CN103876218A - Anoectochilus formosanus extracting solution and preparation method thereof as well as anoectochilus formosanus drinks and preparations method thereof - Google Patents
Anoectochilus formosanus extracting solution and preparation method thereof as well as anoectochilus formosanus drinks and preparations method thereof Download PDFInfo
- Publication number
- CN103876218A CN103876218A CN201310649261.1A CN201310649261A CN103876218A CN 103876218 A CN103876218 A CN 103876218A CN 201310649261 A CN201310649261 A CN 201310649261A CN 103876218 A CN103876218 A CN 103876218A
- Authority
- CN
- China
- Prior art keywords
- terminal bud
- roxburgh anoectochilus
- anoectochilus terminal
- bud extract
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
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- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
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Abstract
The invention discloses a preparation method of an anoectochilus formosanus extracting solution. The preparation method comprises the following steps: a, washing selected anoectochilus formosanus and airing until leaves are withered; b, performing microwave drying on the aired anoectochilus formosanus under a vacuum condition, wherein a tempering process is introduced in a process of microwave drying, and the microwave power of microwave drying in the step is 3000W; and c, crushing the anoectochilus formosanus dried through microwaves, adding a drinkable solvent in the crushed anoectochilus formosanus, performing ultrasonic extraction to obtain an anoectochilus formosanus stock solution, namely, the anoectochilus formosanus extracting solution. The invention further discloses an anoectochilus formosanus extracting solution obtained by adopting the preparation method and two kinds of anoectochilus formosanus drinks containing the anoectochilus formosanus extracting solution and preparation methods of the two kinds of anoectochilus formosanus drinks. According to the anoectochilus formosanus extracting solution and the preparation method thereof and the anoectochilus formosanus drinks and the preparation methods thereof, the anoectochilus formosanus is dried through microwaves in vacuum under the process condition of the microwave power of 3000W, so that contents of polysaccharide, general flavone and free amino acid contained in the anoectochilus formosanus extracting solution are highest.
Description
Technical field
The present invention relates to roxburgh anoectochilus terminal bud manufacture field, refer in particular to roxburgh anoectochilus terminal bud extract and preparation method thereof and Jewel orchid beverage and preparation method thereof.
Background technology
Roxburgh anoectochilus terminal bud is the herbaceos perennial that the orchid family is opened lip Cymbidium.Another name Shorthairy Antenoron, rough melic herb, Shu Caolian, the young grass of money, gold thread taiwan anetochilus herb, gold thread disappear etc. to the marrow.Roxburgh anoectochilus terminal bud is the wider one of use among the people tradition valuable ingredient of traditional Chinese medicine, has the effects such as clearing heat and detoxicating, expelling wind and removing dampness, nourishing Yin and moistening lung, hypotensive, flat liver.Roxburgh anoectochilus terminal bud contains a large amount of valuable pharmacological active materials, mainly comprise: flavone compound (Quercetin, Isorhamnetin), steroid compound (24～isopropenyl cholesterine, open the blue sterol of lip, ergosterol, stigmasterol, campesterol, cupreol etc.), triterpene compound (suberone, butanedioic acid, coumaric acid, forulic acid, daucosterol, palmitic acid, oleanolic acid, ursolic acid), carbohydrate content (polysaccharide 13.326%, compound sugar 11.243%, reduced sugar 9.73%), alkaloid (huperzine and aconitine), Cardiac glycosides, ester class, taurine, several amino acids, trace element and inorganic elements etc.Wherein, amino acid and both content of trace element, all higher than domestic American Ginseng and wild ginseng, have medicinal and economic worth.
For now, the edible way of roxburgh anoectochilus terminal bud is comparatively time-consuming comparatively speaking, and along with improving constantly of people's rhythm of life, how roxburgh anoectochilus terminal bud being applied to fast drink product and can retaining its original composition is a problem that letter is to be solved.Roxburgh anoectochilus terminal bud to be made to fast drink product and just the pharmacological active substance in roxburgh anoectochilus terminal bud need to be extracted, first form roxburgh anoectochilus terminal bud extract, then be modulated into the Jewel orchid beverage that meets people's taste.But due to the most common with hot air drying roxburgh anoectochilus terminal bud on the market at present, its drying finished product brittleness is large, easily be extruded fragmentation, chlorophyll and nutritional labeling loss are serious, finished product is brown, and the highly seasoned distinctive smell of roxburgh anoectochilus terminal bud of having covered of burnt odor, runs off more through the pharmacological active substance that extracts the roxburgh anoectochilus terminal bud extract drawing, and rise can not retain the distinctive smell of roxburgh anoectochilus terminal bud, its redeployed beverage nutritive value not high and rise mouthfeel poor.
Summary of the invention
The invention provides a kind of roxburgh anoectochilus terminal bud extract and preparation method thereof and Jewel orchid beverage and preparation method thereof, its main purpose is to overcome the time-consuming roxburgh anoectochilus terminal bud pharmacological active substance loaded down with trivial details, hot air drying of the existing roxburgh anoectochilus terminal bud edible way more defect that runs off.
For solving the problems of the technologies described above, the present invention adopts following technical scheme:
A preparation method for roxburgh anoectochilus terminal bud extract, comprises the following steps: a, the roxburgh anoectochilus terminal bud of choosing is washed and dried to blade and wither; B, the roxburgh anoectochilus terminal bud after drying is carried out under vacuum condition to microwave drying, wherein in the process of microwave drying, introduce tempering technique, the microwave power of microwave drying is 3000W in this step; C, the roxburgh anoectochilus terminal bud after microwave drying is pulverized, the roxburgh anoectochilus terminal bud after pulverizing adds drinkable solvent, and carries out ultrasonic wave extraction, and the roxburgh anoectochilus terminal bud stoste obtaining is roxburgh anoectochilus terminal bud extract.
