CN107625685A - A kind of antiultraviolet anti-wrinkle cosmetic and preparation method thereof - Google Patents
A kind of antiultraviolet anti-wrinkle cosmetic and preparation method thereof Download PDFInfo
- Publication number
- CN107625685A CN107625685A CN201710940964.8A CN201710940964A CN107625685A CN 107625685 A CN107625685 A CN 107625685A CN 201710940964 A CN201710940964 A CN 201710940964A CN 107625685 A CN107625685 A CN 107625685A
- Authority
- CN
- China
- Prior art keywords
- parts
- preparation
- centrifuge
- wrinkle cosmetic
- antiultraviolet
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Abstract
The invention discloses a kind of preparation method of antiultraviolet anti-wrinkle cosmetic, and camellia, yellow chamomile and Ginkgo biloba leaves are dried and are crushed to 120 200 mesh, forms compound；Lauryl sodium sulfate, isopropyl mercaptan and ethylene glycol salicylate are mixed, when temperature to be heated is to 60 80 DEG C, compound is added thereto, in 40 45 DEG C of 3h of impregnation 1；Above-mentioned solution is put into centrifuge and centrifuges 30 40min, takes the supernatant after centrifugation to add isometric pH=7.0 7.3 liquor kalii acetici, places 10 20min, be then placed again into centrifuge and centrifuge 20 30min, take supernatant standby；Polyoxyethylene sorbitan stearate, propane diols, double imidazolidinyl urea, Phenylbenzimidazolesulfonic acid, lauroyl sarcosine isopropyl ester and gained supernatant are mixed, in 90 110 DEG C of temperature with the 50min of 3000 4000r/min stirring reactions of speed 30；It can obtain the antiultraviolet anti-wrinkle cosmetic after cooling.
Description
Technical field
The invention belongs to cosmetic field, more particularly to a kind of antiultraviolet anti-wrinkle cosmetic and preparation method thereof.
Background technology
Crossing strong ultraviolet radiation most directly influences to be the gradual blackening of skin.Because ultraviolet causes a large amount of melanin
It is deposited in epidermis, causes permanent blackening, vestige is not easy to take off；With the passing of time skin senescence can be accelerated.Ultraviolet injury is not only
Outermost Skin Cell is only destroyed, dermal cell is reached by epidermis, causes a large amount of necrosis of dermal cell and metabolic disorder, carefully
Intracellular impurity can not be metabolized away, make skin sunburn occur, lost elasticity, aging ahead of time, become sensitive, wrinkle occur, heavier
What is wanted is that shouting pain itch unbearably, scratches bleeding, the disease-resistant and resistivity decrease of skin in itself, or even oedema after skin injury,
Ooze out.Form the skin disease that epifolliculitis, furuncle etc. is difficult to cure.The reason for human skin aging 90%%, comes from ultraviolet.But,
What is most attracted people's attention is that excessive ultraviolet irradiation easily induces cutaneum carcinoma.
With the development of science and technology and people's living standards continue to improve, people increasingly focus on quality of life, love
The heart of U.S., owned by everyone, everybody thirsts for keeping young, and full and young appearance adds the self-confident and sharp of people's life
Feelings, therefore, appearance resides permanently to be occupied more and more important as the pursuit of increasing people, anti-wrinkle cosmetic in people live
Position.Known ultraviolet be roughly divided into UV-A (wavelength is 320nm~400nm), UV-B (wavelength is 280nm~320nm) and
UV-C (wavelength is 190nm~280nm), the ultraviolet of any wavelength can cause the deterioration of skin.As protect skin not by
The method of uv damage, there is masking ultraviolet and ultraviolet light splitting is absorbed into this 2 kinds of methods.Side as masking ultraviolet
Method, the use of the inorganic particles such as titanium oxide, zinc oxide can be included.In addition, as the method that ultraviolet is divided to absorption, can arrange
The use of organic uv absorbers is enumerated, as organic uv absorbers, such as commonly known tert-butoxy benzoyl
Methane etc..But in the prior art there has been no the cosmetics for being provided simultaneously with good antiultraviolet and wrinkle resistance, and exist anti-
Ultraviolet and wrinkle resistance can not Synchronous lifting the deficiencies of.
