf, plantain tree and leaf have anti-corrosive fresh-keeping composition, do not need additionally to add Chemical Preservative; In the fugitive constituent of Carambola fruit and carambola leaf, also contain the composition such as palmitinic acid, stearic acid.Palmitinic acid, has another name called 16 (alkane) acid, is a kind of saturated higher fatty acid, is widely used in candle processed, soap, metallic soap, lubricating grease, synthetic detergent, tenderizer; Stearic molecular formula CH3 (CH2) 16COOH, is widely used in makeup processed, stablizer, tensio-active agent, water-resisting agent, rumbling compound, metallic soap, tenderizer, pharmaceuticals and other organic chemicals.
The present invention has added distiller's yeast especially as starter, and the composition in plant material, after distiller's yeast fermentation, has become subacidity material, and clean effect strengthens.
In sum, compared with existing washing composition, washing composition of the present invention has following significant advantage:
(1) raw material adopting is food grade materials, nontoxic, contains natural decontamination composition, has stronger soil removability, does not need to add chemical tensio-active agent; The composition that contains anti-corrosive fresh-keeping, does not need additionally to add chemical sanitas; Contain natural pigment and fragrance, do not need to add artificial color and essence, ensured 100% ecological, environmental protective of washing composition.Product, except being applied to tableware, Glass Containers and stainless steel ware, plastic containers, can also be applied to the field of Liquid soap, bathing agents, is worthy to be popularized.
(2) raw material adopting is food grade materials, and the trace element that contains abundant nutritive ingredient and human body needs, when having stronger clean effect, also has the several functions such as protection and skin nutrition.
(3) product of the present invention does not have foam, and nontoxicity is residual, convenient cleaning, saving water resource.
(4) the formula uniqueness of the technology of the present invention, production technique is simple, and material source is extensive, raw material all comes from the waste of frequently seen plants and fruit, can turn waste into wealth, in production process without waste water, waste gas and solid waste discharge, safety and environmental protection, has utmost point application prospect widely.
Embodiment
Below by embodiment, the invention will be further described.
Embodiment 1
The method of preparing following embodiment 1～6 is:
(1) will be described mix by weight after plant material chopping, put the infusion 30-60 minute that adds water in pot into, then pour out and put paste roller mill into and fully stir, until described plant material all becomes soup compound;
(2) described soup compound is poured in pot and heated, then add plant thickening material to carry out thickening, when heating, constantly stir, until described soup compound becomes mashed prod;
(3) described mashed prod is poured out to nature and cool to 25～35 DEG C, add powdered distiller's yeast to mix thoroughly, then tinning sealing, is placed on temperature and is in the environment of 20～30 DEG C and ferment;
(4) after fully fermenting under the effect at distiller's yeast until the each composition in described plant material, can use;
(5) the ecological washing composition being made into seals preservation in shady and cool environment.
Embodiment 2
Formulation ratio: 7 parts of pomelo peels, 3 parts of peel of Citrus reticulata Blanco, 7 parts of Pericarpium citri sinensiss, 10 parts of Lemon fruits, 7 parts of longan leaves, 6 parts of carambola leaves, 10 parts of sour Carambola fruits, 7 parts, plantain tree stem, 3 parts of potato powders, 0.35 part, distiller's yeast, 180 parts, water.
Wherein, pomelo peel, peel of Citrus reticulata Blanco, Pericarpium citri sinensis, Lemon fruit, longan leaf, sour carambola leaf, sour Carambola fruit, plantain tree cauline leaf are dry product or fresh goods.
According to above-mentioned formula, this ecology washing composition can be made any one in liquid state, solid-state, powdery, paste, pasty state.
Embodiment 3
Formulation ratio: 1 part of pomelo peel, 1 part of peel of Citrus reticulata Blanco, 1 part of Pericarpium citri sinensis, 1 part of Lemon fruit, 1 part of longan leaf, 1 part of carambola leaf, 1 part of sour Carambola fruit, 1 part of bajiao banana leaf, 1 part of Tapioca Starch, 0.05 part, distiller's yeast, 27 parts, water.
According to above-mentioned formula, this ecology washing composition can be made any one in liquid state, solid-state, powdery, paste, pasty state.
Embodiment 4
Formulation ratio: 1 part of pomelo peel, 8 parts of Pericarpium citri sinensiss, 10 parts of Lemon fruits, 1 part of longan leaf, 10 parts of carambola leaves, 5 parts of sour Carambola fruits, 10 parts of bajiao banana leaves, 2 parts of potato powders, 0.3 part, distiller's yeast, 141 parts, water.
According to above-mentioned formula, this ecology washing composition can be made any one in liquid state, solid-state, powdery, paste, pasty state.
