CN105919900A - Hair re-growing and hair loss preventing shampoo and preparation method thereof - Google Patents
Hair re-growing and hair loss preventing shampoo and preparation method thereof Download PDFInfo
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- CN105919900A CN105919900A CN201610482781.1A CN201610482781A CN105919900A CN 105919900 A CN105919900 A CN 105919900A CN 201610482781 A CN201610482781 A CN 201610482781A CN 105919900 A CN105919900 A CN 105919900A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
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Abstract
The invention relates to hair re-growing and hair loss preventing shampoo. Firstly, a traditional Chinese medicinal extracting solution is obtained by extracting from a mixed material consisting of cacumen platycladi, radix polygoni multiflora and radix angelicae sinensis according to reasonable ratios; secondly, the obtained traditional Chinese medicinal extracting solution is uniformly mixed with tea tree essential oil and mandarin essential oil according to a proper weight mixture ratio; the finally-prepared hair re-growing and hair loss preventing shampoo contains a herbaceous plant extracting solution and hair loss preventing active components, and can be used as conventional shampoo to supplement water and nutrition of hairs, help scalp recover natural metabolism, prevent hair loss, delay scalp senescence, improve the color and the gloss of the hairs, and enable the hairs to be smoother and glossier; in addition, the hair re-growing and hair loss preventing shampoo has the advantages of easily-obtained raw materials, low cost and remarkable treatment effect; furthermore, according to a method disclosed by the invention, the cacumen platycladi, the radix polygoni multiflora and the radix angelicae sinensis are mixed according to the reasonable ratios to obtain the mixed material, and effective components are extracted from the mixed material according to a specific method. The method has the advantages that the steps are simple and easily-operated and the effective components of the raw materials are low in loss.
Description
Technical field
The invention belongs to cosmetics of everyday use technical field, be specifically related to one and set out again anticreep shampoo and preparation side thereof
Method.
Background technology
" hair is glossy, without dandruff " is classified as important in man's new concept of health one by World Health Organization (WHO),
And dense hair is a glamour man indispensability.But the problems such as alopecia, dandruff, the whitest, root of hair is fragile
It it is the most common hair problem of male.
Alopecia is the phenomenon of alopecia, have physiological and pathologic point.Physiologic alopecia refers to that hair is just
Normal comes off;Pathologic alopecia refers to hair exception or excessive coming off, and its reason is a lot.According to an investigation
Display, the youngster of 60% is perplexed by alopecia, particularly male personage.This swashs mainly due to competition
Immense pressure in the too fast rhythm of life of strong living environment, frequency, working and learning, easily makes human psychological
Anxiety, anxious state of mind, mental distress, additionally, such as smoke, drink, the bad life such as online all night is practised
Used, cause the sickness rate of alopecia in males more and more higher.
Alopecia not only looks and is old for one's age, and also can reduce the confidence that male participates in social activity.But, current city
Although having a lot for the treatment of or the product of prevention alopecia on field, but its effect inconspicuous.
Summary of the invention
In order to solve the problems referred to above that prior art exists, the invention provides one and can effectively prevent hair to take off
The anticreep shampoo and preparation method thereof of setting out again fallen.Anticreep shampoo of setting out again of the present invention, includes draft
Plant extraction liquid and Anti-hair loss composition and effectiveness, supplement hair moisture and nutrition, help scalp recover natural metabolism,
Pre-Anti-hair loss, delays scalp old and feeble, improves the glossy degree of color development and hair, make hair more compliant glossy.
The technical solution adopted in the present invention is:
One is set out anticreep shampoo again, and raw material components includes:
Cacumen Platycladi, 0.5~3 weight portions;
Radix Polygoni Multiflori, 0.5~3 weight portions;
Angelica root, 0.5~3 weight portions;
Tea tree ethereal oil, 0.1~1 weight portion;
Sweet orange oil, 0.1~1 weight portion.
The raw material components of anticreep shampoo of setting out again described in Jin Yibuyouxuan includes:
Cacumen Platycladi, 2 weight portions;
Radix Polygoni Multiflori, 2 weight portions;
Angelica root, 2 weight portions;
Tea tree ethereal oil, 0.5 weight portion;
Sweet orange oil, 0.5 weight portion.
