CN103767968B - One educates eyebrow liquid and preparation method thereof - Google Patents
One educates eyebrow liquid and preparation method thereof Download PDFInfo
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- CN103767968B CN103767968B CN201410011011.XA CN201410011011A CN103767968B CN 103767968 B CN103767968 B CN 103767968B CN 201410011011 A CN201410011011 A CN 201410011011A CN 103767968 B CN103767968 B CN 103767968B
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Abstract
The present invention provides one to educate eyebrow liquid, and functional component is: Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi, fennelflower seed；As preferably, also include ethanol.Its preparation method is: 1) weigh each raw material by quality proportioning；2) Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi, fennelflower seed are mixed according to proportioning, add 8 15 times of mixture quality, volumn concentration be 10 70% alcohol reflux, concentrate, obtain Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi and the ethanol extract of fennelflower seed；3) in above-mentioned ethanol extract, add additive, stir, obtain educating eyebrow liquid.The eyebrow liquid of educating of the present invention has and well educates eyebrow effect, meeting that eyebrow is rare, fall eyebrow and the demand of the vast colony of scarce eyebrow, also meet people to beautiful and the pursuit of high spirit quality life, educating eyebrow liquid is deep yellow color liquid, there is the medical herbs fragrance of uniqueness, there is good compliance.
Description
Technical field
The invention belongs to cosmetic technical field, be specifically related to one and educate eyebrow liquid and preparation method thereof.
Background technology
As the saying goes and flash amorous glances, raw eyebrow opens fortune, it is seen that eyebrow is at the importance of human face.One perfect woman's beauty
Overall aesthetic is facial indispensable key element；And have thick black dense eyebrow, show the masculine of man, to man
Cause has help greatly.The growth of eyebrow and regeneration depend on the enough nutrition blood supplies to hair follicle.Microcirculation disturbance can affect
The normal nutrition of hair follicle and oxygen supply reduce, thus cause alopecia.Medicine by skin expansion blood vessel, to improve skin micro-
Circulation, increases hair papilla blood supply, improves hair follicle nutrition, promotion tissue new life, and then promote hair growth.
Along with the raising of people's living standard, people to the pursuit of cosmetics the most gradually by both effectiveness to safety transition,
Particularly the demand to the both effectiveness cosmetics of pure natural, is particularly subject to greatly pay close attention in the world.
Chinese invention patent ZL921148089 " Isatis indigotica Fort. eye cosmetic and preparation method thereof " and ZL200910113424
" indirubin educates the purposes of hair as preparation ", discloses and extracts the technique of indirubin from Isatis indigotica Fort. and indirubin is promoting hair
Purposes in growing, but its comparison of ingredients is single, and the effect to promoting eyebrow growth is the most single.
Summary of the invention
The purpose of the present invention is aiming at above-mentioned defect of the prior art, it is provided that a kind of multicomponent mixing, educates eyebrow effect
The best, preparation technology simply educates eyebrow liquid.It is set about from eyebrow growth mechanism, by life eyebrow, supports eyebrow and protects eyebrow Chinese medicine ingredients side entirely
Position adds, and adds absorption and the utilization that can promote that the little molecule infiltration agent of Transdermal absorption promotes functional component.
The present invention screens the medical material with functional components such as hair growth promoting, hair care, Anti-hair loss, Isatis tinctoria L. leaf, side in plant
Cacumen Platycladi (Cacumen Biotae) play sterilization, improve the effect of hair follicle environment, are specially antiinflammatory, the antibacterial and antipruritic effect of playing skin；Radix Polygoni Multiflori
Root, fennelflower seed can nourish hair, are the nutrient substance of a kind of hair regeneration length that can enhance metabolism, supply；Cacumen Platycladi
Play the effect of anticreep, specially give the stimulation that hair follicle is certain, promote hair health growth；By above-mentioned functional component
Effect improve hair follicle physiological function and microcirculating state, activate hair follicle blast cell, promote hair growth.