The content of the invention
For drawbacks described above, it is an object of the invention to provide a kind of antiultraviolet anti-wrinkle cosmetic and preparation method thereof, leads to
Addition multiple additives are crossed, change proportionate relationship between each component of cosmetics, the UV resistance of cosmetics is greatly improved and resists
Wrinkle performance, meets the growing diversification material requisite of people.
A kind of preparation method of antiultraviolet anti-wrinkle cosmetic, is comprised the following steps：
S1：15-20 parts camellia, 10-15 parts yellow chamomile and 20-30 part Ginkgo biloba leaves are dried and are crushed to 120-200
Mesh, form compound；
S2：4-7 parts lauryl sodium sulfate, 10-15 parts isopropyl mercaptan and 10-20 parts ethylene glycol salicylate are mixed and stirred
Mix, when temperature to be heated is to 60-80 DEG C, compound described in step S1 is added thereto, in 40-45 DEG C of impregnation 1-3h；
S3：The solution obtained in step S2 is put into centrifuge and centrifuges 30- in the case where rotating speed is 2500-3000r/min
40min, take the supernatant after centrifugation to add isometric pH=7.0-7.3 liquor kalii acetici, place 10-20min, then again
It is put into centrifuge and centrifuges 20-30min in the case where rotating speed is 3000-4000r/min, takes supernatant standby；
S4：By 8-10 part polyoxyethylene sorbitans stearate, 10-20 parts propane diols, the double imidazolidinyls of 5-8 parts
Gained supernatant mixing in urea, 4-9 parts Phenylbenzimidazolesulfonic acid, 10-15 part lauroyl sarcosine isopropyl esters and S3, in temperature
90-110 DEG C of degree is with speed 3000-4000r/min stirring reactions 30-50min；The antiultraviolet is can obtain after cooling to resist
Cosmetics.
Preferably, 18 parts of camellias described in step S1,13 portions of yellow chamomiles and 26 parts of Ginkgo biloba leaves are dried and are crushed to
130-140 mesh.
Preferably, 6 parts of lauryl sodium sulfate described in step S2,12 parts of isopropyl mercaptans and 18 parts of ethylene glycol salicylates
Mix.
Preferably, when temperature to be heated is to 73 DEG C in step S2, compound described in step S1 is added thereto, in 42 DEG C of leachings
Stain reacts 2.5h.
Preferably, it is put into step S3 in centrifuge and centrifuges 37min in the case where rotating speed is 2800r/min, is taken upper after centrifugation
Clear liquid adds isometric pH=7.1 liquor kalii acetici, places 18min, and it is 3500/ to be then placed again into centrifuge in rotating speed
25min is centrifuged under min.
Preferably, by 9 parts of polyoxyethylene sorbitan stearates, 15 parts of propane diols, 7 parts of double imidazolidines in step S4
Base urea, 6 parts of Phenylbenzimidazolesulfonic acids, 12 parts of lauroyl sarcosine isopropyl esters.
Preferably, in step S4 in 100 DEG C of temperature with speed 3800r/min stirring reactions 42min.
A kind of above-mentioned any one preparation-obtained antiultraviolet anti-wrinkle cosmetic.
Compared with prior art, its advantage is the present invention：
The preparation method of a kind of antiultraviolet anti-wrinkle cosmetic of the present invention, by extracting camellia, yellow chamomile and silver
The active ingredient of apricot leaf, while add polyoxyethylene sorbitan stearate, propane diols, double imidazolidinyl urea, phenyl
The materials such as benzimidazole sulfonic acid, lauroyl sarcosine isopropyl ester, significantly improve the antiultraviolet and wrinkle resistance of cosmetics；
Wherein, three's active ingredient major embodiment prevents ultraviolet function, double imidazolidinyl urea, Phenylbenzimidazolesulfonic acid, lauroyl
Base methyl amimoacetic acid isopropyl ester etc. is used to realize crease-resistant function, and other compositions play balanced two kinds of functions, the effect for making it improve jointly,
So that the cosmetics function admirable being finally prepared, meets customer need.