Further, the vacuum condition that carries out microwave drying in described step b is: vacuum is-75KPa～-65KPa.
The roxburgh anoectochilus terminal bud useful load of further, carrying out microwave drying in described step b is 300g～400g.
Further, the initial moisture content of drying base in described tempering technique is 258%, and the tempering time is 208 minutes.
Further, the vacuum of carrying out the vacuum condition of microwave drying in described step b is-75KPa that the useful load of roxburgh anoectochilus terminal bud is 300g.
Further, the drinkable solvent in described step c is the pure water of making through anti-penetration water purifier, and the roxburgh anoectochilus terminal bud of described pulverizing and the solid-liquid ratio of this pure water are 1:15.
Further, the time that in described step c, ultrasonic wave extracts is 25 minutes, and temperature is 60 ℃.
A kind of roxburgh anoectochilus terminal bud extract, this roxburgh anoectochilus terminal bud extract adopts following steps to be prepared from: a, the roxburgh anoectochilus terminal bud of choosing is washed and dried to blade and wither; B, the roxburgh anoectochilus terminal bud after drying is carried out under vacuum condition to microwave drying, wherein in the process of microwave drying, introduce tempering technique, the microwave power of microwave drying is 3000W in this step; C, the roxburgh anoectochilus terminal bud after microwave drying is pulverized, the roxburgh anoectochilus terminal bud after pulverizing adds drinkable solvent, and carries out ultrasonic wave extraction, and the roxburgh anoectochilus terminal bud stoste obtaining is roxburgh anoectochilus terminal bud extract.
Further, the vacuum condition that carries out microwave drying in described step b is: vacuum is-75KPa～-65KPa.
The roxburgh anoectochilus terminal bud useful load of further, carrying out microwave drying in described step b is 300g～400g.
Further, the initial moisture content of drying base in described tempering technique is 258%, and the tempering time is 208 minutes.
Further, the vacuum of carrying out the vacuum condition of microwave drying in described step b is-75KPa that the useful load of roxburgh anoectochilus terminal bud is 300g.
Further, the drinkable solvent in described step c is the pure water of making through anti-penetration water purifier, and the roxburgh anoectochilus terminal bud of described pulverizing and the solid-liquid ratio of this pure water are 1:15.
Further, the time that in described step c, ultrasonic wave extracts is 25 minutes, and temperature is 60 ℃.。
A kind of roxburgh anoectochilus terminal bud lemon fresh fruit health drink, formed by roxburgh anoectochilus terminal bud extract, lemon juice, sucrose and winter honey allotment, the volume proportion of described roxburgh anoectochilus terminal bud extract and lemon juice is 42:5, the concentration of described sucrose is 0.05 g/ml, the concentration of described winter honey is 0.02 g/ml, and described roxburgh anoectochilus terminal bud extract adopts following steps to be prepared from: a, the roxburgh anoectochilus terminal bud of choosing is washed and dried to blade and wither; B, the roxburgh anoectochilus terminal bud after drying is carried out under vacuum condition to microwave drying, wherein in the process of microwave drying, introduce tempering technique, the microwave power of microwave drying is 3000W in this step; C, the roxburgh anoectochilus terminal bud after microwave drying is pulverized, the roxburgh anoectochilus terminal bud after pulverizing adds drinkable solvent, and carries out ultrasonic wave extraction, and the roxburgh anoectochilus terminal bud stoste obtaining is roxburgh anoectochilus terminal bud extract.
Further, the vacuum condition that carries out microwave drying in described step b is: vacuum is-75KPa～-65KPa.
The roxburgh anoectochilus terminal bud useful load of further, carrying out microwave drying in described step b is 300g～400g.
Further, the initial moisture content of drying base in described tempering technique is 258%, and the tempering time is 208 minutes.
Further, the vacuum of carrying out the vacuum condition of microwave drying in described step b is-75KPa that the useful load of roxburgh anoectochilus terminal bud is 300g.
Further, the drinkable solvent in described step c is the pure water of making through anti-penetration water purifier, and the roxburgh anoectochilus terminal bud of described pulverizing and the solid-liquid ratio of this pure water are 1:15.
Further, the time that in described step c, ultrasonic wave extracts is 25 minutes, and temperature is 60 ℃.
A kind of roxburgh anoectochilus terminal bud dried hawthorn health drink, formed by roxburgh anoectochilus terminal bud extract, hawthorn concentrate, sucrose and honey allotment, the volume proportion of described roxburgh anoectochilus terminal bud extract and hawthorn concentrate is 3.4:1, the concentration of described sucrose is 0.03g/ml, the concentration of described honey is 0.06g/ml, and described roxburgh anoectochilus terminal bud extract adopts following steps to be prepared from: a, the roxburgh anoectochilus terminal bud of choosing is washed and dried to blade and wither; B, the roxburgh anoectochilus terminal bud after drying is carried out under vacuum condition to microwave drying, wherein in the process of microwave drying, introduce tempering technique, the microwave power of microwave drying is 3000W in this step; C, the roxburgh anoectochilus terminal bud after microwave drying is pulverized, the roxburgh anoectochilus terminal bud after pulverizing adds drinkable solvent, and carries out ultrasonic wave extraction, and the roxburgh anoectochilus terminal bud stoste obtaining is roxburgh anoectochilus terminal bud extract.
