CN103898630A - Modified bamboo charcoal polyester fiber with health function - Google Patents
Modified bamboo charcoal polyester fiber with health function Download PDFInfo
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- CN103898630A CN103898630A CN201410144968.1A CN201410144968A CN103898630A CN 103898630 A CN103898630 A CN 103898630A CN 201410144968 A CN201410144968 A CN 201410144968A CN 103898630 A CN103898630 A CN 103898630A
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Abstract
The invention belongs to the field of textile materials, and discloses a modified bamboo charcoal polyester fiber with a health function, which is prepared by the following raw materials in parts by weight: 80 parts of PET slices, 10 parts of bamboo charcoal powder, 3 parts of glyceryl monostearate, 2 parts of hydroxyethyl cellulose, 2 parts of Chinese medical extract, 1 part of chitosan, 1 part of titanium dioxide powder and 1 part of silicon dioxide powder. The prepared modified bamboo charcoal polyester fiber has a better aged health function and can be used for auxiliary treatment of rheumatism.
Description
Technical field
The present invention relates to textile material field, specifically, relate to a kind of modification bamboo charcoal polyster fibre with health care.
Background technology
Rheumatic arthritis is a kind of common disease and frequently-occurring disease, is a kind of common acute or chronic ICT.Can repeatedly show effect and involve heart.Clinical miserable take joint and muscle migration, heavily work, pain is as feature.Belonging to allergic disease, is one of main manifestations of rheumatic fever, mainly with febris acuta and arthralgia onset.
At present, doctor trained in Western medicine is used the medicine such as glucocorticoids, immunodepressant to treat this disease more, though there is certain curative effect, result for the treatment of is unsatisfactory, and such medicine also has suitable toxic and side effect, long-term use patient's harm larger.
Polyster fibre is an important kind in synthetic fiber, is the trade name of China's polyester fiber.It is fiber-forming polymer---the polyethylene terephthalate making through esterification or ester exchange and polycondensation reaction take p-phthalic acid or dimethyl terephthalate (DMT) and ethylene glycol as raw material, the fiber of making through spinning and post processing.Polyster fibre is that in three large synthetic fiber, technique is the simplest a kind of, and price is also more cheap.Adding it has durable, good springiness, not yielding, corrosion-resistant, insulation, the feature such as well-pressed and quick-drying washable, by people are liked.The kind of polyster fibre fabric is more, and except knitting the pure terylene fabric of system, the product that also has many and various textile fabric blend polyesters or interweave, has made up the deficiency of pure dacron, has given play to better performance performance.At present, occurred on the market multiple modified polyester fibre, it,, in retaining original performance, has injected the not available function of polyster fibre.In order to improve the health care of fibrous material, can add the component such as Nano Silver and bamboo charcoal powder, also drug ingedient can be fitted in fibrous material; But above-mentioned material modified fabric color easily changes, feel is hardened, and washing durability is poor, and medicine easily comes off, and duration of efficacy is shorter.
Summary of the invention
In order to overcome the deficiencies in the prior art, the invention provides a kind of modification bamboo charcoal polyster fibre with health care, preparation technology's uniqueness of this modification bamboo charcoal polyster fibre, selection drug matching is reasonable, auxiliary treatment of rheumatic arthritis effectively, meanwhile, the physicochemical property of fibrous material itself does not change, and can be applicable to the market demand.
Technical scheme of the present invention realizes in the following way:
Possess a modification bamboo charcoal polyster fibre for health care, its raw material by following weight portion is prepared from:
80 parts of PET sections, 10 parts of bamboo charcoal powder, 3 parts of glycerin monostearates, 2 parts of hydroxyethylcelluloses, 2 parts of Chinese medical concretes, 1 part of shitosan, 1 part of titanium dioxide powder, 1 part of silicon dioxide powder.
Wherein, more than the particle diameter of bamboo charcoal powder, titanium dioxide powder and silicon dioxide powder is all controlled at 1000 orders.
The preparation method of above-mentioned bamboo carbon dacron fiber comprises:
1) get root of herbaceous peony 20-22 part, Radix Glycyrrhizae 16-18 part, windproof 15-16 part, Radix Angelicae Sinensis 12-13 part, honeysuckle 10-11 part, pseudo-ginseng 8-9 part, Ligusticum wallichii 6-7 part, eleusine indica 4-5 part and dried orange peel 1-2 part according to weight portion, mix, the water that adds 5 times of weight decocts 2 hours at 90 ℃, filter and collect filtrate, then vacuumize obtains the medicinal extract that density is 1.2g/ml;
2) get bamboo charcoal powder according to weight portion, glycerin monostearate, hydroxyethylcellulose, Chinese medical concrete, shitosan, titanium dioxide powder and silicon dioxide powder, insert in twin (double) screw extruder mixing, 260 ℃ of melting temperatures, extruder internal pressure is 8Mpa, mixing speed is 400 revs/min, and mixing time is 5 minutes, makes modified master batch;
3) get PET section according to weight portion, mix with modified master batch, stir, then melt spinning is prepared modification bamboo charcoal polyster fibre.