Embodiment
The present invention is further illustrated with reference to embodiments.
Embodiment 1
S1：15 parts of camellias, 10 portions of yellow chamomiles and 30 parts of Ginkgo biloba leaves are dried and are crushed to 120 mesh, form compound；
S2：4 parts of lauryl sodium sulfate, 15 parts of isopropyl mercaptans and 10 parts of ethylene glycol salicylates are mixed, it is to be added
When hot temperature is to 60 DEG C, compound described in step S1 is added thereto, in 40 DEG C of impregnation 1h；
S3：By the solution obtained in step S2 be put into centrifuge rotating speed be 2500r/min under centrifuge 30min, take from
Supernatant after the heart adds isometric pH=7.0 liquor kalii acetici, places 10min, is then placed again into centrifuge and is turning
Speed is to centrifuge 20min under 3000r/min, takes supernatant standby；
S4：By 8 parts of polyoxyethylene sorbitan stearates, 10 parts of propane diols, 5 parts of double imidazolidinyl ureas, 4 parts of phenyl
Gained supernatant mixing in benzimidazole sulfonic acid, 10 parts of lauroyl sarcosine isopropyl esters and S3, in 90 DEG C of temperature with speed
3000r/min stirring reactions 50min；It can obtain the antiultraviolet anti-wrinkle cosmetic after cooling.
Embodiment 2
S1：20 parts of camellias, 15 portions of yellow chamomiles and 20 parts of Ginkgo biloba leaves are dried and are crushed to 200 mesh, form compound；
S2：7 parts of lauryl sodium sulfate, 10 parts of isopropyl mercaptans and 20 parts of ethylene glycol salicylates are mixed, it is to be added
When hot temperature is to 80 DEG C, compound described in step S1 is added thereto, in 45 DEG C of impregnation 3h；
S3：By the solution obtained in step S2 be put into centrifuge rotating speed be 3000r/min under centrifuge 40min, take from
Supernatant after the heart adds isometric pH=7.3 liquor kalii acetici, places 20min, is then placed again into centrifuge and is turning
Speed is to centrifuge 30min under 4000r/min, takes supernatant standby；
S4：By 10 parts of polyoxyethylene sorbitan stearates, 20 parts of propane diols, 8 parts of double imidazolidinyl ureas, 9 parts of benzene
Gained supernatant mixing in base benzimidazole sulfonic acid, 15 parts of lauroyl sarcosine isopropyl esters and S3, in 110 DEG C of temperature with speed
4000r/min stirring reactions 30min；It can obtain the antiultraviolet anti-wrinkle cosmetic after cooling.
Embodiment 3
S1：17 parts of camellias, 12 portions of yellow chamomiles and 25 parts of Ginkgo biloba leaves are dried and are crushed to 130 mesh, form compound；
S2：5 parts of lauryl sodium sulfate, 14 parts of isopropyl mercaptans and 18 parts of ethylene glycol salicylates are mixed, it is to be added
When hot temperature is to 75 DEG C, compound described in step S1 is added thereto, in 42 DEG C of impregnation 1.5h；
S3：By the solution obtained in step S2 be put into centrifuge rotating speed be 2650r/min under centrifuge 35min, take from
Supernatant after the heart adds isometric pH=7.1 liquor kalii acetici, places 15min, is then placed again into centrifuge and is turning
Speed is to centrifuge 22min under 3500r/min, takes supernatant standby；
S4：By 8 parts of polyoxyethylene sorbitan stearates, 18 parts of propane diols, 7 parts of double imidazolidinyl ureas, 8 parts of phenyl
Gained supernatant mixing in benzimidazole sulfonic acid, 14 parts of lauroyl sarcosine isopropyl esters and S3, in 100 DEG C of temperature with speed
3800r/min stirring reactions 45min；It can obtain the antiultraviolet anti-wrinkle cosmetic after cooling.
