CN103919704B - A kind of anti-ageing Essence - Google Patents
A kind of anti-ageing Essence Download PDFInfo
- Publication number
- CN103919704B CN103919704B CN201410176978.3A CN201410176978A CN103919704B CN 103919704 B CN103919704 B CN 103919704B CN 201410176978 A CN201410176978 A CN 201410176978A CN 103919704 B CN103919704 B CN 103919704B
- Authority
- CN
- China
- Prior art keywords
- component
- parts
- ageing
- extract
- subsequent use
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Cosmetics (AREA)
Abstract
The anti-ageing Essence of one disclosed by the invention, relates to the cosmetics processing technique field in daily-use chemical industry, is to be prepared from by following raw materials according: A component: polyethylene glycol, propane diols, glycerine, butanediol; B component: tea oil, rilanit special, C12-20 alkyl glucoside, stearine, 18 alcohol; C component: methyl hydroxybenzoate, Kathon CG, imidazolidinyl urea; D component: Co-Q10, saualane, pyrrolidone sodium carboxylate; E component: kiss-me extract, centella extract; Citric acid; Surplus is deionized water, adds up to 100 parts; Its preparation process is as follows: 1., A component mix; 2., B component is mixed; 3., AB group is mixed; 4., ABC group is mixed; 5., entirely mix; 6., ageing. Existing good moisturizing effect, has again senile-resistant efficacy, is suitable for different skin quality, has anti-ageing demand crowd to use.
Description
Technical field
The present invention relates to the cosmetics processing technique field in daily-use chemical industry, particularly a kind of anti-ageing essenceChina's liquid.
Technical background
Skin aging is a progressive physiology course, is also heredity, environment, social mentality etc.The result of various factors comprehensive function. Along with the raising of people's living standard, to the merit of skin care itemEnergy requires more and more higher, and the skin care item that possess anti-ageing effect also emerge in an endless stream. Essence, isBe added with skin care item for concentrated high nutritional labeling, according to the specific aim of its formula, haveAnti-ageing, crease-resistant, compact, moisturizing, Bearberry Extract. As the Est é eLauder in the fashionable worldInstant special profit is repaired elite，The compound elite of sisley polywater, JasonNatural esterification C whitening resistOld and feeble perfect Essence etc. In these product compositions, add multiple concentrated elite, also added simultaneouslyMore anticorrisive agents, the especially easily anticorrisive agent of sensitization, as dibutyl hydroxy toluene and phenmethylol. CauseThis, seek safer, milder, more effective skin care item are very urgent. As (special in Chinese patentProfit application number is 201210455923.7) " a kind of Aloe essential liquid ", it is by below by mass partsThe raw material of proportioning forms: plant essence liquid 70%-80%, aloe juice 2%-4%, ursin 0.5%-1%, glycerine 1%-3%, centella 1.5%-3%, hyaluronic acid 0.2%-0.5%, collagen eggWhite 0.1%-0.5%, vitamin e 0.2%-0.5%, Amino acid 0.2%-0.5%, all the other are glycerine;This invention can be dredged the pore that is obstructed, and bactericidal antiphlogistic supplements the required moisture of skin, strengthens cell comprehensivelyVigor and elasticity, increase tight skin density, removes the dim metabolin of epidermis.
Technology contents
The object of the present invention is to provide a kind of existing good moisturizing, moisturizing effect, have againThe skin-protection product of senile-resistant efficacy.
For realizing its object, the technical solution used in the present invention is a kind of anti-ageing Essence of invention:
(i) be, to be prepared from by following raw material by weight:
A component: polyethylene glycol 6-9 part, propane diols 4-8 part, glycerine 5-12 part, butanediol1-3 part;
B component: tea oil 4-6 part, rilanit special 1-4 part, C12-20 alkyl glucoside 1-5Part, stearine 1-5 part, 18 alcohol 0.5-3 parts;
C component: methyl hydroxybenzoate 0.05-0.15 part, Kathon CG 0.2-0.4 part, imidazolidinyl urea0.2-0.3 part;
D component: Co-Q10 0.1-0.5 part, saualane 1-3 part, pyrrolidone sodium carboxylate 1-7Part;
E component: kiss-me extract 12-20 part, centella extract 6-12 part;
Citric acid: 0.01-0.1 part;
Surplus is deionized water, adds up to 100 parts;
(ii), its preparation process is as follows:
1., A component is mixed: all raw materials of A component are joined in deionized water, with 2000The rotating speed of r/min stirs 2-4min, then, is heated to by the programming rate of 2-4 DEG C/min70-80 DEG C, keeps 8-12min, becomes A component compound, for subsequent use;
2., B component is mixed: all raw materials of B component are mixed, with 2000r/min'sRotating speed stirs 2-4min, then, is heated to 60-80 DEG C by the programming rate of 2-4 DEG C/min, keeps8-12min, becomes B component compound, for subsequent use;
3., AB organizes mixing: A component compound for subsequent use is mixed with B component compound,Rotating speed with 500r/min under 60-80 DEG C of condition stirs, pre-emulsification 10-20min, then, and with 1-2 DEG CThe speed slow cooling of/min is during to 50-70 DEG C, then stirs 5-10 with the rotating speed of 3000r/minMin, then pass through successively the high-pressure homogeneous 5-10min of 20-40MPa, 5-15Mpa low pressure homogeneous 5-10minAfter processing, vacuum outgas under 0.1-0.5Mpa condition, becomes AB component compound, for subsequent use;
4., ABC organizes mixing: it is 50-70 DEG C that AB component compound for subsequent use is kept to temperature, constant temperatureThe all raw materials that add C component under condition, mix, and become ABC group compound, for subsequent use;
5., entirely mix: ABC for subsequent use is organized to compound from the 50-70 DEG C of speed with 1-2 DEG C/minBe cooled to 40-60 DEG C, add all raw materials of D component and E component, then add lemon acid for adjusting pHBe worth to 6-7, then, stir and be cooled to 25-35 DEG C with the speed of 1000r/min, become full batch mixing,For subsequent use;
6., ageing: full batch mixing for subsequent use is placed to ageing 25-35h at 20-25 DEG C, anti-ageingOld Essence.