The invention also discloses wrister, knee-pad or the waist support etc. that utilize above-mentioned fibrous material to be formed by weaving.
The beneficial effect that the present invention obtains mainly comprises: drug ingedient compatibility of the present invention is reasonable, preparation method's uniqueness, the modification bamboo charcoal polyster fibre that it is prepared from possesses certain health care for the aged function, can be effectively for prevention or the auxiliary curing of rheumatic arthritis; Bamboo carbon dacron fiber of the present invention has formed fiber multi-cellular structure, and bamboo charcoal powder, titanium dioxide powder, silicon dioxide powder and medicine components can be scattered in micropore; The present invention adopts glycerin monostearate and hydroxyethylcellulose the active ingredient bonding in Chinese medical concrete can be coupled on polyster fibre, has avoided drug ingedient easily to come off and fabric color jaundice, the feel defect such as harden; The shitosan that the present invention selects can form void structure, other additives is embedded wherein to difficult drop-off.
The specific embodiment
Below employing specific embodiment is further explained the present invention, but should regard the restriction to initiative spirit of the present invention as.
Embodiment 1
Possess a modification bamboo charcoal polyster fibre for health care, its raw material by following weight portion is prepared from:
80 parts of PET sections, 10 parts of bamboo charcoal powder, 3 parts of glycerin monostearates, 2 parts of hydroxyethylcelluloses, 2 parts of Chinese medical concretes, 1 part of shitosan, 1 part of titanium dioxide powder, 1 part of silicon dioxide powder.
Wherein, the particle diameter of bamboo charcoal powder, titanium dioxide powder and silicon dioxide powder is all controlled at 1300 orders.
The preparation method of above-mentioned bamboo carbon dacron fiber comprises:
1) get 1 part of 20 parts of the root of herbaceous peonys, 16 parts, Radix Glycyrrhizae, windproof 15 parts, 12 parts of Radix Angelicae Sinensis, 10 parts of honeysuckles, 8 parts of pseudo-ginseng, 6 parts of Ligusticum wallichiis, 4 parts of eleusine indicas and dried orange peel according to weight portion, mix, the water that adds 5 times of weight decocts 2 hours at 90 ℃, filter and collect filtrate, then vacuumize obtains the medicinal extract that density is 1.2g/ml;
2) get bamboo charcoal powder according to weight portion, glycerin monostearate, hydroxyethylcellulose, Chinese medical concrete, shitosan, titanium dioxide powder and silicon dioxide powder, insert in twin (double) screw extruder mixing, 260 ℃ of melting temperatures, extruder internal pressure is 8Mpa, mixing speed is 400 revs/min, and mixing time is 5 minutes, makes modified master batch;
3) get PET section according to weight portion, mix with modified master batch, stir, then melt spinning is prepared modification bamboo charcoal polyster fibre; Concrete spinning technique can be FDY technique: spinning temperature is 260 ℃, and spinning speed is 3200m/min, 160 ℃ of setting temperatures.
The polyster fibre obtaining by above-mentioned preparation technology and polyster fibre of the prior art are in feel, and the physicochemical properties such as fracture strength and percentage elongation do not have notable difference; Leading indicator parameter is: 1.5D × 38mm, monofilament strength: 2.9-3.2cN/dtex; Extension at break: 34%-35%; 180 ℃ of dry-hot shrinkage: 6%-8%; The thickness of knee-pad, wrister and the waist support being prepared from is 3-5mm, and width is 10-30cm, and leading indicator is: (1) quick-drying: 20 ℃ of temperature, in the environment of relative humidity 65%, 120 minutes, moisture content was 0; (2) anti-fluffing, ANTIPILLING reach GB more than 4 grades; (3) go peculiar smell to reach more than 75%, the mildew-resistant degree in 14 days is 1 grade.
Embodiment 2
Possess a modification bamboo charcoal polyster fibre for health care, its raw material by following weight portion is prepared from:
80 parts of PET sections, 10 parts of bamboo charcoal powder, 3 parts of glycerin monostearates, 2 parts of hydroxyethylcelluloses, 2 parts of Chinese medical concretes, 1 part of shitosan, 1 part of titanium dioxide powder, 1 part of silicon dioxide powder.