Further, the vacuum condition that carries out microwave drying in described step b is: vacuum is-75KPa～-65KPa.
The roxburgh anoectochilus terminal bud useful load of further, carrying out microwave drying in described step b is 300g～400g.
Further, the initial moisture content of drying base in described tempering technique is 258%, and the tempering time is 208 minutes.
Further, the vacuum of carrying out the vacuum condition of microwave drying in described step b is-75KPa that the useful load of roxburgh anoectochilus terminal bud is 300g.
Further, the drinkable solvent in described step c is the pure water of making through anti-penetration water purifier, and the roxburgh anoectochilus terminal bud of described pulverizing and the solid-liquid ratio of this pure water are 1:15.
Further, the time that in described step c, ultrasonic wave extracts is 25 minutes, and temperature is 60 ℃.
A preparation method for roxburgh anoectochilus terminal bud lemon fresh fruit health drink, comprises the steps: a, adopts the preparation method of above-mentioned roxburgh anoectochilus terminal bud extract to prepare roxburgh anoectochilus terminal bud extract; B, choose lemon fresh fruit, clean after peeling and add water and squeeze the juice, the amount of water in the process of squeezing the juice is the twice of lemon fresh fruit volume, afterwards the lemon after squeezing the juice and water mixed liquid is filtered, thereby makes lemon juice; C, roxburgh anoectochilus terminal bud extract is fully mixed with lemon juice after, add sucrose and winter honey to allocate, can be made into above-mentioned roxburgh anoectochilus terminal bud lemon fresh fruit health drink, the volume proportion of described roxburgh anoectochilus terminal bud extract and lemon juice is 42:5 in this step, the concentration of described sucrose is 0.05 g/ml, and the concentration of described winter honey is 0.02 g/ml.
A preparation method for roxburgh anoectochilus terminal bud dried hawthorn health drink, comprises the steps: a, adopts the preparation method of above-mentioned roxburgh anoectochilus terminal bud extract to prepare roxburgh anoectochilus terminal bud extract; B, choose dried hawthorn, with emerge in worm water 20 minutes; C, soaked dried hawthorn being added water and decocted, is 20 times of dried hawthorn volume decocting amount of water in process, through decoct concentrated after, in the time of discharge reduction 3/4, can and make hawthorn concentrate; D, roxburgh anoectochilus terminal bud extract is fully mixed with hawthorn concentrate after, add sucrose and honey to allocate, can be made into above-mentioned roxburgh anoectochilus terminal bud dried hawthorn health drink, the volume proportion of described roxburgh anoectochilus terminal bud extract and hawthorn concentrate is 3.4:1 in this step, the concentration of described sucrose is 0.03g/ml, and the concentration of described honey is 0.06g/ml.
Compared to the prior art the beneficial effect that, the present invention produces is:
1, the present invention is by carrying out vacuum microwave drying under the process conditions that are 3000W at microwave power by roxburgh anoectochilus terminal bud, and in dry run, introduce tempering technique, the functional characteristic composition such as contained polysaccharide, flavones and amino acid and distinctive fragrance in dried roxburgh anoectochilus terminal bud are retained effectively, retained through the pharmacological active substance great majority that extract the roxburgh anoectochilus terminal bud extract drawing, and under the process conditions that are 3000W at microwave power, in above-mentioned roxburgh anoectochilus terminal bud extract, the content of contained polysaccharide, general flavone and free amino acid is the highest.
2, in the present invention, can be adjusted to two kinds of Jewel orchid beverages with different health-care efficacies according to above-mentioned roxburgh anoectochilus terminal bud extract.Wherein one is roxburgh anoectochilus terminal bud lemon health drink, the effect of promoting the production of body fluid, quench the thirst, drive away summer heat because lemon has, hear lemon smell, can make people ambition unfold, in high spirits, the fresh winter honey that adds adjustment can play moist and trophism, this beverage can make skin exquisiteness, smooth, high resilience, and can promote digestion, improves immunity, has the sleep of improvement, protects the liver the effect such as be healthy and strong.Wherein another kind is roxburgh anoectochilus terminal bud dried hawthorn health drink, and that this kind of beverage can help digestion is long-pending, scattered silt blood, only dysentery of convergence, and cardiovascular system is also had to very many-sided pharmacological action, and heat falls in appetizing, protects liver and supports spleen, has certain effect to cardiovascular.
Accompanying drawing explanation
Fig. 1 be in embodiment bis-roxburgh anoectochilus terminal bud extract addition and flavour mark mark be related to chart.
Fig. 2 be in embodiment bis-lemon stoste addition and flavour mark mark be related to chart.
Fig. 3 be in embodiment bis-honey addition and flavour mark mark be related to chart.
Fig. 4 be in embodiment bis-sucrose addition and flavour mark mark be related to chart.
Fig. 5 be in embodiment tri-roxburgh anoectochilus terminal bud extract addition and flavour mark mark be related to chart.
Fig. 6 be in embodiment tri-hawthorn stoste addition and flavour mark mark be related to chart.
Fig. 7 be in embodiment tri-honey addition and flavour mark mark be related to chart.
Fig. 8 be in embodiment tri-sucrose addition and flavour mark mark be related to chart.
The specific embodiment
Embodiment mono-
A preparation method for roxburgh anoectochilus terminal bud extract, comprises the following steps:
The first step, washes the roxburgh anoectochilus terminal bud of choosing and dries to blade and wither, in this step roxburgh anoectochilus terminal bud preferably grow fine without disease and pest gold thread lotus leaf.
