CN103920013A - Preparation method of dendrobium officinale ultramicro wall-broken powder - Google Patents
Preparation method of dendrobium officinale ultramicro wall-broken powder Download PDFInfo
- Publication number
- CN103920013A CN103920013A CN201410131416.7A CN201410131416A CN103920013A CN 103920013 A CN103920013 A CN 103920013A CN 201410131416 A CN201410131416 A CN 201410131416A CN 103920013 A CN103920013 A CN 103920013A
- Authority
- CN
- China
- Prior art keywords
- herba dendrobii
- wall
- dendrobium officinale
- broken
- powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Abstract
The invention discloses a preparation method of dendrobium officinale ultramicro wall-broken powder. The preparation method comprises the following steps: (1) removing roots and leaves of fresh dendrobium officinale, cleaning, placing in alcohol to soak for 3-5 minutes, and then washing; (2) after draining off water, cutting the fresh dendrobium officinale into small pieces; (3) drying and sterilizing the obtained small pieces of dendrobium officinale obtained in the step (2); (4) initially smashing the sterilized and dried small pieces of dendrobium officinale; (5) breaking wall of the obtained dendrobium officinale coarse powder to obtain the dendrobium officinale ultramicro wall-broken powder. The preparation method disclosed by the invention has the beneficial effects that the dendrobium officinale ultramicro wall-broken powder prepared by the invention not only maintains the active components to the maximum extent, but also better solves the problems that microorganisms in raw dendrobium officinale powder exceed the standard and the like. The broken rate of the product is over 99%, so that the solubility and bioavailability of the dendrobium officinale product are improved. The product is viridescent powder which is a fully natural and full-component green product easy to absorb.
Description
Technical field
The present invention relates to Chinese herbal medicine preparing technical field, is a kind of preparation method of Herba Dendrobii super-micro wall-broken powder.
Background technology
Herba Dendrobii (Dendrobium.candidumWall.ex Lindl.), herbaceous plant grows nonparasitically upon another plant for the orchid family is perennial.Be born on the wet cloudy rock in mountain region half that height above sea level reaches 1600 meters, the environment of happiness warm and moist weather and half cloudy half light, cold-resistant.Herba Dendrobii is China's tradition rare Chinese medicine, has the effect of reinforcing stomach reg fluid, nourishing YIN and clearing away heat, and for calentura Tianjin wound, xerostomia excessive thirst, deficiency of stomach-Yin, lack of appetite is retched, and deficiency-heat is not moved back after being ill, hyperactivity of fire caused by deficiency of YIN, and muscles and bones flaccidity is soft.Modern study shows, Herba Dendrobii main component is iron sheet polysaccharide, dendrobine, aminoacid, various trace elements.Be specially adapted to modern owing to being busy with one's work, rhythm of life is fast, the symptoms such as the dry mouth and tougue of often staying up late and causing, yin asthenia generating intrinsic heat, for strengthening modern's body constitution, defying age, anti-curing cancers, treatment diabetes and atrophic gastritis, have definite curative effect, to tobacco and wine excessively, overwork, night life excessively, with a brain overwork, vocal cords are hoarse etc., have a good restitution.
Summary of the invention
The present invention will solve the shortcoming of above-mentioned prior art, and a kind of preparation method of Herba Dendrobii super-micro wall-broken powder is provided.
The present invention solves the technical scheme that its technical problem adopts: the preparation method of this Herba Dendrobii super-micro wall-broken powder, the method comprises the steps:
(1) fresh of Herba Dendrobii is removed to root, defoliation, after first cleaning up with tap water, putting into percent by volume trial is that 75% ethanol soaks 3-5min, then rinses well by purified water;
(2), after water drains, with repeatedly medicine cutter, by fresh, be cut into segment;
(3) the Herba Dendrobii segment of step (2) gained is put into belt type microwave dry sterilizer and process 10-15min; The parameter of belt type microwave dry sterilizer is: microwave frequency is 2440-2460MHZ, microwave power 8-12kw, material transmitted frequency 10-15HZ, solid accumulation thickness≤1cm, Herba Dendrobii segment moisture≤5% after processing, total plate count≤10000cfu/g, fungi count≤50cfu/g;
(4) the good Herba Dendrobii segment of sterilizing and drying is put into beater grinder, be tentatively crushed to 40-60 order;
(5) the Herba Dendrobii coarse powder of step (4) gained is carried out to broken wall treatment with low-temperature airflow wall-breaking machine, finally obtain Herba Dendrobii super-micro wall-broken powder; The parameter of low-temperature airflow wall-breaking machine is: compressed air temperature 0-4 ℃, pressure 0.8-1.0Mpa, air-introduced machine frequency 40-45Hz, grading wheel frequency 80-100Hz, reinforced electric machine frequency 10-15Hz, the final Herba Dendrobii wall cell disruption powder obtaining is light green, granularity is 50-80nm, and sporoderm-broken rate is more than 99%.
