CN1037837C - β－紫罗酮的制备 - Google Patents

β－紫罗酮的制备 Download PDF

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Publication number
CN1037837C
CN1037837C CN94106441A CN94106441A CN1037837C CN 1037837 C CN1037837 C CN 1037837C CN 94106441 A CN94106441 A CN 94106441A CN 94106441 A CN94106441 A CN 94106441A CN 1037837 C CN1037837 C CN 1037837C
Authority
CN
China
Prior art keywords
sulfuric acid
ionone
reaction
phase
solvent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN94106441A
Other languages
English (en)
Chinese (zh)
Other versions
CN1099742A (zh
Inventor
K·施泰纳
H·艾尔特尔
H·蒂尔舍
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
D Sm I P Property Co Ltd
Original Assignee
F Hoffmann La Roche AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by F Hoffmann La Roche AG filed Critical F Hoffmann La Roche AG
Publication of CN1099742A publication Critical patent/CN1099742A/zh
Application granted granted Critical
Publication of CN1037837C publication Critical patent/CN1037837C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C403/00—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone
    • C07C403/14—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone having side-chains substituted by doubly-bound oxygen atoms
    • C07C403/16—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone having side-chains substituted by doubly-bound oxygen atoms not being part of —CHO groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/16—Systems containing only non-condensed rings with a six-membered ring the ring being unsaturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN94106441A 1993-06-11 1994-06-10 β－紫罗酮的制备 Expired - Fee Related CN1037837C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH1759/93 1993-06-11
CH175993 1993-06-11

Publications (2)

Publication Number Publication Date
CN1099742A CN1099742A (zh) 1995-03-08
CN1037837C true CN1037837C (zh) 1998-03-25

Family

ID=4217911

Family Applications (1)

Application Number Title Priority Date Filing Date
CN94106441A Expired - Fee Related CN1037837C (zh) 1993-06-11 1994-06-10 β－紫罗酮的制备

Country Status (8)

Country Link
US (1) US5453546A (enExample)
EP (1) EP0628544B1 (enExample)
JP (1) JP3553135B2 (enExample)
CN (1) CN1037837C (enExample)
AT (1) ATE146777T1 (enExample)
DE (1) DE59401379D1 (enExample)
DK (1) DK0628544T3 (enExample)
ES (1) ES2096375T3 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100513400C (zh) * 2006-09-13 2009-07-15 湖南中烟工业有限责任公司 羟基磷酸铜在合成5,6-环氧-β-紫罗兰酮中的应用及合成5,6-环氧-β-紫罗兰酮的方法
EP1921058A1 (en) * 2006-11-10 2008-05-14 DSMIP Assets B.V. Process for the preparation of ionones and vitamin A, vitamin A derivatives, carotenes and carotenoids
CN111138261B (zh) * 2019-12-31 2023-02-24 上虞新和成生物化工有限公司 一种环合制备β-紫罗兰酮的方法
CN111792988A (zh) * 2020-08-04 2020-10-20 李金国 一种制备化妆品用β-紫罗兰酮的方法
CN117964470A (zh) * 2023-12-18 2024-05-03 万华化学集团股份有限公司 一种β-紫罗兰酮的合成方法
CN118186028B (zh) * 2024-04-09 2025-10-03 漳州市农业科学研究所 一种提高七指毛桃叶片中β-紫罗兰酮含量的方法
CN122036478B (zh) * 2026-04-17 2026-07-17 山东豪迈机械制造有限公司 一种β-紫罗兰酮的生产工艺

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6157530A (ja) * 1984-08-24 1986-03-24 バスフ　アクチェン　ゲゼルシャフト ヨノンの製法

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL155006B (nl) * 1968-04-24 1977-11-15 Philips Nv Werkwijze voor de bereiding van beta-ionon.
SU547445A1 (ru) * 1975-07-07 1977-02-25 Всесоюзный Научно-Исследовательский Витаминный Институт Способ получени -ионона
DE3328440A1 (de) * 1983-08-06 1985-02-21 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von jononen

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6157530A (ja) * 1984-08-24 1986-03-24 バスフ　アクチェン　ゲゼルシャフト ヨノンの製法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
CEREAL FOODS WORLD,V0136 1991.11.11 CARBONELL,"EXTRATION OF FLAVORS WITH SUPERCRITICAL CARBON DIOXIDE" *

Also Published As

Publication number Publication date
ATE146777T1 (de) 1997-01-15
DE59401379D1 (de) 1997-02-06
JP3553135B2 (ja) 2004-08-11
EP0628544B1 (de) 1996-12-27
ES2096375T3 (es) 1997-03-01
JPH06345727A (ja) 1994-12-20
EP0628544A1 (de) 1994-12-14
US5453546A (en) 1995-09-26
CN1099742A (zh) 1995-03-08
DK0628544T3 (enExample) 1997-03-17

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Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
ASS Succession or assignment of patent right

Owner name: DSM IP PROPERTY CO., LTD.

Free format text: FORMER OWNER: HOFFMAN-LALUOAI LTD.

Effective date: 20040528

C41 Transfer of patent application or patent right or utility model
TR01 Transfer of patent right

Effective date of registration: 20040528

Address after: Holland Heerlen

Patentee after: D Sm I P Property Company Limited

Address before: Basel

Patentee before: F. Hoffmann-La Roche AG

C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 19980325