Second step, roxburgh anoectochilus terminal bud after drying is carried out under vacuum condition to microwave drying, wherein in the process of microwave drying, introduce tempering technique, the microwave power of microwave drying is 3000W in this step, the vacuum condition that carries out microwave drying in this step is: vacuum is-75KPa～-65KPa, the roxburgh anoectochilus terminal bud useful load of carrying out microwave drying in this step is 300g～400g, described tempering technique process conditions be: initial moisture content of drying base is 258%, and the tempering time is 208 minutes.
The 3rd step, roxburgh anoectochilus terminal bud after microwave drying is pulverized, roxburgh anoectochilus terminal bud after pulverizing adds drinkable solvent, and carry out ultrasonic wave extraction, the roxburgh anoectochilus terminal bud stoste obtaining is roxburgh anoectochilus terminal bud extract, and the drinkable solvent in this step is the pure water of making through anti-penetration water purifier, and the roxburgh anoectochilus terminal bud of described pulverizing and the solid-liquid ratio of this pure water are 1:15, the time that ultrasonic wave extracts is 25 minutes, and temperature is 60 ℃.
Now provide the impact analysis test of each parameter factor to roxburgh anoectochilus terminal bud leading indicator in microwave vacuum technique, microwave power (A), vacuum (B), three of useful loads (C) affect larger as the important technology index in roxburgh anoectochilus terminal bud micro-wave vacuum on active ingredients such as the very dried polysaccharide of roxburgh anoectochilus terminal bud, general flavones.Below the L9 (3 of microwave power, vacuum, useful load three factors optimizations
4) orthogonal experiment data.
Table 1 orthogonal test factor level
| Level | A microwave power (W) | B vacuum (KPa) | C useful load |
| 1 | 2000 | -65 | 200 |
| 2 | 3000 | -75 | 300 |
| 3 | 4000 | -85 | 400 |
The extreme difference of anoectochilus roxburghii polyose content and variance analysis:
Table 2 L
9 (3
4) the orthogonal experiments table of polyoses content
| Tested number | A | B | C | Empty row | Polyoses content (mg/g) |
| 1 | 2000 | -65 | 200 | 1 | 12.432 |
| 2 | 2000 | -75 | 300 | 2 | 15.213 |
| 3 | 2000 | -85 | 400 | 3 | 11.281 |
| 4 | 3000 | -65 | 300 | 3 | 20.068 |
| 5 | 3000 | -75 | 400 | 1 | 16.903 |
| 6 | 3000 | -85 | 200 | 2 | 20.890 |
| 7 | 4000 | -65 | 400 | 2 | 9.775 |
| 8 | 4000 | -75 | 200 | 3 | 17.874 |
| 9 | 4000 | -85 | 300 | 1 | 18.483 |
| K1 | 12.9753 | 13.4250 | 17.0653 | 15.8627 | |
| K2 | 18.6203 | 16.6633 | 17.1780 | 15.2927 | |
| K3 | 15.3007 | 16.8080 | 12.6530 | 15.7410 | |
| R | 5.0843 | 3.0470 | 4.0755 | 0.5134 |
The analysis of variance table of table 3 polyoses content
| Source of variation | Quadratic sum | The free degree | All sides | F value | Conspicuousness |
| Microwave rate A | 48.2934 | 2 | 24.1467 | 89.3155 | * |
| Vacuum B | 21.9524 | 2 | 10.9762 | 40.5996 | * |
| Useful load C | 39.9570 | 2 | 19.9765 | 73.8979 | * |
| Empty row | 0.5407 | 2 | 0.2704 | ||
| Error | 05.407 | 2 | 0.2704 | ||
| Summation | 110.7435 |
A in comparison sheet 2, B, the R value of tri-factors of C, can show that affecting after roxburgh anoectochilus terminal bud micro-wave vacuum the secondary factors of polyoses content in dry product is: A>C>B; F value [F in comprehensive comparison sheet 3
0.05(2,2)=19.00, F
0.01(2,2)=99.00] compare, can it is evident that: microwave power A, useful load C, vacuum B present the level of signifiance to the impact of polyoses content, so, from obtaining roxburgh anoectochilus terminal bud micro-wave vacuum, polyoses content is the highest considers processing technology, and preferred process is: A
2b
2,3c
2, i.e. microwave rate 3000 W, vacuum (65 ,-75KPa) useful load 300g.