In described step (2), the length of Herba Dendrobii segment is 0.7-1mm.
The cellulase and the pectase mixture that when broken wall treatment, add gross mass 1%, the mass ratio of its cellulase and pectase is 1:3.Apply this additive and proportioning, can increase the effect of sporoderm-broken rate.
Compared with prior art, the effect that the present invention is useful is in the present invention: the Herba Dendrobii super-micro wall-broken powder of preparing by the present invention, both farthest retained its active component, and well solved again the problems such as the microorganism of Herba Dendrobii powder exceeds standard of eating something rare.This product sporoderm-broken rate more than 99%, has improved dissolubility and the bioavailability of Herba Dendrobii product.This product is light green powder, is a kind of All Pure Nature, whole part, the easy green product absorbing.
The specific embodiment
Below in conjunction with embodiment, the invention will be further described:
The preparation method of this Herba Dendrobii super-micro wall-broken powder, the method comprises the steps:
(1) fresh of Herba Dendrobii is removed to root, defoliation, after first cleaning up with tap water, putting into percent by volume trial is that 75% ethanol soaks 3-5min, then rinses well by purified water;
(2), after water drains, with repeatedly medicine cutter, by fresh, be cut into the segment that length is 0.7-1mm;
(3) the Herba Dendrobii segment of step (2) gained is put into belt type microwave dry sterilizer and process 10-15min; The parameter of belt type microwave dry sterilizer is: microwave frequency is 2440-2460MHZ, microwave power 8-12kw, material transmitted frequency 10-15HZ, solid accumulation thickness≤1cm, Herba Dendrobii segment moisture≤5% after processing, total plate count≤10000cfu/g, fungi count≤50cfu/g;
(4) the good Herba Dendrobii segment of sterilizing and drying is put into beater grinder, be tentatively crushed to 40-60 order;
(5) the Herba Dendrobii coarse powder of step (4) gained is carried out to broken wall treatment with low-temperature airflow wall-breaking machine, finally obtain Herba Dendrobii super-micro wall-broken powder; The cellulase and the pectase mixture that when broken wall treatment, add gross mass 1%, the quality warp of its cellulase and pectase is 1:3.Apply this additive and proportioning, can increase the effect of sporoderm-broken rate.The parameter of low-temperature airflow wall-breaking machine is: compressed air temperature 0-4 ℃, pressure 0.8-1.0Mpa, air-introduced machine frequency 40-45Hz, grading wheel frequency 80-100Hz, reinforced electric machine frequency 10-15Hz, the final Herba Dendrobii wall cell disruption powder obtaining is light green, granularity is 50-80nm, and sporoderm-broken rate is more than 99%.
Embodiment 1:
Fresh of Herba Dendrobii is removed to root, defoliation, after first cleaning up with tap water, put into 75% ethanol and soak 3min, then rinse well by purified water.After water drains, with repeatedly medicine cutter by fresh segment that is cut into 0.7mm.Then put it in belt type microwave dry sterilizer, adjusting microwave frequency is 2440MHZ, microwave power 8kw, and material transmitted frequency 10HZ, and guarantee solid accumulation thickness≤1cm, process 15min.The Herba Dendrobii segment that sterilizing and drying is good is put into beater grinder, be tentatively crushed to 40-60 order.Then with low-temperature airflow wall-breaking machine, carry out broken wall treatment, control parameter: 1 ℃ of compressed air temperature, pressure 0.8Mpa, air-introduced machine frequency 45Hz, grading wheel is 100Hz frequently, and reinforced electric machine frequency 15Hz, finally obtains Herba Dendrobii super-micro wall-broken powder.
