CN103773658A - Cordyceps militaris wine and preparation method thereof - Google Patents
Cordyceps militaris wine and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a cordyceps militaris wine and a preparation method thereof. The method comprises the following steps: 1) selecting cordyceps militaris which is dried or lyophilized at a low temperature as a raw material and selecting a basic wine; 2) extracting the raw material and the basic wine in a continuous extraction tank so as to obtain a red wine; 3) freezing, filtering, blending and filling the red wine so as to obtain a red cordyceps militaris wine; or concentrating the red wine so as to obtain a concentrated solution, and then diluting, freezing, filtering, blending and filling the concentrated solution so as to obtain the red cordyceps militaris wine. According to the method, active substances such as flavone, flavonoid glycoside, cordycepin and the like in the cordyceps militaris are extracted, so that the concentration of the nutrient active substances in the unit wine is improved; compared with the traditional extraction method, the extraction ratio of the method disclosed by the invention is improved by 213.8%. Thus, the adjuvant therapy efficacy of the cordyceps militaris is more comprehensively and effectively exerted due to the improvement in the concentration of the nutrient active substances in the wine. As a result, the economic and social benefits are obvious.
Description
Technical field
The present invention relates to a kind of red cordyceps wine and preparation method thereof.
Background technology
Cordyceps militaris (L.) Link., is commonly called as Cordyceps militaris, and its pharmaceutical use is similar to Cordyceps sinensis, therefore be recited as again " Cordyceps militaris (L.) Link. " in pharmacopeia.It not only has high nutritive value, and has high nourishing function.Contain the various bioactivators such as cordycepic acid, cordycepin, Flavonoid substances and SOD, Cordyceps polysaccharide and rich in protein and amino acid etc. because of Cordyceps militaris (L.) Link.; so it is in anti-cancer; anticancer; reducing blood-fat, prevents and treats arteriosclerosis, the protection heart, cerebral tissue; tranquilizing soporific; reduce phlegm, relieving asthma, protect the aspects such as lung kidney-nourishing and there is adjuvant treatment efficacy.
Cordyccps-militaris-(L.)-link. Sporophore is approved as new resource food on March 16th, 2009 by the Ministry of Health, stipulates that its use range is: directly edible, drinks, can, seasonings, beverage.
Wine is one of main beverage in human lives, traditional white wine is without color (the micro-band of Maotai-flavor liquor is yellow), and " looking good, smell good and taste good " is the main Connotation of Chinese food culture, in order to develop and to enrich Chinese spirits culture, can allow white wine with certain color by the mode that increases natural product; Simultaneously also for common white spirit has increased certain nutrient substance.(CN101934005A) in patent, propose to utilize Cordyceps sinensis and Stigma Croci to produce " gold look " cordyceps militaris liquor and preparation method thereof " thering is cordyceps militaris liquor of gold look and preparation method thereof ".
Its main technique of above-mentioned patent is the same with most patent, has all adopted traditional base steeping in wine extract material technique, makes base wine with gold look.The extraction of natural product is the process of liquid-solid extraction, and traditional a large amount of solvent of cordyceps militaris liquor extraction needs could be by the solute stripping in material, and the nutrient substance concentration in unit product is reduced, and wine body can only present gold look.
Accompanying drawing explanation
Below in conjunction with accompanying drawing, the present invention is described in detail, to make above-mentioned advantage of the present invention clearer and more definite.Wherein,
Fig. 1 is the preparation method's of embodiment of the present invention cordyceps wine schematic flow sheet.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of cordyceps wine and preparation method thereof.
It is as follows that the present invention solves the problems of the technologies described above taked technical scheme:
A preparation method for cordyceps wine, comprises the following steps:
1) Cordyceps militaris (L.) Link. of choosing oven drying at low temperature or freeze-drying is as raw material; Choose base wine;
2) raw material and base wine are placed in to a continuous extracting pot and extract to obtain red wine liquid;
3) red wine liquid cooling frozen, filter, blend, fillingly obtain red cordyceps wine, or, red wine liquid is concentrated, obtain concentrated solution, and then dilution, freezing, filter, blend, fillingly obtain red cordyceps wine.