The extreme difference of general flavone content and variance analysis:
Table 4 L
9 (3
4) the orthogonal experiments table of general flavone content
| Tested number | A | B | C | Empty row | General flavone content (mg/g) |
| 1 | 2000 | -65 | 200 | 1 | 13.871 |
| 2 | 2000 | -75 | 300 | 2 | 13.134 |
| 3 | 2000 | -85 | 400 | 3 | 12.053 |
| 4 | 3000 | -65 | 300 | 3 | 18.486 |
| 5 | 3000 | -75 | 400 | 1 | 17.012 |
| 6 | 3000 | -85 | 200 | 2 | 17.453 |
| 7 | 4000 | -65 | 400 | 2 | 15.020 |
| 8 | 4000 | -75 | 200 | 3 | 15.942 |
| 9 | 4000 | -85 | 300 | 1 | 16.998 |
| K1 | 13.0193 | 15.7923 | 15.7553 | 15.96.3 | |
| K2 | 17.6503 | 15.3627 | 16.2060 | 15.2030 | |
| K3 | 15.9867 | 15.5013 | 14.6950 | 15.4937 | |
| R | 4.1710 | 0.3870 | 1.3609 | 0.6827 |
The analysis of variance table of table 5 general flavone content
| Source of variation | Quadratic sum | The free degree | All sides | F value | Conspicuousness |
| Microwave rate A | 33.019 | 2 | 16.5095 | 37.6407 | * |
| Vacuum B | 0.2885 | 2 | 0.1443 | 0.3289 | * |
| Useful load C | 3.6105 | 2 | 1.8053 | 4.1159 | * |
| Empty row | 0.8772 | 2 | 0.4386 | ||
| Error | 0.8772 | 2 | 0.4386 | ||
| Summation | 37.7953 |
A in comparison sheet 4, B, the R value of tri-factors of C, can show that affecting after roxburgh anoectochilus terminal bud micro-wave vacuum the secondary factors of general flavone content in dry product is: A>C>B; F value [F in comprehensive comparison sheet 5
0.05(2,2)=19.00, F
0.01(2,2)=99.00] compare, can it is evident that: microwave power A presents the level of signifiance to the impact of general flavone content, and vacuum B and useful load C on the impact of general flavone content the difference without conspicuousness.So from obtaining roxburgh anoectochilus terminal bud micro-wave vacuum, flavones content is the highest considers processing technology, A
2b
1c
2.
The extreme difference of roxburgh anoectochilus terminal bud free aminoacid content and variance analysis:
Table 6 L
9 (3
4) the orthogonal experiments table of amino acid content
| Tested number | A | B | C | Empty row | Amino acid content (mg/g) |
| 1 | 2000 | -65 | 200 | 1 | 79.979 |
| 2 | 2000 | -75 | 300 | 2 | 85.156 |
| 3 | 2000 | -85 | 400 | 3 | 77.011 |
| 4 | 3000 | -65 | 300 | 3 | 116.54 |
| 5 | 3000 | -75 | 400 | 1 | 129.775 |
| 6 | 3000 | -85 | 200 | 2 | 113.865 |
| 7 | 4000 | -65 | 400 | 2 | 96.307 |
| 8 | 4000 | -75 | 200 | 3 | 109.155 |
| 9 | 4000 | -85 | 300 | 1 | 92.483 |
| K1 | 80.7153 | 97.6087 | 100.9997 | 100.7457 | |
| K2 | 120.060 | 108.0287 | 98.0597 | 98.4427 | |
| K3 | 99.3150 | 94.453 | 101.031 | 100.902 | |
| R | 35.4364 | 12.2271 | 2.6762 | 2.2150 |
The analysis of variance table of table 7 amino acid content
| Source of variation | Quadratic sum | The free degree | All sides | F value | Conspicuousness |
| Microwave rate A | 2324.3054 | 2 | 1162.1527 | 204.3064 | * |
| Vacuum B | 302.8334 | 2 | 151.4167 | 26.619 | * |
| Useful load C | 17.4734 | 2 | 8.7367 | 1.5359 | * |
| Empty row | 11.3766 | 2 | 5.6883 | ||
| Error | 11.3766 | 2 | 5.6883 | ||
| Summation | 2655.9888 |
A in comparison sheet 6, B, the R value of tri-factors of C, can show that affecting the secondary factors of dry product Determination of Free Amino Acids after roxburgh anoectochilus terminal bud micro-wave vacuum is: A>B>C; F value [F in comprehensive comparison sheet 7
0.05(2,2)=19.00, F
0.01(2,2)=99.00] compare, can it is evident that: microwave power A presents the level of signifiance to the impact of free aminoacid content, and vacuum B has significant difference to free aminoacid content, useful load C is without the difference of conspicuousness.So from obtaining roxburgh anoectochilus terminal bud micro-wave vacuum, free aminoacid content is the highest considers processing technology, preferred process is: A
2b
2c
3,1.
In single factor experiment and orthogonal test, 3 parallel tests are carried out, test data is averaged, result shows: microwave power A on roxburgh anoectochilus terminal bud micro-wave vacuum after polyoses content, general flavone content and free aminoacid content has significantly or impact extremely significantly, and optimum level is 3000W; Vacuum B on roxburgh anoectochilus terminal bud micro-wave vacuum after the impact of polysaccharide and free aminoacid content significantly, not remarkable on general flavone content impact, can determine be chosen as-75kPa of optimum level; Useful load C on roxburgh anoectochilus terminal bud micro-wave vacuum after polyoses content impact significantly, not remarkable on general flavone and free aminoacid content impact, can determine that optimum level is chosen as 300g.
By orthogonal test, the Optimizing Technical of roxburgh anoectochilus terminal bud micro-wave vacuum is finally defined as: A
2b
2c
2, microwave power be 3000W, vacuum for-75kPa, useful load be 300g.
Embodiment bis-
The present embodiment relates to the roxburgh anoectochilus terminal bud lemon health drink of the roxburgh anoectochilus terminal bud extract drawing in a kind of embodiment of containing, and the following mode of this roxburgh anoectochilus terminal bud lemon health drink is prepared from:
The first step, adopts the preparation method of roxburgh anoectochilus terminal bud extract in embodiment mono-to prepare roxburgh anoectochilus terminal bud extract.
Second step, chooses lemon fresh fruit, after clean peeling, adds water and squeezes the juice, and the amount of water in the process of squeezing the juice is the twice of lemon fresh fruit volume, afterwards the lemon after squeezing the juice and water mixed liquid is filtered, thereby makes lemon juice.