Embodiment 5
Formulation ratio: 10 parts of pomelo peels, 10 parts of peel of Citrus reticulata Blanco, 5 parts of Lemon fruits, 10 parts of longan leaves, 3 parts of carambola leaves, 4 parts of sour Carambola fruits, 10 parts, plantain tree stem, 3 parts of potato powders, 0.25 part, distiller's yeast, 165 parts, water.
According to above-mentioned formula, this ecology washing composition is made any one in liquid state, solid-state, powdery, paste, pasty state.
Embodiment 6
Formulation ratio: 5 parts of peel of Citrus reticulata Blanco, 10 parts of Pericarpium citri sinensiss, 3 parts of longan leaves, 2 parts of carambola leaves, 3 parts of sour Carambola fruits, 1 part, plantain tree stem, 5 parts of Tapioca Starchs, 0.2 part, distiller's yeast, 87 parts, water.
According to above-mentioned formula, this ecology washing composition is made any one in liquid state, solid-state, powdery, paste, pasty state.
Embodiment 7
Formulation ratio: 10 parts of peel of Citrus reticulata Blanco, 3 parts of longan leaves, 2 parts of carambola leaves, 1 part of sour Carambola fruit, 3 parts of bajiao banana leaves, 1 part of Tapioca Starch, 0.1 part, distiller's yeast, 60 parts, water.
According to above-mentioned formula, this ecology washing composition is made any one in liquid state, solid-state, powdery, paste, pasty state.
Embodiment 8 performance tests
(1) toxotest
1. experimental technique: according to GB15193.3-2003 acute oral toxicity test, ecological washing composition of the present invention is carried out to toxicity test, choose 20 of healthy Kunming mouses, female 10, male 10, body weight 18-20g; Dosage is designed to 10000mg/kg, 4640mg/kg, 2150mg/kg, tetra-dosage groups of 1000mg/kg, when experiment, tests according to 0.2ml/10g per os gavage.Animal fasting 16h before gavage, freely drinks water.After gavage, continue to give normal diet after fasting 2h.Observation 4h, records toxicity symptom and death condition is as shown in table 1.
2. experimental result: obvious Novel presentation does not all appear in each dosage group, and within the observation period of 14d, Novel presentation does not appear in animal, after off-test, animal is done to gross anatomy and shows no obvious abnormalities yet.Ecological washings of the present invention is actual to chmice acute Oral toxicity is nontoxic.
Table 1 acute oral toxicity test result
| Dosage grouping (mg/kg) | Sex | Number of animals (only) | Dead animal number (only) | Mortality ratio (%) |
| 10000 | ♀ | 5 | 0 | 0 |
| 4640 | ♂ | 5 | 0 | 0 |
| 2150 | ♀ | 5 | 0 | 0 |
| 1000 | ♂ | 5 | 0 | 0 |
(2) washing effect test
1. the detersive power to clothing
According to the washing effect of GB GBT13174-2008 test above-described embodiment.Evaluation index taking B value (whiteness maintenance ratio) as washing effect, in the time of B >=1.0, washing composition detersive power is qualified; When B<1.0, washing composition detersive power is defective.
Test sample comprises JB-01 (carbon black greasy dirt cloth), JB-02 (albumen soiled cotton), JB-03 (sebum soiled cotton).
Wash conditions: detergent concentration 0.2% in washings, 30 DEG C of wash temperatures, washing time 20min, water hardness 250mg/kg.
Test result is shown in table 2.As can be seen from the table, the soil removability of the ecological washing composition of embodiment of the present invention 1-6 all, in qualified index, can be removed the pollutent being attached on clothing fast and up hill and dale.
Table 2 detergency test result
2. the washing effect to tableware
The washing composition that adopts the embodiment of the present invention, in the water of 20 DEG C, washs respectively 30 dish in the mode of hand-washing respectively, and dish comes from certain Sichuan cuisine restaurant, and greasy dirt area accounts for more than 60%, all has remarkable greasy dirt.After getting 3g washing composition and kneading on rag, wiping dish surface gently, after rinsing for 5 seconds with tap water again, observe, the equal washes clean of all dish, dish surface is without visible oil stain, and without dirt, dish is as before bright and clean, and all there is good fresh scent, clean personnel's the not dry tight sensation of hand.
