CN103876218B - A kind of Jewel orchid beverage and preparation method thereof - Google Patents

A kind of Jewel orchid beverage and preparation method thereof Download PDF

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Publication number
CN103876218B
CN103876218B CN201310649261.1A CN201310649261A CN103876218B CN 103876218 B CN103876218 B CN 103876218B CN 201310649261 A CN201310649261 A CN 201310649261A CN 103876218 B CN103876218 B CN 103876218B
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terminal bud
roxburgh anoectochilus
anoectochilus terminal
microwave drying
extract
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CN103876218A (en
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王昭毅
郭龙龙
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ZHENXI BIOTECHNOLOGY Co Ltd FUJIAN
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ZHENXI BIOTECHNOLOGY Co Ltd FUJIAN
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    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • A23L2/04—Extraction of juices
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52—Adding ingredients
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/105—Plant extracts, their artificial duplicates or their derivatives
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs

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Abstract

A kind of roxburgh anoectochilus terminal bud lemon fresh fruit health drink, formed by roxburgh anoectochilus terminal bud extract, lemon juice, sucrose and winter honey allotment, the volume proportion of described roxburgh anoectochilus terminal bud extract and lemon juice is 42:5, the concentration of described sucrose is 0.05g/mL, the concentration of described winter honey is 0.02g/mL, described roxburgh anoectochilus terminal bud extract adopts following steps to be prepared from, and a, is carried out washing by the roxburgh anoectochilus terminal bud chosen and dries to blade and wither; B, the roxburgh anoectochilus terminal bud after drying is carried out microwave drying under vacuum, wherein in the process of microwave drying, introduce tempering technique, the microwave power of microwave drying is in this step 3000W; C, pulverized by the roxburgh anoectochilus terminal bud after microwave drying, roxburgh anoectochilus terminal bud after being pulverized adds drinkable solvent, and carries out ultrasonic wave extraction.The beverage that the present invention obtains can make that skin is fine and smooth, smooth, high resilience, and can promote digestion, improves immunity, has improving water flood, protects the liver effects such as being healthy and strong.

Description

A kind of Jewel orchid beverage and preparation method thereof
Technical field
The present invention relates to roxburgh anoectochilus terminal bud manufacture field, refer in particular to roxburgh anoectochilus terminal bud extract and preparation method thereof and Jewel orchid beverage and preparation method thereof.
Background technology
Roxburgh anoectochilus terminal bud is the herbaceos perennial of the orchid family Anoectochilus Blume.The young grass of another name Shorthairy Antenoron, rough melic herb, Shu Caolian, money, gold thread taiwan anetochilus herb, gold thread disappear to the marrow.Roxburgh anoectochilus terminal bud is the wider one tradition valuable ingredient of traditional Chinese medicine of use among the people, has the effects such as clearing heat and detoxicating, expelling wind and removing dampness, nourishing Yin and moistening lung, hypotensive, flat liver.Roxburgh anoectochilus terminal bud contains a large amount of valuable pharmacological active material, mainly comprise: flavone compound (Quercetin, Isorhamnetin), steroid compound (24 ~ isopropenyl cholesterine, open the blue sterol of lip, ergosterol, stigmasterol, campesterol, cupreol etc.), triterpene compound (suberone, butanedioic acid, coumaric acid, forulic acid, daucosterol, palmitic acid, oleanolic acid, ursolic acid), carbohydrate content (polysaccharide 13.326%, compound sugar 11.243%, reduced sugar 9.73%), alkaloid (huperzine and aconitine), Cardiac glycosides, ester class, taurine, several amino acids, trace element and inorganic elements etc.Wherein, the content of amino acid and trace element, all higher than domestic American Ginseng and wild ginseng, has medicinal and economic worth.
For now, the edible way of roxburgh anoectochilus terminal bud is comparatively time-consuming comparatively speaking, and along with improving constantly of people's rhythm of life, how roxburgh anoectochilus terminal bud being applied to fast drink product and can retaining its original composition is letter problem to be solved.Roxburgh anoectochilus terminal bud to being made fast drink product with regard to needing, the pharmacological active substance in roxburgh anoectochilus terminal bud to be extracted, first forming roxburgh anoectochilus terminal bud extract, then being modulated into the Jewel orchid beverage meeting people's taste.But due to the most common with hot air drying roxburgh anoectochilus terminal bud on the market at present, its drying finished product brittleness is large, easily be extruded fragmentation, chlorophyll and nutrient component damages serious, finished product is brown, and burnt odor is highly seasoned masks the distinctive smell of roxburgh anoectochilus terminal bud, runs off more through the pharmacological active substance extracting the roxburgh anoectochilus terminal bud extract drawn, and rise can not retain the distinctive smell of roxburgh anoectochilus terminal bud, its redeployed beverage nutritive value not high and rise mouthfeel poor.
Summary of the invention
The invention provides a kind of roxburgh anoectochilus terminal bud extract and preparation method thereof and Jewel orchid beverage and preparation method thereof, its main purpose is to overcome the time-consuming roxburgh anoectochilus terminal bud pharmacological active substance that is loaded down with trivial details, hot air drying of existing roxburgh anoectochilus terminal bud edible way and runs off more defect.