The 3rd step, after roxburgh anoectochilus terminal bud extract is fully mixed with lemon juice, add sucrose and winter honey to allocate, can be made into above-mentioned roxburgh anoectochilus terminal bud lemon fresh fruit health drink, the volume proportion of described roxburgh anoectochilus terminal bud extract and lemon juice is 42:5 in this step, the concentration of described sucrose is 0.05 g/ml, and the concentration of described winter honey is 0.02 g/ml.The roxburgh anoectochilus terminal bud lemon health drink making through said method, the effect of promoting the production of body fluid, quench the thirst, drive away summer heat because lemon has, hear lemon smell, can make people ambition unfold, in high spirits, the fresh winter honey that adds adjustment can play moist and trophism, this beverage can make skin exquisiteness, smooth, high resilience, and can promote digestion, improves immunity, has the sleep of improvement, protects the liver the effect such as be healthy and strong.
Now provide the impact analysis test of the each formula factors of roxburgh anoectochilus terminal bud lemon fresh fruit health drink to roxburgh anoectochilus terminal bud lemon fresh fruit health drink mouthfeel, roxburgh anoectochilus terminal bud extract (A), lemon juice (B), winter honey (C) and four formula factors as roxburgh anoectochilus terminal bud lemon fresh fruit health drink of sucrose (D) are larger on the impact of roxburgh anoectochilus terminal bud lemon fresh fruit health drink mouthfeel.Below the L9 (3 of roxburgh anoectochilus terminal bud extract (A), lemon juice (B), winter honey (C) and this four factors optimization of sucrose (D)
4) orthogonal experiment data.
Lemon taste factor and level:
Table 8 factor and level
| Level | A roxburgh anoectochilus terminal bud extract/ml | B lemon juice/ml | C honey/(gml -1) | D sucrose/(gml -1) |
| 1 | 210 | 25 | 0.01 | 0.02 |
| 2 | 338 | 50 | 0.02 | 0.05 |
| 3 | 400 | 75 | 0.03 | 0.08 |
Preferendum sense organ by people carries out taste test, and gives a mark according to following table.
Table 9 flavour mark standard (hundred-mark system)
Note: the full marks of local flavor, sweet taste, tart flavour, aftertaste are 25 points
Flavour mark standard (duplicate):
Mouthfeel degree of liking: the overall feeling of beverage; Sweet taste degree of liking: you like this sweet taste;
Tart flavour degree of liking: whether tart flavour is that you like; Aftertaste degree of liking: drink later oral cavity throat impression OK.
Give a mark through human body evaluation:
| 21-25 | Be delithted with | 16-20 | Like | 11-15 | Generally |
| 6-10 | Do not like | 1-6 | No good cake |
Table 10 L
9(3
4) orthogonal experiments
| Tested number | A | B | C | D | Score |
| 1 | 1 | 1 | 1 | 1 | 46.5 |
| 2 | 1 | 2 | 2 | 2 | 48.5 |
| 3 | 1 | 3 | 3 | 3 | 72 |
| 4 | 2 | 1 | 1 | 3 | 61 |
| 5 | 2 | 2 | 2 | 1 | 57.3 |
| 6 | 2 | 3 | 3 | 2 | 64.3 |
| 7 | 3 | 1 | 1 | 2 | 72.6 |
| 8 | 3 | 2 | 2 | 3 | 67.3 |
| 9 | 3 | 3 | 3 | 1 | 65.6 |
| K1 | 166.9 | 179.9 | 178.2 | 169.2 | |
| K2 | 182.9 | 202.2 | 201.9 | 200.3 | |
| K3 | 205.5 | 171.5 | 178.5 | 185.8 | |
| R | 38.6 | 30.7 | 23.4 | 31.1 |
With reference to Fig. 1-Fig. 4, as above-mentioned experiment, the best sugar-acid ratio formula of summary lemon taste roxburgh anoectochilus terminal bud is: roxburgh anoectochilus terminal bud extract 420 ml+ lemon stoste 50 ml+ sucrose 0.05g/ml+ honey 0.02 g/ml.
Embodiment tri-
The present embodiment relates to the roxburgh anoectochilus terminal bud dried hawthorn health drink of the roxburgh anoectochilus terminal bud extract drawing in a kind of embodiment of containing, and the following mode of this roxburgh anoectochilus terminal bud dried hawthorn health drink is prepared from:
The first step, adopts the preparation method of roxburgh anoectochilus terminal bud extract in embodiment mono-to prepare roxburgh anoectochilus terminal bud extract.
Second step, chooses dried hawthorn, uses emerge in worm water 20 minutes.
The 3rd step, adds water soaked dried hawthorn to decoct, and is 20 times of dried hawthorn volume decocting amount of water in process, through decoct concentrated after, in the time of discharge reduction 3/4, can and make hawthorn concentrate.
The 4th step, after roxburgh anoectochilus terminal bud extract is fully mixed with hawthorn concentrate, add sucrose and honey to allocate, can be made into above-mentioned roxburgh anoectochilus terminal bud dried hawthorn health drink, be 3.4:1 at the volume proportion of roxburgh anoectochilus terminal bud extract described in this step and hawthorn concentrate, the concentration of described sucrose is 0.03g/ml, and the concentration of described honey is 0.06g/ml.That this kind of roxburgh anoectochilus terminal bud dried hawthorn health drink can help digestion is long-pending, scattered silt blood, only dysentery of convergence, and cardiovascular system is also had to very many-sided pharmacological action, and heat falls in appetizing, protects liver and supports spleen, has certain effect to cardiovascular.