Preferably, further comprise: 4) by red cordyceps wine lixiviate Chinese medicine, integration of drinking and medicinal herbs or new resource food, or, add Chinese medicine, integration of drinking and medicinal herbs or new resource food extracting solution, modulate the red health preserving wine of difference in functionality machine local flavor.
Preferably, step 1) in, described Cordyceps militaris (L.) Link. is selected from one or more in Cordyccps-militaris-(L.)-link. Sporophore, cordyceps mycelium, Cordyceps militaris (L.) Link. polypide and Cordyceps militaris (L.) Link. culture.
Preferably, step 1) in, choose 30-50 ℃ of oven dry or freeze-drying Cordyccps-militaris-(L.)-link. Sporophore as raw material; Choosing alcoholic strength is the base wine of 30%-70%.
Preferably, step 1) in, choose 30-50 ℃ of oven dry or freeze-drying Cordyccps-militaris-(L.)-link. Sporophore, turf or annesl mycelia as raw material, choosing alcoholic strength is the base wine of 30%-70%.
Preferably, step 1) in, choose 50 ℃ dry or freeze-drying Cordyccps-militaris-(L.)-link. Sporophore as raw material, choose alcoholic strength and be 70% base wine.
Preferably, step 2) in, in extractor, solid-liquid ratio is 1: 10-20 (weightmeasurement ratio), dynamic extraction 3-5 time, extractor temperature 30-70 ℃;
Extractor volume is doubly (weight/volume) of 20-30 of extracting weight of material, and its liquid amount is the 1/3-2/3 of extractor height;
Concentration tank is 3-5 times of extractor volume, and total solid-liquid ratio is 1: 10-70 (weightmeasurement ratio), total extraction time is 1-2h.
Preferably, step 3) in, by red wine liquid in-1~-10 ℃ of freezing 24h, filter, blend, fillingly obtain red cordyceps wine.
Preferably, step 3) in, by concentrated red wine liquid 5-30 doubly, obtain concentrated solution, and then dilution ,-1~-10 ℃ of freezing 24h, filter, blend, fillingly obtain red cordyceps wine.
A kind of cordyceps wine, is prepared from according to above any preparation method.
After the present invention has taked such scheme, flavones in Cordyceps militaris (L.) Link., flavonoid glycoside, cordycepin isoreactivity material can be extracted, alcohol dissolubility active substance extracts completely, improved the nutrient substance concentration in unit product, and extraction yield has improved 213.8% than traditional extraction.In wine, the raising of nutrient substance concentration can be brought into play the adjuvant treatment efficacy of Cordyceps militaris (L.) Link. more comprehensively, effectively, has significant economic benefit and social benefit.
Other features and advantages of the present invention will be set forth in the following description, and, partly from specification sheets, become apparent, or understand by implementing the present invention.Object of the present invention and other advantages can be realized and be obtained by specifically noted structure in write specification sheets, claims and accompanying drawing.
Embodiment
Describe embodiments of the present invention in detail below with reference to drawings and Examples, to the present invention, how utilisation technology means solve technical problem whereby, and the implementation procedure of reaching technique effect can fully understand and implement according to this.It should be noted that, only otherwise form conflict, each feature in each embodiment and each embodiment in the present invention can mutually combine, and the technical scheme forming is all within protection scope of the present invention.
Specifically, as shown in Figure 1, this inventive method comprises the following steps, and wherein, the experimental technique in following embodiment, if no special instructions, is ordinary method.Test materials used in following embodiment, if no special instructions, is routine and is commercially available.
1) Cordyceps militaris (L.) Link. of choosing oven drying at low temperature or freeze-drying is as raw material; Choose base wine;
2) raw material and base wine are placed in to a continuous extracting pot jointly and extract to obtain red wine liquid;
3) red wine liquid cooling frozen, filter, blend, fillingly obtain red cordyceps wine, or, red wine liquid is concentrated, obtain concentrated solution, and then dilution, freezing, filter, blend, fillingly obtain red cordyceps wine.