Embodiment 4
S1：19 parts of camellias, 14 portions of yellow chamomiles and 22 parts of Ginkgo biloba leaves are dried and are crushed to 140 mesh, form compound；
S2：7 parts of lauryl sodium sulfate, 11 parts of isopropyl mercaptans and 12 parts of ethylene glycol salicylates are mixed, it is to be added
When hot temperature is to 65 DEG C, compound described in step S1 is added thereto, in 44 DEG C of impregnation 2.5h；
S3：By the solution obtained in step S2 be put into centrifuge rotating speed be 2850r/min under centrifuge 38min, take from
Supernatant after the heart adds isometric pH=7.2 liquor kalii acetici, places 11min, is then placed again into centrifuge and is turning
Speed is to centrifuge 27min under 3800r/min, takes supernatant standby；
S4：By 9 parts of polyoxyethylene sorbitan stearates, 12 parts of propane diols, 5 parts of double imidazolidinyl ureas, 5 parts of phenyl
Gained supernatant mixing in benzimidazole sulfonic acid, 12 parts of lauroyl sarcosine isopropyl esters and S3, in 105 DEG C of temperature with speed
3200r/min stirring reactions 38min；It can obtain the antiultraviolet anti-wrinkle cosmetic after cooling.
Embodiment 5
S1：18 parts of camellias, 13 portions of yellow chamomiles and 26 parts of Ginkgo biloba leaves are dried and are crushed to 140 mesh, form compound；
S2：6 parts of lauryl sodium sulfate, 12 parts of isopropyl mercaptans and 18 parts of ethylene glycol salicylates are mixed, it is to be added
When hot temperature is to 73 DEG C, compound described in step S1 is added thereto, in 42 DEG C of impregnation 2.5h；
S3：By the solution obtained in step S2 be put into centrifuge rotating speed be 2800r/min under centrifuge 37min, take from
Supernatant after the heart adds isometric pH=7.1 liquor kalii acetici, places 18min, is then placed again into centrifuge and is turning
Speed is to centrifuge 25min under 3500r/min, takes supernatant standby；
S4：By 9 parts of polyoxyethylene sorbitan stearates, 15 parts of propane diols, 7 parts of double imidazolidinyl ureas, 6 parts of phenyl
Gained supernatant mixing in benzimidazole sulfonic acid, 12 parts of lauroyl sarcosine isopropyl esters and S3, in 100 DEG C of temperature with speed
3800r/min stirring reactions 42min；It can obtain the antiultraviolet anti-wrinkle cosmetic after cooling.
The antiultraviolet anti-wrinkle cosmetic performance test obtained to above-mentioned each embodiment, detailed results see the table below：
| Experiment | SPF | PFA | Crease-resistant rate (%) |
| Embodiment 1 | 25.3 | 8.16 | 75.8 |
| Embodiment 2 | 28.7 | 8.38 | 77.1 |
| Embodiment 3 | 31.9 | 8.64 | 78.7 |
| Embodiment 4 | 33.4 | 8.72 | 81.4 |
| Embodiment 5 | 35.1 | 8.91 | 83.1 |
The invention is not restricted to embodiment here, those skilled in the art do not depart from the present invention according to the announcement of the present invention
The improvement and modification that category is made all should be within protection scope of the present invention.
