CN105919900A - Hair re-growing and hair loss preventing shampoo and preparation method thereof - Google Patents

Hair re-growing and hair loss preventing shampoo and preparation method thereof Download PDF

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Publication number
CN105919900A
CN105919900A CN201610482781.1A CN201610482781A CN105919900A CN 105919900 A CN105919900 A CN 105919900A CN 201610482781 A CN201610482781 A CN 201610482781A CN 105919900 A CN105919900 A CN 105919900A
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weight portion
hair
shampoo
out again
anticreep shampoo
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吴庆辉
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Beijing Universal Biotechnology Co Ltd
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Beijing Universal Biotechnology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q7/00Preparations for affecting hair growth

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  • Gerontology & Geriatric Medicine (AREA)
  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Cosmetics (AREA)

Abstract

The invention relates to hair re-growing and hair loss preventing shampoo. Firstly, a traditional Chinese medicinal extracting solution is obtained by extracting from a mixed material consisting of cacumen platycladi, radix polygoni multiflora and radix angelicae sinensis according to reasonable ratios; secondly, the obtained traditional Chinese medicinal extracting solution is uniformly mixed with tea tree essential oil and mandarin essential oil according to a proper weight mixture ratio; the finally-prepared hair re-growing and hair loss preventing shampoo contains a herbaceous plant extracting solution and hair loss preventing active components, and can be used as conventional shampoo to supplement water and nutrition of hairs, help scalp recover natural metabolism, prevent hair loss, delay scalp senescence, improve the color and the gloss of the hairs, and enable the hairs to be smoother and glossier; in addition, the hair re-growing and hair loss preventing shampoo has the advantages of easily-obtained raw materials, low cost and remarkable treatment effect; furthermore, according to a method disclosed by the invention, the cacumen platycladi, the radix polygoni multiflora and the radix angelicae sinensis are mixed according to the reasonable ratios to obtain the mixed material, and effective components are extracted from the mixed material according to a specific method. The method has the advantages that the steps are simple and easily-operated and the effective components of the raw materials are low in loss.

Description

Set out again anticreep shampoo and preparation method thereof
Technical field
The invention belongs to cosmetics of everyday use technical field, be specifically related to one and set out again anticreep shampoo and preparation side thereof Method.
Background technology
" hair is glossy, without dandruff " is classified as important in man's new concept of health one by World Health Organization (WHO), And dense hair is a glamour man indispensability.But the problems such as alopecia, dandruff, the whitest, root of hair is fragile It it is the most common hair problem of male.
Alopecia is the phenomenon of alopecia, have physiological and pathologic point.Physiologic alopecia refers to that hair is just Normal comes off;Pathologic alopecia refers to hair exception or excessive coming off, and its reason is a lot.According to an investigation Display, the youngster of 60% is perplexed by alopecia, particularly male personage.This swashs mainly due to competition Immense pressure in the too fast rhythm of life of strong living environment, frequency, working and learning, easily makes human psychological Anxiety, anxious state of mind, mental distress, additionally, such as smoke, drink, the bad life such as online all night is practised Used, cause the sickness rate of alopecia in males more and more higher.
Alopecia not only looks and is old for one's age, and also can reduce the confidence that male participates in social activity.But, current city Although having a lot for the treatment of or the product of prevention alopecia on field, but its effect inconspicuous.
Summary of the invention
In order to solve the problems referred to above that prior art exists, the invention provides one and can effectively prevent hair to take off The anticreep shampoo and preparation method thereof of setting out again fallen.Anticreep shampoo of setting out again of the present invention, includes draft Plant extraction liquid and Anti-hair loss composition and effectiveness, supplement hair moisture and nutrition, help scalp recover natural metabolism, Pre-Anti-hair loss, delays scalp old and feeble, improves the glossy degree of color development and hair, make hair more compliant glossy.
