CN109423700A - A kind of modification bamboo charcoal polyester fiber with health care function - Google Patents
A kind of modification bamboo charcoal polyester fiber with health care function Download PDFInfo
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- CN109423700A CN109423700A CN201710738384.0A CN201710738384A CN109423700A CN 109423700 A CN109423700 A CN 109423700A CN 201710738384 A CN201710738384 A CN 201710738384A CN 109423700 A CN109423700 A CN 109423700A
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/92—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Artificial Filaments (AREA)
- Professional, Industrial, Or Sporting Protective Garments (AREA)
Abstract
The invention belongs to textile material fields, disclose a kind of modification bamboo charcoal polyester fiber for having healthcare function, it is prepared by the raw material of following parts by weight, PET is sliced 80 parts, 10 parts of bamboo charcoal powder, 3 parts of glycerin monostearate, 2 parts of hydroxyethyl cellulose, 2 parts of Chinese medical concrete, 1 part of chitosan, 1 part of titanium dioxide powder, 1 part of silicon dioxide powder.Modification bamboo charcoal polyester fiber prepared by the present invention has preferable health care for the aged function, can be used in assisting in the treatment of rheumatism.
Description
Technical field
The present invention relates to textile material fields, specifically, it is fine to be related to a kind of modification bamboo charcoal terylene with health care function
Dimension.
Background technique
Rheumatic arthritis is a kind of common disease and frequently-occurring disease, is a kind of common acute or chronic connective tissue inflammation.
Recurrent exerbation and heart can be involved.Clinic by joint and muscle it is migrans it is miserable, rewrite, characterized by pain.Belong to allergy
Disease is one of main performance of rheumatic fever, mostly with febris acuta and arthralgia onset.
Currently, doctor trained in Western medicine mostly treats the disease using drugs such as glucocorticoids, immunosuppressor, though have certain
Curative effect, but therapeutic effect is unsatisfactory, and such drug is there are also comparable toxic side effect, be used for a long time to patient's harm compared with
Greatly.
Polyester fiber is an important species in synthetic fibers, is the product name of China's polyester fiber.It is with essence
Terephthalic acid (TPA) or dimethyl terephthalate (DMT) and ethylene glycol be raw material through prepared by esterification or transesterification and polycondensation reaction at
Fine high polymer --- polyethylene terephthalate through spinning and post-processes manufactured fiber.Polyester fiber is three big synthesis
The simplest one kind of technique, price are also relatively cheap in fiber.Along with it has, durable, elasticity is good, is unlikely to deform, corrosion resistant
The features such as losing, insulating, is well-pressed and quick-drying washable, is liked by people.The type of polyester fiber fabric is more, except weaving pure wash
Outside synthetic fibre fabric, there are many more the products with various textile fabric blend polyesters or intertexture, compensate for the deficiency of pure polyester fabric, send out
It shoots and preferably plays performance.Currently, having had already appeared a variety of modified polyester fibres on the market, retaining the same of original performance
When, it is filled with function not available for polyester fiber.In order to improve the healthcare function of fibrous material, can add nano silver and
Drug ingedient can also be fitted in fibrous material by the components such as bamboo charcoal powder；But above-mentioned modified material fabric color is easy to change
Change, feel are hardened, and washing resistance performance is poor, and drug is easy to fall off, and duration of efficacy is shorter.
Summary of the invention
For overcome the deficiencies in the prior art, the present invention provides a kind of modification bamboo charcoal terylene with health care function is fine
Dimension, the preparation process of the modification bamboo charcoal polyester fiber is unique, selects drug matching reasonable, being capable of effectively auxiliary treatment of rheumatic
Arthritis, meanwhile, the physicochemical property of fibrous material itself does not change, can be applied to the market demand.
The technical scheme is that realizing in the following way:
A kind of modification bamboo charcoal polyester fiber having healthcare function, is prepared by the raw material of following parts by weight:
PET is sliced 80 parts, and 10 parts of bamboo charcoal powder, 3 parts of glycerin monostearate, 2 parts of hydroxyethyl cellulose, 2 parts of Chinese medical concrete, shell is poly-
1 part, 1 part of titanium dioxide powder, 1 part of silicon dioxide powder of sugar.
Wherein, the partial size of bamboo charcoal powder, titanium dioxide powder and silicon dioxide powder controls more than 1000 mesh.
