CN103860425B - A kind of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream and preparation method thereof - Google Patents
A kind of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream and preparation method thereof Download PDFInfo
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Abstract
The invention belongs to cosmetic field, in particular to a kind of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream and preparation method thereof, this Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream comprises the raw material of following percentage by weight number meter, Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides 5-10%, wetting agent 8-12%, antiseptic 0.5-1%, antioxidant 0.5-1%, nourishing additive agent 2-4%, oiliness raw material 10-15%, thickening agent 1-2%, metal ion chelation agent 0.2-0.4%, nertralizer 0.2-0.4%, brightening agent 1-2%, anti-allergic agent 0.05-0.1%, Flos Rosae Rugosae quintessence oil 0.3-0.5%, surplus is deionized water.Through test, the total antioxidant capacity of this protective skin cream is better, after using three days continuously, skin moisture content increases by more than 230%, and skin collagen fiber content increases by more than 78%, and skin elasticity improves more than 235%, a kind of low price, the significant skin care item of cosmetic result.
Description
Technical field
The invention belongs to cosmetic field, particularly a kind of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream and preparation method thereof.
Background technology
Protective skin cream is a kind of cosmetics and skincare product spreading on face, is form natural sebum film at the epidermis of skin, keeps the skin wet and nutritional labeling to skin, can repair the damaged cell of epiderm skin simultaneously, improves the elasticity of skin, pliability and brightness.The kind of protective skin cream is a lot, and wherein Sargassum crude polysaccharides protective skin cream adds Sargassum crude polysaccharides composition, can provide moisturizing, antioxidation, the effects such as radioprotective, makes skin remain fine and smooth glossy.
Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) is subordinate to Sargassum, discontinuously arranged at China coast, is North Western Pacific distinctive warm temperate zone Sargassum.Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) fast growth, Biomass is large, and the important function risen in shallow-sea ecology environment, cause the concern of marine ecology scholar and Sargassum worker, be listed in the first-selected species of warm temperate zone marine eco-environment biological restoration and there is the cultivation Sargassum of good DEVELOPMENT PROSPECT.
Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) is not only the quality raw materials of algin industry, and be also widely used in industries such as medicine, food, feedstuff, organic fertilizers, commercial value is higher.Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides has the characteristic of good antioxidation, radioprotective, moisture retention etc., if people constantly can research and develop effect of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides, utilize the performance of its antioxidation, radioprotective, moisture retention etc., be developed to the protective skin cream with antioxidation, moisturizing and anti-ageing effect of waiting for a long time, open up the new application of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.).
Utilize Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides to prepare protective skin cream, existing document and report in not yet have described in.
Summary of the invention
The object of this invention is to provide a kind of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream, this protective skin cream can improve skin non-oxidizability, obvious Glycerin, increases skin elasticity, slows down skin aging.
Another object of the present invention is to provide a kind of preparation method of above-mentioned Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream.
Object of the present invention can be achieved through the following technical solutions:
A kind of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream, is characterized in that, comprise the raw material of following percentage by weight number meter:
Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides 5-10%, wetting agent 8-12%, antiseptic 0.5-1%, antioxidant 0.5-1%, nourishing additive agent 2-4%, oiliness raw material 10-15%, thickening agent 1-2%, metal ion chelation agent 0.2-0.4%, nertralizer 0.2-0.4%, brightening agent 1-2%, anti-allergic agent 0.05-0.1%, Flos Rosae Rugosae quintessence oil 0.3-0.5%, surplus is deionized water.
The preparation method of above-mentioned Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides is, Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) being immersed in mass concentration is 12-24 hour in the alcoholic solution of 75%, filters, dries; The Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) of oven dry and distilled water are soaked 2-4 hour according to the proportioning that weight ratio is 1:20-40, smashs post-heating to pieces to 85-95 DEG C and keep 1-2 hour, cooling, cross leaching filtrate, centrifugalize after filtrate heating is concentrated; Filter after ethanol precipitate with ethanol 24-28h, taking precipitate lyophilizing, obtain Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides.
Described wetting agent is the mixture of one or more in D-lactic acid sodium, propylene glycol, butanediol.Preferably, described wetting agent is the mixture of D-lactic acid sodium, propylene glycol, butanediol, and wherein, the weight ratio of D-lactic acid sodium, propylene glycol, butanediol is 2:1-2:1-2.