The one that the present invention provides educates eyebrow liquid, described in educate the functional component of eyebrow liquid and be: Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, side
Cacumen Platycladi (Cacumen Biotae), fennelflower seed；As preferably, also include ethanol.
Isatis tinctoria L. (Isatis tinctoria L .), is referred to as Wu Sima grass, raw eyebrow grass, is the Uygur nationality in Xinjiang
A kind of raw eyebrow plant commonly used among the people, has heat-clearing and toxic substances removing, effect of blood cooling and ecchymoses removing.Uygur nationality of Xijiang almost every household all exists
Around the house plantation Isatis indigotica Fort. (Wu Sima), people squeezing juice with its leaf and smear double eyebrow, making eyebrows shiny black close, until becoming every day
Year, as washing one's face, day by day, year after year, within thousand, proved recipe is passed on from generation to generation everyday.This traditional promotion eyebrow growth
Technology and eyebrow is treasured in China various nationalities peerless.
Radix Polygoni Multiflori, is the tuber of Polygonaceae arsesmart, warm in nature, bitter in the mouth, dry and astringent, chemical composition contain lecithin, rheum emodin,
The nutritional labeling such as chrysophanol, chrysophanic acid, has the merit of nourishing blood to expel wind, has regulation nerve, endocrine function and the work of hairy root nourishing
With, promote the melanic generation of hair, make hair more black.Meanwhile, Radix Polygoni Multiflori chrysophanol and much starch, be preparation hair-conditioning
The optimal raw material of Chinese medicine of agent.De-originator is often moistened foster for asthenia of essence and blood, a mistake, and Radix Polygoni Multiflori gets final product the blood of nourishing the liver and kidney, treats with it
Poliosis and alopecia, especially seborrheic alopecia, effect is more preferable.According to modern pharmacology it is demonstrated experimentally that lecithin contained by Radix Polygoni Multiflori is
The important source material of cell membrane, can promote metabolism and the growth promoter of cell, thus delay the aging of cell, life prolonging.
Cacumen Platycladi: Cacumen Platycladi (Cacumen platycladi) is mainly composed of flavone compound, tannin and volatile oil
Deng, there is anti-inflammation, expansion blood vessel and anti-dandruff anticreep and the effects such as beard and hair can be given birth to.Hair follicle development growth can be improved, the most right
Staphylococcus aureus, Staphylococcus albus etc. are inhibited, energy dandruff, strengthen hair follicle metabolism function, by thorn
Swash hair follicle, promote blood microcirculation, it is provided that the means such as natural on-off cycles of hair growth nutrient, reach to promote hair regeneration.Research proves Cacumen Platycladi
The pharmacological action of middle total flavones composition essentially consists in activation hair follicle and blood circulation promoting, makes hair growth ability fail
Hair follicle brings back to life and supplements the nutrients after blood circulation promoting and play and give birth to and bring up hair effect.The mechanism of removing scurf and relieving itching is suppression
The speed that scalp epidermis cell is degenerated, postpones to come off, and reduces the generation of seborrheic dermatosis.The present invention uses 10-70% ethanol to carry
Taking can total flavones in extraction side Cacumen Platycladi (Cacumen Biotae) so that educate eyebrow better.
Fennelflower seed: Nigella damascena L. is that Ranunculaceae (Raunnculaceae) Nigella damascena L. belongs to (Nigella), main product Xinjiang.Medicine
Semen Nigellae is had another name called with tumor fruit blackwort symphytum.Tumor fruit blackwort symphytum seed takes in the most each version " Chinese Pharmacopoeia " in 1977 as Uigurs medicine,
Have black hair, diuresis, supplementing the brain, the kidney invigorating, invigorate blood circulation, detoxify, stimulating milk secretion, stimulate the menstrual flow, cough-relieving, anti-ageing effect of waiting for a long time, " China's draft " is recorded
It has antitumor action.Discovered in recent years it also have certain curative effect in the many-side such as blood fat reducing, blood sugar lowering." Uigurs medicine will " is recorded black
Plant grass seed ethanol extraction and have lipoid peroxidization resistant, illustrate that it has defying age and promotes hair growth effect.