Embodiment 2:
Fresh of Herba Dendrobii is removed to root, defoliation, after first cleaning up with tap water, put into 75% ethanol and soak 4min, then rinse well by purified water.After water drains, with repeatedly medicine cutter by fresh segment that is cut into 0.8mm.Then put it in belt type microwave dry sterilizer, adjusting microwave frequency is 2450MHZ, microwave power 10kw, and material transmitted frequency 12HZ, and guarantee solid accumulation thickness≤1cm, process 12min.The Herba Dendrobii segment that sterilizing and drying is good is put into beater grinder, be tentatively crushed to 40-60 order.Then with low-temperature airflow wall-breaking machine, carry out broken wall treatment, control parameter: 2 ℃ of compressed air temperature, pressure 0.9Mpa, air-introduced machine frequency 42Hz, grading wheel is 90Hz frequently, and reinforced electric machine frequency 12Hz, finally obtains Herba Dendrobii super-micro wall-broken powder.
Embodiment 3:
Fresh of Herba Dendrobii is removed to root, defoliation, after first cleaning up with tap water, put into 75% ethanol and soak 5min, then rinse well by purified water.After water drains, with repeatedly medicine cutter by fresh segment that is cut into 0.9mm.Then put it in belt type microwave dry sterilizer, adjusting microwave frequency is 2460MHZ, microwave power 12kw, and material transmitted frequency 15HZ, and guarantee solid accumulation thickness≤1cm, process 10min.The Herba Dendrobii segment that sterilizing and drying is good is put into beater grinder, be tentatively crushed to 40-60 order.Then with low-temperature airflow wall-breaking machine, carry out broken wall treatment, add cellulase and the pectase mixture of gross mass 1% when broken wall treatment, the mass ratio of its cellulase and pectase is 1:3.Apply this additive and proportioning, can increase the effect of sporoderm-broken rate.Control parameter: 3 ℃ of compressed air temperature, pressure 1.0Mpa, air-introduced machine frequency 40Hz, grading wheel is 80Hz frequently, and reinforced electric machine frequency 10Hz, finally obtains Herba Dendrobii super-micro wall-broken powder.
In addition to the implementation, the present invention can also have other embodiments.All employings are equal to the technical scheme of replacement or equivalent transformation formation, all drop on the protection domain of requirement of the present invention.
Claims (3)
1. a preparation method for Herba Dendrobii super-micro wall-broken powder, is characterized in that: the method comprises the steps:
(1) fresh of Herba Dendrobii is removed to root, defoliation, after first cleaning up with tap water, putting into percent by volume trial is that 75% ethanol soaks 3-5min, then rinses well by purified water;
(2), after water drains, with repeatedly medicine cutter, by fresh, be cut into segment;
(3) the Herba Dendrobii segment of step (2) gained is put into belt type microwave dry sterilizer and process 10-15min; The parameter of belt type microwave dry sterilizer is: microwave frequency is 2440-2460MHZ, microwave power 8-12kw, material transmitted frequency 10-15HZ, solid accumulation thickness≤1cm, Herba Dendrobii segment moisture≤5% after processing, total plate count≤10000cfu/g, fungi count≤50cfu/g;
(4) the good Herba Dendrobii segment of sterilizing and drying is put into beater grinder, be tentatively crushed to 40-60 order;
(5) the Herba Dendrobii coarse powder of step (4) gained is carried out to broken wall treatment with low-temperature airflow wall-breaking machine, finally obtain Herba Dendrobii super-micro wall-broken powder; The parameter of low-temperature airflow wall-breaking machine is: compressed air temperature 0-4 ℃, pressure 0.8-1.0Mpa, air-introduced machine frequency 40-45Hz, grading wheel frequency 80-100Hz, reinforced electric machine frequency 10-15Hz, the final Herba Dendrobii wall cell disruption powder obtaining is light green, granularity is 50-80nm, and sporoderm-broken rate is more than 99%.
2. the preparation method of Herba Dendrobii super-micro wall-broken powder according to claim 1, is characterized in that: in described step (2), the length of Herba Dendrobii segment is 0.7-1mm.