The technical solution adopted in the present invention is:
One is set out anticreep shampoo again, and raw material components includes:
Cacumen Platycladi, 0.5~3 weight portions;
Radix Polygoni Multiflori, 0.5~3 weight portions;
Angelica root, 0.5~3 weight portions;
Tea tree ethereal oil, 0.1~1 weight portion;
Sweet orange oil, 0.1~1 weight portion.
The raw material components of anticreep shampoo of setting out again described in Jin Yibuyouxuan includes:
Cacumen Platycladi, 2 weight portions;
Radix Polygoni Multiflori, 2 weight portions;
Angelica root, 2 weight portions;
Tea tree ethereal oil, 0.5 weight portion;
Sweet orange oil, 0.5 weight portion.
The raw material components of described anticreep shampoo of setting out again also include 2~6 weight portion sodium lauryl sulfate, 12~ 18 weight portion sodium laureth sulfate, 2~6 weight portion cocamido propyl betaine, 0.5~2 weight Part Ethylene Glycol Distearate, 0.1~1 weight portion cetearyl alcohol, 0.1~0.6 weight portion Polyquaternium-10, 0.1~0.6 weight portion guar gum, 0.1~0.6 weight portion DMDM Hydantoin, 0.05~0.2 weight portion Citric acid, 0.05~0.2 weight portion EDTA-disodium, 0.1~0.5 weight portion methyl hydroxybenzoate, 0.1~0.4 weight Amount part ethyl hydroxybenzoate.
A kind of method preparing described anticreep shampoo of setting out again, comprises the steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to described weight portion and be sufficiently mixed, Obtain compound;
(2) in gained compound, add deionized water to carry out boiling carrying, obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, add deionized water to carry out boiling carrying, obtain the second medicinal liquid With the second medicinal residues;
(4) obtaining stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution is through for the first time Heating is concentrated under reduced pressure to give concentrated solution;
(5) ethanol adding 1~4 times of volume in step (4) described concentrated solution settles, and has settled Carry out after one-tenth filtering and collecting filtrate;
(6) step (5) described filtrate is carried out second time and heat concentrating under reduced pressure, whole ethanol is evaporated off, To Chinese medicine extraction liquid;
(7) in step (6) described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed Uniformly, obtain described in set out again anticreep shampoo.
The preparation method of the most described anticreep shampoo of setting out again, comprises the steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to described weight portion and be sufficiently mixed, Obtain compound;
(2) in gained compound, add deionized water to carry out boiling carrying, obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, add deionized water to carry out boiling carrying, obtain the second medicinal liquid With the second medicinal residues;
(4) obtaining stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution is through for the first time Heating is concentrated under reduced pressure to give concentrated solution;
(5) ethanol adding 1~4 times of volume in step (4) described concentrated solution settles, and has settled Carry out after one-tenth filtering and collecting filtrate;
(6) step (5) described filtrate is carried out second time and heat concentrating under reduced pressure, whole ethanol is evaporated off, To Chinese medicine extraction liquid;
(7) in step (6) described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed Uniformly, sodium lauryl sulfate, sodium laureth sulfate, cocamidopropyl propyl amide it are sequentially added into afterwards sweet Dish alkali, Ethylene Glycol Distearate, cetearyl alcohol, Polyquaternium-10, guar gum, DMDM second Interior uride, citric acid, EDTA-disodium, methyl hydroxybenzoate, ethyl hydroxybenzoate, be sufficiently mixed uniformly, obtain institute State anticreep shampoo of setting out again.
In step (2), the mass ratio of described compound and described deionized water is 1:6~1:9, described in boil and carry Carrying out for normal pressure, temperature is 95~100 DEG C, and extraction time is 0.5~3h.
In step (3), the mass ratio of described first medicinal residues and described deionized water is 1:6~1:9, described in boil Carrying and carrying out for normal pressure, temperature is 95~100 DEG C, and extraction time is 0.5~3h.
Step (4) is carried out described first time heating concentrating under reduced pressure temperature be 63~68 DEG C, pressure be-0.04~ -0.07MPa, described concentrated solution is 1:2~1:4 with the mass ratio of described stock solution.