Now provide the impact analysis test of the each formula factors of roxburgh anoectochilus terminal bud dried hawthorn health drink to roxburgh anoectochilus terminal bud dried hawthorn health drink mouthfeel, roxburgh anoectochilus terminal bud extract (A), hawthorn concentrate (B), honey (C) and four formula factors as roxburgh anoectochilus terminal bud dried hawthorn health drink of sucrose (D) are larger on the impact of roxburgh anoectochilus terminal bud dried hawthorn health drink mouthfeel.Below the L9 (3 of roxburgh anoectochilus terminal bud extract (A), hawthorn concentrate (B), honey (C) and this four factors optimization of sucrose (D)
4) orthogonal experiment data.
Table 11 factor and level
| Level | A roxburgh anoectochilus terminal bud Extract/ml | B hawthorn concentrate /ml | C honey/ (g·ml -1 ) | D sucrose/ (g·ml -1 ) |
| 1 | 210 | 50 | 0.01 | 0.02 |
| 2 | 338 | 72 | 0.02 | 0.04 |
| 3 | 400 | 100 | 0.03 | 0.06 |
Table 12 L
9(3
4) orthogonal experiments
| Tested number | A | B | C | D | Score |
| 1 | 1 | 1 | 1 | 1 | 63 |
| 2 | 1 | 2 | 2 | 2 | 56 |
| 3 | 1 | 3 | 3 | 3 | 78.6 |
| 4 | 2 | 1 | 1 | 3 | 70.8 |
| 5 | 2 | 2 | 2 | 1 | 76.4 |
| 6 | 2 | 3 | 3 | 2 | 72.8 |
| 7 | 3 | 1 | 1 | 2 | 66.8 |
| 8 | 3 | 2 | 2 | 3 | 69 |
| 9 | 3 | 3 | 3 | 1 | 57.8 |
| K1 | 197.6 | 200.7 | 204.8 | 197.2 | |
| K2 | 220 | 201.4 | 184.6 | 195.6 | |
| K3 | 193.6 | 209.2 | 221.8 | 218.4 | |
| R | 26.4 | 8.6 | 37.2 | 22.8 |
With reference to Fig. 5-Fig. 8, and associative list 11 and table 12 result of the test are known, while investigating index with appraisal result, the size order that affects of 4 factors is: honey > roxburgh anoectochilus terminal bud concentrate > sucrose > hawthorn concentrate.Analysis optimum formula is: A
2b
3c
3d
3, when roxburgh anoectochilus terminal bud extract 338 ml+hawthorn concentrate 100 ml+sucrose 0.03g/ml+honey 0.06g/ml, mouthfeel is best.
Above are only the specific embodiment of the present invention, but design concept of the present invention is not limited to this, allly utilizes this design to carry out the change of unsubstantiality to the present invention, all should belong to the behavior of invading protection domain of the present invention.
Claims (12)
1. a preparation method for roxburgh anoectochilus terminal bud extract, is characterized in that, comprises the following steps: a, the roxburgh anoectochilus terminal bud of choosing is washed and dried to blade and wither; B, the roxburgh anoectochilus terminal bud after drying is carried out under vacuum condition to microwave drying, wherein in the process of microwave drying, introduce tempering technique, the microwave power of microwave drying is 3000W in this step; C, the roxburgh anoectochilus terminal bud after microwave drying is pulverized, the roxburgh anoectochilus terminal bud after pulverizing adds drinkable solvent, and carries out ultrasonic wave extraction, and the roxburgh anoectochilus terminal bud stoste obtaining is roxburgh anoectochilus terminal bud extract.
2. the preparation method of a kind of roxburgh anoectochilus terminal bud extract as claimed in claim 1, is characterized in that, the vacuum condition that carries out microwave drying in described step b is: vacuum is-75KPa～-65KPa.
3. a kind of roxburgh anoectochilus terminal bud extract as claimed in claim 2, is characterized in that: the roxburgh anoectochilus terminal bud useful load of carrying out microwave drying in described step b is 300g～400g.
4. the preparation method of a kind of roxburgh anoectochilus terminal bud extract as claimed in claim 1, is characterized in that: the initial moisture content of drying base in described tempering technique is 258%, and the tempering time is 208 minutes.
5. the preparation method of a kind of roxburgh anoectochilus terminal bud extract as claimed in claim 1, is characterized in that: the vacuum of carrying out the vacuum condition of microwave drying in described step b is-75KPa that the useful load of roxburgh anoectochilus terminal bud is 300g.
6. the preparation method of a kind of roxburgh anoectochilus terminal bud extract as claimed in claim 1, is characterized in that: the drinkable solvent in described step c is the pure water of making through anti-penetration water purifier, and the roxburgh anoectochilus terminal bud of described pulverizing and the solid-liquid ratio of this pure water are 1:15.
7. the preparation method of a kind of roxburgh anoectochilus terminal bud extract as claimed in claim 6, is characterized in that: the time that in described step c, ultrasonic wave extracts is 25 minutes, and temperature is 60 ℃.
8. a roxburgh anoectochilus terminal bud extract, is characterized in that: this roxburgh anoectochilus terminal bud extract adopts the preparation method of the roxburgh anoectochilus terminal bud extract as described in any one in claim 1-7 to be prepared from.