3. the preparation method of Herba Dendrobii super-micro wall-broken powder according to claim 1, is characterized in that: when broken wall treatment, add cellulase and the pectase mixture of gross mass 1%, the mass ratio of its cellulase and pectase is 1:3.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410131416.7A CN103920013A (en) | 2014-04-02 | 2014-04-02 | Preparation method of dendrobium officinale ultramicro wall-broken powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410131416.7A CN103920013A (en) | 2014-04-02 | 2014-04-02 | Preparation method of dendrobium officinale ultramicro wall-broken powder |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103920013A true CN103920013A (en) | 2014-07-16 |
Family
ID=51138555
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410131416.7A Pending CN103920013A (en) | 2014-04-02 | 2014-04-02 | Preparation method of dendrobium officinale ultramicro wall-broken powder |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103920013A (en) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105380974A (en) * | 2015-12-22 | 2016-03-09 | 广州今典精方医药科技有限公司 | Production method of ginseng cell wall-breaking powder |
| CN105560888A (en) * | 2015-12-15 | 2016-05-11 | 云南民族大学 | Method for increasing leaching rate of polyphenols in dendrobium officinale kimura et migo |
| CN105726986A (en) * | 2016-03-10 | 2016-07-06 | 浙江万寿康药业有限公司 | Production process of Dendrobium officinale fine powder |
| CN105907523A (en) * | 2015-02-10 | 2016-08-31 | 余芳 | Brewing method of dendrobe healthcare wine |
| CN106256268A (en) * | 2015-06-15 | 2016-12-28 | 王林华 | A kind of formula of Herba Dendrobii breaking cellular wall new product |
| CN106421426A (en) * | 2016-11-22 | 2017-02-22 | 张家港昊盛实业投资有限公司 | Dendrobium officinale powder and making method thereof |
| CN106544256A (en) * | 2016-12-22 | 2017-03-29 | 西南林业大学 | A kind of dendrobium officinale health wine and preparation method thereof |
| CN111513304A (en) * | 2020-05-09 | 2020-08-11 | 张盛南 | Dendrobium officinale leaf and flower food additive and preparation method thereof |
| CN111920846A (en) * | 2020-08-27 | 2020-11-13 | 海南正生堂食品科技有限公司 | Preparation method of beautiful millettia root wall-breaking powder electuary |
| CN113058720A (en) * | 2021-03-15 | 2021-07-02 | 霍山县斛状元科技有限公司 | Method for preparing fresh dendrobe juice powder |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101810330A (en) * | 2010-04-19 | 2010-08-25 | 奉化益珍海藻科技有限公司 | Enteromorpha clathrata-dendrobium refined flour |
| CN101884650A (en) * | 2010-07-19 | 2010-11-17 | 江苏丘陵地区镇江农业科学研究所 | Method for producing Chinese herbal medicine powder by using superfine grinding and enzymatic wall-breaking combined technology |
| CN101979639A (en) * | 2010-09-27 | 2011-02-23 | 广东光宇生物科技有限公司 | Dendrobium polysaccharide with hypoglycemic activity and extracting method thereof |
| CN102526497A (en) * | 2012-01-16 | 2012-07-04 | 澄思源生物科技（上海）有限公司 | Preparation method and application of Dendrobium officinale health product |
| CN102552699A (en) * | 2012-01-16 | 2012-07-11 | 澄思源生物科技（上海）有限公司 | Preparation method of dendrobium candidum ultrafine powder |
| CN102964461A (en) * | 2012-11-20 | 2013-03-13 | 六安同济生生物科技有限公司 | Auxiliary extraction method of biological enzyme for improving dissolution rate of dendrobe bioactive polysaccharide |
| CN103301322A (en) * | 2013-06-01 | 2013-09-18 | 普洱淞茂制药股份有限公司 | Dendrobium ultramicro-pure powder, as well as preparation method and preparation thereof |
-
2014
- 2014-04-02 CN CN201410131416.7A patent/CN103920013A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101810330A (en) * | 2010-04-19 | 2010-08-25 | 奉化益珍海藻科技有限公司 | Enteromorpha clathrata-dendrobium refined flour |
| CN101884650A (en) * | 2010-07-19 | 2010-11-17 | 江苏丘陵地区镇江农业科学研究所 | Method for producing Chinese herbal medicine powder by using superfine grinding and enzymatic wall-breaking combined technology |
| CN101979639A (en) * | 2010-09-27 | 2011-02-23 | 广东光宇生物科技有限公司 | Dendrobium polysaccharide with hypoglycemic activity and extracting method thereof |
| CN102526497A (en) * | 2012-01-16 | 2012-07-04 | 澄思源生物科技（上海）有限公司 | Preparation method and application of Dendrobium officinale health product |
| CN102552699A (en) * | 2012-01-16 | 2012-07-11 | 澄思源生物科技（上海）有限公司 | Preparation method of dendrobium candidum ultrafine powder |