Described in step (5), the volumetric concentration of ethanol is 60~80%, carry out time of described sedimentation be 12~ 36h。
Step (6) is carried out described second time heating concentrating under reduced pressure temperature be 40~50 DEG C, pressure be-0.04~ -0.07MPa, the time carrying out described second time heating concentrating under reduced pressure is 2~5h.
For the ease of understanding the present invention, below the raw material in the present invention and drug effect are further elaborated.
Cacumen Platycladi: for Cupressaceae aiphyllium young leaf of plant, gas delicate fragrance, bitter and puckery flavor, micro-pungent.Cooling blood for hemostasis, Growing and blacking hair, for heat in blood alopecia, early whitening of beard and hair." Compendium of Materia Medica valley " is recorded: " hair is not given birth to.With Cacumen Platycladi is dried in the shade and grinds into powder, and Oleum Sesami is embrocated.”
Radix Polygoni Multiflori: bitter in the mouth, sweet, puckery, warm in nature.There are tonifying liver, kidney tonifying, nourish blood, the effect dispeled the wind.For Treatment hepatic and renal YIN deficiency, sending out must be the whitest, and blood deficiency is dizzy, and waist knee joint is weak, and muscles and bones is ached, seminal emission, metrorrhagia and leukorrhagia, for a long time Malaria, chronic dysentery, chronic hepatitis, carbuncle, scrofula, hemorrhoidal hamorrhage, haemorrhoids.
Angelica root: sweet in the mouth, pungent, warm in nature.There is effect of replenishing and activating blood, menstruction regulating and pain relieving, loosening bowel to relieve constipation.With In treatment blood deficiency and yellow complexion, dizziness cardiopalmus, menoxenia, amenorrhea dysmenorrhoea, asthenia cold abdominalgia, rheumatic arthralgia, fall Beat the diseases such as damage, dryness of the intestine constipation.Radix Angelicae Sinensis is with its Gan Run to enrich blood, and pungent scattered temperature passes to invigorate blood circulation, and can enrich blood, Can invigorate blood circulation again, be described as " the gas medicine in blood, the panacea in blood ".
Tea tree ethereal oil originates in Australia, for the extract of Camellia sinensis.There is bactericidal antiphlogistic, convergence pore, treatment Common Cold, cough, rhinitis, asthma, improve the effects such as dysmenorrhea, menoxenia and genital infection.Suitable For oiliness and acne-prone skin, treatment suppurative wound and burn, tan severely, tinea pedis and dandruff.Make brains clear Wake up, rejuvenate, anti-depression.
Sweet orange oil, is one of contrastimulant quintessence oil of minority, has the sweet orange oil of Fructus Citri sinensis fragrance, Intense strain and pressure can be expelled, improve the insomnia caused by anxiety, owing to Pericarpium Citri junoris containing substantial amounts of dimension He orders C, can preventing cold, skin is had moistening effect, can balance skin the salty value of acid, help collagen shape Becoming, the growth for bodily tissue has good effect with repairing.Diaphoresis can be promoted, thus can help to block Skin discharge toxin, the most helpful to oiliness, skin sore or dry skin person.
The invention have the benefit that
1, anticreep shampoo of setting out again of the present invention, by first from Cacumen Platycladi, Radix Polygoni Multiflori, angelica root according to The compound of rational proportion composition extracts and obtains Chinese medicine extraction liquid, then by gained Chinese medicine extraction liquid and Camellia sinensis essence Oil and sweet orange oil carry out mix homogeneously according to applicable weight proportion, final prepared setting out again in anticreep shampoo Containing herbaceous plant extracting solution and Anti-hair loss composition and effectiveness, can use as conventional shampoo, supplement hair moisture Recover natural metabolism, pre-Anti-hair loss with nutrition, help scalp, delay scalp old and feeble, improve color development and hair Glossy degree, make hair more compliant glossy, and raw material be easy to get, low cost, therapeutic effect is obvious.