Described antiseptic is one or both the mixture in phenoxyethanol or Sang Pu K15; Preferably, described antiseptic is the mixture of phenoxyethanol and Sang Pu K15, and wherein, the weight ratio of phenoxyethanol and Sang Pu K15 is 1:1-2.
Described anti-allergic agent is one or both the mixture in water solublity a-bisabolol or glycyrrhizic acid dipotassium.Preferably, described anti-allergic agent is the mixture in water solublity a-bisabolol and glycyrrhizic acid dipotassium, and wherein, the weight ratio of water solublity a-bisabolol and glycyrrhizic acid dipotassium is 1:1-2.
Described nourishing additive agent is the mixture of one or more in ceramide, silk fibroin powder, Margarita hydrolyzed solution and polymerization almond protein.Preferably, described nourishing additive agent is the mixture of ceramide, silk fibroin powder, Margarita hydrolyzed solution and polymerization almond protein, and wherein, the weight ratio of described ceramide, silk fibroin powder, Margarita hydrolyzed solution and polymerization almond protein is 1-2:1-2:1:1.
Described oiliness raw material is one or both the mixture in Jojoba oil, isopropyl myristate (IPM).Preferably, described oiliness raw material is the mixture of Jojoba oil, IPM, and wherein, the weight ratio of Jojoba oil, IPM is 1:1-2.
Described antioxidant is red wine polyphenols.
Described metal ion chelation agent is left-handed VC.
Described nertralizer is triethanolamine.
Described brightening agent is one or both the mixture in Trenaxmine or vitamin B3.Preferably, described brightening agent is the mixture of Trenaxmine and vitamin B3, and wherein the weight ratio of Trenaxmine and vitamin B3 is 1:1-2.
Described thickening agent is one or both mixture of high molecular cellulose or HANSHENGJIAO.Preferably, described thickening agent is the mixture of high molecular cellulose and HANSHENGJIAO, and wherein, the weight ratio of high molecular cellulose and HANSHENGJIAO is 1:1-2.
The preparation method of above-mentioned Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream, its step comprises:
(1), by Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) being immersed in mass concentration is 12-24 hour in the alcoholic solution of 75%, filters, dries; The Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) of oven dry and distilled water are soaked 2-4 hour according to the proportioning that weight ratio is 1:20-40, smashs post-heating to pieces to 85-95 DEG C and keep 1-2 hour, cooling, cross leaching filtrate, centrifugalize after filtrate heating is concentrated; Filter after ethanol precipitate with ethanol 24-28h, taking precipitate lyophilizing, obtain Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides.
(2), various raw material has been weighed according to formula.
(3), by Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides adding in deionized water constantly to stir makes it swelling, dissolves under being heated to 70 DEG C of-75 DEG C of temperature; Oiliness raw material is heating for dissolving under 70 DEG C of-75 DEG C of conditions, then both mixing, emulsifying is stirred; Emulsion is cooled to 50-60 DEG C, adds wetting agent, antioxidant, antiseptic, anti-allergic agent, nourishing additive agent, metal ion chelation agent, nertralizer and brightening agent, stirs; Emulsion is cooled to 40-45 DEG C, adds tackifier, Flos Rosae Rugosae quintessence oil stirs.
In described step (1), the mass concentration of the alcoholic solution used by ethanol precipitate with ethanol is 70-75%.
Compared with prior art, beneficial effect of the present invention is:
1, described Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream can significantly improve skin antioxidation, moisturizing and defying age ability, and wherein, the total antioxidant capacity of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream is more than 36mM/g; Continuous use is after three days, and skin moisture content increases by more than 230%, and skin collagen fiber content increases by more than 78%, and skin elasticity improves more than 235%.
2, the preparation method of described Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream is simple, easy to operate, and raw material is easy to get, cost is low, low price, and the medicine added in preparation process does not only injure skin, and environmentally safe, green, environmental protection.
Accompanying drawing explanation
Fig. 1 is the FRAP method standard curve in embodiment 1.
Fig. 2 is the Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides emollient cream water content detection result in embodiment 1.