The technical scheme of its optimization is to be prepared from by following raw material by weight:
A component: 6 parts of polyethylene glycol, 7 parts of propane diols, 12 parts of glycerine, 1 part of butanediol;
B component: 4 parts of tea oil, 1 part of rilanit special, 1 part of C12-20 alkyl glucoside, glycerine2 parts of stearates, 1.5 parts of 18 alcohol;
C component: 0.05 part of methyl hydroxybenzoate, 0.2 part of Kathon CG, 0.3 part of imidazolidinyl urea;
D component: 0.1 part of Co-Q10,2.5 parts of saualanes, 3 parts of pyrrolidone sodium carboxylates;
E component: 16 parts of kiss-me extracts, 10 parts of centella extracts;
Citric acid: 0.02 part;
Surplus is deionized water, adds up to 100 parts.
Described tea oil is commercially available refining tea oil. Also can adopt following method to be prepared from: by commercially availableRefining tea oil, be heated to 45-55 DEG C, constant temperature keep 15-25min; Then, be cooled to 3-5 DEG C,Growing the grain 10-15h; Under 0-4 DEG C of cryogenic conditions, vacuum filtration, isolates liquid fat and solid againBody lipid, the liquid fat of collecting gained, is required tea oil.
Described kiss-me extract is that kiss-me herb deionized water is cleaned up, and squeezes itJuice, gained after filtering. Also can be prepared from as follows: by clear kiss-me herb deionized waterWash clean, squeezes its juice, after filtration, obtains respectively filtrate A and residual filter residue; In residual filter residue, add againThe 1.5-2.5 times of ethanol that weight, volumetric concentration are 45-55%, soaks 10-15 at normal temperatures and pressuresHour, filter, obtain soak; The method that again soak is adopted to reduced pressure concentration, is concentrated into original volumeHalf, obtain liquor B; Merging filtrate A and liquor B, be required kiss-me extract. Above-mentionedKiss-me used is to adopt fresh kiss-me herb.
Described centella extract is that centella is cleaned up, according to the weight ratio of solid-liquid ratio 1:5Example adds pure water, boils and extracts 1 hour, gained after filtering. Also can prepare as follows andBecome: centella is cleaned up by deionized water, add according to the part by weight of solid-liquid ratio 1:10-20Deionized water, is heated to 90-110 DEG C, constant temperature extract 1-3 hour, filter, respectively once carryGet liquid and filter residue; Press again the part by weight of solid-liquid ratio 1:10-20, in filter residue, add deionized water,Boil and extract 0.5-2 hour, filter, obtain secondary raffinate; Merge extracted twice liquid, and adopt trueEmpty concentrated method, is concentrated into the half of original volume, is required centella extract.