Preferably, further comprise: 4) by red cordyceps wine lixiviate Chinese medicine, integration of drinking and medicinal herbs or new resource food, or, add Chinese medicine, integration of drinking and medicinal herbs or new resource food extracting solution, modulate the red health preserving wine of difference in functionality machine local flavor.
In addition, in step 1) in, described Cordyceps militaris (L.) Link. is selected from one or more in Cordyccps-militaris-(L.)-link. Sporophore, cordyceps mycelium, Cordyceps militaris (L.) Link. polypide and Cordyceps militaris (L.) Link. culture.
Preferred 30-50 ℃ of oven dry or freeze-drying Cordyccps-militaris-(L.)-link. Sporophore are as raw material; Choosing alcoholic strength is the base wine of 30%-70%.
Or, in preferred another embodiment, choose 30-50 ℃ of oven dry or freeze-drying Cordyccps-militaris-(L.)-link. Sporophore, turf or annesl mycelia as raw material, choosing alcoholic strength is the base wine of 30%-70%.
Wherein, step 2) in, in extractor, solid-liquid ratio is 1: 10-20 (weightmeasurement ratio), dynamic extraction 3-5 time, extractor temperature 30-70 ℃;
Extractor volume is doubly (weight/volume) of 20-30 of extracting weight of material, and its liquid amount is the 1/3-2/3 of extractor height;
Concentration tank is 3-5 times of extractor volume, and total solid-liquid ratio is 1: 10-70 (weightmeasurement ratio), total extraction time is 1-2h.
Preferably, step 3) in, by red wine liquid in-1~-10 ℃ of freezing 24h, filter, blend, fillingly obtain red cordyceps wine.
Preferably, step 3) in, by concentrated red wine liquid 5-30 doubly, obtain concentrated solution, and then dilution ,-1~-10 ℃ of freezing 24h, filter, blend, fillingly obtain red cordyceps wine.
Wherein, preparation method of the present invention is different from traditional leach extraction method, and extraction yield has improved 213.8% than traditional extraction.In wine, the raising of nutrient substance concentration can be brought into play the adjuvant treatment efficacy of Cordyceps militaris (L.) Link. more comprehensively, effectively, has significant economic benefit and social benefit.
embodiment 1
1) material choice: choose 50 ℃ of oven dry or freeze-drying Cordyccps-militaris-(L.)-link. Sporophore, turf or annesl mycelia as raw material;
2) base wine concentration is selected: choose alcoholic strength and be 70% base wine;
3) by step 1) in raw material be placed in continuous extracting pot and extract, in extractor, solid-liquid ratio is 1: 10-20 (weightmeasurement ratio), dynamic extraction 5 times, extractor temperature 70 C.
Extractor volume is 30 times (weight/volume) extracting weight of material, and its liquid amount is 2/3 of extractor height.Concentration tank is 5 times of extractor volume, and total solid-liquid ratio is 1: 70 (weightmeasurement ratio), and total extraction time is 2h;
4) by step 3) obtain obtain red wine liquid-10 ℃ freezing 24h, filter, blend, fillingly obtain red cordyceps wine; Also can be by step 3) obtain obtain concentrated 15 times of red wine liquid, obtain concentrated solution, and then dilution ,-10 ℃ of freezing 24h, filter, blend, fillingly obtain red cordyceps wine;
embodiment 2
1) material choice: choose 50 ℃ of oven dry or freeze-drying Cordyccps-militaris-(L.)-link. Sporophore, turf or annesl mycelia as raw material;
2) base wine concentration is selected: choose alcoholic strength and be 70% base wine;
3) by step 1) in raw material be placed in continuous extracting pot and extract, in extractor, solid-liquid ratio is 1: 10-20 (weightmeasurement ratio), dynamic extraction 5 times, extractor temperature 70 C.Extractor volume is 30 times (weight/volume) extracting weight of material, and its liquid amount is 2/3 of extractor height.Concentration tank is 5 times of extractor volume, and total solid-liquid ratio is 1: 70 (weightmeasurement ratio), and total extraction time is 2h;
4) by step 3) obtain obtain red wine liquid-10 ℃ freezing 24h, filter, blend, fillingly obtain red cordyceps wine; Also can be by step 3) obtain obtain concentrated 15 times of red wine liquid, obtain concentrated solution, and then dilution ,-10 ℃ of freezing 24h, filter, blend, fillingly obtain red cordyceps wine;
5) step 4) obtain obtain red cordyceps wine lixiviate ginseng; Or add Radix Ginseng extractive solution, modulate the red Cordyceps militaris (L.) Link. ginseng health preserving wine of difference in functionality machine local flavor.