Claims (8)
1. a kind of preparation method of antiultraviolet anti-wrinkle cosmetic, it is characterised in that comprise the following steps：
S1：15-20 parts camellia, 10-15 parts yellow chamomile and 20-30 part Ginkgo biloba leaves are dried and are crushed to 120-200 mesh, shape
Into compound；
S2：4-7 parts lauryl sodium sulfate, 10-15 parts isopropyl mercaptan and 10-20 parts ethylene glycol salicylate are mixed,
When temperature to be heated is to 60-80 DEG C, compound described in step S1 is added thereto, in 40-45 DEG C of impregnation 1-3h；
S3：The solution obtained in step S2 is put into centrifuge and centrifuges 30-40min in the case where rotating speed is 2500-3000r/min,
Take the supernatant after centrifugation to add isometric pH=7.0-7.3 liquor kalii acetici, place 10-20min, be then placed again into from
20-30min is centrifuged in the case where rotating speed is 3000-4000r/min in scheming, takes supernatant standby；
S4：By 8-10 part polyoxyethylene sorbitans stearate, 10-20 parts propane diols, 5-8 parts double imidazolidinyl urea, 4-9
Gained supernatant mixing in part Phenylbenzimidazolesulfonic acid, 10-15 part lauroyl sarcosine isopropyl esters and S3, in temperature 90-
110 DEG C with speed 3000-4000r/min stirring reactions 30-50min；It can obtain antiultraviolet crease-resistantization after cooling
Cosmetic.
2. the preparation method of a kind of antiultraviolet anti-wrinkle cosmetic according to claim 1, it is characterised in that in step S1
18 parts of camellias, 13 portions of yellow chamomiles and 26 parts of Ginkgo biloba leaves are dried and are crushed to 130-140 mesh.
3. the preparation method of a kind of antiultraviolet anti-wrinkle cosmetic according to claim 1, it is characterised in that in step S2
6 parts of lauryl sodium sulfate, 12 parts of isopropyl mercaptans and 18 parts of ethylene glycol salicylates mix.
4. the preparation method of a kind of antiultraviolet anti-wrinkle cosmetic according to claim 1, it is characterised in that in step S2
When temperature to be heated is to 73 DEG C, compound described in step S1 is added thereto, in 42 DEG C of impregnation 2.5h.
5. the preparation method of a kind of antiultraviolet anti-wrinkle cosmetic according to claim 1, it is characterised in that in step S3
It is put into centrifuge and centrifuges 37min in the case where rotating speed is 2800r/min, takes the supernatant after centrifugation to add isometric pH=7.1's
Liquor kalii acetici, 18min is placed, be then placed again into centrifuge and centrifuge 25min in the case where rotating speed is 3500/min.
6. the preparation method of a kind of antiultraviolet anti-wrinkle cosmetic according to claim 1, it is characterised in that in step S4
By 9 parts of polyoxyethylene sorbitan stearates, 15 parts of propane diols, 7 parts of double imidazolidinyl ureas, 6 parts of phenylbenzimidazol sulphurs
Acid, 12 parts of lauroyl sarcosine isopropyl esters.
7. the preparation method of a kind of antiultraviolet anti-wrinkle cosmetic according to claim 1, it is characterised in that in step S4
In 100 DEG C of temperature with speed 3800r/min stirring reactions 42min.
8. according to a kind of any one preparation-obtained antiultraviolet anti-wrinkle cosmetic of claim 1-7.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710940964.8A CN107625685A (en) | 2017-10-11 | 2017-10-11 | A kind of antiultraviolet anti-wrinkle cosmetic and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710940964.8A CN107625685A (en) | 2017-10-11 | 2017-10-11 | A kind of antiultraviolet anti-wrinkle cosmetic and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107625685A true CN107625685A (en) | 2018-01-26 |
Family
ID=61103784
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710940964.8A Pending CN107625685A (en) | 2017-10-11 | 2017-10-11 | A kind of antiultraviolet anti-wrinkle cosmetic and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107625685A (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101405056A (en) * | 2006-03-22 | 2009-04-08 | 宝洁公司 | Cosmetic composition comprising gingko biloba and sunscreen agents |
| CN101677929A (en) * | 2007-02-23 | 2010-03-24 | 株式会社资生堂 | Composition for skin or hair |