2, anticreep shampoo of setting out again of the present invention, by by Cacumen Platycladi, Radix Polygoni Multiflori, angelica root according to conjunction The compound of reason proportioning composition extracts and obtains Chinese medicine extraction liquid, then by gained Chinese medicine extraction liquid and tea tree ethereal oil Carry out mix homogeneously with sweet orange oil according to applicable weight proportion, be finally also added with sodium lauryl sulfate, the moon Laureth sodium sulfovinate, cocamido propyl betaine, Ethylene Glycol Distearate, cetearyl alcohol, Polyquaternium-10, guar gum, DMDM Hydantoin, citric acid, EDTA-disodium, methyl hydroxybenzoate And ethyl hydroxybenzoate, the final anticreep shampoo of setting out again prepared contains herbaceous plant extracting solution and Anti-hair loss composition and effectiveness, And can use as conventional shampoo, supplement hair moisture and nutrition, help scalp to recover natural metabolism, Pre-Anti-hair loss, delays scalp old and feeble, improves the glossy degree of color development and hair, make hair more compliant glossy, And raw material is easy to get, low cost, therapeutic effect is obvious.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further elaborated.
Following example represent 1g with 1 weight portion.
Embodiment 1
The present embodiment provides one to set out anticreep shampoo again, and its raw material components includes:
0.5 weight portion Cacumen Platycladi, 3 weight portion Radix Polygoni Multiflori, 0.5 weight portion angelica root, 1 weight portion tea tree ethereal oil, 0.1 weight portion sweet orange oil.
A kind of method preparing described anticreep shampoo of setting out again, comprises the steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to above-mentioned weight portion and be sufficiently mixed, Obtain compound;
(2) in gained compound, add the deionized water of 6 times of quality, be placed in extraction still at 95~100 DEG C Under the conditions of carry out normal pressure and boil and carry 3h, obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, the deionized water of 6 times of quality is added at 95~100 DEG C Under the conditions of carry out normal pressure and boil and carry 3h, obtain the second medicinal liquid and the second medicinal residues;
(4) obtain stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution 63~ 68 DEG C ,-0.04~-0.07MPa carry out heating for the first time being concentrated under reduced pressure to give concentrated solution, and described concentrated solution is institute State the 1/2 of stock solution quality;
(5) in step (4) described concentrated solution, add 1 times of volume ethanol (volumetric concentration is 60%) to enter Row sedimentation 12h, carries out after having settled filtering and collecting filtrate;
(6) at 40~50 DEG C ,-0.04~-0.07MPa, step (5) described filtrate is carried out second time to heat Concentrating under reduced pressure 5h, is evaporated off whole ethanol, obtains Chinese medicine extraction liquid;
(7) in step (6) described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed Uniformly, obtain described in set out again anticreep shampoo.
Embodiment 2
The present embodiment provides one to set out anticreep shampoo again, and its raw material components includes:
3 weight portion Cacumen Platycladis, 0.5 weight portion Radix Polygoni Multiflori, 3 weight portion angelica roots, 0.1 weight portion tea tree ethereal oil, 1 weight portion sweet orange oil, 2 weight portion sodium lauryl sulfate, 18 weight portion sodium laureth sulfate, 2 weight portion cocamido propyl betaine, 2 weight portion Ethylene Glycol Distearate, 0.1 weight portion spermaceti are hard Acyl in lipidol, 0.6 weight portion Polyquaternium-10,0.1 weight portion guar gum, 0.6 weight portion DMDM second Urea, 0.05 parts by weight of lemon acid, 0.2 weight portion EDTA-disodium, 0.1 weight portion methyl hydroxybenzoate, 0.4 weight Part ethyl hydroxybenzoate.