Wherein, the particle diameter of bamboo charcoal powder, titanium dioxide powder and silicon dioxide powder is all controlled at 1200 orders.
The preparation method of above-mentioned bamboo carbon dacron fiber comprises:
1) get 2 parts of 22 parts of the root of herbaceous peonys, 18 parts, Radix Glycyrrhizae, windproof 16 parts, 13 parts of Radix Angelicae Sinensis, 11 parts of honeysuckles, 9 parts of pseudo-ginseng, 7 parts of Ligusticum wallichiis, 5 parts of eleusine indicas and dried orange peels according to weight portion, mix, the water that adds 5 times of weight decocts 2 hours at 90 ℃, filter and collect filtrate, then vacuumize obtains the medicinal extract that density is 1.2g/ml;
2) get bamboo charcoal powder according to weight portion, glycerin monostearate, hydroxyethylcellulose, Chinese medical concrete, shitosan, titanium dioxide powder and silicon dioxide powder, insert in twin (double) screw extruder mixing, 260 ℃ of melting temperatures, extruder internal pressure is 8Mpa, mixing speed is 400 revs/min, and mixing time is 5 minutes, makes modified master batch;
3) get PET section according to weight portion, mix with modified master batch, stir, then melt spinning is prepared modification bamboo charcoal polyster fibre; Concrete spinning technique can be FDY technique: spinning temperature is 300 ℃, and spinning speed is 3500m/min, 180 ℃ of setting temperatures.
The polyster fibre obtaining by above-mentioned preparation technology and polyster fibre of the prior art are in feel, and the physicochemical properties such as fracture strength and percentage elongation do not have notable difference; Leading indicator parameter is: monofilament strength: 2.8-3.0cN/dtex; Extension at break: 35%-36%; 180 ℃ of dry-hot shrinkage: 6%-8%; The thickness of knee-pad, wrister and the waist support being prepared from is 3-5mm, and width is 10-30cm, and leading indicator is: (1) quick-drying: 20 ℃ of temperature, in the environment of relative humidity 65%, 120 minutes, moisture content was 0; (2) anti-fluffing, ANTIPILLING reach GB more than 4 grades; (3) go peculiar smell to reach more than 75%, the mildew-resistant degree in 14 days is 1 grade.
Embodiment 3
Utilize wrister, knee-pad and waist support etc. prepared by the embodiment 1 modification bamboo charcoal polyster fibre auxiliary therapeutic action to rheumatic arthritis.
Case selection: in 100 routine patients, age 43-76 year, the course of disease is many at 6 months to 10 years, 59 years old mean age.Be equally divided at random two groups, experimental group 50 people and control group 50 people; Before treatment, all obtain patient's informed consent.
Diagnostic criteria: draft with reference to " rheumatism branch of Chinese Medical Association arthritis diagnosis and treatment guide draft gonitis diagnostic criteria in 2002 ": 1. nearly one month frequent gonalgia repeatedly; 2. X-ray film (erect position or Weight carrying position) joint space narrows; 3. limpid, the thickness of joint fluid (at least 2 times), WBC≤200/ml; 4. person in middle and old age person (>=40 years old); 5. knee joint deadlock≤30 minute in morning; 6. when movable, there is fricative.Meet above-mentioned 1. with 2., or 3., 5. with 6., or 1., 4., 5. with 6. item forms diagnosis.According to sign: 1. gonalgia, walking function obstacle, when fatigue and stair activity, symptom increases the weight of, and involves periarticular myalgia.2. unrestrained swollen, the kneecap of health check-up knee joint and inside and outside Xiyan place tenderness+, kneecap grinds pain, floating patella test+, it is limited that knee joint stretches flex, atrophy of quadriceps femoris.
Treatment evaluation criteria, " traditional Chinese medical science disease Standardization of diagnosis and curative effect " formulated according to State Administration of Traditional Chinese Medicine judged:
Cure: knee joint swelling, pain disappear, bend and stretch scope of activities and recover normal, walking freely;
Effective: knee joint swelling substantially disappears or obviously goes down, and pain obviously alleviates, bend and stretch scope of activities normal;
Take a turn for the better: knee joint swelling and pain all have and alleviates in various degree and alleviate, and bend and stretch scope of activities and are also improved;
Invalid: knee joint swelling and pain are all without alleviating.