Anti-ageing Essence of the present invention, the main raw material(s) adopting comprises:
A, polyethylene glycol: i.e. PEG-600 is a kind of water-soluble polymer of nonionic, chemistryStable in properties, in the present invention as lubricant and wetting agent;
B, propane diols: coordinate as wetting agent with glycerine in the present invention;
C, glycerine: i.e. glycerine, in the present invention as NMF;
D, butanediol: having another name called 1,3-dihydroxy butane, is the one of polyalcohol, in the present inventionMiddle as NMF and solvent;
E, stearine: in the present invention as emulsifying agent;
F, tea oil: faint yellow transparent liquid is the kind benevolence by oil tea section plant oil tea(CamelliaoleiferaAbel) squeeze the grease of gained, contain more than 85% unsaturated lipidFat acid, is the active ingredient in the present invention, uses as softening agent;
G, rilanit special: can promote dispersed in product of oil phase maintenance composition, at thisIn invention, be used as solubilizer;
H, C12-20 alkyl glucoside: a kind of non-ionic surface active agent of low stimulation, in the present inventionMiddle as emulsifying agent, emulsion stabilizer use;
I, 18 alcohol: be the base stock of cosmetics cream frost, emulsion, there is the effect of thickening emulsion,Use as emulsion stabilizer in the present invention;
J, citric acid: in order to prepare cushioning liquid, keep the pH value of toner system stable,In the present invention as buffer;
K, Co-Q10: be a kind of powerful antioxidant, can suppress peroxidatic reaction of lipid, reduce certainlyBy the generation of base, protection SOD activated centre and structure thereof are avoided Free radicals injury, improve in bodyThe enzymatic activitys such as SOD, suppress the Apoptosis of response to oxidative stress induction, have significantly anti-oxidant,The effect delaying senility.
L, saualane: the squalene extracting from deepwater shark liver makes through hydrogenation, have goodAntioxygenic property, can good affine skin, muting sensitive and low stimulation, and can accelerate skin to otherThe absorption of active component;
M, pyrrolidone sodium carboxylate (PCA-Na): claiming again sodium pyroglutamate, is natural moisture preserving in skinThe main component of factor NMF, has very strong moisture-keeping function, and long-term moisture retention is strong, to skin veryGentleness, in the present invention as NMF;
N, Kathon CG: be called for short OIT, soluble in water and low-carbon alcohols, the best pH value 4-8 that uses,Toxicity is low, has advantages of that antibacterial action is in extensive range and antibacterial effect is strong, coordinates with methyl hydroxybenzoateResult of use is better;
O, methyl hydroxybenzoate: having another name called methyl p-hydroxybenzoate, is white crystalline powder or colourless knotCrystalline substance, is soluble in alcohol, and ether and acetone, have phenolic hydroxyl structure, and antibacterium performance is superior;
P, imidazolidinyl urea: white powder, very easily water-soluble, in the present invention as anticorrisive agent;
Q, kiss-me extract: extract from saxifragaceae plant kiss-me (SaxifragaStoloniferaCurt.), micro-bitter, acrid, cold, dispels the wind, heat-clearing, removing pattogenic heat from the blood and toxic material from the body.
R, centella extract: extract from samphire centella (Centellaasiatica (L.)Urban), nature and flavor: bitter, acrid, cold, return liver,spleen,kidney warp, can be clearing heat and detoxicating, inducing diuresis and reducing edema.Centella extract contains abundant asiaticosid (Asiaticoside), has the collagenocyte of promotion syntheticWith new Angiogenesis, stimulate the important function such as granulation growth, and there is certain anti-oxidation function, canSuppress free radical activity, improve skin blood circulation, promote skin cell regeneration.
Anti-ageing Essence of the present invention, has added tea oil and moisturizing composition pyrrolidone sodium carboxylate, andAdopting Co-Q10, saualane, kiss-me extract and centella extract is main anti-ageing composition,Pin on the one hand moisture of skin, increase skin elasticity, in the present invention, be added with Co-Q10 on the other hand,Can penetrate into the oxidation reaction that skin growth layer weakens photon, under the assistance of fertility alcohol, can startSpecific phosphorylated tyrosine kinases, prevents the oxidative damage of DNA, suppresses UV-irradiation servantThe expression of skin fibroblast Collagenase, protection skin avoids damage, smears and contains coenzymeThe skin care item of Q10, can increase the absorption of cell to Co-Q10, thereby reduce the formation of wrinkle; TigerThe anti-oxidation function that Auricled Hedyotis Herb extract and centella extract possess, can delaying skin aging. Therefore,Anti-ageing Essence of the present invention, not only has good moisturizing, moisturizing effect, and it is powerful anti-ageingOld ability, also can provide for skin is anti-ageing power endlessly.
Anti-ageing Essence of the present invention, the detection index of its product (taking embodiment five as sample) andFunctional evaluation is as follows:
One, sanitary index and sense organ physical and chemical index
The every sanitary index of anti-ageing Essence of the present invention and organoleptic indicator all meet QB/T after testingThe standard of 2660-2004 toner.
Following table 1 is sanitary index and the sense organ physical and chemical index of anti-ageing Essence of the present invention.