A kind of method preparing described anticreep shampoo of setting out again, comprises the steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to above-mentioned weight portion and be sufficiently mixed, Obtain compound;
(2) in gained compound, add the deionized water of 9 times of quality, be placed in extraction still at 95~100 DEG C Under the conditions of carry out normal pressure and boil and carry 0.5h, obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, the deionized water of 9 times of quality is added at 95~100 DEG C Under the conditions of carry out normal pressure and boil and carry 0.5h, obtain the second medicinal liquid and the second medicinal residues;
(4) obtain stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution 63~ 68 DEG C ,-0.04~-0.07MPa carry out heating for the first time being concentrated under reduced pressure to give concentrated solution, and described concentrated solution is institute State the 1/4 of stock solution quality;
(5) in step (4) described concentrated solution, add the ethanol (volumetric concentration is 80%) of 4 times of volumes Carry out settling 36h, carry out after having settled filtering and collecting filtrate;
(6) at 40~50 DEG C ,-0.04~-0.07MPa, step (5) described filtrate is carried out second time to heat Concentrating under reduced pressure 2h, is evaporated off whole ethanol, obtains Chinese medicine extraction liquid;
(7) in step (6) described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed Uniformly, sodium lauryl sulfate, sodium laureth sulfate, cocamidopropyl propyl amide it are sequentially added into afterwards sweet Dish alkali, Ethylene Glycol Distearate, cetearyl alcohol, Polyquaternium-10, guar gum, DMDM second Interior uride, citric acid, EDTA-disodium, methyl hydroxybenzoate, ethyl hydroxybenzoate, be sufficiently mixed uniformly, obtain institute State anticreep shampoo of setting out again.
Embodiment 3
The present embodiment provides one to set out anticreep shampoo again, and its raw material components includes:
2 weight portion Cacumen Platycladis, 2 weight portion Radix Polygoni Multiflori, 2 weight portion angelica roots, 0.5 weight portion tea tree ethereal oil, 0.5 weight portion sweet orange oil, 6 weight portion sodium lauryl sulfate, 12 weight portion sodium laureth sulfate, 6 weight portion cocamido propyl betaine, 0.5 weight portion Ethylene Glycol Distearate, 1 weight portion spermaceti are hard Acyl in lipidol, 0.1 weight portion Polyquaternium-10,0.6 weight portion guar gum, 0.1 weight portion DMDM second Urea, 0.2 parts by weight of lemon acid, 0.05 weight portion EDTA-disodium, 0.5 weight portion methyl hydroxybenzoate, 0.1 weight Part ethyl hydroxybenzoate.
A kind of method preparing described anticreep shampoo of setting out again, comprises the steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to above-mentioned weight portion and be sufficiently mixed, Obtain compound;
(2) in gained compound, add the deionized water of 8 times of quality, be placed in extraction still at 95~100 DEG C Under the conditions of carry out normal pressure and boil and carry 1.5h, obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, the deionized water of 8 times of quality is added at 95~100 DEG C Under the conditions of carry out normal pressure and boil and carry 1.5h, obtain the second medicinal liquid and the second medicinal residues;
(4) obtain stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution 63~ 68 DEG C ,-0.04~-0.07MPa carry out heating for the first time being concentrated under reduced pressure to give concentrated solution, and described concentrated solution is institute State the 1/3 of stock solution quality;
(5) in step (4) described concentrated solution, add the ethanol (volumetric concentration is 60%) of 2 times of volumes Carry out settling 12h, carry out after having settled filtering and collecting filtrate;
(6) at 40~50 DEG C ,-0.04~-0.07MPa, step (5) described filtrate is carried out second time to heat Concentrating under reduced pressure 3h, is evaporated off whole ethanol, obtains Chinese medicine extraction liquid;
(7) in described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed uniformly, afterwards It is sequentially added into sodium lauryl sulfate, sodium laureth sulfate, cocamido propyl betaine, second two Alcohol double stearate, cetearyl alcohol, Polyquaternium-10, guar gum, DMDM Hydantoin, lemon Lemon acid, EDTA-disodium, methyl hydroxybenzoate, ethyl hydroxybenzoate, be sufficiently mixed uniformly, obtain described in set out again anti- De-shampoo.