For solving the problems of the technologies described above, the present invention adopts following technical scheme:
A preparation method for roxburgh anoectochilus terminal bud extract, comprises the following steps: a, carried out washing by the roxburgh anoectochilus terminal bud chosen and dry to blade and wither; B, the roxburgh anoectochilus terminal bud after drying is carried out microwave drying under vacuum, wherein in the process of microwave drying, introduce tempering technique, the microwave power of microwave drying is in this step 3000W; C, pulverized by the roxburgh anoectochilus terminal bud after microwave drying, roxburgh anoectochilus terminal bud after being pulverized adds drinkable solvent, and carries out ultrasonic wave extraction, and the roxburgh anoectochilus terminal bud stoste obtained is roxburgh anoectochilus terminal bud extract.
Further, the vacuum condition carrying out microwave drying in described step b is: vacuum is-75KPa ~-65KPa.
Further, the roxburgh anoectochilus terminal bud useful load of carrying out microwave drying in described step b is 300g ~ 400g.
Further, the initial moisture content of drying base in described tempering technique is 258%, and the tempering time is 208 minutes.
Further, the vacuum of carrying out the vacuum condition of microwave drying in described step b is-75KPa, and the useful load of roxburgh anoectochilus terminal bud is 300g.
Further, the drinkable solvent in described step c is the pure water made through anti-penetration water purifier, and the roxburgh anoectochilus terminal bud of described pulverizing and the solid-liquid ratio of this pure water are 1:15.
Further, the time that in described step c, ultrasonic wave extracts is 25 minutes, and temperature is 60 DEG C.
A kind of roxburgh anoectochilus terminal bud extract, this roxburgh anoectochilus terminal bud extract adopts following steps to be prepared from: a, carried out washing by the roxburgh anoectochilus terminal bud chosen and dry to blade and wither; B, the roxburgh anoectochilus terminal bud after drying is carried out microwave drying under vacuum, wherein in the process of microwave drying, introduce tempering technique, the microwave power of microwave drying is in this step 3000W; C, pulverized by the roxburgh anoectochilus terminal bud after microwave drying, roxburgh anoectochilus terminal bud after being pulverized adds drinkable solvent, and carries out ultrasonic wave extraction, and the roxburgh anoectochilus terminal bud stoste obtained is roxburgh anoectochilus terminal bud extract.
Further, the vacuum condition carrying out microwave drying in described step b is: vacuum is-75KPa ~-65KPa.
Further, the roxburgh anoectochilus terminal bud useful load of carrying out microwave drying in described step b is 300g ~ 400g.
Further, the initial moisture content of drying base in described tempering technique is 258%, and the tempering time is 208 minutes.
Further, the vacuum of carrying out the vacuum condition of microwave drying in described step b is-75KPa, and the useful load of roxburgh anoectochilus terminal bud is 300g.
Further, the drinkable solvent in described step c is the pure water made through anti-penetration water purifier, and the roxburgh anoectochilus terminal bud of described pulverizing and the solid-liquid ratio of this pure water are 1:15.
Further, the time that in described step c, ultrasonic wave extracts is 25 minutes, and temperature is 60 DEG C.。
A kind of roxburgh anoectochilus terminal bud lemon fresh fruit health drink, formed by roxburgh anoectochilus terminal bud extract, lemon juice, sucrose and winter honey allotment, the volume proportion of described roxburgh anoectochilus terminal bud extract and lemon juice is 42:5, the concentration of described sucrose is 0.05g/mL, the concentration of described winter honey is 0.02g/mL, and described roxburgh anoectochilus terminal bud extract adopts following steps to be prepared from: a, carried out washing by the roxburgh anoectochilus terminal bud chosen and dry to blade and wither; B, the roxburgh anoectochilus terminal bud after drying is carried out microwave drying under vacuum, wherein in the process of microwave drying, introduce tempering technique, the microwave power of microwave drying is in this step 3000W; C, pulverized by the roxburgh anoectochilus terminal bud after microwave drying, roxburgh anoectochilus terminal bud after being pulverized adds drinkable solvent, and carries out ultrasonic wave extraction, and the roxburgh anoectochilus terminal bud stoste obtained is roxburgh anoectochilus terminal bud extract.
Further, the vacuum condition carrying out microwave drying in described step b is: vacuum is-75KPa ~-65KPa.
Further, the roxburgh anoectochilus terminal bud useful load of carrying out microwave drying in described step b is 300g ~ 400g.
Further, the initial moisture content of drying base in described tempering technique is 258%, and the tempering time is 208 minutes.
Further, the vacuum of carrying out the vacuum condition of microwave drying in described step b is-75KPa, and the useful load of roxburgh anoectochilus terminal bud is 300g.
Further, the drinkable solvent in described step c is the pure water made through anti-penetration water purifier, and the roxburgh anoectochilus terminal bud of described pulverizing and the solid-liquid ratio of this pure water are 1:15.