The preparation method of above-mentioned bamboo carbon dacron fiber includes:
1) 20-22 parts of Radix Paeoniae Alba, 16-18 parts of Radix Glycyrrhizae, 15-16 parts of radix saposhnikoviae, 12-13 parts of Radix Angelicae Sinensis, honeysuckle 10-11 are taken according to parts by weight
Part, 8-9 parts of Radix Notoginseng, 6-7 parts of Rhizoma Chuanxiong, 4-5 parts of herba eleusines indicae and 1-2 parts of dried orange peel, mixing add the water of 5 times of weight to decoct 2 at 90 DEG C
Hour, filtrate is collected by filtration, then vacuum drying obtains the medicinal extract that density is 1.2g/ml；
2) bamboo charcoal powder, glycerin monostearate, hydroxyethyl cellulose, Chinese medical concrete, chitosan, titanium dioxide are taken according to parts by weight
Powder and silicon dioxide powder are placed in twin (double) screw extruder and are kneaded, and 260 DEG C of melting temperature, pressure is 8Mpa in extruder, are kneaded
Speed is 400 revs/min, and mixing time is 5 minutes, and modified master batch is made；
3) it takes PET to be sliced according to parts by weight, is mixed with modified master batch, stirred evenly, then melt spinning prepares modification bamboo charcoal and washs
Synthetic fibre fiber.
The invention also discloses the wrist guard being formed by weaving using above-mentioned fibrous material, knee-pad or waist supports etc..
The beneficial effect that the present invention obtains specifically includes that drug ingedient compatibility of the present invention is reasonable, and preparation method is unique, system
Modification bamboo charcoal polyester fiber made of standby has certain health care for the aged function, can be efficiently used for the pre- of rheumatic arthritis
Anti- or adjuvant treatment；Bamboo carbon dacron fiber of the present invention forms fiber multi-cellular structure, makes bamboo charcoal powder, titanium dioxide powder, dioxy
SiClx powder and medicine components can be scattered in micropore；The present invention can be incited somebody to action using glycerin monostearate and hydroxyethyl cellulose
In Chinese medical concrete effective component bonding is coupled on polyester fiber, avoid drug ingedient be easy to fall off and fabric color hair
The defects of yellow, feel is hardened；The chitosan that the present invention selects can form void structure, other additives are embedded, no
It is easy to fall off.
Specific embodiment
It will should not be construed as below using specific embodiment come the present invention will be further explained to this hair
The limitation of bright initiative spirit.
Embodiment 1
A kind of modification bamboo charcoal polyester fiber having healthcare function, is prepared by the raw material of following parts by weight:
PET is sliced 80 parts, and 10 parts of bamboo charcoal powder, 3 parts of glycerin monostearate, 2 parts of hydroxyethyl cellulose, 2 parts of Chinese medical concrete, shell is poly-
1 part, 1 part of titanium dioxide powder, 1 part of silicon dioxide powder of sugar.
Wherein, the partial size of bamboo charcoal powder, titanium dioxide powder and silicon dioxide powder is controlled in 1300 mesh.
The preparation method of above-mentioned bamboo carbon dacron fiber includes:
1) 20 parts of Radix Paeoniae Alba, 16 parts of Radix Glycyrrhizae, windproof 15 parts, 12 parts of Radix Angelicae Sinensis, 10 parts of honeysuckle, 8 parts of Radix Notoginseng, Rhizoma Chuanxiong are taken according to parts by weight
6 parts, 4 parts of herba eleusines indicae and 1 part of dried orange peel, mixing add the water of 5 times of weight to decoct 2 hours at 90 DEG C, filtrate are collected by filtration, then
Vacuum drying obtains the medicinal extract that density is 1.2g/ml；
2) bamboo charcoal powder, glycerin monostearate, hydroxyethyl cellulose, Chinese medical concrete, chitosan, titanium dioxide are taken according to parts by weight
Powder and silicon dioxide powder are placed in twin (double) screw extruder and are kneaded, and 260 DEG C of melting temperature, pressure is 8Mpa in extruder, are kneaded
Speed is 400 revs/min, and mixing time is 5 minutes, and modified master batch is made；
3) it takes PET to be sliced according to parts by weight, is mixed with modified master batch, stirred evenly, then melt spinning prepares modification bamboo charcoal and washs
Synthetic fibre fiber；Specific spinning technique can be FDY technique: spinning temperature is 260 DEG C, spinning speed 3200m/min, setting temperature
160℃。
The polyester fiber and polyester fiber in the prior art obtained by above-mentioned preparation process in feel, breaking strength and
The physicochemical properties such as elongation do not have notable difference；Main indicator parameter are as follows: 1.5D × 38mm, monofilament strength: 2.9-3.2cN/
dtex；Extension at break: 34%-35%；180 DEG C of dry-hot shrinkages: 6%-8%；Knee-pad, wrist guard and the waist support being prepared
With a thickness of 3-5mm, width 10-30cm, main indicator are as follows: (1) quick-drying: at 20 DEG C of temperature, the environment of relative humidity 65%
In, 120 minutes, moisture content 0；(2) anti-fluffing, anti pilling reach 4 grades of national standard or more；(3) go peculiar smell up to 75% or more, 14
Mould proof degree in it is 1 grade.