Therapeutic modality: control group and treatment group all adopt ibuprofen sustained release capsules, 600mg/ time, 2 times on the one, 7 days is a course for the treatment of, uses 2 courses for the treatment of; Treatment group is worn knee-pad, wrister or waist support etc. as auxiliary curing mode at painful area simultaneously.Concrete result for the treatment of is in table 1:
Table 1
Group | Cure | Effective | Take a turn for the better | Invalid | Total effective rate |
Control group | 6 | 19 | 10 | 15 | 70% |
Treatment group | 14 | 21 | 9 | 6 | 88% |
Conclusion: by auxiliary curing mode, the cure rate for the treatment of group and total effective rate are all obviously better than control group, have significant difference.
Finally, it is also to be noted that, what more than enumerate is only several specific embodiments of the present invention.Obviously, the invention is not restricted to above embodiment, can also have many distortion.All distortion that those of ordinary skill in the art can directly derive or associate from content disclosed by the invention, all should think protection scope of the present invention.
Claims (2)
1. possess a modification bamboo charcoal polyster fibre for health care, its raw material by following weight portion is prepared from:
80 parts of PET sections, 10 parts of bamboo charcoal powder, 3 parts of glycerin monostearates, 2 parts of hydroxyethylcelluloses, 2 parts of Chinese medical concretes, 1 part of shitosan, 1 part of titanium dioxide powder, 1 part of silicon dioxide powder;
Wherein, more than the particle diameter of described bamboo charcoal powder, titanium dioxide powder or silicon dioxide powder is all controlled at 1000 orders;
The preparation method of described modification bamboo charcoal polyster fibre comprises:
1) get root of herbaceous peony 20-22 part, Radix Glycyrrhizae 16-18 part, windproof 15-16 part, Radix Angelicae Sinensis 12-13 part, honeysuckle 10-11 part, pseudo-ginseng 8-9 part, Ligusticum wallichii 6-7 part, eleusine indica 4-5 part and dried orange peel 1-2 part according to weight portion, mix, the water that adds 5 times of weight decocts 2 hours at 90 ℃, filter and collect filtrate, then vacuumize obtains the medicinal extract that density is 1.2g/ml;
2) get bamboo charcoal powder according to weight portion, glycerin monostearate, hydroxyethylcellulose, Chinese medical concrete, shitosan, titanium dioxide powder and silicon dioxide powder, insert in twin (double) screw extruder mixing, 260 ℃ of melting temperatures, extruder internal pressure is 8Mpa, mixing speed is 400 revs/min, and mixing time is 5 minutes, makes modified master batch;
3) get PET section according to weight portion, mix with modified master batch, stir, then melt spinning is prepared modification bamboo charcoal polyster fibre.
2. the purposes of modification bamboo charcoal polyster fibre claimed in claim 1 in auxiliary treatment of rheumatic arthritis.
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Cited By (8)
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CN104264493A (en) * | 2014-09-09 | 2015-01-07 | 江苏蓝品纤维科技发展有限公司 | Preparation method of multifunctional polyester fiber |
CN107190358A (en) * | 2017-06-30 | 2017-09-22 | 太仓红桥服饰有限公司 | A kind of environment-friendly antibacterial anti-radiation garment fabric |
CN107201568A (en) * | 2017-06-30 | 2017-09-26 | 太仓红桥服饰有限公司 | A kind of environment-friendly antibacterial Anti-ultraviolet Garment Fabric |
CN107217326A (en) * | 2017-06-30 | 2017-09-29 | 太仓红桥服饰有限公司 | A kind of environment-friendly antibacterial flame-retardant garment plus material |
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CN107190358A (en) * | 2017-06-30 | 2017-09-22 | 太仓红桥服饰有限公司 | A kind of environment-friendly antibacterial anti-radiation garment fabric |
CN107201568A (en) * | 2017-06-30 | 2017-09-26 | 太仓红桥服饰有限公司 | A kind of environment-friendly antibacterial Anti-ultraviolet Garment Fabric |
CN107217326A (en) * | 2017-06-30 | 2017-09-29 | 太仓红桥服饰有限公司 | A kind of environment-friendly antibacterial flame-retardant garment plus material |
CN107268114A (en) * | 2017-06-30 | 2017-10-20 | 太仓红桥服饰有限公司 | A kind of environment-friendly antibacterial deodorization garment material |
CN108998846A (en) * | 2018-08-10 | 2018-12-14 | 苏州郎旭志远科技有限公司 | A kind of environment-friendly antibacterial composite high-molecular fiber and preparation method |
WO2023196410A1 (en) | 2022-04-05 | 2023-10-12 | Momentive Performance Materials Inc. | Modified natural and green particles for cosmetic application |
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