Ethanol solution: serve not only as solvent, key function is to improve percutaneous absorption rate, can strengthen and become Chinese medicine
The absorption divided, and combine with calcium, the magnesium ion further elasticity promoting hair and gloss.
As preferably, described in educate eyebrow liquid and include following component: Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi, fennelflower seed
Ethanol extraction；It is highly preferred that also include additive.
Preferably, described Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi, the mass ratio of fennelflower seed are 2-4:2-4:1-3:
1-3；Preferably, mass ratio is 3:3:2:2.Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi, the content of each component of fennelflower seed are wanted
In suitable scope, the effect preferably promoting eyebrow growth just can be played；Through test, time within the above range, effect is preferable,
When each constituent mass ratio is during for 3:3:2:2, can promote that eyebrow grows best.
Preferably, described additive is
(1) preservative and water；Or
(2) thickening agent, wetting agent, solubilizing agent and preservative；Or
(3) thickening agent, wetting agent, solubilizing agent, preservative and water.
As cosmetics, add appropriate thickening agent, wetting agent, solubilizing agent so that product appearance, sense organ and property
Shape more meets consumption habit, also can promote the skin absorption to functional component simultaneously；Add appropriate preservative to extend and educate
The shelf-life of eyebrow liquid.
As preferably, described in educate the mass percent of each component in eyebrow liquid and be: Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi
Ethanol extract 25.0-97.0% with fennelflower seed；Thickening agent 0-1.5%；Wetting agent 0-3%；Solubilizing agent 0-1%；Preservative
0.6-1%；Remaining is deionized water.
Thickening agent of the present invention is one or more in hydroxyethyl cellulose, guar gum, xanthan gum.
Wetting agent of the present invention is one or more in propylene glycol, glycerol, D-panthenol, hyaluronic acid.
Solubilizing agent of the present invention is one or more in Cremophor RH40, Tween-60 or tween 80.
Propylene glycol: serve not only as excellent wetting agent, can improve the hydration of skin with it, so can be beneficial to through
Skin absorbs.This is because when, after the Hydration Force of nitrogen-containing compound in the keratin improving corneocyte, cell self occurs swollen
Swollen, the compactness extent of structure reduces, and the permeability of material increases, and at this moment aqueous solution and polar substances are easier to from corneocyte
Passing through, addition glycerol and propylene glycol improve the absorption of effective ingredient.
D-panthenol: the nursing role on skin, shows as the wetting agent penetrated deep into, and stimulates the growth of epithelial cell, promotees
Enter wound healing, play antiinflammation；Nursing role on hair shows as lasting moisture-keeping functions, prevents hair jag, impaired,
Increase the density of hair, improve the gloss of hair.
Cremophor RH40: have good solubilizing effect, makes liquid uniform, also serves as one simultaneously and be widely used
Chemosmosis agent, stimulation will not be caused in suitable scope.
Second object of the present invention is to provide the above-mentioned preparation method educating eyebrow liquid, comprises the following steps:
1) each raw material is weighed by quality proportioning；
2) Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi, fennelflower seed are mixed according to proportioning, add mixture quality
8-15 times, volumn concentration be the alcohol reflux of 10-70%, concentrate, obtain Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi
Ethanol extract with fennelflower seed；
3) Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi, fennelflower seed ethanol extract in, add additive, stirring
Uniformly, obtain educating eyebrow liquid.
Wherein, the addition sequence of described additive is
(1) preservative is added together with water；Or
(2) thickening agent, wetting agent, solubilizing agent and preservative it are sequentially added into；Or
(3) water is added together with thickening agent, sequentially add wetting agent, solubilizing agent and preservative.
Preferably, addition 10 times of mixture quality, volumn concentration are the alcohol reflux of 70%.