Fig. 3 is the Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides emollient cream collagen fabric testing result in embodiment 1.
Fig. 4 is the Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides emollient cream elastomeric check result in embodiment 1.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described:
Embodiment 1
(1) preparation of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides
Filter after the fresh Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) alcoholic solution (mass concentration is 75%) gathered is soaked 12 hours, dry, Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) after oven dry adds in distilled water, wherein, the amount ratio of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) and distilled water is 1g:20mL, by after the immersion Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) tissue mashing of 2 hours at 90 DEG C heated at constant temperature 1h, cooled and filtered; Filtrate is concentrated (it is 95% that filtrate is concentrated into water content) centrifugalize afterwards under 70 DEG C of heating, filters, obtain Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides after taking precipitate lyophilizing with after alcoholic solution (mass concentration is 75%) precipitate with ethanol 24h.
(2) preparation of protective skin cream
A, weigh (percentage by weight) according to following formula:
Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides: 10%;
Wetting agent: 10%(wherein, D-lactic acid sodium: 4%, propylene glycol: 3%, butanediol: 3%);
Antiseptic: 1%(wherein, phenoxyethanol: 0.5%, Sang Pu K15:0.5%);
Anti-allergic agent: 0.1%(wherein, water solublity a-bisabolol: 0.05%, glycyrrhizic acid dipotassium: 0.05%);
Nourishing additive agent: 4%(wherein, ceramide: 1%, silk fibroin powder: 1%, Margarita hydrolyzed solution: 1%, be polymerized almond protein: 1%);
Oiliness raw material: 15%(wherein, Jojoba oil: 10%, IPM:5%);
Red wine polyphenols: 0.5%;
The left-handed VC of metal ion chelation agent: 0.2%();
Nertralizer: 0.2%(triethanolamine);
Brightening agent: 2%(wherein, Trenaxmine: 1%, vitamin B3: 1%);
Thickening agent: 2%(wherein, high molecular cellulose: 1%, HANSHENGJIAO: 1%);
Flos Rosae Rugosae quintessence oil: 0.5%;
Surplus is deionized water.
B, Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides joined in deionized water constantly to stir and make it swelling, be heated to 70 DEG C of dissolvings; Both mixing, emulsifying, 70 DEG C of heating for dissolving, are then stirred by oiliness raw material; Emulsion is cooled to 50-60 DEG C, adds wetting agent, antioxidant, antiseptic, anti-allergic agent, nourishing additive agent, metal ion chelation agent, nertralizer and brightening agent, stirs 3 minutes; Emulsion is cooled to 40-45 DEG C, adds tackifier, Flos Rosae Rugosae quintessence oil stirs.
(3) testing result
A, total antioxidation are tested
Measure total antioxidant capacity by FRAP method, testing procedure is as follows:
By specification requires configuration FRAP working solution, hatches for 37 DEG C.Configuration 100mmol/LFeSO
4standard solution, and be diluted with distilled water into 0.15,0.3,0.6,0.9,1.2 and 1.5mmol/L.Take Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream 0.025g obtained in above-mentioned steps (2), add 0.4mL distilled water diluting and dissolve.180 microlitre FRAP working solutions are added in each detect aperture of 96 orifice plates.5 microlitre distilled water are added, if 4 repetitions in blank control wells; Add 5 microlitres respectively in standard curve detect aperture, concentration is the FeSO of 0.15,0.3,0.6,0.9,1.2 and 1.5mmol/L concentration
4standard solution, if 4 repetitions; 5 microlitre Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream samples are added, if 4 repetitions in sample detection hole; Mix gently.37 DEG C hatch 3-5 minute after record standard solution and Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream mean OD value at 595nm place, obtain standard curve: y=0.3745+0.004, specifically as shown in Figure 1.
1mmol/LFeSO is calculated according to standard curve
4the absorbance of standard solution is 0.3785, and Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream is at 595nm place mean OD value 0.3417, and total antioxidant capacity is: (0.3417/0.3785) mM/0.025g=36.11mM/g, the larger oxidation resistance of this numerical value is stronger.
B, moisturizing and defying age performance test
Before test, inside experimenter's arm of cleaning, and with wet gauze (with deionized water) scrub, water temperature is room temperature, measurement markers is carried out at experimenter's both hands inner forearm after cleaning, each test zone interval 1cm, often locating pilot region is 4cm*4cm, within before recipient site 2-3 days, can not use any cosmetic product; Experimenter sits quietly after 30min in room temperature environment, use capacitance method moisture of skin analyzer (SG-5D) to measure the moisture value in each region, measure skin collagen fiber content and elasticity indexes with 2,000,000 pixel CCD50X portable high-definition intelligent skin detection instrument (EH-800U).Afterwards by test products uniform application in arm trial zone, carry out measurement and the observation in tested region after 40min, each region parallel assay five times according to the order of sequence, draws meansigma methods.Tested region METHOD FOR CONTINUOUS DETERMINATION three days, every day measures and observes after product smears 40min.
After result display uses three days continuously, moisture increases by 232%, and specifically as shown in Figure 2, collagen fabric content increases by 78%, and specifically as shown in Figure 3, elasticity improves 237%, specifically as shown in Figure 4.
Embodiment 2
(1) preparation of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides is with embodiment 1.
(2) preparation of protective skin cream
A, weigh (percentage by weight) according to following formula:
Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides: 10%;
Wetting agent: 10%(wherein, D-lactic acid sodium: 6%, propylene glycol: 2%, butanediol: 2%);
Antiseptic: 0.5%(wherein, phenoxyethanol: 0.25%, Sang Pu K15:0.25%);
Anti-allergic agent: 0.1%(wherein, water solublity a-bisabolol: 0.05%, glycyrrhizic acid dipotassium: 0.05%);
Nourishing additive agent: 3%(wherein, ceramide: 1%, silk fibroin powder: 1%, Margarita hydrolyzed solution: 0.5%, be polymerized almond protein: 0.5%);
Oiliness raw material: 15%(wherein, Jojoba oil: 10%, IPM:5%);
Red wine polyphenols: 0.75%;
The left-handed VC of metal ion chelation agent: 0.3%();
Nertralizer: 0.2%(triethanolamine);
Brightening agent: 2%(wherein, Trenaxmine: 1%, vitamin B3: 1%);
Thickening agent: 2%(wherein, high molecular cellulose: 1%, HANSHENGJIAO: 1%);
Flos Rosae Rugosae quintessence oil: 0.5%;
Surplus is deionized water.
B, Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides joined in deionized water constantly to stir and make it swelling, be heated to 70 DEG C of dissolvings; Both mixing, emulsifying, 70 DEG C of heating for dissolving, are then stirred by oiliness raw material; Emulsion is cooled to 50-60 DEG C, adds wetting agent, antioxidant, antiseptic, anti-allergic agent, nourishing additive agent, metal ion chelation agent, nertralizer and brightening agent, stirs 3 minutes; Emulsion is cooled to 40-45 DEG C, adds tackifier, Flos Rosae Rugosae quintessence oil stirs.
(3) testing result
A, total antioxidation method of testing are with embodiment 1, and total antioxidant capacity is: 37.23mM/g.
B, moisturizing and defying age performance test methods with embodiment 1,
After test result display uses three days continuously, moisture increases by 241%, and collagen fabric content increases by 81%, and elasticity improves 235%.
In sum, by the display of above-mentioned detection data, the antioxidation of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream prepared by the present invention, moisturizing and defying age are very capable, are a kind of low price, the significant skin care item of cosmetic result.
The above is preferred embodiment of the present invention, but the present invention should not be confined to the content disclosed in this embodiment.The equivalence completed under not departing from spirit disclosed in this invention so every or amendment, all fall into the scope of protection of the invention.
Claims (9)
1. a Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream, is characterized in that, comprises the raw material of following percentage by weight number meter:
Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides 5-10%, wetting agent 8-12%, antiseptic 0.5-1%, antioxidant 0.5-1%, nourishing additive agent 2-4%, oiliness raw material 10-15%, thickening agent 1-2%, metal ion chelation agent 0.2-0.4%, nertralizer 0.2-0.4%, brightening agent 1-2%, anti-allergic agent 0.05-0.1%, Flos Rosae Rugosae quintessence oil 0.3-0.5%, surplus is deionized water;
Described Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides is prepared by the following method, and Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) being immersed in mass concentration is 12-24 hour in the alcoholic solution of 75%, filters, dries; The Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) of oven dry and distilled water are soaked 2-4 hour according to the proportioning that weight ratio is 1:20-40, smashs post-heating to pieces to 85-95 DEG C and keep 1-2 hour, cooling, cross leaching filtrate, centrifugalize after filtrate heating is concentrated; Filter after ethanol precipitate with ethanol 24-28h, taking precipitate lyophilizing, obtain Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides.
2. Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream according to claim 1, is characterized in that: described wetting agent is the mixture of one or more in D-lactic acid sodium, propylene glycol, butanediol.
3. Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream according to claim 1, is characterized in that: described antiseptic is one or both the mixture in phenoxyethanol or Sang Pu K15; Described anti-allergic agent is one or both the mixture in water solublity α-bisabolol or glycyrrhizic acid dipotassium.
4. Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream according to claim 1, is characterized in that: described nourishing additive agent is the mixture of one or more in ceramide, silk fibroin powder, Margarita hydrolyzed solution and polymerization almond protein.
5. Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream according to claim 1, is characterized in that: described oiliness raw material is one or both the mixture in Jojoba oil, isopropyl myristate; Described antioxidant is red wine polyphenols.
6. Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream according to claim 1, is characterized in that: described metal ion chelation agent is left-handed VC; Described nertralizer is triethanolamine; Described brightening agent is one or both the mixture in Trenaxmine or vitamin B3.
7. Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream according to claim 1, is characterized in that: described thickening agent is one or both mixture of high molecular cellulose or HANSHENGJIAO.
8. a preparation method for Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream as claimed in claim 1, its step comprises:
(1), by Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) being immersed in mass concentration is 12-24 hour in the alcoholic solution of 75%, filters, dries; The Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) of oven dry and distilled water are soaked 2-4 hour according to the proportioning that weight ratio is 1:20-40, smashs post-heating to pieces to 85-95 DEG C and keep 1-2 hour, cooling, cross leaching filtrate, centrifugalize after filtrate heating is concentrated; Filter after ethanol precipitate with ethanol 24-28h, taking precipitate lyophilizing, obtain Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides;
(2), various raw material has been weighed according to formula;
(3), by Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides adding in deionized water constantly to stir makes it swelling, dissolves under being heated to 70 DEG C of-75 DEG C of temperature; Oiliness raw material is heating for dissolving under 70 DEG C of-75 DEG C of conditions, then both mixing, emulsifying is stirred; Emulsion is cooled to 50-60 DEG C, adds wetting agent, antioxidant, antiseptic, anti-allergic agent, nourishing additive agent, metal ion chelation agent, nertralizer and brightening agent, stirs; Emulsion is cooled to 40-45 DEG C, adds thickening agent, Flos Rosae Rugosae quintessence oil stirs.
9. the preparation method of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) crude polysaccharides protective skin cream according to claim 8, is characterized in that: in described step (1), the mass concentration of the alcoholic solution used by ethanol precipitate with ethanol is 70-75%.
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| CN105919868A (en) * | 2016-06-01 | 2016-09-07 | 合肥丰瑞隆生物科技有限公司 | Black fungus crude polysaccharide skin care product and preparation method thereof |
| CN105902442A (en) * | 2016-06-01 | 2016-08-31 | 合肥丰瑞隆生物科技有限公司 | Cordyceps militaris crude polysaccharide skin-care product and preparation method thereof |
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| CN106074232A (en) * | 2016-06-01 | 2016-11-09 | 合肥丰瑞隆生物科技有限公司 | Pleurotus eryngii crude polysaccharides skin care item and preparation method thereof |
| CN105919869A (en) * | 2016-06-01 | 2016-09-07 | 合肥丰瑞隆生物科技有限公司 | Cordyceps militaris mud mask and preparation method thereof |
| CN105902480A (en) * | 2016-06-01 | 2016-08-31 | 合肥丰瑞隆生物科技有限公司 | Chanterelle paste mask and preparation method thereof |
| CN105902479A (en) * | 2016-06-01 | 2016-08-31 | 合肥丰瑞隆生物科技有限公司 | Toadstool sludge mask and preparation method thereof |
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