Embodiment 2
A kind of modification bamboo charcoal polyester fiber having healthcare function, is prepared by the raw material of following parts by weight:
PET is sliced 80 parts, and 10 parts of bamboo charcoal powder, 3 parts of glycerin monostearate, 2 parts of hydroxyethyl cellulose, 2 parts of Chinese medical concrete, shell is poly-
1 part, 1 part of titanium dioxide powder, 1 part of silicon dioxide powder of sugar.
Wherein, the partial size of bamboo charcoal powder, titanium dioxide powder and silicon dioxide powder is controlled in 1200 mesh.
The preparation method of above-mentioned bamboo carbon dacron fiber includes:
1) 22 parts of Radix Paeoniae Alba, 18 parts of Radix Glycyrrhizae, windproof 16 parts, 13 parts of Radix Angelicae Sinensis, 11 parts of honeysuckle, 9 parts of Radix Notoginseng, Rhizoma Chuanxiong are taken according to parts by weight
7 parts, 5 parts of herba eleusines indicae and 2 parts of dried orange peel, mixing add the water of 5 times of weight to decoct 2 hours at 90 DEG C, filtrate are collected by filtration, then
Vacuum drying obtains the medicinal extract that density is 1.2g/ml；
2) bamboo charcoal powder, glycerin monostearate, hydroxyethyl cellulose, Chinese medical concrete, chitosan, titanium dioxide are taken according to parts by weight
Powder and silicon dioxide powder are placed in twin (double) screw extruder and are kneaded, and 260 DEG C of melting temperature, pressure is 8Mpa in extruder, are kneaded
Speed is 400 revs/min, and mixing time is 5 minutes, and modified master batch is made；
3) it takes PET to be sliced according to parts by weight, is mixed with modified master batch, stirred evenly, then melt spinning prepares modification bamboo charcoal and washs
Synthetic fibre fiber；Specific spinning technique can be FDY technique: spinning temperature is 300 DEG C, spinning speed 3500m/min, setting temperature
180℃。
The polyester fiber and polyester fiber in the prior art obtained by above-mentioned preparation process in feel, breaking strength and
The physicochemical properties such as elongation do not have notable difference；Main indicator parameter are as follows: monofilament strength: 2.8-3.0cN/dtex；Fracture is stretched
It is long: 35%-36%；180 DEG C of dry-hot shrinkages: 6%-8%；Knee-pad, wrist guard and the waist support being prepared with a thickness of 3-
5mm, width 10-30cm, main indicator are as follows: (1) quick-drying: in 20 DEG C of temperature, the environment of relative humidity 65%, 120 points
Clock, moisture content 0；(2) anti-fluffing, anti pilling reach 4 grades of national standard or more；(3) go peculiar smell up to 75% or more, it is anti-in 14 days
Mould degree is 1 grade.
Embodiment 3
The auxiliary to rheumatic arthritis such as wrist guard, knee-pad and waist support using the preparation of 1 modification bamboo charcoal polyester fiber of embodiment
Therapeutic effect.
Case selection: in 100 patients, the age 43-76 years old, the course of disease was mostly at 6 months to 10 years, average age 59 years old.With
Machine is equally divided into two groups, 50 people of 50 people of experimental group and control group；Patient's informed consent is obtained before treatment.
Diagnostic criteria: referring to " rheumatism branch, Chinese Medical Association arthritis diagnosis and treatment draft guidelines gonitis in 2002 is examined
Disconnected standard " it drafts: 1. nearly one month frequent gonalgia repeatedly；2. X-ray film (erect position or Weight carrying position) joint space narrows；
Joint fluid 3. (at least 2 times) limpid, sticky, WBC≤200/ml；4. person in middle and old age person (>=40 years old)；5. knee joint morning stiffness≤30 point
Clock；6. having fricative when activity.Meet it is above-mentioned 1. with 2. item, or 3., 5. with 6. item, or 1., 4., 5. with 6. item i.e. constitute examine
It is disconnected.According to sign: 1. gonalgia, walking function obstacle, exacerbation of symptoms when tired and stair activity involve periarticular flesh
Meat pain.2. physical examination knee joint is unrestrained swollen, tenderness at kneecap and inside and outside Xiyan+, kneecap grinds pain, floating patella test+, knee joint is stretched
Straight flex is limited, atrophy of quadriceps femoris.