The raw material components of described anticreep shampoo of setting out again also include 2~6 weight portion sodium lauryl sulfate, 12~
18 weight portion sodium laureth sulfate, 2~6 weight portion cocamido propyl betaine, 0.5~2 weight
Part Ethylene Glycol Distearate, 0.1~1 weight portion cetearyl alcohol, 0.1~0.6 weight portion Polyquaternium-10,
0.1~0.6 weight portion guar gum, 0.1~0.6 weight portion DMDM Hydantoin, 0.05~0.2 weight portion
Citric acid, 0.05~0.2 weight portion EDTA-disodium, 0.1~0.5 weight portion methyl hydroxybenzoate, 0.1~0.4 weight
Amount part ethyl hydroxybenzoate.
A kind of method preparing described anticreep shampoo of setting out again, comprises the steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to described weight portion and be sufficiently mixed,
Obtain compound;
(2) in gained compound, add deionized water to carry out boiling carrying, obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, add deionized water to carry out boiling carrying, obtain the second medicinal liquid
With the second medicinal residues;
(4) obtaining stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution is through for the first time
Heating is concentrated under reduced pressure to give concentrated solution;
(5) ethanol adding 1~4 times of volume in step (4) described concentrated solution settles, and has settled
Carry out after one-tenth filtering and collecting filtrate;
(6) step (5) described filtrate is carried out second time and heat concentrating under reduced pressure, whole ethanol is evaporated off,
To Chinese medicine extraction liquid;
(7) in step (6) described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed
Uniformly, obtain described in set out again anticreep shampoo.
The preparation method of the most described anticreep shampoo of setting out again, comprises the steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to described weight portion and be sufficiently mixed,
Obtain compound;
(2) in gained compound, add deionized water to carry out boiling carrying, obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, add deionized water to carry out boiling carrying, obtain the second medicinal liquid
With the second medicinal residues;
(4) obtaining stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution is through for the first time
Heating is concentrated under reduced pressure to give concentrated solution;
(5) ethanol adding 1~4 times of volume in step (4) described concentrated solution settles, and has settled
Carry out after one-tenth filtering and collecting filtrate;
(6) step (5) described filtrate is carried out second time and heat concentrating under reduced pressure, whole ethanol is evaporated off,
To Chinese medicine extraction liquid;
(7) in step (6) described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed
Uniformly, sodium lauryl sulfate, sodium laureth sulfate, cocamidopropyl propyl amide it are sequentially added into afterwards sweet
Dish alkali, Ethylene Glycol Distearate, cetearyl alcohol, Polyquaternium-10, guar gum, DMDM second
Interior uride, citric acid, EDTA-disodium, methyl hydroxybenzoate, ethyl hydroxybenzoate, be sufficiently mixed uniformly, obtain institute
State anticreep shampoo of setting out again.
In step (2), the mass ratio of described compound and described deionized water is 1:6~1:9, described in boil and carry
Carrying out for normal pressure, temperature is 95~100 DEG C, and extraction time is 0.5~3h.
In step (3), the mass ratio of described first medicinal residues and described deionized water is 1:6~1:9, described in boil
Carrying and carrying out for normal pressure, temperature is 95~100 DEG C, and extraction time is 0.5~3h.
Step (4) is carried out described first time heating concentrating under reduced pressure temperature be 63~68 DEG C, pressure be-0.04~
-0.07MPa, described concentrated solution is 1:2~1:4 with the mass ratio of described stock solution.
Described in step (5), the volumetric concentration of ethanol is 60~80%, carry out time of described sedimentation be 12~
36h。
Step (6) is carried out described second time heating concentrating under reduced pressure temperature be 40~50 DEG C, pressure be-0.04~
-0.07MPa, the time carrying out described second time heating concentrating under reduced pressure is 2~5h.
For the ease of understanding the present invention, below the raw material in the present invention and drug effect are further elaborated.
Cacumen Platycladi: for Cupressaceae aiphyllium young leaf of plant, gas delicate fragrance, bitter and puckery flavor, micro-pungent.Cooling blood for hemostasis,
Growing and blacking hair, for heat in blood alopecia, early whitening of beard and hair." Compendium of Materia Medica valley " is recorded: " hair is not given birth to.With
Cacumen Platycladi is dried in the shade and grinds into powder, and Oleum Sesami is embrocated.”
Radix Polygoni Multiflori: bitter in the mouth, sweet, puckery, warm in nature.There are tonifying liver, kidney tonifying, nourish blood, the effect dispeled the wind.For
Treatment hepatic and renal YIN deficiency, sending out must be the whitest, and blood deficiency is dizzy, and waist knee joint is weak, and muscles and bones is ached, seminal emission, metrorrhagia and leukorrhagia, for a long time
Malaria, chronic dysentery, chronic hepatitis, carbuncle, scrofula, hemorrhoidal hamorrhage, haemorrhoids.