9. a roxburgh anoectochilus terminal bud lemon fresh fruit health drink, it is characterized in that: formed by roxburgh anoectochilus terminal bud extract, lemon juice, sucrose and winter honey allotment, described roxburgh anoectochilus terminal bud extract adopts roxburgh anoectochilus terminal bud extract as claimed in claim 8, the volume proportion of described roxburgh anoectochilus terminal bud extract and lemon juice is 42:5, the concentration of described sucrose is 0.05 g/ml, and the concentration of described winter honey is 0.02 g/ml.
10. a roxburgh anoectochilus terminal bud dried hawthorn health drink, it is characterized in that: formed by roxburgh anoectochilus terminal bud extract, hawthorn concentrate, sucrose and honey allotment, described roxburgh anoectochilus terminal bud extract adopts roxburgh anoectochilus terminal bud extract as claimed in claim 8, the volume proportion of described roxburgh anoectochilus terminal bud extract and hawthorn concentrate is 3.4:1, the concentration of described sucrose is 0.03g/ml, and the concentration of described honey is 0.06g/ml.
The preparation method of 11. 1 kinds of roxburgh anoectochilus terminal bud lemon fresh fruit health drinks, is characterized in that, comprises the steps: a, adopts the preparation method of the roxburgh anoectochilus terminal bud extract as described in any one in claim 1-7 to prepare roxburgh anoectochilus terminal bud extract; B, choose lemon fresh fruit, clean after peeling and add water and squeeze the juice, the amount of water in the process of squeezing the juice is the twice of lemon fresh fruit volume, afterwards the lemon after squeezing the juice and water mixed liquid is filtered, thereby makes lemon juice; C, roxburgh anoectochilus terminal bud extract is fully mixed with lemon juice after, add sucrose and winter honey to allocate, can be made into above-mentioned roxburgh anoectochilus terminal bud lemon fresh fruit health drink, the volume proportion of described roxburgh anoectochilus terminal bud extract and lemon juice is 42:5 in this step, the concentration of described sucrose is 0.05 g/ml, and the concentration of described winter honey is 0.02 g/ml.
The preparation method of 12. 1 kinds of roxburgh anoectochilus terminal bud dried hawthorn health drinks, is characterized in that, comprises the steps: a, adopts the preparation method of the roxburgh anoectochilus terminal bud extract as described in any one in claim 1-7 to prepare roxburgh anoectochilus terminal bud extract; B, choose dried hawthorn, with emerge in worm water 20 minutes; C, soaked dried hawthorn being added water and decocted, is 20 times of dried hawthorn volume decocting amount of water in process, through decoct concentrated after, in the time of discharge reduction 3/4, can and make hawthorn concentrate; D, roxburgh anoectochilus terminal bud extract is fully mixed with hawthorn concentrate after, add sucrose and honey to allocate, can be made into above-mentioned roxburgh anoectochilus terminal bud dried hawthorn health drink, the volume proportion of described roxburgh anoectochilus terminal bud extract and hawthorn concentrate is 3.4:1 in this step, the concentration of described sucrose is 0.03g/ml, and the concentration of described honey is 0.06g/ml.
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| CN104522470A (en) * | 2015-01-12 | 2015-04-22 | 福建农林大学 | Phedimus aizoon health-care beverage and method for making phedimus aizoon health-care beverage |
| CN105085696A (en) * | 2015-07-13 | 2015-11-25 | 福建省亚热带植物研究所 | Method for extracting Anoectochilus roxburghii polysaccharides |
| CN105315381A (en) * | 2014-07-22 | 2016-02-10 | 漳州市亚热带园艺技术有限公司 | Anoectochilus roxburghii polysaccharide extraction and preliminary purifying method and preparation method for oral liquid of anoectochilus roxburghii polysaccharide |
| CN105495214A (en) * | 2015-12-21 | 2016-04-20 | 武杰 | Anoectochilus roxburghii (Wall.) Lindl and strawbaeery juice beverage and making method thereof |
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| CN112816577A (en) * | 2020-12-30 | 2021-05-18 | 联和东浩(厦门)药业有限公司 | Detection and analysis method for active ingredients of anoectochilus formosanus |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105315381A (en) * | 2014-07-22 | 2016-02-10 | 漳州市亚热带园艺技术有限公司 | Anoectochilus roxburghii polysaccharide extraction and preliminary purifying method and preparation method for oral liquid of anoectochilus roxburghii polysaccharide |
| CN104522470A (en) * | 2015-01-12 | 2015-04-22 | 福建农林大学 | Phedimus aizoon health-care beverage and method for making phedimus aizoon health-care beverage |
| CN105085696A (en) * | 2015-07-13 | 2015-11-25 | 福建省亚热带植物研究所 | Method for extracting Anoectochilus roxburghii polysaccharides |
| CN105495214A (en) * | 2015-12-21 | 2016-04-20 | 武杰 | Anoectochilus roxburghii (Wall.) Lindl and strawbaeery juice beverage and making method thereof |
| CN106262804A (en) * | 2016-07-26 | 2017-01-04 | 福建省麟阳农业科技有限公司 | A kind of preparation technology of Herba Anoectochili roxburghii ferment |
| CN107753879A (en) * | 2017-12-08 | 2018-03-06 | 唐佳艳 | The Chinese medicine composition and its preparation method of a kind of reducing blood lipid |
| CN112587618A (en) * | 2020-12-30 | 2021-04-02 | 联和东浩(厦门)药业有限公司 | Method for separating anoectochilus formosanus total alkaloids from anoectochilus formosanus extract |
| CN112816577A (en) * | 2020-12-30 | 2021-05-18 | 联和东浩(厦门)药业有限公司 | Detection and analysis method for active ingredients of anoectochilus formosanus |
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