When ethanol quality is 8-15 times of mixture quality, can fully by the extracts active ingredients in mixture out,
Although ethanol too much can preferably extract, but can cause the increase of cost；When 10 times that ethanol volume is volume of mixture,
Economically be most suitable from the point of view of extraction effect.
The ethanol of certain volume percent concentration can will have in Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi, fennelflower seed
The composition of the effects such as sterilization, nourishing, black hair preferably extracts, and advantageously promotes the growth of hair.Through test, at 10-70%
Time functional component preferably can be extracted.And the above-mentioned medical material of ethanol extraction applying concentration expressed in percentage by volume to be 70% has
The functional component yield of black hair, hair care and Anti-hair loss is the highest, and the addition of ethanol simultaneously decreases macromolecular substances and hinders skin to inhale
Receive impact.
Preferably, Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi, the mixture of fennelflower seed and extraction in described extracting solution
The mass ratio of liquid is 1:(2-10)；It is highly preferred that mixture is 1:5 with the mass ratio of extracting solution in described extracting solution.
In said extracted liquid, Chinese crude drug quality selects 1:(2-10 with the mass ratio of extracting solution), can guarantee that containing of ethanol
Measure moderate, it is possible to increase percutaneous absorption rate, strengthen the absorption to Chinese medicine ingredients, and the increasing further that combines with calcium, magnesium ion
Enter elasticity and the gloss of hair.If the too high meeting of ethanol content causes the allergy of part population, too low, do not reach the effect of product；
When both mass ratioes are 1:5, effect reaches optimal.
Preferably, described alcohol reflux 2 times, each 1-3 hour；Preferably, reflux extracting time is 2 hours.
When above-mentioned reflux extracting time number of times, most effective ingredient can be extracted within the shortest time, comprehensively
Cost is minimum.
Third object of the present invention is to provide above-mentioned eyebrow liquid of educating in the application that eyebrow falls in eyebrow less of scarce eyebrow.
The invention have the benefit that the present invention combines the market demand, excavate Xinjiang characteristic resource to greatest extent, by sky
So plant material Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi and fennelflower seed four taste Chinese medicine are combined, and obtain optimum proportioning,
The most appropriate thickening agent, wetting agent, solubilizing agent and preservative are allocated, and stir, are educated eyebrow liquid liquid uniformly.
The eyebrow liquid of educating of the present invention has and good educates eyebrow effect, meets that eyebrow is rare, fall eyebrow and the demand of the vast colony of scarce eyebrow, also full
Foot people are to beautiful and the pursuit of high spirit quality life, and to educate eyebrow liquid be deep yellow color liquid, have the medical herbs fragrance of uniqueness, have
Well compliance.
Detailed description of the invention
Below example facilitates a better understanding of the present invention, but does not limit the present invention.Experiment in following embodiment
Method, if no special instructions, is conventional method.
Embodiment 1
The formula educating eyebrow liquid of the present invention is as follows: water 641g, xanthan gum 3g, Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi and
Ethanol extract 325g, 10g D-panthenol, 10g propylene glycol, 5g Cremophor RH40 and the 6g preservative of fennelflower seed.
The preparation method step educating eyebrow liquid of the present invention is as follows:
A, Isatis tinctoria L. leaf 48.75g is cut into 1-3cm segment, Radix Polygoni Multiflori root 48.75g is ground into footpath grain thick less than 3cm
Granule, takes Cacumen Platycladi prepared slices of Chinese crude drugs 32.5g, fennelflower seed prepared slices of Chinese crude drugs 32.5g, by above-mentioned four kinds of raw material mix homogeneously, with mixed
The volume mass mark of compound gross mass 8 times is 50% alcohol reflux 2 times, each 1 hour, filters, merging filtrate, vacuum
Be evaporated to 325g, i.e. medical material and extracting solution mass ratio is 1:2,6000r/min, centrifugal 8min, abandons precipitation, takes supernatant,
To Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi and the ethanol extract of fennelflower seed；
B, use water dissolution 3g xanthan gum, until being completely dissolved；
C, solution step a, b obtained mix, and are sequentially added into 10g D-panthenol, 10g propylene glycol, 5g PEG-40 hydrogenation
Oleum Ricini and 6g preservative, stir, and i.e. can obtain educating eyebrow liquid.