Embodiment 4
The present embodiment provides one to set out anticreep shampoo again, and its raw material components includes:
1 weight portion Cacumen Platycladi, 1 weight portion Radix Polygoni Multiflori, 1 weight portion angelica root, 0.4 weight portion tea tree ethereal oil, 0.4 weight portion sweet orange oil, 4 weight portion sodium lauryl sulfate, 15 weight portion sodium laureth sulfate, 5 weight portion cocamido propyl betaine, 1 weight portion Ethylene Glycol Distearate, 0.5 weight portion spermaceti are hard Acyl in lipidol, 0.3 weight portion Polyquaternium-10,0.3 weight portion guar gum, 0.3 weight portion DMDM second Urea, 0.1 parts by weight of lemon acid, 0.1 weight portion EDTA-disodium, 0.25 weight portion methyl hydroxybenzoate, 0.2 weight Part ethyl hydroxybenzoate.
A kind of method preparing described anticreep shampoo of setting out again, comprises the steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to above-mentioned weight portion and be sufficiently mixed, Obtain compound;
(2) in gained compound, add the deionized water of 8 times of quality, be placed in extraction still at 95~100 DEG C Under the conditions of carry out normal pressure and boil and carry 3 hours, obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, the deionized water of 8 times of quality is added at 95~100 DEG C Under the conditions of carry out normal pressure and boil and carry 0.5h, obtain the second medicinal liquid and the second medicinal residues;
(4) obtain stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution 63~ 68 DEG C ,-0.04~-0.07MPa carry out heating for the first time being concentrated under reduced pressure to give concentrated solution, and described concentrated solution is institute State the 1/2 of stock solution quality;
(5) in step (4) described concentrated solution, add the ethanol (volumetric concentration is 60%) of 2 times of volumes Carry out settling 36h, carry out after having settled filtering and collecting filtrate;
(6) at 40~50 DEG C ,-0.04~-0.07MPa, step (5) described filtrate is carried out second time to heat Concentrating under reduced pressure 3h, is evaporated off whole ethanol, obtains Chinese medicine extraction liquid;
(7) in step (6) described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed Uniformly, sodium lauryl sulfate, sodium laureth sulfate, cocamidopropyl propyl amide it are sequentially added into afterwards sweet Dish alkali, Ethylene Glycol Distearate, cetearyl alcohol, Polyquaternium-10, guar gum, DMDM second Interior uride, citric acid, EDTA-disodium, methyl hydroxybenzoate, ethyl hydroxybenzoate, be sufficiently mixed uniformly, obtain institute State anticreep shampoo of setting out again.
Embodiment 5
The present embodiment provides one to set out anticreep shampoo again, and its raw material components includes:
1 weight portion Cacumen Platycladi, 2 weight portion Radix Polygoni Multiflori, 1 weight portion angelica root, 0.8 weight portion tea tree ethereal oil, 0.6 weight portion sweet orange oil, 4 weight portion sodium lauryl sulfate, 15 weight portion sodium laureth sulfate, 5 weight portion cocamido propyl betaine, 1 weight portion Ethylene Glycol Distearate, 0.5 weight portion spermaceti are hard Acyl in lipidol, 0.3 weight portion Polyquaternium-10,0.3 weight portion guar gum, 0.3 weight portion DMDM second Urea, 0.1 parts by weight of lemon acid, 0.1 weight portion EDTA-disodium, 0.25 weight portion methyl hydroxybenzoate, 0.2 weight Part ethyl hydroxybenzoate.