Angelica root: sweet in the mouth, pungent, warm in nature.There is effect of replenishing and activating blood, menstruction regulating and pain relieving, loosening bowel to relieve constipation.With
In treatment blood deficiency and yellow complexion, dizziness cardiopalmus, menoxenia, amenorrhea dysmenorrhoea, asthenia cold abdominalgia, rheumatic arthralgia, fall
Beat the diseases such as damage, dryness of the intestine constipation.Radix Angelicae Sinensis is with its Gan Run to enrich blood, and pungent scattered temperature passes to invigorate blood circulation, and can enrich blood,
Can invigorate blood circulation again, be described as " the gas medicine in blood, the panacea in blood ".
Tea tree ethereal oil originates in Australia, for the extract of Camellia sinensis.There is bactericidal antiphlogistic, convergence pore, treatment
Common Cold, cough, rhinitis, asthma, improve the effects such as dysmenorrhea, menoxenia and genital infection.Suitable
For oiliness and acne-prone skin, treatment suppurative wound and burn, tan severely, tinea pedis and dandruff.Make brains clear
Wake up, rejuvenate, anti-depression.
Sweet orange oil, is one of contrastimulant quintessence oil of minority, has the sweet orange oil of Fructus Citri sinensis fragrance,
Intense strain and pressure can be expelled, improve the insomnia caused by anxiety, owing to Pericarpium Citri junoris containing substantial amounts of dimension
He orders C, can preventing cold, skin is had moistening effect, can balance skin the salty value of acid, help collagen shape
Becoming, the growth for bodily tissue has good effect with repairing.Diaphoresis can be promoted, thus can help to block
Skin discharge toxin, the most helpful to oiliness, skin sore or dry skin person.
The invention have the benefit that
1, anticreep shampoo of setting out again of the present invention, by first from Cacumen Platycladi, Radix Polygoni Multiflori, angelica root according to
The compound of rational proportion composition extracts and obtains Chinese medicine extraction liquid, then by gained Chinese medicine extraction liquid and Camellia sinensis essence
Oil and sweet orange oil carry out mix homogeneously according to applicable weight proportion, final prepared setting out again in anticreep shampoo
Containing herbaceous plant extracting solution and Anti-hair loss composition and effectiveness, can use as conventional shampoo, supplement hair moisture
Recover natural metabolism, pre-Anti-hair loss with nutrition, help scalp, delay scalp old and feeble, improve color development and hair
Glossy degree, make hair more compliant glossy, and raw material be easy to get, low cost, therapeutic effect is obvious.
2, anticreep shampoo of setting out again of the present invention, by by Cacumen Platycladi, Radix Polygoni Multiflori, angelica root according to conjunction
The compound of reason proportioning composition extracts and obtains Chinese medicine extraction liquid, then by gained Chinese medicine extraction liquid and tea tree ethereal oil
Carry out mix homogeneously with sweet orange oil according to applicable weight proportion, be finally also added with sodium lauryl sulfate, the moon
Laureth sodium sulfovinate, cocamido propyl betaine, Ethylene Glycol Distearate, cetearyl alcohol,
Polyquaternium-10, guar gum, DMDM Hydantoin, citric acid, EDTA-disodium, methyl hydroxybenzoate
And ethyl hydroxybenzoate, the final anticreep shampoo of setting out again prepared contains herbaceous plant extracting solution and Anti-hair loss composition and effectiveness,
And can use as conventional shampoo, supplement hair moisture and nutrition, help scalp to recover natural metabolism,
Pre-Anti-hair loss, delays scalp old and feeble, improves the glossy degree of color development and hair, make hair more compliant glossy,
And raw material is easy to get, low cost, therapeutic effect is obvious.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further elaborated.
Following example represent 1g with 1 weight portion.
Embodiment 1
The present embodiment provides one to set out anticreep shampoo again, and its raw material components includes:
0.5 weight portion Cacumen Platycladi, 3 weight portion Radix Polygoni Multiflori, 0.5 weight portion angelica root, 1 weight portion tea tree ethereal oil,
0.1 weight portion sweet orange oil.