Embodiment 2
The formula educating eyebrow liquid of the present invention is as follows: water 647g, hydroxyethyl cellulose 10g, Isatis tinctoria L. leaf, Radix Polygoni Multiflori root,
The ethanol extract 300g of Cacumen Platycladi and fennelflower seed, glycerol 30g, Cremophor RH40 5g and preservative 8g.
The preparation method step educating eyebrow liquid of the present invention is as follows:
A, Isatis tinctoria L. leaf 20g is cut into 1-3cm segment, Radix Polygoni Multiflori root 20g is ground into thick less than 3cm of footpath grain
Grain, takes Cacumen Platycladi prepared slices of Chinese crude drugs 10g, takes fennelflower seed prepared slices of Chinese crude drugs 10g, by four kinds of raw material mix homogeneously, with the total matter of mixture
The volume mass mark measuring 10 times is 60% alcohol reflux 2 times, each 1.5 hours, filters, and merging filtrate, vacuum decompression is dense
Be reduced to 300g, i.e. medical material and extracting solution mass ratio is 1:5,6000r/min, centrifugal 8 minutes, abandons precipitation, takes supernatant, obtain Europe
Isatis indigotica Fort. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi and the ethanol extract of fennelflower seed；
B, use water dissolution 10g hydroxyethyl cellulose, until being completely dissolved；
C, solution step a, b obtained mix, and are sequentially added into glycerol 30g, Cremophor RH40 5g and preservative
8g, stirs, and i.e. can obtain educating eyebrow liquid.
Embodiment 3
The formula educating eyebrow liquid of the present invention is as follows:
Hydroxyethyl cellulose 5g, Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi and Nigella damascena L. ethanol extract 964g, D-are general
Alcohol 10g, propylene glycol 10g, Cremophor RH40 5g, preservative 6g.
The preparation method step educating eyebrow liquid of the present invention is as follows:
A, Isatis tinctoria L. leaf 57.84g is cut into 1-3cm segment, Radix Polygoni Multiflori root 57.84g is ground into particle diameter less than 3cm's
Coarse granule, takes Cacumen Platycladi prepared slices of Chinese crude drugs 38.56g, fennelflower seed prepared slices of Chinese crude drugs 38.56g, by four kinds of raw material mix homogeneously, with mixed
The concentration expressed in percentage by volume that compound gross mass is 15 times is 70% alcohol reflux 2 times, each 2 hours, filters, merging filtrate, vacuum
Be evaporated to 964g, i.e. medical material and extracting solution mass ratio is 1:5,6000r/min, centrifugal 8min, abandons precipitation, takes supernatant,
To Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi and the ethanol extract of fennelflower seed；
B, with above-mentioned ethanol extract dissolve 5g hydroxyethyl cellulose, until being completely dissolved；
C, be sequentially added in the solution that step b obtains 10g D-panthenol, 10g propylene glycol, Cremophor RH40 5g,
Preservative 6g, stirs, and i.e. can obtain educating eyebrow liquid.
Embodiment 4
The formula educating eyebrow liquid of the present invention is as follows:
Water 673g, hydroxyethyl cellulose 10g, Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi and the ethanol extraction of fennelflower seed
Liquid 280g, D-panthenol 10g, propylene glycol 10g, Cremophor RH40 7g, preservative 10g.