Further, the time that in described step c, ultrasonic wave extracts is 25 minutes, and temperature is 60 DEG C.
A kind of roxburgh anoectochilus terminal bud dried hawthorn health drink, allocated by roxburgh anoectochilus terminal bud extract, hawthorn concentrate, sucrose and honey and form, the volume proportion of described roxburgh anoectochilus terminal bud extract and hawthorn concentrate is 3.4:1, the concentration of described sucrose is 0.03g/mL, the concentration of described honey is 0.06g/mL, and described roxburgh anoectochilus terminal bud extract adopts following steps to be prepared from: a, carried out washing by the roxburgh anoectochilus terminal bud chosen and dry to blade and wither; B, the roxburgh anoectochilus terminal bud after drying is carried out microwave drying under vacuum, wherein in the process of microwave drying, introduce tempering technique, the microwave power of microwave drying is in this step 3000W; C, pulverized by the roxburgh anoectochilus terminal bud after microwave drying, roxburgh anoectochilus terminal bud after being pulverized adds drinkable solvent, and carries out ultrasonic wave extraction, and the roxburgh anoectochilus terminal bud stoste obtained is roxburgh anoectochilus terminal bud extract.
Further, the vacuum condition carrying out microwave drying in described step b is: vacuum is-75KPa ~-65KPa.
Further, the roxburgh anoectochilus terminal bud useful load of carrying out microwave drying in described step b is 300g ~ 400g.
Further, the initial moisture content of drying base in described tempering technique is 258%, and the tempering time is 208 minutes.
Further, the vacuum of carrying out the vacuum condition of microwave drying in described step b is-75KPa, and the useful load of roxburgh anoectochilus terminal bud is 300g.
Further, the drinkable solvent in described step c is the pure water made through anti-penetration water purifier, and the roxburgh anoectochilus terminal bud of described pulverizing and the solid-liquid ratio of this pure water are 1:15.
Further, the time that in described step c, ultrasonic wave extracts is 25 minutes, and temperature is 60 DEG C.
A preparation method for roxburgh anoectochilus terminal bud lemon fresh fruit health drink, comprises the steps: a, adopts the preparation method of above-mentioned roxburgh anoectochilus terminal bud extract to prepare roxburgh anoectochilus terminal bud extract; B, choose lemon fresh fruit, add water after cleaning peeling and squeeze the juice, the amount of water in juice-extracting process is the twice of lemon fresh fruit volume, the lemon after squeezing the juice and water mixed liquid is filtered afterwards, thus makes lemon juice; C, roxburgh anoectochilus terminal bud extract is fully mixed with lemon juice after, add sucrose and winter honey is allocated, namely can be made into above-mentioned roxburgh anoectochilus terminal bud lemon fresh fruit health drink, the volume proportion of described roxburgh anoectochilus terminal bud extract and lemon juice is 42:5 in this step, the concentration of described sucrose is 0.05g/mL, and the concentration of described winter honey is 0.02g/mL.
A preparation method for roxburgh anoectochilus terminal bud dried hawthorn health drink, comprises the steps: a, adopts the preparation method of above-mentioned roxburgh anoectochilus terminal bud extract to prepare roxburgh anoectochilus terminal bud extract; B, choose dried hawthorn, with emerge in worm water 20 minutes; C, being added water by soaked dried hawthorn decocts, and is decocting 20 times that the amount of water in process is dried hawthorn volume, through decoct concentrated after, when discharge reduction 3/4, can and obtained hawthorn concentrate; D, roxburgh anoectochilus terminal bud extract is fully mixed with hawthorn concentrate after, add sucrose and honey is allocated, namely can be made into above-mentioned roxburgh anoectochilus terminal bud dried hawthorn health drink, the volume proportion of described roxburgh anoectochilus terminal bud extract and hawthorn concentrate is 3.4:1 in this step, the concentration of described sucrose is 0.03g/mL, and the concentration of described honey is 0.06g/mL.
Compared to the prior art, the beneficial effect that the present invention produces is:
1, the present invention by by roxburgh anoectochilus terminal bud at microwave power be 3000W process conditions under carry out vacuum microwave drying, and in dry run, introduce tempering technique, the functional characteristic compositions such as polysaccharide, flavones and amino acid contained by making in dried roxburgh anoectochilus terminal bud and distinctive fragrance are retained effectively, pharmacological active substance great majority through extracting the roxburgh anoectochilus terminal bud extract drawn are retained, and be under the process conditions of 3000W at microwave power, in above-mentioned roxburgh anoectochilus terminal bud extract, the content of contained polysaccharide, general flavone and free amino acid is the highest.