embodiment 3
1) material choice: choose 50 ℃ and dry or freeze-drying Cordyccps-militaris-(L.)-link. Sporophore;
2) base wine concentration is selected: choose alcoholic strength and be 70% base wine;
3) by step 1) in raw material be placed in continuous extracting pot and extract, in extractor, solid-liquid ratio is 1: 10-20 (weightmeasurement ratio), dynamic extraction 5 times, extractor temperature 70 C.Extractor volume is 30 times (weight/volume) extracting weight of material, and its liquid amount is 2/3 of extractor height.Concentration tank is 5 times of extractor volume, and total solid-liquid ratio is 1: 70 (weightmeasurement ratio), and total extraction time is 2h;
4) by step 3) obtain obtain red wine liquid-10 ℃ freezing 24h, filter, blend, fillingly obtain red cordyceps wine; Also can be by step 3) obtain obtain concentrated 15 times of red wine liquid, obtain concentrated solution, and then dilution ,-10 ℃ of freezing 24h, filter, blend, fillingly obtain red cordyceps wine;
5) step 4) obtain obtain red cordyceps wine lixiviate ginseng, matrimony vine, glossy ganoderma; Or add ginseng, matrimony vine, lucidum extracting liquid, modulate red Cordyceps militaris (L.) Link. nourishing and health preserving wine.
embodiment 4
1) material choice: choosing 50 ℃ of oven dry or freeze-drying Cordyccps-militaris-(L.)-link. Sporophore is raw material;
2) base wine concentration is selected: choose alcoholic strength and be 70% base wine;
3) by step 1) in raw material be placed in continuous extracting pot and extract, in extractor, solid-liquid ratio is 1: 10-20 (weightmeasurement ratio), dynamic extraction 5 times, extractor temperature 70 C.Extractor volume is 30 times (weight/volume) extracting weight of material, and its liquid amount is 2/3 of extractor height.Concentration tank is 5 times of extractor volume, and total solid-liquid ratio is 1: 70 (weightmeasurement ratio), and total extraction time is 2h;
4) by step 3) obtain obtain red wine liquid-10 ℃ freezing 24h, filter, blend, fillingly obtain red cordyceps wine; Also can be by step 3) obtain obtain concentrated 15 times of red wine liquid, obtain concentrated solution, and then dilution ,-10 ℃ of freezing 24h, filter, blend, fillingly obtain red cordyceps wine;
5) step 4) obtain obtain red cordyceps wine lixiviate ginseng, matrimony vine, glossy ganoderma; Or add ginseng, matrimony vine, lucidum extracting liquid, modulate red Cordyceps militaris (L.) Link. nourishing and health preserving wine.