The sanitary index of table 1 anti-ageing Essence of the present invention and sense organ physical and chemical index
Two, functional evaluation
1, evaluate principle
ORAC is oxyradical absorbability (OxygenRadicalAbsorptionCapacity)Abbreviation, oxyradical absorbability is called again oxidation resistance. ORAC reaction be one classicalThe oxidizing process that hydrogen atom shifts. Under experimental condition, the AAPH of a part loses a part nitrogen,Generate two molecule AAPH free radicals (1). In air, AAPH free radical and the oxygen reaction of generation,Generate metastable peroxy radical ROO (2). The degree that weakens of fluorescer shows that peroxide freelyBase is to its destructiveness. Under the condition that has antioxidant content to exist, ROO obtains from antioxidant contentObtain a hydrogen atom, generate ROOH and a stable antioxidant free radical ArO (3).
R－N＝N－R→2R·+N2(1)
R·+O2→ROO·(2)
ROO·+ArOH→ArO·+ROOH(3)
Set two groups of contrasts, do not add free radical FL fluorescence Natural Attenuation contrast (AAPH) andFree Radical contrast (+AAPH) while thering is no antioxidant. The oxidation resistance of sample withUnder Free Radical fluorescence decline curve to delay part area directly related.
2, measurement result
Add fluorescence decline curve area under anti-ageing Essence effect of the present invention with without the present inventionThe fluorescence decline curve of anti-ageing Essence Free Radical while existing under area poor, fluorescence puts outThe protected area that the decay part area NetAUC of curve of going out is antioxidant. The oxygen of antioxidantRadical scavenging activity ORAC value, is called again the ORAC of antioxidant, is by glimmeringCompared with the protected area of the protected area of light decline curve and standard antioxygen material, draw. ORAC value withTrolox equivalent/μ mol, μ molTrolox equivalent/ml and μ molTrolox equivalent/mg tableReach. Its computing formula is:
ORAC value=[(AUCsample－AUC+AAPH)/AUGTrolox－AUC+AAPH]×(molarityofTrolox/molarityofsample)
The ORAC value result of anti-ageing Essence of the present invention is 12 μ molTE/ml.
3, in-vitro evaluation
Anti-ageing Essence of the present invention, its senile-resistant efficacy is through in-vitro evaluation (invitro) examinationTest, prove that it has oxidation resistant effect.
Anti-ageing Essence of the present invention, in-vitro evaluation test is as follows:
(i), test crowd
(1), the age is between 25-40 year;
, healthy, rule of life;
(3), without skin disease and allergies.
According to mentioned above principle, determine testing crew 40 people,
(ii), test method
(1), skin moisture content assay method:
Test environment temperature is 25 DEG C, and relative humidity (RelativeHumidity) is 60-90%,Before measuring, 10min exposes tested position, allows examinee keep tranquil simultaneously. On the forearm of left and rightRespectively mark the square Experimental Area of 4 4cm × 4cm, and Experimental Area is numbered to X1, X2,X3, X4, Y1, Y2, Y3, Y4, left arm is as the test section of smearing the anti-ageing Essence of the present invention,The symmetrical region of right arm is blank district, uses the mixture of A, B, C component. Use skin beauty waterDivide analyzer difference determination test region 5 times, record result; Consumption according to 1ml/cm is smearedThis money Essence is massaged into after absorption gently, at 15min, 30min, 60min, 120minDuring with 240min, use moisture of skin tester to measure respectively, test out keratoderma moistureContent value (representing with a.u.), and record test result. In order better to evaluate the data obtained,Introduce the concept of skin moisture-keeping increase rate, be about to each detection and use the moisture recording after productThe difference of value moisture content value during with spread product not, the moisture content value during divided by spread product not,The result obtaining is skin moisture-keeping increase rate. Use different time after this money Essence by calculatingPoint moisture of skin percentage change, can well evaluate product and whether have moisture retention and moisturizing effectReally.
(2), skin elasticity assay method:
Tester 40 people, the square test block of respectively marking 4 4cm × 4cm on the forearm of left and rightTerritory, and by Experimental Area numbering, left arm is as the test section of smearing the anti-ageing Essence of the present invention, the right sideThe symmetrical region of arm is blank district, uses the mixture of A, B, C component. According to 1ml/cmConsumption smear this money Essence and be massaged into gently after absorption, 30min, 60min, 120min,When 240min and 480min, use skin elasticity tester to survey respectively test section and check plotAmount. In order to evaluate better the data of gained, introduce the concept of skin elasticity increase rate, be about to eachWhen the skin elasticity value recording after detection use product and not spread product, skin elasticity value is poor, then removesSkin elasticity value during with spread product not, acquired results is skin elasticity value increase rate. By calculatingUse the percentage of this money Essence in different time points skin skin elasticity value, can evaluate wellWhether product has the skin elasticity of maintenance effect.
(3), result of the test
Table 2 skin test result
As shown in Table 2, use anti-ageing Essence of the present invention, can improve significantly the moisturizing of skinRate, and there is the effect that improves skin elasticity. Therefore, anti-ageing Essence of the present invention, to skinSkin has good moist maintenance to use.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further illustrated. Explanation is below to exemplifyMode, but protection scope of the present invention is not limited to this.