2, in the present invention, can be adjusted to according to above-mentioned roxburgh anoectochilus terminal bud extract the Jewel orchid beverage that two kinds have different health-care efficacy.Wherein one is roxburgh anoectochilus terminal bud lemon health drink, promote the production of body fluid because lemon has, quench the thirst, the effect of driving away summer heat, hear lemon smell, people ambition can be made to unfold, in high spirits, add that the fresh winter honey of adjustment can play to moisten and trophism, this beverage can make that skin is fine and smooth, smooth, high resilience, and can promote digestion, improves immunity, has improving water flood, protects the liver effects such as being healthy and strong.Wherein another kind is roxburgh anoectochilus terminal bud dried hawthorn health drink, and this kind of beverage can help digestion long-pending, scattered silt blood, convergence only dysentery, and also have very many-sided pharmacological action to cardiovascular system, heat falls in appetizing, protects liver and supports spleen, have certain effect to cardiovascular.
Accompanying drawing explanation
Fig. 1 is the relation chart of roxburgh anoectochilus terminal bud extract addition and flavour mark mark in embodiment two.
Fig. 2 is the relation chart of lemon stoste addition and flavour mark mark in embodiment two.
Fig. 3 is the relation chart of winter honey addition and flavour mark mark in embodiment two.
Fig. 4 is the relation chart of sucrose addition and flavour mark mark in embodiment two.
Fig. 5 is the relation chart of roxburgh anoectochilus terminal bud extract addition and flavour mark mark in embodiment three.
Fig. 6 is the relation chart of hawthorn stoste addition and flavour mark mark in embodiment three.
Fig. 7 is the relation chart of honey addition and flavour mark mark in embodiment three.
Fig. 8 is the relation chart of sucrose addition and flavour mark mark in embodiment three.
Detailed description of the invention
Embodiment one
A preparation method for roxburgh anoectochilus terminal bud extract, comprises the following steps:
The first step, is undertaken washing by the roxburgh anoectochilus terminal bud chosen and dries to blade and wither, in this step roxburgh anoectochilus terminal bud preferably grow fine without disease and pest gold thread lotus leaf.
Second step, roxburgh anoectochilus terminal bud after drying is carried out microwave drying under vacuum, wherein in the process of microwave drying, introduce tempering technique, the microwave power of microwave drying is 3000W in this step, the vacuum condition carrying out microwave drying in this step is: vacuum is-75KPa ~-65KPa, the roxburgh anoectochilus terminal bud useful load of carrying out microwave drying in this step is 300g ~ 400g, described tempering technique process conditions be: initial moisture content of drying base is 258%, and the tempering time is 208 minutes.
3rd step, roxburgh anoectochilus terminal bud after microwave drying is pulverized, roxburgh anoectochilus terminal bud after being pulverized adds drinkable solvent, and carry out ultrasonic wave extraction, the roxburgh anoectochilus terminal bud stoste obtained is roxburgh anoectochilus terminal bud extract, and the drinkable solvent in this step is the pure water made through anti-penetration water purifier, and the roxburgh anoectochilus terminal bud of described pulverizing and the solid-liquid ratio of this pure water are 1:15, the time that ultrasonic wave extracts is 25 minutes, and temperature is 60 DEG C.
Now provide each parameter factor in microwave vacuum technique to test the impact analysis of roxburgh anoectochilus terminal bud leading indicator, microwave power (A), vacuum (B), useful load (C) three are larger on active ingredient impacts such as the very dried polysaccharide of roxburgh anoectochilus terminal bud, general flavones as the important technology index in roxburgh anoectochilus terminal bud micro-wave vacuum.Below the L9 (3 of microwave power, vacuum, the optimization of useful load Three factors 4) orthogonal experiment data.
Table 1 orthogonal test factor level
Level A microwave power (W) B vacuum (KPa) C useful load
1 2000 -65 200
2 3000 -75 300
3 4000 -85 400
The extreme difference of anoectochilus roxburghii polyose content and variance analysis:
Table 2L 9 (3 4) the orthogonal experiments table of polyoses content
Tested number A B C Empty row Polyoses content (mg/g)
1 2000 -65 200 1 12.432
2 2000 -75 300 2 15.213
3 2000 -85 400 3 11.281
4 3000 -65 300 3 20.068
5 3000 -75 400 1 16.903
6 3000 -85 200 2 20.890
7 4000 -65 400 2 9.775
8 4000 -75 200 3 17.874
9 4000 -85 300 1 18.483
K1 12.9753 13.4250 17.0653 15.8627
K2 18.6203 16.6633 17.1780 15.2927
K3 15.3007 16.8080 12.6530 15.7410
R 5.0843 3.0470 4.0755 0.5134
The analysis of variance table of table 3 polyoses content
Source of variation Quadratic sum The free degree All square F value Conspicuousness
Microwave rate A 48.2934 2 24.1467 89.3155 *
Vacuum B 21.9524 2 10.9762 40.5996 *
Useful load C 39.9570 2 19.9765 73.8979 *
Empty row 0.5407 2 0.2704
Error 05.407 2 0.2704
Summation 110.7435
The R value of A, B, C tri-factors in comparison sheet 2, can show that the secondary factors of polyoses content in dry product after affecting roxburgh anoectochilus terminal bud micro-wave vacuum is: A>C>B; F value [F in Integrated comparative table 3 0.05(2,2)=19.00, F 0.01(2,2)=99.00] compare, can it is evident that: microwave power A, useful load C, the vacuum B impact on polyoses content presents the level of signifiance, so, after acquisition roxburgh anoectochilus terminal bud micro-wave vacuum, polyoses content is the highest considers processing technology, and preferred process is: A 2b 2,3c 2, i.e. microwave rate 3000W, vacuum (-65 ,-75KPa) useful load 300g.