Evaluation criteria is treated, is determined according to the Standards for Diagnosis and Curative Effect of Chinese Medical Symptom that State Administration of Traditional Chinese Medicine formulates:
Cure: knee joint swelling, pain disappear, and flexion-extension motion range restores normal, and walking is freely；
Effective: knee joint swelling disappears substantially or obvious decline, and pain is substantially reduced, and flexion-extension motion range is normal；
Improve: knee joint swelling and pain have mitigation in various degree and alleviate, and flexion-extension motion range also has improvement；
Invalid: knee joint swelling and pain are without alleviation.
Therapeutic modality: control group and treatment group are all made of ibuprofen sustained release capsules, and 600mg/ times, 2 times a day, 7 days are one
The course for the treatment of applies 2 courses for the treatment of；Treatment group wears knee-pad, wrist guard or waist support etc. in painful area simultaneously and is used as adjuvant treatment modality.
Concrete result for the treatment is shown in Table 1:
Table 1
| Group | It cures | It is effective | It improves | In vain | Total effective rate |
| Control group | 6 | 19 | 10 | 15 | 70% |
| Treatment group | 14 | 21 | 9 | 6 | 88% |
Conclusion: by adjuvant treatment modality, the cure rate and total effective rate for the treatment of group are significantly better than that control group, have conspicuousness poor
It is different.
The above list is only a few specific embodiments of the present invention for finally, it should also be noted that.Obviously, this hair
Bright to be not limited to above embodiments, acceptable there are many deformations.Those skilled in the art can be from present disclosure
All deformations for directly exporting or associating, are considered as protection scope of the present invention.
Claims (2)
1. a kind of modification bamboo charcoal polyester fiber for having healthcare function, is prepared by the raw material of following parts by weight:
PET is sliced 80 parts, and 10 parts of bamboo charcoal powder, 3 parts of glycerin monostearate, 2 parts of hydroxyethyl cellulose, 2 parts of Chinese medical concrete, shell is poly-
1 part, 1 part of titanium dioxide powder, 1 part of silicon dioxide powder of sugar；
Wherein, the partial size of the bamboo charcoal powder, titanium dioxide powder or silicon dioxide powder controls more than 1000 mesh；
The preparation method of the modification bamboo charcoal polyester fiber includes:
1) 20-22 parts of Radix Paeoniae Alba, 16-18 parts of Radix Glycyrrhizae, 15-16 parts of radix saposhnikoviae, 12-13 parts of Radix Angelicae Sinensis, honeysuckle 10-11 are taken according to parts by weight
Part, 8-9 parts of Radix Notoginseng, 6-7 parts of Rhizoma Chuanxiong, 4-5 parts of herba eleusines indicae and 1-2 parts of dried orange peel, mixing add the water of 5 times of weight to decoct 2 at 90 DEG C
Hour, filtrate is collected by filtration, then vacuum drying obtains the medicinal extract that density is 1.2g/ml；
2) bamboo charcoal powder, glycerin monostearate, hydroxyethyl cellulose, Chinese medical concrete, chitosan, titanium dioxide are taken according to parts by weight
Powder and silicon dioxide powder are placed in twin (double) screw extruder and are kneaded, and 260 DEG C of melting temperature, pressure is 8Mpa in extruder, are kneaded
Speed is 400 revs/min, and mixing time is 5 minutes, and modified master batch is made；
3) it takes PET to be sliced according to parts by weight, is mixed with modified master batch, stirred evenly, then melt spinning prepares modification bamboo charcoal and washs
Synthetic fibre fiber.
2. purposes of the modification bamboo charcoal polyester fiber described in claim 1 in auxiliary treatment of rheumatic arthritis.
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| CN201710738384.0A CN109423700A (en) | 2017-08-24 | 2017-08-24 | A kind of modification bamboo charcoal polyester fiber with health care function |
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| CN201710738384.0A CN109423700A (en) | 2017-08-24 | 2017-08-24 | A kind of modification bamboo charcoal polyester fiber with health care function |
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Cited By (1)
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| CN110055613A (en) * | 2019-04-11 | 2019-07-26 | 中科纺织研究院（青岛）有限公司 | A kind of Paeonol terylene chips fiber and preparation method thereof |
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- 2017-08-24 CN CN201710738384.0A patent/CN109423700A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110055613A (en) * | 2019-04-11 | 2019-07-26 | 中科纺织研究院（青岛）有限公司 | A kind of Paeonol terylene chips fiber and preparation method thereof |
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Application publication date: 20190305 |