A kind of method preparing described anticreep shampoo of setting out again, comprises the steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to above-mentioned weight portion and be sufficiently mixed,
Obtain compound;
(2) in gained compound, add the deionized water of 6 times of quality, be placed in extraction still at 95~100 DEG C
Under the conditions of carry out normal pressure and boil and carry 3h, obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, the deionized water of 6 times of quality is added at 95~100 DEG C
Under the conditions of carry out normal pressure and boil and carry 3h, obtain the second medicinal liquid and the second medicinal residues;
(4) obtain stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution 63~
68 DEG C ,-0.04~-0.07MPa carry out heating for the first time being concentrated under reduced pressure to give concentrated solution, and described concentrated solution is institute
State the 1/2 of stock solution quality;
(5) in step (4) described concentrated solution, add 1 times of volume ethanol (volumetric concentration is 60%) to enter
Row sedimentation 12h, carries out after having settled filtering and collecting filtrate;
(6) at 40~50 DEG C ,-0.04~-0.07MPa, step (5) described filtrate is carried out second time to heat
Concentrating under reduced pressure 5h, is evaporated off whole ethanol, obtains Chinese medicine extraction liquid;
(7) in step (6) described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed
Uniformly, obtain described in set out again anticreep shampoo.
Embodiment 2
The present embodiment provides one to set out anticreep shampoo again, and its raw material components includes:
3 weight portion Cacumen Platycladis, 0.5 weight portion Radix Polygoni Multiflori, 3 weight portion angelica roots, 0.1 weight portion tea tree ethereal oil,
1 weight portion sweet orange oil, 2 weight portion sodium lauryl sulfate, 18 weight portion sodium laureth sulfate,
2 weight portion cocamido propyl betaine, 2 weight portion Ethylene Glycol Distearate, 0.1 weight portion spermaceti are hard
Acyl in lipidol, 0.6 weight portion Polyquaternium-10,0.1 weight portion guar gum, 0.6 weight portion DMDM second
Urea, 0.05 parts by weight of lemon acid, 0.2 weight portion EDTA-disodium, 0.1 weight portion methyl hydroxybenzoate, 0.4 weight
Part ethyl hydroxybenzoate.
A kind of method preparing described anticreep shampoo of setting out again, comprises the steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to above-mentioned weight portion and be sufficiently mixed,
Obtain compound;
(2) in gained compound, add the deionized water of 9 times of quality, be placed in extraction still at 95~100 DEG C
Under the conditions of carry out normal pressure and boil and carry 0.5h, obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, the deionized water of 9 times of quality is added at 95~100 DEG C
Under the conditions of carry out normal pressure and boil and carry 0.5h, obtain the second medicinal liquid and the second medicinal residues;
(4) obtain stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution 63~
68 DEG C ,-0.04~-0.07MPa carry out heating for the first time being concentrated under reduced pressure to give concentrated solution, and described concentrated solution is institute
State the 1/4 of stock solution quality;
(5) in step (4) described concentrated solution, add the ethanol (volumetric concentration is 80%) of 4 times of volumes
Carry out settling 36h, carry out after having settled filtering and collecting filtrate;
(6) at 40~50 DEG C ,-0.04~-0.07MPa, step (5) described filtrate is carried out second time to heat
Concentrating under reduced pressure 2h, is evaporated off whole ethanol, obtains Chinese medicine extraction liquid;
(7) in step (6) described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed
Uniformly, sodium lauryl sulfate, sodium laureth sulfate, cocamidopropyl propyl amide it are sequentially added into afterwards sweet
Dish alkali, Ethylene Glycol Distearate, cetearyl alcohol, Polyquaternium-10, guar gum, DMDM second
Interior uride, citric acid, EDTA-disodium, methyl hydroxybenzoate, ethyl hydroxybenzoate, be sufficiently mixed uniformly, obtain institute
State anticreep shampoo of setting out again.
Embodiment 3
The present embodiment provides one to set out anticreep shampoo again, and its raw material components includes:
2 weight portion Cacumen Platycladis, 2 weight portion Radix Polygoni Multiflori, 2 weight portion angelica roots, 0.5 weight portion tea tree ethereal oil,
0.5 weight portion sweet orange oil, 6 weight portion sodium lauryl sulfate, 12 weight portion sodium laureth sulfate,
6 weight portion cocamido propyl betaine, 0.5 weight portion Ethylene Glycol Distearate, 1 weight portion spermaceti are hard
Acyl in lipidol, 0.1 weight portion Polyquaternium-10,0.6 weight portion guar gum, 0.1 weight portion DMDM second
Urea, 0.2 parts by weight of lemon acid, 0.05 weight portion EDTA-disodium, 0.5 weight portion methyl hydroxybenzoate, 0.1 weight
Part ethyl hydroxybenzoate.