| CN101766555A (en) * | 2008-12-31 | 2010-07-07 | 云南恒冠实业有限公司 | Anti-aging, wrinkle-eliminating and anti-wrinkle cosmetic composition |
| CN102920645A (en) * | 2012-11-29 | 2013-02-13 | 昆明然华生物科技有限公司 | Cosmetic composition with functions of moisture preservation and wrinkle resistance |
| CN103622848A (en) * | 2013-11-22 | 2014-03-12 | 山西医科大学 | Green biological sunscreen cosmetic |
| CN104138346A (en) * | 2014-08-07 | 2014-11-12 | 广州雅纯化妆品制造有限公司 | Anti-wrinkle cosmetic composition and preparation method thereof |
-
2017
- 2017-10-11 CN CN201710940964.8A patent/CN107625685A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101405056A (en) * | 2006-03-22 | 2009-04-08 | 宝洁公司 | Cosmetic composition comprising gingko biloba and sunscreen agents |
| CN101677929A (en) * | 2007-02-23 | 2010-03-24 | 株式会社资生堂 | Composition for skin or hair |
| CN101766555A (en) * | 2008-12-31 | 2010-07-07 | 云南恒冠实业有限公司 | Anti-aging, wrinkle-eliminating and anti-wrinkle cosmetic composition |
| CN102920645A (en) * | 2012-11-29 | 2013-02-13 | 昆明然华生物科技有限公司 | Cosmetic composition with functions of moisture preservation and wrinkle resistance |
| CN103622848A (en) * | 2013-11-22 | 2014-03-12 | 山西医科大学 | Green biological sunscreen cosmetic |
| CN104138346A (en) * | 2014-08-07 | 2014-11-12 | 广州雅纯化妆品制造有限公司 | Anti-wrinkle cosmetic composition and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104013566B (en) | A kind of Chinese medicine composition with white-skinned face function, its preparation method and its cosmetic applications | |
| CN105381007B (en) | External medicine composition, preparation with white-skinned face function and its preparation method and application | |
| CN105078875B (en) | A kind of cosmetics and preparation method thereof containing peony extract | |
| CN105616280B (en) | One kind is releived antiallergic maintenance ice pellets water | |
| Cetin et al. | Incision wound healing activity of pine bark extract containing topical formulations: A study with histopathological and biochemical analyses in albino rats | |
| CN105147551A (en) | Skin-protecting product containing peony active ingredients and production method thereof | |
| CN115778882B (en) | Hair-growing essence and preparation method thereof | |
| CN103628168A (en) | Nature antibacterial health-care ultraviolet-proofing polypropylene fiber | |
| Khan et al. | Neferine prevents ultraviolet radiation‑induced skin photoaging | |
| CN108078904A (en) | One kind contains anthocyanidin and Bee Pollen facial mask and preparation method thereof | |
| CN106727150A (en) | A kind of sun-proof skin care cosmetic composition and its application | |
| CN105078830A (en) | Natural preservative children plant sunscreen lotion and preparation method thereof | |
| CN109248135A (en) | A kind of sheen highlights, the external-use skin care of concealing moisturizing combination and preparation method thereof | |
| CN107468568A (en) | A kind of persimmon leaf polyphenol with whitening sun protection activity and its preparation method and application | |
| CN107625685A (en) | A kind of antiultraviolet anti-wrinkle cosmetic and preparation method thereof | |
| CN105963206A (en) | Facial mask with dendrobium huoshanense and method for preparing facial mask | |
| CN101744839A (en) | Application of Uygur medicine of nutgall and extract thereof with functions of inhibiting cutaneous pigmentation, screening sun and whitening | |
| CN108030737B (en) | Concentrated spray for promoting white hair to turn black, fixing hair and growing hair and preparation method thereof | |
| CN106361643A (en) | Eupatorium adenophora spreng. skin-whitening mask | |
| CN106265374A (en) | A kind of freckle-removing mask and preparation technology thereof | |
| CN105663595B (en) | A kind of melanin inhibitor, skin care compositions and its application | |
| KR102470447B1 (en) | Cosmetic composition for uv protection and manufacturing method thereof | |
| CN106539731A (en) | A kind of hair care hair care silk gum shampoo paste and preparation method thereof | |
| CN106491477A (en) | A kind of skin care item and preparation method thereof | |
| CN108078830A (en) | A kind of herbal essences floral water and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180126 |
|
| RJ01 | Rejection of invention patent application after publication |