embodiment 5
1) material choice: choose 30 ℃ of oven dry or freeze-drying Cordyccps-militaris-(L.)-link. Sporophore as raw material;
2) base wine concentration is selected: choose alcoholic strength and be 50% base wine;
3) by step 1) in raw material be placed in continuous extracting pot and extract, in extractor, solid-liquid ratio is 1: 10-20 (weightmeasurement ratio), dynamic extraction 5 times, extractor temperature 70 C.Extractor volume is 30 times (weight/volume) extracting weight of material, and its liquid amount is 2/3 of extractor height.Concentration tank is 5 times of extractor volume, and total solid-liquid ratio is 1: 70 (weightmeasurement ratio), and total extraction time is 2h;
4) by step 3) obtain obtain red wine liquid-10 ℃ freezing 24h, filter, blend, fillingly obtain red cordyceps wine; Also can be by step 3) obtain obtain concentrated 15 times of red wine liquid, obtain concentrated solution, and then dilution ,-10 ℃ of freezing 24h, filter, blend, fillingly obtain red cordyceps wine;
5) step 4) obtain obtain red cordyceps wine lixiviate ginseng, matrimony vine, glossy ganoderma; Or add ginseng, matrimony vine, lucidum extracting liquid, modulate red Cordyceps militaris (L.) Link. nourishing and health preserving wine.
embodiment 6
1) material choice: choose 40 ℃ of oven dry or freeze-drying Cordyccps-militaris-(L.)-link. Sporophore as raw material;
2) base wine concentration is selected: choose alcoholic strength and be 30% base wine;
3) by step 1) in raw material be placed in continuous extracting pot and extract, in extractor, solid-liquid ratio is 1: 10-20 (weightmeasurement ratio), dynamic extraction 5 times, extractor temperature 70 C.Extractor volume is 30 times (weight/volume) extracting weight of material, and its liquid amount is 2/3 of extractor height.Concentration tank is 5 times of extractor volume, and total solid-liquid ratio is 1: 70 (weightmeasurement ratio), and total extraction time is 2h;
4) by step 3) obtain obtain red wine liquid-10 ℃ freezing 24h, filter, blend, fillingly obtain red cordyceps wine; Also can be by step 3) obtain obtain concentrated 15 times of red wine liquid, obtain concentrated solution, and then dilution ,-10 ℃ of freezing 24h, filter, blend, fillingly obtain red cordyceps wine;
5) step 4) obtain obtain red cordyceps wine lixiviate ginseng, matrimony vine, glossy ganoderma; Or add ginseng, matrimony vine, lucidum extracting liquid, modulate red Cordyceps militaris (L.) Link. nourishing and health preserving wine.
embodiment 7
1) material choice: choose 60 ℃ of oven dry or freeze-drying Cordyccps-militaris-(L.)-link. Sporophore as raw material;
2) base wine concentration is selected: choose alcoholic strength and be 60% base wine;
3) by step 1) in raw material be placed in continuous extracting pot and extract, in extractor, solid-liquid ratio is 1: 10-20 (weightmeasurement ratio), dynamic extraction 5 times, extractor temperature 70 C.Extractor volume is 30 times (weight/volume) extracting weight of material, and its liquid amount is 2/3 of extractor height.Concentration tank is 5 times of extractor volume, and total solid-liquid ratio is 1: 70 (weightmeasurement ratio), and total extraction time is 2h;
4) by step 3) obtain obtain red wine liquid-10 ℃ freezing 24h, filter, blend, fillingly obtain red cordyceps wine; Also can be by step 3) obtain obtain concentrated 15 times of red wine liquid, obtain concentrated solution, and then dilution ,-10 ℃ of freezing 24h, filter, blend, fillingly obtain red cordyceps wine;
5) step 4) obtain obtain red cordyceps wine lixiviate ginseng, matrimony vine, glossy ganoderma; Or add ginseng, matrimony vine, lucidum extracting liquid, modulate red Cordyceps militaris (L.) Link. nourishing and health preserving wine.
It should be noted that, for aforesaid method embodiment, for simple description, therefore it is all expressed as to a series of combination of actions, but those skilled in the art should know, the application is not subject to the restriction of described sequence of operation, because according to the application, some step can adopt other orders or carry out simultaneously.Secondly, those skilled in the art also should know, the embodiment described in specification sheets all belongs to preferred embodiment, and related action and module might not be that the application is necessary.
Finally it should be noted that: the foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, although the present invention is had been described in detail with reference to previous embodiment, for a person skilled in the art, its technical scheme that still can record aforementioned each embodiment is modified, or part technical characterictic is wherein equal to replacement.Within the spirit and principles in the present invention all, any modification of doing, be equal to replacement, improvement etc., within all should being included in protection scope of the present invention.