A kind of method preparing described anticreep shampoo of setting out again, comprises the steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to above-mentioned weight portion and be sufficiently mixed,
Obtain compound;
(2) in gained compound, add the deionized water of 8 times of quality, be placed in extraction still at 95~100 DEG C
Under the conditions of carry out normal pressure and boil and carry 1.5h, obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, the deionized water of 8 times of quality is added at 95~100 DEG C
Under the conditions of carry out normal pressure and boil and carry 1.5h, obtain the second medicinal liquid and the second medicinal residues;
(4) obtain stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution 63~
68 DEG C ,-0.04~-0.07MPa carry out heating for the first time being concentrated under reduced pressure to give concentrated solution, and described concentrated solution is institute
State the 1/3 of stock solution quality;
(5) in step (4) described concentrated solution, add the ethanol (volumetric concentration is 60%) of 2 times of volumes
Carry out settling 12h, carry out after having settled filtering and collecting filtrate;
(6) at 40~50 DEG C ,-0.04~-0.07MPa, step (5) described filtrate is carried out second time to heat
Concentrating under reduced pressure 3h, is evaporated off whole ethanol, obtains Chinese medicine extraction liquid;
(7) in described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed uniformly, afterwards
It is sequentially added into sodium lauryl sulfate, sodium laureth sulfate, cocamido propyl betaine, second two
Alcohol double stearate, cetearyl alcohol, Polyquaternium-10, guar gum, DMDM Hydantoin, lemon
Lemon acid, EDTA-disodium, methyl hydroxybenzoate, ethyl hydroxybenzoate, be sufficiently mixed uniformly, obtain described in set out again anti-
De-shampoo.
Embodiment 4
The present embodiment provides one to set out anticreep shampoo again, and its raw material components includes:
1 weight portion Cacumen Platycladi, 1 weight portion Radix Polygoni Multiflori, 1 weight portion angelica root, 0.4 weight portion tea tree ethereal oil,
0.4 weight portion sweet orange oil, 4 weight portion sodium lauryl sulfate, 15 weight portion sodium laureth sulfate,
5 weight portion cocamido propyl betaine, 1 weight portion Ethylene Glycol Distearate, 0.5 weight portion spermaceti are hard
Acyl in lipidol, 0.3 weight portion Polyquaternium-10,0.3 weight portion guar gum, 0.3 weight portion DMDM second
Urea, 0.1 parts by weight of lemon acid, 0.1 weight portion EDTA-disodium, 0.25 weight portion methyl hydroxybenzoate, 0.2 weight
Part ethyl hydroxybenzoate.
A kind of method preparing described anticreep shampoo of setting out again, comprises the steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to above-mentioned weight portion and be sufficiently mixed,
Obtain compound;
(2) in gained compound, add the deionized water of 8 times of quality, be placed in extraction still at 95~100 DEG C
Under the conditions of carry out normal pressure and boil and carry 3 hours, obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, the deionized water of 8 times of quality is added at 95~100 DEG C
Under the conditions of carry out normal pressure and boil and carry 0.5h, obtain the second medicinal liquid and the second medicinal residues;
(4) obtain stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution 63~
68 DEG C ,-0.04~-0.07MPa carry out heating for the first time being concentrated under reduced pressure to give concentrated solution, and described concentrated solution is institute
State the 1/2 of stock solution quality;
(5) in step (4) described concentrated solution, add the ethanol (volumetric concentration is 60%) of 2 times of volumes
Carry out settling 36h, carry out after having settled filtering and collecting filtrate;
(6) at 40~50 DEG C ,-0.04~-0.07MPa, step (5) described filtrate is carried out second time to heat
Concentrating under reduced pressure 3h, is evaporated off whole ethanol, obtains Chinese medicine extraction liquid;
(7) in step (6) described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed
Uniformly, sodium lauryl sulfate, sodium laureth sulfate, cocamidopropyl propyl amide it are sequentially added into afterwards sweet
Dish alkali, Ethylene Glycol Distearate, cetearyl alcohol, Polyquaternium-10, guar gum, DMDM second
Interior uride, citric acid, EDTA-disodium, methyl hydroxybenzoate, ethyl hydroxybenzoate, be sufficiently mixed uniformly, obtain institute
State anticreep shampoo of setting out again.