Embodiment mono-:
The anti-ageing Essence of the present embodiment, its preparation process comprises:
(i), raw material is prepared
1, get the raw materials ready: take off respectively by weight row raw material for standby:
A component: 6 parts of polyethylene glycol, 4 parts of propane diols, 9 parts of glycerine, 1 part of butanediol;
B component: 4 parts of tea oil, 2 parts of rilanit specials, 3 parts of C12-20 alkyl glucosides, glycerine1 part of stearate, 0.5 part of 18 alcohol;
C component: 0.05 part of methyl hydroxybenzoate, 0.2 part of Kathon CG, 0.2 part of imidazolidinyl urea;
D component: 0.1 part of Co-Q10,1 part of saualane, 1 part of pyrrolidone sodium carboxylate;
E component: 12 parts of kiss-me extracts, 6 parts of centella extracts;
Citric acid: 0.02 part;
Surplus is deionized water, adds up to 100 parts;
2, raw material processing
1., tea oil processing: by commercially available refining tea oil, be heated to 50 DEG C, constant temperature keeps 20min;Then, be cooled to 4 DEG C, growing the grain 12h; Under 0-4 DEG C of cryogenic conditions, vacuum filtration, separates againGo out liquid fat and solid lipid, collect the liquid fat of gained, be required tea oil, for subsequent use;
2., kiss-me extract preparation: by deionized water for kiss-me herb (fresh) (note:This deionized water is not counted in raw material total amount) clean up, squeeze its juice, after filtration, obtain respectively filtrateA and residual filter residue; In residual filter residue, add the ethanol that 2 times of weight, volumetric concentration are 50% again, oftenUnder normal temperature and pressure, soak 12 hours, filter, obtain soak; Again soak is adopted to the side of reduced pressure concentrationMethod, is concentrated into the half of original volume, obtains liquor B; Merging filtrate A and liquor B, be required tigerAuricled Hedyotis Herb extract, for subsequent use;
3., centella extract preparation: by deionized water for centella (dry product) (note: this go fromSub-water is not counted in raw material total amount) clean up, according to the part by weight of solid-liquid ratio 1:15 add fromSub-water, is heated to 100 DEG C, and constant temperature extracts 2 hours, filter, respectively extract and filter residue;Press again the part by weight of solid-liquid ratio 1:15, in filter residue, add deionized water, boil and extract 1 hour,Filter, obtain secondary raffinate; Merge extracted twice liquid, and adopt the method for Vacuum Concentration, be concentrated intoThe half of original volume, is required centella extract, for subsequent use;
(ii), its preparation process is as follows:
1., A component is mixed: all raw materials of A component are joined in deionized water, with 2000The rotating speed of r/min stirs 3min, then, is heated to 70-80 DEG C by the programming rate of 3 DEG C/min,Keep 10min, become A component compound, for subsequent use;
2., B component is mixed: all raw materials of B component are mixed, with 2000r/min'sRotating speed stirs 3min, then, is heated to 60-80 DEG C by the programming rate of 3 DEG C/min, keeps 10min,Become B component compound, for subsequent use;
3., AB organizes mixing: A component compound for subsequent use is mixed with B component compound, at 80 DEG CRotating speed with 500r/min under condition stirs, pre-emulsification 15min, then, and with 1-2 DEG C/min'sSpeed is from 80 DEG C of slow coolings to 70 DEG C, then stirs 5min with the rotating speed of 3000r/min, thenSuccessively after the high-pressure homogeneous 5min of 20MPa, 5Mpa low pressure homogeneous 5min process, 0.5Vacuum outgas under Mpa condition, becomes AB component compound, for subsequent use;
4., ABC organizes mixing: AB component compound for subsequent use is cooled to 60 DEG C from 70 DEG C, addsAll raw materials of C component, mix, and become ABC group compound, for subsequent use;
5., entirely mix: ABC for subsequent use group compound is cooled to 50 DEG C from 60 DEG C, adds D groupPoint and all raw materials of E component, then add lemon acid for adjusting pH value to 6-7, then, with 1000The speed of r/min stirs and is cooled to 25-35 DEG C, becomes full batch mixing, for subsequent use;
6., ageing: full batch mixing for subsequent use is placed to ageing 30h at 20-25 DEG C, anti-ageingEssence.
When the anti-ageing Essence of the present embodiment uses, suitable after clean face skin, use and make upWater, then get appropriate anti-ageing Essence and be applied on the face, pat gently and promote to absorb. Note making at every turnWith unsuitable excessive, also should not in the irritated situation of skin, use.