The preparation method step educating eyebrow liquid of the present invention is as follows:
A, Isatis tinctoria L. leaf 40g is cut into 1-3cm segment, Radix Polygoni Multiflori root 40g is ground into thick less than 3cm of particle diameter
Grain, takes Cacumen Platycladi prepared slices of Chinese crude drugs 30g, fennelflower seed prepared slices of Chinese crude drugs 30g, by four kinds of raw material mix homogeneously, with mixture gross mass
The concentration expressed in percentage by volume of 10 times is 40% alcohol reflux 2 times, each 3 hours, filters, and merging filtrate, vacuum-concentrcted is extremely
280g, i.e. medical material and extracting solution mass ratio is 1:2,6000r/min, centrifugal 8min, abandons precipitation, takes supernatant, obtains Isatis tinctoria L.
Leaf, Radix Polygoni Multiflori root, Cacumen Platycladi and the ethanol extract of fennelflower seed；
B, use water dissolution 10g hydroxyethyl cellulose, until being completely dissolved；
C, solution step a, b obtained mix, and are sequentially added into 10gD-pantothenylol, 10g propylene glycol, 7gPEG-40 hydrogenate castor
Oleum Sesami, 10g preservative, stir, and i.e. can obtain educating eyebrow liquid.
Embodiment 5
The formula educating eyebrow liquid of the present invention is as follows:
Water 713.5g, guar gum 15g, Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi and the ethanol extract of fennelflower seed
250g, glycerol 10g, Tween-60 2.5g, preservative 9g.
The preparation method step educating eyebrow liquid of the present invention is as follows:
A, Isatis tinctoria L. leaf 15.625g is cut into 1-3cm segment, Radix Polygoni Multiflori root 15.625g is ground into footpath grain less than 3cm
Coarse granule, takes Cacumen Platycladi prepared slices of Chinese crude drugs 15.625g, takes fennelflower seed prepared slices of Chinese crude drugs 15.625g, by four kinds of raw material mix homogeneously,
It is 10% alcohol reflux 2 times with the concentration expressed in percentage by volume of mixture gross mass 10 times, each 1 hour, filters, merging filtrate,
Vacuum-concentrcted is to 250g, i.e. medical material and extracting solution mass ratio is 1:4,6000r/min, centrifugal 8min, abandons precipitation, takes
Clearly, Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi and the ethanol extract of fennelflower seed are obtained；
B, use water dissolution 15g guar gum, until being completely dissolved；
C, solution step a, b obtained mix, and are sequentially added into 10g glycerol, 2.5g Tween-60 and 9g preservative, stirring
Uniformly, i.e. can obtain educating eyebrow liquid.
Embodiment 6
The formula educating eyebrow liquid of the present invention is as follows:
The ethanol extract 970g of xanthan gum 4g, Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi and fennelflower seed, hyalomitome
Acid 4g, propylene glycol 6g, tween 80 10g, preservative 6g.
The preparation method step educating eyebrow liquid of the present invention is as follows:
A, Isatis tinctoria L. leaf 38.8g is cut into 1-3cm segment, Radix Polygoni Multiflori root 38.8g is ground into footpath grain less than thick of 3cm
Grain, takes Cacumen Platycladi prepared slices of Chinese crude drugs 9.7g, takes fennelflower seed prepared slices of Chinese crude drugs 9.7g, by above-mentioned four kinds of raw material mix homogeneously, with mixing
The concentration expressed in percentage by volume that thing gross mass is 10 times is 20% alcohol reflux 2 times, each 3 hours, filters, and merging filtrate, vacuum subtracts
Pressure is concentrated into 970g, i.e. medical material and extracting solution mass ratio is 1:10,6000r/min, centrifugal 8min, abandons precipitation, takes supernatant, obtains
Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi and the ethanol extract of fennelflower seed；
B, with above-mentioned ethanol extract dissolve 4g xanthan gum, until being completely dissolved；
C, in the solution that step b obtains, it is sequentially added into 4g hyaluronic acid, 6g propylene glycol, 10g tween 80,6g preservative,
Stir, i.e. can obtain educating eyebrow liquid.