Embodiment 5
The present embodiment provides one to set out anticreep shampoo again, and its raw material components includes:
1 weight portion Cacumen Platycladi, 2 weight portion Radix Polygoni Multiflori, 1 weight portion angelica root, 0.8 weight portion tea tree ethereal oil,
0.6 weight portion sweet orange oil, 4 weight portion sodium lauryl sulfate, 15 weight portion sodium laureth sulfate,
5 weight portion cocamido propyl betaine, 1 weight portion Ethylene Glycol Distearate, 0.5 weight portion spermaceti are hard
Acyl in lipidol, 0.3 weight portion Polyquaternium-10,0.3 weight portion guar gum, 0.3 weight portion DMDM second
Urea, 0.1 parts by weight of lemon acid, 0.1 weight portion EDTA-disodium, 0.25 weight portion methyl hydroxybenzoate, 0.2 weight
Part ethyl hydroxybenzoate.
A kind of method preparing described anticreep shampoo of setting out again, comprises the steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to above-mentioned weight portion and be sufficiently mixed,
Obtain compound;
(2) in gained compound, add the deionized water of 9 times of quality, be placed in extraction still at 95~100 DEG C
Under the conditions of carry out normal pressure and boil and carry 2h and obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, the deionized water of 9 times of quality is added at 95~100 DEG C
Under the conditions of carry out normal pressure and boil and carry 2h, obtain the second medicinal liquid and the second medicinal residues;
(4) obtain stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution 63~
68 DEG C ,-0.04~-0.07MPa carry out heating for the first time being concentrated under reduced pressure to give concentrated solution, and described concentrated solution is institute
State the 1/2 of stock solution quality;
(5) in step (4) described concentrated solution, add the ethanol (volumetric concentration is 65%) of 2 times of volumes
Carry out settling 12h, carry out after having settled filtering and collecting filtrate;
(6) at 40~50 DEG C ,-0.04~-0.07MPa, step (5) described filtrate is carried out second time to heat
Concentrating under reduced pressure 3h, is evaporated off whole ethanol, obtains Chinese medicine extraction liquid;
(7) in step (6) described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed
Uniformly, sodium lauryl sulfate, sodium laureth sulfate, cocamidopropyl propyl amide it are sequentially added into afterwards sweet
Dish alkali, Ethylene Glycol Distearate, cetearyl alcohol, Polyquaternium-10, guar gum, DMDM second
Interior uride, citric acid, EDTA-disodium, methyl hydroxybenzoate, ethyl hydroxybenzoate, be sufficiently mixed uniformly, obtain institute
State anticreep shampoo of setting out again.
Embodiment 6
The present embodiment provides one to set out anticreep shampoo again, and its raw material components includes:
1 weight portion Cacumen Platycladi, 2 weight portion Radix Polygoni Multiflori, 1 weight portion angelica root, 0.6 weight portion tea tree ethereal oil,
0.4 weight portion sweet orange oil, 4 weight portion sodium lauryl sulfate, 15 weight portion sodium laureth sulfate,
5 weight portion cocamido propyl betaine, 1 weight portion Ethylene Glycol Distearate, 0.5 weight portion spermaceti are hard
Acyl in lipidol, 0.3 weight portion Polyquaternium-10,0.3 weight portion guar gum, 0.3 weight portion DMDM second
Urea, 0.1 parts by weight of lemon acid, 0.1 weight portion EDTA-disodium, 0.25 weight portion methyl hydroxybenzoate, 0.2 weight
Part ethyl hydroxybenzoate.
A kind of method preparing described anticreep shampoo of setting out again, comprises the steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to above-mentioned weight portion and be sufficiently mixed,
Obtain compound;
(2) in gained compound, add the deionized water of 6 times of quality, be placed in extraction still at 95~100 DEG C
Under the conditions of carry out normal pressure and boil and carry 1.5h, obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, the deionized water of 6 times of quality is added at 95~100 DEG C
Under the conditions of carry out normal pressure and boil and carry 1.5h, obtain the second medicinal liquid and the second medicinal residues;
(4) obtain stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution through 63~
68 DEG C ,-0.04~-0.07MPa carry out heating for the first time being concentrated under reduced pressure to give concentrated solution, and described concentrated solution is institute
State the 1/2 of stock solution quality;
(5) in step (4) described concentrated solution, add the ethanol (volumetric concentration is 75%) of 2.5 times of volumes
Carry out settling 12h, carry out after having settled filtering and collecting filtrate;
(6) at 40~50 DEG C ,-0.04~-0.07MPa, step (5) described filtrate is carried out second time to heat
Concentrating under reduced pressure 3h, is evaporated off whole ethanol, obtains described Chinese medicine extraction liquid;
(7) in step (6) described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed
Uniformly, sodium lauryl sulfate, sodium laureth sulfate, cocamidopropyl propyl amide it are sequentially added into afterwards sweet
Dish alkali, Ethylene Glycol Distearate, cetearyl alcohol, Polyquaternium-10, guar gum, DMDM second
Interior uride, citric acid, EDTA-disodium, methyl hydroxybenzoate, ethyl hydroxybenzoate, be sufficiently mixed uniformly, obtain institute
State anticreep shampoo of setting out again.