Embodiment bis-:
The anti-ageing Essence of the present embodiment, its preparation process comprises:
(i), raw material is prepared
1, get the raw materials ready: take off respectively by weight row raw material for standby:
A component: 7 parts of polyethylene glycol, 6 parts of propane diols, 8 parts of glycerine, 1.5 parts of butanediols;
B component: 4.5 parts of tea oil, 2 parts of rilanit specials, 4 parts of C12-20 alkyl glucosides, sweet2.5 parts of oleostearin acid esters, 1.5 parts of 18 alcohol;
C component: 0.08 part of methyl hydroxybenzoate, 0.3 part of Kathon CG, 0.2 part of imidazolidinyl urea;
D component: 0.2 part of Co-Q10,1.75 parts of saualanes, 3 parts of pyrrolidone sodium carboxylates;
E component: 15 parts of kiss-me extracts, 8 parts of centella extracts;
Citric acid: 0.03 part;
Surplus is deionized water, adds up to 100 parts;
Other is identical with embodiment mono-.
Embodiment tri-:
The anti-ageing Essence of the present embodiment, its preparation process comprises:
(i), raw material is prepared
1, get the raw materials ready: take off respectively by weight row raw material for standby:
A component: 8 parts of polyethylene glycol, 8 parts of propane diols, 6.5 parts of glycerine, 2 parts of butanediols;
B component: 5 parts of tea oil, 3 parts of rilanit specials, 5 parts of C12-20 alkyl glucosides, glycerine3.5 parts of stearates, 2.5 parts of 18 alcohol;
C component: 0.11 part of methyl hydroxybenzoate, 0.4 part of Kathon CG, 0.3 part of imidazolidinyl urea;
D component: 0.3 part of Co-Q10,2.5 parts of saualanes, 5 parts of pyrrolidone sodium carboxylates;
E component: 18 parts of kiss-me extracts, 10 parts of centella extracts;
Citric acid: 0.02 part;
Surplus is deionized water, adds up to 100 parts;
Other is identical with embodiment mono-.
Embodiment tetra-:
The anti-ageing Essence of the present embodiment, its preparation process comprises:
(i), raw material is prepared
1, get the raw materials ready: take off respectively by weight row raw material for standby:
A component: 9 parts of polyethylene glycol, 8 parts of propane diols, 5 parts of glycerine, 3 parts of butanediols;
B component: 6 parts of tea oil, 4 parts of rilanit specials, 5 parts of C12-20 alkyl glucosides, glycerine5 parts of stearates, 3 parts of 18 alcohol;
C component: 0.15 part of methyl hydroxybenzoate, 0.4 part of Kathon CG, 0.3 part of imidazolidinyl urea;
D component: 0.5 part of Co-Q10,3 parts of saualanes, 7 parts of pyrrolidone sodium carboxylates;
E component: 20 parts of kiss-me extracts, 12 parts of centella extracts;
Citric acid: 0.01 part;
Surplus is deionized water, adds up to 100 parts;
Other is identical with embodiment mono-.
Embodiment five:
The anti-ageing Essence of the present embodiment, its preparation process comprises:
(i), raw material is prepared
1, get the raw materials ready: take off respectively by weight row raw material for standby:
A component: 6 parts of polyethylene glycol, 7 parts of propane diols, 12 parts of glycerine, 1 part of butanediol;
B component: 4 parts of tea oil, 1 part of rilanit special, 1 part of C12-20 alkyl glucoside, glycerine2 parts of stearates, 1.5 parts of 18 alcohol;
C component: 0.05 part of methyl hydroxybenzoate, 0.2 part of Kathon CG, 0.3 part of imidazolidinyl urea;
D component: 0.1 part of Co-Q10,2.5 parts of saualanes, 3 parts of pyrrolidone sodium carboxylates;
E component: 16 parts of kiss-me extracts, 10 parts of centella extracts;
Citric acid: 0.02 part;
Surplus is deionized water, adds up to 100 parts;
Other is identical with embodiment mono-.
Anti-ageing Essence of the present invention, the crowd who is suitable for different skin quality, all ages and classes uses.