The extreme difference of general flavone content and variance analysis:
Table 4L 9 (3 4) the orthogonal experiments table of general flavone content
Tested number A B C Empty row General flavone content (mg/g)
1 2000 -65 200 1 13.871
2 2000 -75 300 2 13.134
3 2000 -85 400 3 12.053
4 3000 -65 300 3 18.486
5 3000 -75 400 1 17.012
6 3000 -85 200 2 17.453
7 4000 -65 400 2 15.020
8 4000 -75 200 3 15.942
9 4000 -85 300 1 16.998
K1 13.0193 15.7923 15.7553 15.96.3
K2 17.6503 15.3627 16.2060 15.2030
K3 15.9867 15.5013 14.6950 15.4937
R 4.1710 0.3870 1.3609 0.6827
The analysis of variance table of table 5 general flavone content
Source of variation Quadratic sum The free degree All square F value Conspicuousness
Microwave rate A 33.019 2 16.5095 37.6407 *
Vacuum B 0.2885 2 0.1443 0.3289 *
Useful load C 3.6105 2 1.8053 4.1159 *
Empty row 0.8772 2 0.4386
Error 0.8772 2 0.4386
Summation 37.7953
The R value of A, B, C tri-factors in comparison sheet 4, can show that the secondary factors of general flavone content in dry product after affecting roxburgh anoectochilus terminal bud micro-wave vacuum is: A>C>B; F value [F in Integrated comparative table 5 0.05(2,2)=19.00, F 0.01(2,2)=99.00] compare, can it is evident that: the impact of microwave power A on general flavone content presents the level of signifiance, and vacuum B and useful load C is on the difference of the impact of general flavone content without conspicuousness.So after acquisition roxburgh anoectochilus terminal bud micro-wave vacuum, flavones content is the highest considers processing technology, A 2b 1c 2.
The extreme difference of roxburgh anoectochilus terminal bud free aminoacid content and variance analysis:
Table 6L 9 (3 4) the orthogonal experiments table of amino acid content
Tested number A B C Empty row Amino acid content (mg/g)
1 2000 -65 200 1 79.979
2 2000 -75 300 2 85.156
3 2000 -85 400 3 77.011
4 3000 -65 300 3 116.54
5 3000 -75 400 1 129.775
6 3000 -85 200 2 113.865
7 4000 -65 400 2 96.307
8 4000 -75 200 3 109.155
9 4000 -85 300 1 92.483
K1 80.7153 97.6087 100.9997 100.7457
K2 120.060 108.0287 98.0597 98.4427
K3 99.3150 94.453 101.031 100.902
R 35.4364 12.2271 2.6762 2.2150
The analysis of variance table of table 7 amino acid content
Source of variation Quadratic sum The free degree All square F value Conspicuousness
Microwave rate A 2324.3054 2 1162.1527 204.3064 *
Vacuum B 302.8334 2 151.4167 26.619 *
Useful load C 17.4734 2 8.7367 1.5359 *
Empty row 11.3766 2 5.6883
Error 11.3766 2 5.6883
Summation 2655.9888
The R value of A, B, C tri-factors in comparison sheet 6, can show that the secondary factors of dry product Determination of Free Amino Acids after affecting roxburgh anoectochilus terminal bud micro-wave vacuum is: A>B>C; F value [F in Integrated comparative table 7 0.05(2,2)=19.00, F 0.01(2,2)=99.00] compare, can it is evident that: the impact of microwave power A on free aminoacid content presents the level of signifiance, and vacuum B has significant difference to free aminoacid content, and useful load C is without the difference of conspicuousness.So after acquisition roxburgh anoectochilus terminal bud micro-wave vacuum, free aminoacid content is the highest considers processing technology, and preferred process is: A 2b 2c 3,1.
In single factor experiment and orthogonal test, 3 parallel tests are carried out, test data is averaged, result shows: microwave power A has polyoses content, general flavone content and free aminoacid content after roxburgh anoectochilus terminal bud micro-wave vacuum significantly or extremely significantly to be affected, and optimum level is 3000W; Vacuum B affects significantly on polysaccharide after roxburgh anoectochilus terminal bud micro-wave vacuum and free aminoacid content, remarkable on general flavone content impact, can determine that optimum level is chosen as-75kPa; Useful load C on polyoses content impact after roxburgh anoectochilus terminal bud micro-wave vacuum significantly, affects general flavone and free aminoacid content remarkable, can determine that optimum level is chosen as 300g.
By orthogonal test, the Optimizing Technical of roxburgh anoectochilus terminal bud micro-wave vacuum is finally defined as: A 2b 2c 2, namely microwave power is 3000W, vacuum is-75kPa, useful load is 300g.