Experimental example
The present inventor is by using anticreep shampoo of setting out again of the present invention to clinical 100 example hair loss patients
Observe, the maleest 53 examples, female 47 example, minimum 26 years old of age, maximum 66 years old.
Using method: wash hair as shampoo once a day, each 10ml.
Efficacy assessment standard:
Cure: alopecia transference cure, 70 examples.
Effective: alopecia symptom is obviously improved, 27 examples.
Invalid: alopecia symptom is not improved 3 examples.Total effective rate 97%.
Typical clinical case:
Wang, man, 28 years old, deskman, alopecia when washing hair of combing one's hair was a lot of, uses the present invention real
After executing the anticreep shampoo 30 days of setting out again described in example 3, hair the most no longer comes off, the color development of hair and gloss
Degree all has clear improvement.
Lu, female, 33 years old, certain enterprise personnel, alopecia was serious, and hair is sparse withered and yellow, uses the present invention real
After executing the anticreep shampoo 40 days of setting out again described in example 4, alopecia phenomenon is obviously improved, and adheres to using 80
In the future, the most no longer alopecia, color development blackening, glossy.
Chen, man, 58 years old, peasant, alopecia was serious, and setting out again described in the use embodiment of the present invention 5 is anti-
After de-shampoo 90 days, hair no longer comes off.
The present invention is not limited to above-mentioned preferred forms, and anyone can draw it under the enlightenment of the present invention
His various forms of products, no matter but in its shape or structure, make any change, every have and the application
Technical scheme as same or like, within all falling within protection scope of the present invention.
Claims (10)
1. an anticreep shampoo of setting out again, it is characterised in that raw material components includes:
Cacumen Platycladi, 0.5~3 weight portions;
Radix Polygoni Multiflori, 0.5~3 weight portions;
Angelica root, 0.5~3 weight portions;
Tea tree ethereal oil, 0.1~1 weight portion;
Sweet orange oil, 0.1~1 weight portion.
Anticreep shampoo of setting out again the most according to claim 1, it is characterised in that raw material components includes:
Cacumen Platycladi, 2 weight portions;
Radix Polygoni Multiflori, 2 weight portions;
Angelica root, 2 weight portions;
Tea tree ethereal oil, 0.5 weight portion;
Sweet orange oil, 0.5 weight portion.
Anticreep shampoo of setting out again the most according to claim 1 and 2, it is characterised in that raw material components is also
Including 2~6 weight portion sodium lauryl sulfate, 12~18 weight portion sodium laureth sulfate, 2~6
Weight portion cocamido propyl betaine, 0.5~2 weight portion Ethylene Glycol Distearate, 0.1~1 weight portion
Cetearyl alcohol, 0.1~0.6 weight portion Polyquaternium-10,0.1~0.6 weight portion guar gum, 0.1~0.6
Weight portion DMDM Hydantoin, 0.05~0.2 parts by weight of lemon acid, 0.05~0.2 weight portion EDTA-
Disodium, 0.1~0.5 weight portion methyl hydroxybenzoate, 0.1~0.4 weight portion ethyl hydroxybenzoate.
4. the method for the anticreep shampoo of setting out again prepared described in claim 1, it is characterised in that include
Following steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to described weight portion and be sufficiently mixed,
Obtain compound;
(2) in gained compound, add deionized water to carry out boiling carrying, obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, add deionized water to carry out boiling again carrying, obtain the second medicine
Liquid and the second medicinal residues;
(4) obtaining stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution is through for the first time
Heating is concentrated under reduced pressure to give concentrated solution;
(5) ethanol adding 1~4 times of volume in step (4) described concentrated solution settles, and has settled
Carry out after one-tenth filtering and collecting filtrate;
(6) step (5) described filtrate is carried out second time and heat concentrating under reduced pressure, whole ethanol is evaporated off,
To Chinese medicine extraction liquid;
(7) in step (6) described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed
Uniformly, obtain described in set out again anticreep shampoo.