Claims (10)
1. a preparation method for cordyceps wine, is characterized in that, comprises the following steps:
1) Cordyceps militaris (L.) Link. of choosing oven drying at low temperature or freeze-drying is as raw material; Choose base wine;
2) raw material and base wine are placed in to a continuous extracting pot and extract to obtain red wine liquid;
3) red wine liquid cooling frozen, filter, blend, fillingly obtain red cordyceps wine, or, red wine liquid is concentrated, obtain concentrated solution, and then dilution, freezing, filter, blend, fillingly obtain red cordyceps wine.
2. the preparation method of cordyceps wine according to claim 1, is characterized in that, further comprises: 4) by red cordyceps wine lixiviate Chinese medicine, integration of drinking and medicinal herbs or new resource food,
Or, add Chinese medicine, integration of drinking and medicinal herbs or new resource food extracting solution, modulate the red health preserving wine of difference in functionality machine local flavor.
3. the preparation method of cordyceps wine according to claim 1 and 2, is characterized in that step 1) in, described Cordyceps militaris (L.) Link. is selected from one or more in Cordyccps-militaris-(L.)-link. Sporophore, cordyceps mycelium, Cordyceps militaris (L.) Link. polypide and Cordyceps militaris (L.) Link. culture.
4. the preparation method of cordyceps wine according to claim 3, is characterized in that step 1) in, 30-50 ℃ of oven dry or freeze-drying Cordyccps-militaris-(L.)-link. Sporophore chosen as raw material; Choosing alcoholic strength is the base wine of 30%-70%.
5. the preparation method of cordyceps wine according to claim 3, is characterized in that step 1) in, choose 30-50 ℃ of oven dry or freeze-drying Cordyccps-militaris-(L.)-link. Sporophore, turf or annesl mycelia as raw material, choosing alcoholic strength is the base wine of 30%-70%.
6. according to the preparation method of the cordyceps wine described in claim 4 or 5, it is characterized in that step 1) in, choose 50 ℃ dry or freeze-drying Cordyccps-militaris-(L.)-link. Sporophore as raw material, choose alcoholic strength and be 70% base wine.
7. the preparation method of cordyceps wine according to claim 1 and 2, is characterized in that step 2) in, in extractor, solid-liquid ratio is 1: 10-20 (weightmeasurement ratio), dynamic extraction 3-5 time, extractor temperature 30-70 ℃;
Extractor volume is doubly (weight/volume) of 20-30 of extracting weight of material, and its liquid amount is the 1/3-2/3 of extractor height;
Concentration tank is 3-5 times of extractor volume, and total solid-liquid ratio is 1: 10-70 (weightmeasurement ratio), total extraction time is 1-2h.
8. the preparation method of cordyceps wine according to claim 1 and 2, is characterized in that step 3) in, by red wine liquid in-1~-10 ℃ of freezing 24h, filter, blend, fillingly obtain red cordyceps wine.
9. the preparation method of cordyceps wine according to claim 1 and 2, it is characterized in that step 3) in, by concentrated red wine liquid 5-30 doubly, obtain concentrated solution, and then dilution ,-1~-10 ℃ of freezing 24h, filter, blend, fillingly obtain red cordyceps wine.
10. a cordyceps wine, is characterized in that, according to claim 1~9, any preparation method is prepared from.
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CN105838558A (en) * | 2015-08-27 | 2016-08-10 | 泸州老窖集团养生酒业有限责任公司 | Cordyceps militaris wine and preparation method thereof |
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CN107043671A (en) * | 2017-06-08 | 2017-08-15 | 株洲千金药业股份有限公司 | A kind of classical collection health preserving wine and its preparation method and application |
CN108728314A (en) * | 2018-06-12 | 2018-11-02 | 深圳市鑫木森实业发展有限公司 | A kind of SOD white wine preparation methods for supporting kidney function effect with protect liver |
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