Embodiment two
The present embodiment relates to a kind of roxburgh anoectochilus terminal bud lemon health drink of the roxburgh anoectochilus terminal bud extract containing drawing in embodiment one, and this roxburgh anoectochilus terminal bud lemon health drink is prepared from under type:
The first step, adopts the preparation method of roxburgh anoectochilus terminal bud extract in embodiment one to prepare roxburgh anoectochilus terminal bud extract.
Second step, chooses lemon fresh fruit, and add water and squeeze the juice after cleaning peeling, the amount of water in juice-extracting process is the twice of lemon fresh fruit volume, the lemon after squeezing the juice and water mixed liquid is filtered afterwards, thus makes lemon juice.
3rd step, after roxburgh anoectochilus terminal bud extract is fully mixed with lemon juice, add sucrose and winter honey is allocated, namely can be made into above-mentioned roxburgh anoectochilus terminal bud lemon fresh fruit health drink, the volume proportion of described roxburgh anoectochilus terminal bud extract and lemon juice is 42:5 in this step, the concentration of described sucrose is 0.05g/mL, and the concentration of described winter honey is 0.02g/mL.Through the roxburgh anoectochilus terminal bud lemon health drink that said method is obtained, promote the production of body fluid because lemon has, quench the thirst, the effect of driving away summer heat, hear lemon smell, people ambition can be made to unfold, in high spirits, add that the fresh winter honey of adjustment can play to moisten and trophism, this beverage can make that skin is fine and smooth, smooth, high resilience, and can promote digestion, improves immunity, has improving water flood, protects the liver effects such as being healthy and strong.
Now provide each formula factors of roxburgh anoectochilus terminal bud lemon fresh fruit health drink to test the impact analysis of roxburgh anoectochilus terminal bud lemon fresh fruit health drink mouthfeel, roxburgh anoectochilus terminal bud extract (A), lemon juice (B), winter honey (C) and sucrose (D) four are larger as the impact of formula factors on roxburgh anoectochilus terminal bud lemon fresh fruit health drink mouthfeel of roxburgh anoectochilus terminal bud lemon fresh fruit health drink.Below the L9 (3 of roxburgh anoectochilus terminal bud extract (A), lemon juice (B), winter honey (C) and sucrose (D) this four factors optimization 4) orthogonal experiment data.
Lemon taste factor and level:
Table 8 factor and level
Level A roxburgh anoectochilus terminal bud extract/ml B lemon juice/ml C honey/(gml -1) D sucrose/(gml -1)
1 210 25 0.01 0.02
2 338 50 0.02 0.05
3 400 75 0.03 0.08
Carry out taste test by the preferendum sense organ of people, and give a mark according to following table.
Table 9 flavour mark standard (hundred-mark system)
Note: the full marks of local flavor, sweet taste, tart flavour, aftertaste are 25 points
Flavour mark standard (duplicate):
Mouthfeel degree of liking: the overall feeling of beverage; Sweet taste degree of liking: this sweet taste you like;
Tart flavour degree of liking: whether tart flavour is that you like; Aftertaste degree of liking: after drinking oral cavity throat impression OK.
Give a mark through human body evaluation:
21-25 Be delithted with 16-20 Like 11-15 Generally
6-10 Do not like 1-6 No good cake
Table 10L 9(3 4) orthogonal experiments
Tested number A B C D Score
1 1 1 1 1 46.5
2 1 2 2 2 48.5
3 1 3 3 3 72
4 2 1 1 3 61
5 2 2 2 1 57.3
6 2 3 3 2 64.3
7 3 1 1 2 72.6
8 3 2 2 3 67.3
9 3 3 3 1 65.6
K1 166.9 179.9 178.2 169.2
K2 182.9 202.2 201.9 200.3
K3 205.5 171.5 178.5 185.8
R 38.6 30.7 23.4 31.1
Fig. 1 is the relation chart of roxburgh anoectochilus terminal bud extract addition and flavour mark mark in the present embodiment, Fig. 2 is the relation chart of lemon stoste addition and flavour mark mark in the present embodiment, Fig. 3 is the relation chart of sucrose addition and flavour mark mark in the present embodiment, Fig. 4 is the relation chart of winter honey addition and flavour mark mark in the present embodiment, with reference to Fig. 1-Fig. 4, as above-mentioned experiment, summing up the best sugar-acid ratio formula of lemon taste roxburgh anoectochilus terminal bud is: roxburgh anoectochilus terminal bud extract 420ml+ lemon stoste 50ml+ sucrose 0.05g/mL+ winter honey 0.02g/mL.
Embodiment three
The present embodiment relates to a kind of roxburgh anoectochilus terminal bud dried hawthorn health drink of the roxburgh anoectochilus terminal bud extract containing drawing in embodiment one, and this roxburgh anoectochilus terminal bud dried hawthorn health drink is prepared from under type:
The first step, adopts the preparation method of roxburgh anoectochilus terminal bud extract in embodiment one to prepare roxburgh anoectochilus terminal bud extract.
Second step, chose dried hawthorn, with emerge in worm water 20 minutes.