Embodiment 7
The formula educating eyebrow liquid of the present invention is as follows:
Water 30g, Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi and fennelflower seed ethanol extract 964g, preservative 6g.
The preparation method step educating eyebrow liquid of the present invention is as follows:
A, Isatis tinctoria L. leaf 57.84g is cut into 1-3cm segment, Radix Polygoni Multiflori root 57.84g is ground into particle diameter less than 3cm's
Coarse granule, takes Cacumen Platycladi prepared slices of Chinese crude drugs 38.56g, fennelflower seed prepared slices of Chinese crude drugs 38.56g, by four kinds of raw material mix homogeneously, with mixed
The concentration expressed in percentage by volume that compound gross mass is 10 times is 70% alcohol reflux 2 times, each 2 hours, filters, merging filtrate, vacuum
Be evaporated to 964g, i.e. medical material and extracting solution mass ratio is 1:5,6000r/min, centrifugal 8min, abandons precipitation, takes supernatant,
To Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi and the ethanol extract of fennelflower seed；
B, mix with 30g water with above-mentioned ethanol extract, stir, add preservative 6g, i.e. can obtain educating eyebrow liquid.
Embodiment 8
Carry out educating the clinical trial of the raw eyebrow effect of eyebrow with above-mentioned eyebrow liquid of educating.
Observing time: in the case of technical solution of the present invention does not disclose, select July two in June, 2013 to 2013
Individual month.
Tested crowd: experimenter is volunteer 20 example that eyebrow is sparse；Man's 10 examples, female 10 example；Age: 16-25 year
10 examples, 25-35 year 10 examples, occupation: student 10 example, office worker 10 example；Using method: after morning and evening every day face cleaning, rub eyebrow with finger
Portion smeared along the direction of eyebrow 2 times after 1-2 minute, within one month, was a course for the treatment of, and two courses for the treatment of, as observation of curative effect, observe and use
Before and after medicine, effect is evaluated, and clinical naked eyes decision method is as follows, and effect standard is divided into: notable: eyebrow is sparse substantially to be changed
Kind, new hair or fine hair on birds or animals staple length go out >=80%；Effective: eyebrow is sparse to be effectively controlled, new hair or fine hair on birds or animals staple length go out >=60%；Have
Effect: eyebrow is sparse must be controlled, and new hair or fine hair on birds or animals staple length go out >=30%；Invalid: to go out without new hair growth or fine hair on birds or animals staple length.
Notable 5 examples in 20 examples as a result, effective 5, effective 5 examples, invalid 4 examples, 1 example lost to follow-up, total effective rate reaches 78.9%.
Notable 3 examples of man, effective 2 examples: effective 3 examples, effective percentage is 80%；Notable 2 examples of female, effective 3 examples, effective 2 examples, effectively
Rate is 77.7%, and this invention of rough estimates is the most obvious to the accretion of man's eyebrow.
Finally it is noted that the foregoing is only the preferred embodiments of the present invention, it is not limited to the present invention,
Although being described in detail the present invention with reference to previous embodiment, for a person skilled in the art, it still may be used
So that the technical scheme described in foregoing embodiments to be modified, or wherein portion of techniques feature is carried out equivalent.
All within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. made, should be included in the present invention's
Within protection domain.
Claims (11)
1. educate eyebrow liquid for one kind, it is characterised in that educate eyebrow liquid described in: and include following component: Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi
Leaf, the ethanol extract of fennelflower seed；Described Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi, the mass ratio of fennelflower seed are 2-4:
2-4:1-3:1-3。
The most according to claim 1 educate eyebrow liquid, it is characterised in that educate eyebrow liquid described in: and also include additive.
The most according to claim 1 and 2 educate eyebrow liquid, it is characterised in that: described Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi,
The mass ratio of fennelflower seed is 3:3:2:2.
The most according to claim 2 educate eyebrow liquid, it is characterised in that: described additive is
(1) preservative and water；Or
(2) thickening agent, wetting agent, solubilizing agent and preservative；Or
(3) thickening agent, wetting agent, solubilizing agent, preservative and water.