3. washing effect comparison before and after fermentation
Applicant has also tested the washing effect difference of ecological washing composition of the present invention before and after fermentation, testing method is: the ink of coating respectively diameter 4cm at 10 people's the left hand palm of the hand, wherein 5 people use the work in-process washing composition that does not add starter to clean hand, another 5 people use the finished product after fermentation to clean hand, dosage of scour is identical, be 0.5g, when washing, rub 10 times by right finger after with clear water rinse 8 seconds.Result shows: after work in-process clean, wherein 3 people's hand also has fuzzy dirty print, and the hand that fermentation finished product washing composition later cleaned is all completely clean, thereby shows through fermentation detergent washing better effects if later.Everyone wipes dry hand and all thinks that hand is moist comfortable after cleaning, there is no tight sensation, illustrates that product gentleness of the present invention does not stimulate, can skin care.
(3) stability test
Above-mentioned Betengent product, at normal temperatures and pressures, in open air flowing environment, place one month, three months, six months, within 12 months, also observe in the last day of correlation time respectively, all there is not the phenomenon such as precipitation, local muddiness, show that product of the present invention has fabulous stability.
(4) degerming sterilization effect test
Respectively to intestinal bacteria, staphylococcus aureus, subtilis, Candida albicans is tested, experiment is carried out under 20 DEG C of room temperatures, first the thermostatically heating in test tube by the bacterial strain suspension of above-mentioned three kinds of bacterial classifications and washing composition, then in sterile test tube, add 1ml to adopt bacteria suspension and the 4ml washing composition of bovine serum albumin as substratum, mix rear abundant concussion 5 minutes, then calculate sterilizing rate (average colony number in the bacteria suspension of determination experiment front and back), experimental result shows, the washing composition of embodiments of the invention 1～6 to intestinal bacteria killing rate all higher than 95%, show extremely strong killing action, to the killing rate of staphylococcus aureus all higher than 92%, there is significant germicidal action, for subtilis, Candida albicans, embodiment killing rate is higher than 90%, there is obvious sterilization effect.
Claims (9)
1. an ecological washing composition, it is characterized in that being made by the raw material of following weight part: 8～57 parts of plant materials, 27～180 parts, 2～5 parts of plant thickening materials, 0.05～0.35 part of starter and water are made, described plant material comprises one or more in peel of Citrus reticulata Blanco, pomelo peel, Pericarpium citri sinensis, Lemon fruit, also comprises the stem of longan leaf, plantain tree or leaf, carambola leaf, sour Carambola fruit.
2. the ecological washing composition of one according to claim 1, is characterized in that: in described plant material, each component is the stem of 1～10 part of peel of Citrus reticulata Blanco, 1～10 part of pomelo peel, 1～10 part of Pericarpium citri sinensis, 1～10 part of Lemon fruit, 1～10 part of longan leaf, plantain tree or 1～10 part, leaf, 1～10 part of carambola leaf, 1～10 part of sour Carambola fruit by weight.
3. the ecological washing composition of one according to claim 2, is characterized in that: described plant material is plant material dry product or fresh goods.
4. the ecological washing composition of one according to claim 3, is characterized in that: described plant thickening material is yam starch or tapioca (flour).
5. the ecological washing composition of one according to claim 4, is characterized in that: described starter is distiller's yeast.
6. the ecological washing composition of one according to claim 5, is characterized in that: the weight of described water is plant material and plant thickening material gross weight 3 times.
7. the ecological washing composition of one according to claim 6, is characterized in that being made up of the raw material of following weight part:
(1) plant material: 7 parts, the stem of 7 parts of pomelo peels, 3 parts of peel of Citrus reticulata Blanco, 7 parts of Pericarpium citri sinensiss, 10 parts of Lemon fruits, 7 parts of longan leaves, 6 parts of carambola leaves, 10 parts of sour Carambola fruits, plantain tree or leaf;
(2) plant thickening material: 3 parts of potato or tapioca (flour)s;
(3) starter: 0.25 part, distiller's yeast;
(4) water: 180 parts.
8. according to the ecological washing composition of one described in claim 1～7, it is characterized in that: the form of described ecological washing composition is any one in liquid, solid-state, powdery, paste, pasty state.
9. according to the making method of a kind of ecological washing composition described in claim 1～8, it is characterized in that comprising following steps:
(1) will be described mix by weight after plant material chopping, put the infusion 30-60 minute that adds water in pot into, then pour out and put paste roller mill into and fully stir, until described plant material all becomes soup compound;
(2) described soup compound is poured in pot and heated, then add plant thickening material to carry out thickening, when heating, constantly stir, until described soup compound becomes mashed prod;
(3) described mashed prod is poured out to nature and cool to 25～35 DEG C, add powdered starter to mix thoroughly, then tinning sealing, be placed in the environment of 20～30 DEG C of temperature and ferment;
(4), can use under the effect at distiller's yeast fully after fermentation until each component of described plant material;
(5) the ecological washing composition being made into seals preservation in shady and cool environment.
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