3rd step, adds water soaked dried hawthorn and decocts, and is decocting 20 times that the amount of water in process is dried hawthorn volume, after decocting and concentrating, when discharge reduction 3/4, gets final product and obtained hawthorn concentrate.
4th step, after roxburgh anoectochilus terminal bud extract is fully mixed with hawthorn concentrate, add sucrose and honey is allocated, namely can be made into above-mentioned roxburgh anoectochilus terminal bud dried hawthorn health drink, described in this step, the volume proportion of roxburgh anoectochilus terminal bud extract and hawthorn concentrate is 3.4:1, the concentration of described sucrose is 0.03g/mL, and the concentration of described honey is 0.06g/mL.This kind of roxburgh anoectochilus terminal bud dried hawthorn health drink can help digestion long-pending, scattered silt blood, convergence only dysentery, and also have very many-sided pharmacological action to cardiovascular system, heat falls in appetizing, protects liver and supports spleen, have certain effect to cardiovascular.
Now provide each formula factors of roxburgh anoectochilus terminal bud dried hawthorn health drink to test the impact analysis of roxburgh anoectochilus terminal bud dried hawthorn health drink mouthfeel, roxburgh anoectochilus terminal bud extract (A), hawthorn concentrate (B), honey (C) and sucrose (D) four are larger as the impact of formula factors on roxburgh anoectochilus terminal bud dried hawthorn health drink mouthfeel of roxburgh anoectochilus terminal bud dried hawthorn health drink.Below the L9 (3 of roxburgh anoectochilus terminal bud extract (A), hawthorn concentrate (B), honey (C) and sucrose (D) this four factors optimization 4) orthogonal experiment data.
Table 11 factor and level
Level A roxburgh anoectochilus terminal bud Extract/ml B hawthorn concentrate /ml C honey/ (g·ml -1 ) D sucrose/ (g·ml -1 )
1 210 50 0.01 0.02
2 338 72 0.02 0.04
3 400 100 0.03 0.06
Table 12L 9(3 4) orthogonal experiments
Tested number A B C D Score
1 1 1 1 1 63
2 1 2 2 2 56
3 1 3 3 3 78.6
4 2 1 1 3 70.8
5 2 2 2 1 76.4
6 2 3 3 2 72.8
7 3 1 1 2 66.8
8 3 2 2 3 69
9 3 3 3 1 57.8
K1 197.6 200.7 204.8 197.2
K2 220 201.4 184.6 195.6
K3 193.6 209.2 221.8 218.4
R 26.4 8.6 37.2 22.8
Fig. 5 is the relation chart of roxburgh anoectochilus terminal bud extract addition and flavour mark mark in the present embodiment, Fig. 6 is the relation chart of hawthorn stoste addition and flavour mark mark in the present embodiment, Fig. 7 is the relation chart of sucrose addition and flavour mark mark in the present embodiment, Fig. 8 is the relation chart of honey addition and flavour mark mark in the present embodiment, with reference to Fig. 5-Fig. 8, and associative list 11 and table 12 result of the test known, during with appraisal result inspection target, the size order that affects of 4 factors is: honey > roxburgh anoectochilus terminal bud concentrate > sucrose > hawthorn concentrate.Analysis optimum formula is: A 2b 3c 3d 3, during roxburgh anoectochilus terminal bud extract 338ml+ hawthorn concentrate 100ml+ sucrose 0.03g/mL+ honey 0.06g/mL, mouthfeel is best.
Above are only the specific embodiment of the present invention, but design concept of the present invention is not limited thereto, all changes utilizing this design the present invention to be carried out to unsubstantiality, all should belong to the behavior of invading scope.

Claims (4)

1. a roxburgh anoectochilus terminal bud lemon fresh fruit health drink, it is characterized in that: formed by roxburgh anoectochilus terminal bud extract, lemon juice, sucrose and winter honey allotment, the volume proportion of described roxburgh anoectochilus terminal bud extract and lemon juice is 42:5, the concentration of described sucrose is 0.05g/mL, the concentration of described winter honey is 0.02g/mL, described roxburgh anoectochilus terminal bud extract adopts following steps to be prepared from, and a, is carried out washing by the roxburgh anoectochilus terminal bud chosen and dries to blade and wither; B, the roxburgh anoectochilus terminal bud after drying is carried out microwave drying under vacuum, wherein in the process of microwave drying, introduce tempering technique, the microwave power of microwave drying is in this step 3000W; C, pulverized by the roxburgh anoectochilus terminal bud after microwave drying, roxburgh anoectochilus terminal bud after being pulverized adds drinkable solvent, and carries out ultrasonic wave extraction, and the roxburgh anoectochilus terminal bud stoste obtained is roxburgh anoectochilus terminal bud extract.