Claims (5)
1. an anti-ageing Essence, is characterized in that:
(i) be, to be prepared from by following raw material by weight:
A component: polyethylene glycol 6-9 part, propane diols 4-8 part, glycerine 5-12 part, butanediol1-3 part;
B component: tea oil 4-6 part, rilanit special 1-4 part, C12-20 alkyl glucoside 1-5Part, stearine 1-5 part, 18 alcohol 0.5-3 parts;
C component: methyl hydroxybenzoate 0.05-0.15 part, Kathon CG 0.2-0.4 part, imidazolidinyl urea0.2-0.3 part;
D component: Co-Q10 0.1-0.5 part, saualane 1-3 part, pyrrolidone sodium carboxylate 1-7Part;
E component: kiss-me extract 12-20 part, centella extract 6-12 part;
Citric acid: 0.01-0.1 part;
Surplus is deionized water, adds up to 100 parts;
(ii), its preparation process is as follows:
1., A component is mixed: all raw materials of A component are joined in deionized water, with 2000The rotating speed of r/min stirs 2-4min, then, is heated to by the programming rate of 2-4 DEG C/min70-80 DEG C, keeps 8-12min, becomes A component compound, for subsequent use;
2., B component is mixed: all raw materials of B component are mixed, with 2000r/min'sRotating speed stirs 2-4min, then, is heated to 60-80 DEG C by the programming rate of 2-4 DEG C/min, keeps8-12min, becomes B component compound, for subsequent use;
3., AB organizes mixing: A component compound for subsequent use is mixed with B component compound,Rotating speed with 500r/min under 60-80 DEG C of condition stirs, pre-emulsification 10-20min, then, and with 1-2 DEG CThe speed slow cooling of/min is during to 50-70 DEG C, then stirs 5-10 with the rotating speed of 3000r/minMin, then pass through successively the high-pressure homogeneous 5-10min of 20-40MPa, 5-15Mpa low pressure homogeneous 5-10minAfter, vacuum outgas under 0.1-0.5Mpa condition, becomes AB component compound, for subsequent use;
4., ABC organizes mixing: it is 50-70 DEG C that AB component compound for subsequent use is kept to temperature, constant temperatureThe all raw materials that add C component under condition, mix, and become ABC group compound, for subsequent use;
5., entirely mix: ABC for subsequent use is organized to compound from the 50-70 DEG C of speed with 1-2 DEG C/minBe cooled to 50-60 DEG C, add all raw materials of D component and E component, then add lemon acid for adjusting pHBe worth to 6-7, then, stir and be cooled to 25-35 DEG C with the speed of 1000r/min, become full batch mixing,For subsequent use;
6., ageing: full batch mixing for subsequent use is placed to ageing 25-35h at 20-25 DEG C, anti-ageingOld Essence.
2. anti-ageing Essence according to claim 1, it is characterized in that by following by heavyThe raw material of amount part is prepared from:
A component: 6 parts of polyethylene glycol, 7 parts of propane diols, 12 parts of glycerine, 1 part of butanediol;
B component: 4 parts of tea oil, 1 part of rilanit special, 1 part of C12-20 alkyl glucoside, glycerine2 parts of stearates, 1.5 parts of 18 alcohol;
C component: 0.05 part of methyl hydroxybenzoate, 0.2 part of Kathon CG, 0.3 part of imidazolidinyl urea;
D component: 0.1 part of Co-Q10,2.5 parts of saualanes, 3 parts of pyrrolidone sodium carboxylates;
E component: 16 parts of kiss-me extracts, 10 parts of centella extracts;
Citric acid: 0.02 part;
Surplus is deionized water, adds up to 100 parts.
3. anti-ageing Essence according to claim 1 and 2, is characterized in that, describedTea oil is to be prepared from as follows: by commercially available refining tea oil, be heated to 45-55 DEG C, perseveranceTemperature keeps 15-25min; Then, be cooled to 3-5 DEG C, growing the grain 10-15h; Again at 0-4 DEG C of low temperatureUnder condition, vacuum filtration, isolates liquid fat and solid lipid, collects the liquid fat of gained,Be required tea oil.
4. anti-ageing Essence according to claim 1 and 2, is characterized in that, describedKiss-me extract is to be prepared from as follows: kiss-me herb is dry by washed with de-ionized waterOnly, squeeze its juice, after filtration, obtain respectively filtrate A and residual filter residue; In residual filter residue, add 1.5-2.5 againThe ethanol that times weight, volumetric concentration are 45-55%, soaks 10-15 hour, mistake at normal temperatures and pressuresFilter, obtains soak; Again soak is adopted to the method for reduced pressure concentration, is concentrated into the half of original volume,Obtain liquor B; Merging filtrate A and liquor B, be required kiss-me extract.