| CN102964461A (en) * | 2012-11-20 | 2013-03-13 | 六安同济生生物科技有限公司 | Auxiliary extraction method of biological enzyme for improving dissolution rate of dendrobe bioactive polysaccharide |
| CN103301322A (en) * | 2013-06-01 | 2013-09-18 | 普洱淞茂制药股份有限公司 | Dendrobium ultramicro-pure powder, as well as preparation method and preparation thereof |
Non-Patent Citations (1)
| Title |
|---|
| 张阳德编著: "《纳米生物材料学》", 30 June 2005, 化学工业出版社 * |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105907523A (en) * | 2015-02-10 | 2016-08-31 | 余芳 | Brewing method of dendrobe healthcare wine |
| CN106256268A (en) * | 2015-06-15 | 2016-12-28 | 王林华 | A kind of formula of Herba Dendrobii breaking cellular wall new product |
| CN105560888A (en) * | 2015-12-15 | 2016-05-11 | 云南民族大学 | Method for increasing leaching rate of polyphenols in dendrobium officinale kimura et migo |
| CN105380974A (en) * | 2015-12-22 | 2016-03-09 | 广州今典精方医药科技有限公司 | Production method of ginseng cell wall-breaking powder |
| CN105380974B (en) * | 2015-12-22 | 2019-02-15 | 广州今典精方医药科技有限公司 | A kind of production method of ginseng-cell wall cell disruption powder |
| CN105726986A (en) * | 2016-03-10 | 2016-07-06 | 浙江万寿康药业有限公司 | Production process of Dendrobium officinale fine powder |
| CN106421426A (en) * | 2016-11-22 | 2017-02-22 | 张家港昊盛实业投资有限公司 | Dendrobium officinale powder and making method thereof |
| CN106544256A (en) * | 2016-12-22 | 2017-03-29 | 西南林业大学 | A kind of dendrobium officinale health wine and preparation method thereof |
| CN111513304A (en) * | 2020-05-09 | 2020-08-11 | 张盛南 | Dendrobium officinale leaf and flower food additive and preparation method thereof |
| CN111920846A (en) * | 2020-08-27 | 2020-11-13 | 海南正生堂食品科技有限公司 | Preparation method of beautiful millettia root wall-breaking powder electuary |
| CN113058720A (en) * | 2021-03-15 | 2021-07-02 | 霍山县斛状元科技有限公司 | Method for preparing fresh dendrobe juice powder |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103920013A (en) | Preparation method of dendrobium officinale ultramicro wall-broken powder | |
| CN102224910B (en) | Method for producing food ingredient rich in nitrite and flavonoid by use of celery leaves | |
| CN102178341A (en) | Method for processing stalk filaments of tobacco stalks | |
| CN102018272A (en) | Pretreatment method of burley tobacco shred and application thereof in cigarette product | |
| CN105695080A (en) | Preparation method of tea oil | |
| CN103420369A (en) | Preparation method of active carbon by adopting zinc chloride activated loofah sponge | |
| CN104782269A (en) | Cultivation method of cyclocarya paliurus seeds | |
| CN102949373B (en) | Foot bath effervescent tablets and preparation method thereof | |
| CN105639002A (en) | Processing method for ginkgo leaf tea | |
| CN105325595A (en) | Preparation process of wild fu brick black tea | |
| CN105400609A (en) | Cleaning agent of koji-making plant for preparing koji | |
| CN105475539A (en) | Autumn health-preserving tea and preparation method thereof | |
| KR101212718B1 (en) | Preparing method for soybean sauce using Salicornia herbacea powder by high pressure water extracting | |
| CN104187470B (en) | A kind of auricularia auriculajudae cucumber congee that can alleviate canker sore | |
| KR100939976B1 (en) | Making method of guava leaf tee | |
| CN102745688A (en) | Process for preparing bamboo shoot shell based activated carbon by means of zinc chloride activation method | |
| CN106676881A (en) | Nano zinc oxide antibacterial true silk fabric and manufacturing technique thereof | |
| CN105211277A (en) | A kind of leafy vegetable antistaling agent | |
| CN109527905A (en) | A kind of agalloch eaglewood pillow and preparation method thereof | |
| CN212937760U (en) | CO (carbon monoxide)2Deastringency pot | |
| CN105968227A (en) | Process of extracting pectin from snake gourd peel | |
| CN102948540A (en) | Male drinking tea | |
| CN105394505A (en) | Method for comprehensive utilization of moso bamboo leftover material | |
| CN105211275A (en) | A kind of fresh-keeping agent of watermelon | |
| CN104543606A (en) | Steamed rice dumpling leaf rich in sodium copper chlorophyllin and making method of steamed rice dumpling leaf |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20140716 |
|
| RJ01 | Rejection of invention patent application after publication |