5. the method for the anticreep shampoo of setting out again prepared described in claim 3, it is characterised in that include
Following steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to described weight portion and be sufficiently mixed,
Obtain compound;
(2) in gained compound, add deionized water to carry out boiling carrying, obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, add deionized water to carry out boiling carrying, obtain the second medicinal liquid
With the second medicinal residues;
(4) obtaining stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution is through for the first time
Heating is concentrated under reduced pressure to give concentrated solution;
(5) ethanol adding 1~4 times of volume in step (4) described concentrated solution settles, and has settled
Carry out after one-tenth filtering and collecting filtrate;
(6) step (5) described filtrate is carried out second time and heat concentrating under reduced pressure, whole ethanol is evaporated off,
To Chinese medicine extraction liquid;
(7) in step (6) described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed
Uniformly, sodium lauryl sulfate, sodium laureth sulfate, cocamidopropyl propyl amide it are sequentially added into afterwards sweet
Dish alkali, Ethylene Glycol Distearate, cetearyl alcohol, Polyquaternium-10, guar gum, DMDM second
Interior uride, citric acid, EDTA-disodium, methyl hydroxybenzoate, ethyl hydroxybenzoate, be sufficiently mixed uniformly, obtain institute
State anticreep shampoo of setting out again.
6. according to the method for the anticreep shampoo of setting out again described in claim 4 or 5, it is characterised in that step
(2), in, the mass ratio of described compound and described deionized water is 1:6~1:9, described in boil to carry and enter for normal pressure
OK, temperature is 95~100 DEG C, and extraction time is 0.5~3h.
7. according to the method for the anticreep shampoo of setting out again described in claim 4 or 5, it is characterised in that step
(3), in, the mass ratio of described first medicinal residues and described deionized water is 1:6~1:9, described in boil and carry as normal pressure
Carrying out, temperature is 95~100 DEG C, and extraction time is 0.5~3h.
8. according to the method for the anticreep shampoo of setting out again described in claim 4 or 5, it is characterised in that step
(4) carry out in described first time heating concentrating under reduced pressure temperature be 63~68 DEG C, pressure be-0.04~
-0.07MPa, described concentrated solution is 1:2~1:4 with the mass ratio of described stock solution.
9. according to the method for the anticreep shampoo of setting out again described in claim 4 or 5, it is characterised in that step
(5) volumetric concentration of ethanol described in is 60~80%, and the time carrying out described sedimentation is 12~36h.
10. according to the method for the anticreep shampoo of setting out again described in claim 4 or 5, it is characterised in that step
Suddenly (6) are carried out described second time heating concentrating under reduced pressure temperature be 40~50 DEG C, pressure be-0.04~
-0.07MPa, the time carrying out described second time heating concentrating under reduced pressure is 2~5h.
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CN108042403A (en) * | 2018-02-05 | 2018-05-18 | 淮安智品企业管理有限公司 | A kind of no silicone oil anticreep hair-care shampoo |
CN108403607A (en) * | 2018-05-31 | 2018-08-17 | 云南健牛生物科技有限公司 | A kind of natural hair oil preparation method |
CN110025510A (en) * | 2019-05-29 | 2019-07-19 | 龙春艳 | Essential oils of herbs shampoo and preparation method thereof |
CN111714436A (en) * | 2020-07-24 | 2020-09-29 | 南京佰宏卓越科技有限公司 | Anti-hair loss shampoo and preparation method thereof |
CN113069390A (en) * | 2020-01-06 | 2021-07-06 | 广州樱奈儿化妆品有限公司 | Anti-hair-loss hair-growing lotion and preparation method thereof |
CN115836992A (en) * | 2023-02-27 | 2023-03-24 | 北京普世安生物科技有限公司 | Anti-hair loss shampoo and preparation method thereof |
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CN108042403A (en) * | 2018-02-05 | 2018-05-18 | 淮安智品企业管理有限公司 | A kind of no silicone oil anticreep hair-care shampoo |
CN108403607A (en) * | 2018-05-31 | 2018-08-17 | 云南健牛生物科技有限公司 | A kind of natural hair oil preparation method |
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CN113069390A (en) * | 2020-01-06 | 2021-07-06 | 广州樱奈儿化妆品有限公司 | Anti-hair-loss hair-growing lotion and preparation method thereof |
CN111714436A (en) * | 2020-07-24 | 2020-09-29 | 南京佰宏卓越科技有限公司 | Anti-hair loss shampoo and preparation method thereof |
CN111714436B (en) * | 2020-07-24 | 2021-05-07 | 佛山市百分之秀化妆品有限公司 | Anti-hair loss shampoo and preparation method thereof |
CN115836992A (en) * | 2023-02-27 | 2023-03-24 | 北京普世安生物科技有限公司 | Anti-hair loss shampoo and preparation method thereof |
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