5. anti-ageing Essence according to claim 1 and 2, is characterized in that, describedCentella extract is to be prepared from as follows: centella is cleaned up by deionized water, pressThe part by weight of taking care of liquor ratio 1:10-20 adds deionized water, is heated to 90-110 DEG C, and constant temperature is carriedGet 1-3 hour, filter, respectively extract and filter residue; Press again the weight of solid-liquid ratio 1:10-20Amount ratio adds deionized water in filter residue, boils and extracts 0.5-2 hour, filters, and obtains secondary and carriesGet liquid; Merge extracted twice liquid, and adopt the method for Vacuum Concentration, be concentrated into the half of original volume,Be required centella extract.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410176978.3A CN103919704B (en) | 2014-04-29 | 2014-04-29 | A kind of anti-ageing Essence |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410176978.3A CN103919704B (en) | 2014-04-29 | 2014-04-29 | A kind of anti-ageing Essence |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103919704A CN103919704A (en) | 2014-07-16 |
| CN103919704B true CN103919704B (en) | 2016-05-04 |
Family
ID=51138266
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410176978.3A Active CN103919704B (en) | 2014-04-29 | 2014-04-29 | A kind of anti-ageing Essence |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103919704B (en) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104523530A (en) * | 2015-01-09 | 2015-04-22 | 湖南新金浩茶油股份有限公司 | Anti-aging facial mask and preparation method thereof |
| CN104546609B (en) * | 2015-01-09 | 2017-09-19 | 湖南新金浩茶油股份有限公司 | A kind of crease-resistant nursing oil of oil tea |
| CN106333917A (en) * | 2016-10-09 | 2017-01-18 | 上海兰葹生物科技有限公司 | Dendrobium nobile skin regeneration promotion combination essence |
| CN106860258A (en) * | 2017-01-19 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment anti-aging Essence |
| CN106860083A (en) * | 2017-01-19 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment anti-aging Essence |
| CN106860084A (en) * | 2017-01-19 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment anti-aging Essence |
| CN108078857A (en) * | 2018-01-22 | 2018-05-29 | 尹淑珍 | A kind of anti crease and anti senile old essence lotion and preparation method thereof |
| CN108498445A (en) * | 2018-06-26 | 2018-09-07 | 四川自然菲科技有限公司 | A kind of novel anti-aging type Essence |
| CN111166707B (en) * | 2020-01-19 | 2022-04-22 | 广州市柏姿生物科技有限公司 | Facial anti-aging repairing and nursing composition and preparation method and application thereof |
| CN111700847B (en) * | 2020-07-22 | 2020-12-22 | 广州杨森药业有限公司 | Composition for treating dark eye circles by synergistic laser, eye essence and preparation method |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101190174A (en) * | 2006-12-01 | 2008-06-04 | 高宝化妆品（中国）有限公司 | Moisture-keeping crease-shedding skin-care cream and preparation method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4091824B2 (en) * | 2002-02-05 | 2008-05-28 | 株式会社コーセー | Skin preparation |
-
2014
- 2014-04-29 CN CN201410176978.3A patent/CN103919704B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101190174A (en) * | 2006-12-01 | 2008-06-04 | 高宝化妆品（中国）有限公司 | Moisture-keeping crease-shedding skin-care cream and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103919704A (en) | 2014-07-16 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103919704B (en) | A kind of anti-ageing Essence | |
| CN107213063B (en) | Fair and bright facial mask and preparation method thereof | |
| CN102258442B (en) | Compound traditional Chinese medicine extract and application thereof to whitening, moisturizing and anti-aging skin care product | |
| KR101796694B1 (en) | Cosmetic composition for improving skin whitening and lifting | |
| CN110420152B (en) | Refreshing and mild double-layer cleansing lotion and preparation method thereof | |
| KR101781556B1 (en) | Cosmetic composition for anti-aging containing red algae extracts | |
| KR102443708B1 (en) | Hair cosmetic composition for preventing hair loss and improving scalp | |
| CN103494719B (en) | Preparation method of anti-aging cream | |
| CN115154403B (en) | Skin repair composition and preparation method and application thereof | |
| CN110787091A (en) | Itching-relieving and anti-allergy infant washing and protecting preparation and application thereof | |
| CN115919709A (en) | Camellia essential oil with repairing and anti-aging effects | |
| CN114099393B (en) | Composition with tightening and anti-aging effects and preparation method and application thereof | |
| CN109044941A (en) | A kind of skin-tightening nourishes moisture-keeping composition and its preparation method and application | |
| CN108852951A (en) | A kind of moistening and cleaning skin composition and plant body wash | |
| CN108272655A (en) | The high moisture saver mask Essence of tremella polysaccharides and facial mask and preparation method thereof | |
| CN110037958A (en) | A kind of pox-eliminating whitening moisture saver mask of the ingredient containing trollflower and preparation method thereof | |
| CN111467276B (en) | Essential oil bath gel and preparation method thereof | |
| CN110302121A (en) | A kind of baby's diaper ointment and preparation method thereof containing plant essence | |
| KR102286679B1 (en) | External composition for skin containing an enzyme-treated saponin fraction derived from the root of Camellia sinensis | |
| CN107961174A (en) | Lipstick containing stem cell secretion factors and preparation method thereof | |
| CN112236201B (en) | Use of extract of rosewood (BIXA ORELLANA) | |
| CN110448510B (en) | Skin conditioning type plant extract composition, makeup remover, makeup removing film and preparation method thereof | |
| US20190343746A1 (en) | Cosmetic composition including gamma-pga as active ingredient | |
| CN104188808B (en) | A kind of nti-freckle is dispelled yellow gel and preparation method thereof | |
| CN113230188A (en) | A herba Lycopodii pine needle polysaccharide facial mask with moisturizing and antioxidant effects, and its preparation method |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |