CN104138346B - A kind of anti-wrinkle cosmetic composition and preparation method thereof - Google Patents

A kind of anti-wrinkle cosmetic composition and preparation method thereof Download PDF

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CN104138346B
CN104138346B CN201410386230.6A CN201410386230A CN104138346B CN 104138346 B CN104138346 B CN 104138346B CN 201410386230 A CN201410386230 A CN 201410386230A CN 104138346 B CN104138346 B CN 104138346B
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extract
phase
wrinkle
cosmetic composition
wrinkle cosmetic
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CN104138346A (en
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赖洪宣
程传深
冯文华
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GUANGZHOU BESE CLEAN COSMETICS MANUFACTURER CO Ltd
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GUANGZHOU BESE CLEAN COSMETICS MANUFACTURER CO Ltd
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Abstract

The invention provides a kind of anti-wrinkle cosmetic composition and preparation method thereof, described anti-wrinkle cosmetic composition includes C phase and D phase, wherein C phase contains by weight percentage: Narcissus Tazetta L. Var extract 0.5 ~ 1%, Noni extract 0.5 ~ 2%, gooseberry extract 0.5 ~ 2%, Aesculus hippocastanum L. extract 0.5 ~ 2%, Cranberry extract 1 ~ 4%, oat extract 1 ~ 4% and monkey-bread tree extract 2 ~ 8%, and D phase contains by weight percentage: conventional cosmetic additive 82 ~ 94%;Anti-wrinkle cosmetic composition of the present invention is that natural material prepares, after trier is on probation, skin elasticity substantially increases, the highest increase by 40.84%, minimum increase by 21.75%, and trier's skin texture degree is decreased obviously, the highest decline 43.05%, minimum decline 34.77%, anti-wrinkle cosmetic of the present invention is elastic to human body skin, the improvement of texture all has good effect, is a cosmetics with excellent anti-wrinkle effect.

Description

A kind of anti-wrinkle cosmetic composition and preparation method thereof
Technical field
The present invention relates to a kind of cosmetics and preparation method thereof, particularly to a kind of improvement anti-wrinkle cosmetic composition and Its preparation method.
Background technology
Saying from biologically, aging is the most spontaneous biological necessary process, and it is the naturally existing of complexity As, its degeneration showing as structure and the decline of function.The appearance of wrinkle, is the notable performance of human senility.Except nature Beyond physiologic factor, human skin aging situation also with extended sleep quality, ultraviolet irradiation, working environment, living habit, battalion Support the factors such as situation and skin care relevant.
1956, it is theoretical that Englishman D.Harman proposes free radical theory.This theory is thought: the aging of cell is intracellular There is the result that in chemical reaction process, harmful substance is piled up.The metabolic processes of human body can constantly produce with the most right Claiming atom or the molecule of electronics, this atom with asymmetric electronics or molecule are referred to as free radical (chemical particle).Freely Base is badly in need of grabbing the electronics of pairing from other atom or molecule, thus its chemical reaction is very competent.Under normal circumstances, Free radical in human body is among the dynamic equilibrium that constantly produces and eliminate.If free radical produces too much or removed Slowly, it will unsaturated fatty acids acid reaction in attack cells film, mitochondrial membrane, with film, form lipid peroxide, cause lipid Peroxidating strengthens.Lipid peroxidation product can be analyzed to more free radical, causes the chain reaction of free radical.So membrane structure Integrity destroyed, cause brain cell, muscle cell, hepatocyte and subcellular structure, mitochondrion, DNA, RNA etc. wide General damage, accelerates the aging of body, until causing body dead.
Under normal circumstances, though producing free radical in human body body, but can be destroyed by internal enzyme system rapidly, Bu Huizao Become infringement.
Intracellular free radicals is removed mainly by antioxidation, and every polyphenoils all can be described as free radical scavenging Agent.The main mechanism of free radical scavenger is: directly provides electronics to make radical reduction, strengthens activities of antioxidant enzymes, from And eliminate rapidly free radical.
At present, common anti-aging cosmetics is vitamins and the big class of enzyme two, but some vitamin and enzyme pair Human body has certain side effect, the safest.In recent years, research finds the extract obtained from natural plants, both has The highest safety, has again good anti-aging effects.
Summary of the invention
It is an object of the invention to overcome the defect of prior art, it is provided that the anti-wrinkle cosmetic composition of a kind of improvement and Its preparation method.
For solving above-mentioned technical problem, the present invention adopts the following technical scheme that
Described anti-wrinkle cosmetic composition includes C phase and D phase, and wherein C phase contains by weight percentage: Narcissus Tazetta L. Var carries Take thing 0.5 ~ 1%, Noni extract 0.5 ~ 2%, gooseberry extract 0.5 ~ 2%, Aesculus hippocastanum L. extract 0.5 ~ 2%, cranberry Extract 1 ~ 4%, oat extract 1 ~ 4% and monkey-bread tree extract 2 ~ 8%, D phase contains by weight percentage: conventional cosmetic Product additive 82 ~ 94%;
Further, described conventional cosmetic additive is surfactant (0 ~ 4%), binding agent (0.1 ~ 1%), wetting agent The mixture of one or more in (1 ~ 30%) and preservative (0.1 ~ 0.5%).
Further, described surfactant is lecithin, cetearyl glucoside, sorbitan stearate, polyoxy One in ethylene Span60.
Further, the one during described binding agent is card ripple, xanthan gum, carrageenan.
Further, the one during described wetting agent is glycerol, propylene glycol, hyaluronic acid, trehalose.
Further, described preservative is methyl hydroxybenzoate, propylparaben, Methylisothiazolinone, double imidazolidinyl One in urea.
Further, described anti-wrinkle cosmetic composition also includes A phase and B phase, and A phase contains by weight percentage: Water 88.5%, EDTA disodium 0.1% and glycerol 5%;B phase contains by weight percentage: methyl hydroxybenzoate 0.1%.
Further, described anti-wrinkle cosmetic composition also includes A phase and B phase, and A phase contains by weight percentage: Water 54.3%, EDTA disodium 0.1%, glycerol 5% and xanthan gum 0.2%;B phase contains by weight percentage: cetearyl glucose Glycosides 2%, iso-octyl palmitate 5%, caprylic/capric triglyceride 5%, cetostearyl alcohol 3%, dimethicone 2% and methyl hydroxybenzoate 0.1%。
Further, described anti-wrinkle cosmetic composition also includes A phase, B phase and E phase, and A phase contains by weight percentage Have: water 81.5%, EDTA disodium 0.1%, card ripple 0.5% and glycerol 5%;B phase contains by weight percentage: methyl hydroxybenzoate 0.1%;E phase contains by weight percentage: triethanolamine 0.1%.
Another technical problem that the invention solves the problems that is to provide the preparation method of a kind of anti-wrinkle cosmetic composition.
For solving above-mentioned technical problem, the present invention adopts the following technical scheme that and comprises the following steps:
Comprise the following steps: above-mentioned plant extract is provided according to the present invention with cosmetics additive customary in the art Ratio carry out mixing both available described anti-wrinkle cosmetics.
A kind of anti-wrinkle cosmetic composition of the present invention provides the benefit that: prepared by the material of pure natural, and trier tries out Rear skin elasticity substantially increases, the highest increase by 40.84%, minimum increase by 21.75%, and trier's skin texture degree is decreased obviously, The highest decline 43.05%, minimum decline 34.77%, anti-wrinkle cosmetic of the present invention is elastic to human body skin, the improvement of texture all has very Good effect, is a cosmetics with excellent anti-wrinkle effect.
Detailed description of the invention
Do below by way of a kind of anti-wrinkle cosmetic composition that the present invention is provided by detailed description of the invention and preparation method thereof More detailed description further.
Correlation test
One, skin elasticity method of testing
(1) anti-wrinkle cosmetic of the present invention is taken.
(2) selecting the left and right inboard arm of experimenter is Test sites at palm base portion 10 centimeters.
(3) first skin elasticity tester (Cutometer dual MPA580) determination experiment portion is used by technical staff The skin elasticity numerical value before cosmetics is smeared in position, surveys five times, averages for every.
(4) experimenter smears sample at left arm Test sites, and every day smears twice sooner or later, and right arm Test sites is right According to, not swab.During experiment, experimenter can not smear other cosmetics any at Test sites.
(5) experimenter is behind make continuously to apply some make up one week, two weeks, three weeks, surrounding, five weeks, six weeks, seven weeks and eight weeks, Use skin elasticity tester (Cutometer dual MPA580) test skin elasticity numerical value.
(6) experimenter will smear position and clean, tester use skin elasticity tester (Cutometer dual MPA580) mensuration smears the elastic numerical value at position, surveys five times, averages for every.
(7) numerical value that statistics subject position records every time, analyzes its skin elasticity Changing Pattern, so that it is determined that anti- Effect that skin elasticity is improved by cosmetics.
Two, skin texture degree method of testing
(1) anti-wrinkle cosmetic of the present invention is taken.
(2) selecting the left and right inboard arm of experimenter is Test sites at palm base portion 10 centimeters.
(3) first skin image is used to analyze system (Skin Visiometer SV600) determination experiment by technical staff The skin texture degree before cosmetics is smeared at position, surveys five times, averages for every.
(4) experimenter smears sample at left arm Test sites, and every day smears twice sooner or later, and right arm Test sites is right According to, not swab.During experiment, experimenter can not smear other cosmetics any at Test sites.
(5) experimenter is behind make continuously to apply some make up one week, two weeks, three weeks, surrounding, five weeks, six weeks, seven weeks and eight weeks, Skin image is used to analyze system (Skin Visiometer SV600) test skin texture degree.
(6) experimenter will smear position and clean, tester use skin image to analyze system (Skin Visiometer SV600) mensuration smears the skin texture degree at position, surveys five times, averages for every.
(7) numerical value that statistics subject position records every time, analyzes its skin texture Changing Pattern, so that it is determined that anti- Effect that skin texture is improved by cosmetics.
Three, the crease-resistant experiment of human body skin
The crease-resistant experiment of human body skin is test anti-wrinkle effect most straightforward approach.
Under the guidance of technical staff, tested crowd use cosmetics, then use skin elasticity tester (Cutometer dual MPA580) measures the elastic change in value situation smearing position.
(1) anti-wrinkle cosmetic of the present invention is taken.
(2) selecting experimenter's inboard arm is Test sites at palm base portion 10 centimeters.
(3) sample is smeared at experimenter's inboard arm position, and every day smears twice sooner or later, and the photo before smearing is comparison.Real Testing period, experimenter can not smear other cosmetics any at Test sites.
(4) experimenter continuously use anti-wrinkle cosmetic one week, two weeks, three weeks, surrounding, five weeks, six weeks, seven weeks and eight weeks After, contrast with skin elasticity numerical value before and after using anti-wrinkle cosmetic of the present invention.
(5) numerical value that statistics subject position records every time, analyzes its skin elasticity Changing Pattern, to evaluate its skin Skin Flexible change situation.
Test population: the mean age is the person 20 that has wrinkle in 35-45 year.Wherein, male 8, female 12, skin health Not damaged.
The test result that skin elasticity is changed by the anti-wrinkle cosmetic that the present invention provides, is shown in Table 1.
Table 1 skin elasticity variation tendency
Under the guidance of technical staff, tested crowd use cosmetics, then use skin image to analyze system (Skin Visiometer SV600) measure the texture situation of change smearing position.
(1) anti-wrinkle cosmetic of the present invention is taken.
(2) selecting experimenter's inboard arm is Test sites at palm base portion 10 centimeters.
(3) sample is smeared at experimenter's inboard arm position, and every day smears twice sooner or later, and the photo before smearing is comparison.Real Testing period, experimenter can not smear other cosmetics any at Test sites.
(4) experimenter continuously use anti-wrinkle cosmetic one week, two weeks, three weeks, surrounding, five weeks, six weeks, seven weeks and eight weeks After, contrast with skin texture degree before and after using anti-wrinkle cosmetic of the present invention.
(5) numerical value that statistics subject position records every time, analyzes its skin texture degree Changing Pattern, to evaluate it Wrinkle of skin situation of change.
Test population: the mean age is the person 20 that has wrinkle in 35-45 year.Wherein, male 8, women 12, skin is good for Health not damaged.
The test result that skin texture degree is changed by the anti-wrinkle cosmetic that the present invention provides, is shown in Table 2.
Table 2 skin texture degree variation tendency
Experimenter 0 week 1 week 2 weeks 3 weeks 4 weeks 5 weeks 6 weeks 7 weeks 8 weeks Changing value Rate of change (%)
No. 1 53.6 52.3 49.5 44.8 42.1 41.4 37.6 34.9 32.1 -21.5 -40.11
No. 2 52.1 51 48.5 45.1 42.5 40.1 37.5 35.1 32.5 -19.6 -37.62
No. 3 56.3 54.9 51.7 49.5 45.7 43.9 40.1 37.9 35.6 -21.7 -38.54
No. 4 48.6 47.5 44.1 40.6 39.1 37.7 34.2 31.7 30.2 -19.4 -39.92
No. 5 50.8 49.5 45.8 43.2 40.5 37.8 35.1 32.4 29.7 -21.1 -41.54
No. 6 53.5 52.3 48.7 46.2 43.5 41 38.3 35.8 33.1 -20.4 -38.13
No. 7 55.3 53.8 50 47.2 44.3 41.4 38.5 35.7 32.8 -22.5 -40.69
No. 8 54.8 53.4 49.8 47.1 44.3 41.6 38.9 37.2 34.4 -21.4 -39.05
No. 9 49.5 48.4 45.1 42.7 40.3 37.9 35.4 33.1 30.6 -18.9 -38.18
No. 10 51.6 50.4 47.8 46.3 41.6 40.1 36.4 33.9 31.2 -20.4 -39.53
No. 11 52.7 50.3 47.6 44.9 42.1 39.4 36.6 33.9 32.7 -21.6 -40.99
No. 12 54.5 52 49.2 46.4 43.5 42.7 37.8 35 32.1 -22.4 -41.1
No. 13 52.9 50.7 48.1 45.6 43.9 40.4 37.7 35.2 32.5 -20.4 -38.56
No. 14 55.6 53 50.1 47.2 44.2 43.2 38.2 35.3 34.3 -23.3 -41.91
No. 15 53.4 51.3 48.8 45.4 43.8 42.4 38.8 37.4 33.8 -19.6 -36.7
No. 16 55.7 53.2 48.4 47.6 44.7 41.8 38.9 36.1 33.2 -22.5 -40.39
No. 17 53.2 50.6 46.8 44.9 43 39.1 34.1 33.3 31.3 -22.9 -43.05
No. 18 52.8 49.5 47.9 45.3 43.2 42.9 37.2 34.6 31.9 -20.9 -39.58
No. 19 50.6 48.3 45.7 43.1 39.4 36.8 35.1 32.5 29.8 -20.8 -41.11
No. 20 53.2 51.2 48.9 47.6 44.2 40.8 39.4 38.1 36.7 -18.5 -34.77
Meansigma methods 53.0 51.2 48.1 45.5 42.8 40.6 37.3 35.0 32.5 -20.99 -39.57
As it can be seen from table 1 after using this anti-wrinkle cosmetic 8 weeks, subjects skin is elastic substantially to be increased, minimum increase 21.75%, the highest increase by 40.84%, subjects skin's average elastic increase by 32.04%.
From table 2 it can be seen that after using this anti-wrinkle cosmetic 8 weeks, subjects skin's texture is decreased obviously, the most lowly Fall 34.77%, the highest decline 43.05%, experimenter's texture averagely declines 39.57%.
Summary experimental result is visible, and anti-wrinkle cosmetic of the present invention is elastic to human body skin, the improvement of texture all has very Good effect, is the obvious anti-wrinkle cosmetic of a effect.
Embodiment 1:
The raw material chosen accordingly and percentage by weight are shown in Table 3, and preparation process is as follows:
A phase and B are added in water preparation pot, stir, heated and stirred to 80 ~ 85 degree;
It is incubated 20 minutes;
Open cooling water temperature;
Cooling to 45 ~ 50 degree, addition C phase, D phase stir;
Stir 10 minutes, detect qualified rear discharging.
Table 3: raw material and percentage by weight
Embodiment 2:
The raw material chosen accordingly and percentage by weight are shown in Table 4, and preparation process is as follows:
A is added to aqueous phase pot, stirs, heated and stirred to 80 ~ 85 degree;
B is added in oil phase pot, stirs, heated and stirred to 80 ~ 85 degree;
By in material suction emulsifying pot in aqueous phase pot, by material suction emulsifying pot in oil phase pot, stir, then By evacuation in emulsifying pot, emulsifying 8 minutes;
It is incubated 20 minutes, then opens cooling water temperature to 45 ~ 50 degree;
Add C phase, D phase, stir, stir 10 minutes, detect qualified rear discharging.
Table 4: raw material and percentage by weight
Embodiment 3:
The raw material chosen accordingly and percentage by weight are shown in Table 5, and preparation process is as follows:
A phase and B being added in water preparation pot, stir, heated and stirred to 80 ~ 85 degree is also incubated 20 minutes;
Open cooling water temperature to 65 ~ 70 degree, add C phase, stir;
Cool to 45 ~ 50 degree, add D phase and E phase, stir, stir 10 minutes, detect qualified rear discharging.
Table 5: raw material and percentage by weight
Above in association with most preferred embodiment, invention has been described, but the invention is not limited in enforcement disclosed above Example, and simple modification, the equivalent combinations that the various essence according to the present invention is carried out should be contained.

Claims (1)

1. an anti-wrinkle cosmetic composition, it is characterised in that described anti-wrinkle cosmetic composition includes C phase and D phase, wherein C Contain by weight percentage mutually: Narcissus Tazetta L. Var extract 0.5 ~ 1%, Noni extract 0.5 ~ 2%, gooseberry extract 0.5 ~ 2%, Aesculus hippocastanum L. extract 0.5 ~ 2%, Cranberry extract 1 ~ 4%, oat extract 1 ~ 4% and monkey-bread tree extract 2 ~ 8%, D phase contains by weight percentage: conventional cosmetic additive 82 ~ 94%, and described conventional cosmetic additive is to live in surface The mixture of one or more in property agent 0 ~ 4%, binding agent 0.1 ~ 1%, wetting agent 1 ~ 30% and preservative 0.1 ~ 0.5%, described Surfactant is lecithin, cetearyl glucoside, sorbitan stearate, polyoxyethylene sorbitan stearate In one, described binding agent is the one in card ripple, xanthan gum, carrageenan, and described wetting agent is glycerol, propylene glycol, transparent One in matter acid, trehalose, described preservative is methyl hydroxybenzoate, propylparaben, Methylisothiazolinone, double imidazolidine One in base urea, described anti-wrinkle cosmetic composition also includes A phase, B phase and E phase, and A phase contains by weight percentage: Water 81.5%, EDTA disodium 0.1%, card ripple 0.5% and glycerol 5%;B phase contains by weight percentage: methyl hydroxybenzoate 0.1%;E Containing by weight percentage mutually: triethanolamine 0.1%, the preparation method of described anti-wrinkle cosmetic composition comprises the following steps: Above-mentioned plant extract is carried out mixing both available described with cosmetics additive customary in the art according to the ratio provided Anti-wrinkle cosmetic.
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