2. a preparation method for roxburgh anoectochilus terminal bud lemon fresh fruit health drink, is characterized in that, comprises the steps: a, prepares roxburgh anoectochilus terminal bud extract: a1, carried out washing by the roxburgh anoectochilus terminal bud chosen and dry to blade and wither; A2, the roxburgh anoectochilus terminal bud after drying is carried out microwave drying under vacuum, wherein in the process of microwave drying, introduce tempering technique, the microwave power of microwave drying is in this step 3000W; A3, pulverized by the roxburgh anoectochilus terminal bud after microwave drying, roxburgh anoectochilus terminal bud after being pulverized adds drinkable solvent, and carries out ultrasonic wave extraction, and the roxburgh anoectochilus terminal bud stoste obtained is roxburgh anoectochilus terminal bud extract; B, choose lemon fresh fruit, add water after cleaning peeling and squeeze the juice, the amount of water in juice-extracting process is the twice of lemon fresh fruit volume, the lemon after squeezing the juice and water mixed liquid is filtered afterwards, thus makes lemon juice; C, roxburgh anoectochilus terminal bud extract is fully mixed with lemon juice after, add sucrose and winter honey is allocated, namely can be made into above-mentioned roxburgh anoectochilus terminal bud lemon fresh fruit health drink, the volume proportion of described roxburgh anoectochilus terminal bud extract and lemon juice is 42:5 in this step, the concentration of described sucrose is 0.05g/mL, and the concentration of described winter honey is 0.02g/mL.
3. a roxburgh anoectochilus terminal bud dried hawthorn health drink, it is characterized in that: allocated forming by roxburgh anoectochilus terminal bud extract, hawthorn concentrate, sucrose and honey, the volume proportion of described roxburgh anoectochilus terminal bud extract and hawthorn concentrate is 3.4:1, the concentration of described sucrose is 0.03g/mL, the concentration of described honey is 0.06g/mL, described roxburgh anoectochilus terminal bud extract adopts following steps to be prepared from, and a, is carried out washing by the roxburgh anoectochilus terminal bud chosen and dries to blade and wither; B, the roxburgh anoectochilus terminal bud after drying is carried out microwave drying under vacuum, wherein in the process of microwave drying, introduce tempering technique, the microwave power of microwave drying is in this step 3000W; C, pulverized by the roxburgh anoectochilus terminal bud after microwave drying, roxburgh anoectochilus terminal bud after being pulverized adds drinkable solvent, and carries out ultrasonic wave extraction, and the roxburgh anoectochilus terminal bud stoste obtained is roxburgh anoectochilus terminal bud extract.
4. a preparation method for roxburgh anoectochilus terminal bud dried hawthorn health drink, is characterized in that, comprises the steps: a, prepares roxburgh anoectochilus terminal bud extract: a1, carried out washing by the roxburgh anoectochilus terminal bud chosen and dry to blade and wither; A2, the roxburgh anoectochilus terminal bud after drying is carried out microwave drying under vacuum, wherein in the process of microwave drying, introduce tempering technique, the microwave power of microwave drying is in this step 3000W; A3, pulverized by the roxburgh anoectochilus terminal bud after microwave drying, roxburgh anoectochilus terminal bud after being pulverized adds drinkable solvent, and carries out ultrasonic wave extraction, and the roxburgh anoectochilus terminal bud stoste obtained is roxburgh anoectochilus terminal bud extract; B, choose dried hawthorn, with emerge in worm water 20 minutes; C, being added water by soaked dried hawthorn decocts, and is decocting 20 times that the amount of water in process is dried hawthorn volume, through decoct concentrated after, when discharge reduction 3/4, can and obtained hawthorn concentrate; D, roxburgh anoectochilus terminal bud extract is fully mixed with hawthorn concentrate after, add sucrose and honey is allocated, namely can be made into above-mentioned roxburgh anoectochilus terminal bud dried hawthorn health drink, the volume proportion of described roxburgh anoectochilus terminal bud extract and hawthorn concentrate is 3.4:1 in this step, the concentration of described sucrose is 0.03g/mL, and the concentration of described honey is 0.06g/mL.
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CN105315381A (en) * 2014-07-22 2016-02-10 漳州市亚热带园艺技术有限公司 Anoectochilus roxburghii polysaccharide extraction and preliminary purifying method and preparation method for oral liquid of anoectochilus roxburghii polysaccharide
CN104522470A (en) * 2015-01-12 2015-04-22 福建农林大学 Phedimus aizoon health-care beverage and method for making phedimus aizoon health-care beverage
CN105085696A (en) * 2015-07-13 2015-11-25 福建省亚热带植物研究所 Method for extracting Anoectochilus roxburghii polysaccharides
CN105495214A (en) * 2015-12-21 2016-04-20 武杰 Anoectochilus roxburghii (Wall.) Lindl and strawbaeery juice beverage and making method thereof
CN106262804A (en) * 2016-07-26 2017-01-04 福建省麟阳农业科技有限公司 A kind of preparation technology of Herba Anoectochili roxburghii ferment
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CN112816577A (en) * 2020-12-30 2021-05-18 联和东浩(厦门)药业有限公司 Detection and analysis method for active ingredients of anoectochilus formosanus
CN112587618A (en) * 2020-12-30 2021-04-02 联和东浩(厦门)药业有限公司 Method for separating anoectochilus formosanus total alkaloids from anoectochilus formosanus extract

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