The most according to claim 4 educate eyebrow liquid, it is characterised in that educating the mass percent of each component in eyebrow liquid described in: is:
The ethanol extract 25.0-97.0% of Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi and fennelflower seed；Thickening agent 0-1.5%；Moisturizing
Agent 0-3%；Solubilizing agent 0-1%；Preservative 0.6-1%；Remaining is deionized water.
6. the arbitrary described preparation method educating eyebrow liquid of claim 1-5, it is characterised in that: comprise the following steps:
1) each raw material is weighed by quality proportioning；
2) Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi, fennelflower seed are mixed according to proportioning, add the 8-15 of mixture quality
Times, volumn concentration be the alcohol reflux of 10-70%, concentrate, obtain Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi and black
Plant the ethanol extract of grass seed；
3) adding additive in the ethanol extract of Isatis tinctoria L. leaf, Radix Polygoni Multiflori root, Cacumen Platycladi and fennelflower seed, stirring is all
Even, obtain educating eyebrow liquid.
Preparation method the most according to claim 6, it is characterised in that: add 10 times of mixture quality, volume basis contains
Amount is the alcohol reflux of 70%.
Preparation method the most according to claim 6, it is characterised in that: Isatis tinctoria L. leaf in described extracting solution, Radix Polygoni Multiflori root,
Cacumen Platycladi, the mixture of fennelflower seed are 1:(2-10 with the mass ratio of extracting solution).
Preparation method the most according to claim 8, it is characterised in that: Isatis tinctoria L. leaf in described extracting solution, Radix Polygoni Multiflori root,
Cacumen Platycladi, the mixture of fennelflower seed are 1:5 with the mass ratio of extracting solution.
Preparation method the most according to claim 6, it is characterised in that: described alcohol reflux 2 times, each 1-3 is little
Time.
11. preparation methoies according to claim 10, it is characterised in that: the time of described alcohol reflux is 2 little
Time.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109431893A (en) * | 2018-11-15 | 2019-03-08 | 广州艾蓓生物科技有限公司 | A kind of eyebrow style keeping liquid having repairing effect |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1088775A (en) * | 1992-12-31 | 1994-07-06 | 新疆自治区药物研究所 | Aosiman eye cosmetic and preparation method thereof |
| CN1397266A (en) * | 2002-08-15 | 2003-02-19 | 上海交通大学 | Natural hair-growing cream coated on eyebrow |
| CN101658518A (en) * | 2009-08-19 | 2010-03-03 | 刘庆华 | Application of indirubin for preparing hair culture |
| CN101716129A (en) * | 2009-12-24 | 2010-06-02 | 刘庆华 | Method for preparing eyebrow generating liquid |
| CN102764226A (en) * | 2012-07-13 | 2012-11-07 | 新疆奥斯曼生物资源有限公司 | Eyebrow nourishing liquid, and preparation method and application thereof |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1088775A (en) * | 1992-12-31 | 1994-07-06 | 新疆自治区药物研究所 | Aosiman eye cosmetic and preparation method thereof |
| CN1397266A (en) * | 2002-08-15 | 2003-02-19 | 上海交通大学 | Natural hair-growing cream coated on eyebrow |
| CN101658518A (en) * | 2009-08-19 | 2010-03-03 | 刘庆华 | Application of indirubin for preparing hair culture |
| CN101716129A (en) * | 2009-12-24 | 2010-06-02 | 刘庆华 | Method for preparing eyebrow generating liquid |
| CN102764226A (en) * | 2012-07-13 | 2012-11-07 | 新疆奥斯曼生物资源有限公司 | Eyebrow nourishing liquid, and preparation method and application thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109431893A (en) * | 2018-11-15 | 2019-03-08 | 广州艾蓓生物科技有限公司 | A kind of eyebrow style keeping liquid having repairing effect |
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