A kind of method preparing described anticreep shampoo of setting out again, comprises the steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to above-mentioned weight portion and be sufficiently mixed, Obtain compound;
(2) in gained compound, add the deionized water of 9 times of quality, be placed in extraction still at 95~100 DEG C Under the conditions of carry out normal pressure and boil and carry 2h and obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, the deionized water of 9 times of quality is added at 95~100 DEG C Under the conditions of carry out normal pressure and boil and carry 2h, obtain the second medicinal liquid and the second medicinal residues;
(4) obtain stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution 63~ 68 DEG C ,-0.04~-0.07MPa carry out heating for the first time being concentrated under reduced pressure to give concentrated solution, and described concentrated solution is institute State the 1/2 of stock solution quality;
(5) in step (4) described concentrated solution, add the ethanol (volumetric concentration is 65%) of 2 times of volumes Carry out settling 12h, carry out after having settled filtering and collecting filtrate;
(6) at 40~50 DEG C ,-0.04~-0.07MPa, step (5) described filtrate is carried out second time to heat Concentrating under reduced pressure 3h, is evaporated off whole ethanol, obtains Chinese medicine extraction liquid;
(7) in step (6) described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed Uniformly, sodium lauryl sulfate, sodium laureth sulfate, cocamidopropyl propyl amide it are sequentially added into afterwards sweet Dish alkali, Ethylene Glycol Distearate, cetearyl alcohol, Polyquaternium-10, guar gum, DMDM second Interior uride, citric acid, EDTA-disodium, methyl hydroxybenzoate, ethyl hydroxybenzoate, be sufficiently mixed uniformly, obtain institute State anticreep shampoo of setting out again.
Embodiment 6
The present embodiment provides one to set out anticreep shampoo again, and its raw material components includes:
1 weight portion Cacumen Platycladi, 2 weight portion Radix Polygoni Multiflori, 1 weight portion angelica root, 0.6 weight portion tea tree ethereal oil, 0.4 weight portion sweet orange oil, 4 weight portion sodium lauryl sulfate, 15 weight portion sodium laureth sulfate, 5 weight portion cocamido propyl betaine, 1 weight portion Ethylene Glycol Distearate, 0.5 weight portion spermaceti are hard Acyl in lipidol, 0.3 weight portion Polyquaternium-10,0.3 weight portion guar gum, 0.3 weight portion DMDM second Urea, 0.1 parts by weight of lemon acid, 0.1 weight portion EDTA-disodium, 0.25 weight portion methyl hydroxybenzoate, 0.2 weight Part ethyl hydroxybenzoate.
A kind of method preparing described anticreep shampoo of setting out again, comprises the steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to above-mentioned weight portion and be sufficiently mixed, Obtain compound;
(2) in gained compound, add the deionized water of 6 times of quality, be placed in extraction still at 95~100 DEG C Under the conditions of carry out normal pressure and boil and carry 1.5h, obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, the deionized water of 6 times of quality is added at 95~100 DEG C Under the conditions of carry out normal pressure and boil and carry 1.5h, obtain the second medicinal liquid and the second medicinal residues;
(4) obtain stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution through 63~ 68 DEG C ,-0.04~-0.07MPa carry out heating for the first time being concentrated under reduced pressure to give concentrated solution, and described concentrated solution is institute State the 1/2 of stock solution quality;
(5) in step (4) described concentrated solution, add the ethanol (volumetric concentration is 75%) of 2.5 times of volumes Carry out settling 12h, carry out after having settled filtering and collecting filtrate;
(6) at 40~50 DEG C ,-0.04~-0.07MPa, step (5) described filtrate is carried out second time to heat Concentrating under reduced pressure 3h, is evaporated off whole ethanol, obtains described Chinese medicine extraction liquid;
(7) in step (6) described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed Uniformly, sodium lauryl sulfate, sodium laureth sulfate, cocamidopropyl propyl amide it are sequentially added into afterwards sweet Dish alkali, Ethylene Glycol Distearate, cetearyl alcohol, Polyquaternium-10, guar gum, DMDM second Interior uride, citric acid, EDTA-disodium, methyl hydroxybenzoate, ethyl hydroxybenzoate, be sufficiently mixed uniformly, obtain institute State anticreep shampoo of setting out again.
Experimental example
The present inventor is by using anticreep shampoo of setting out again of the present invention to clinical 100 example hair loss patients Observe, the maleest 53 examples, female 47 example, minimum 26 years old of age, maximum 66 years old.
Using method: wash hair as shampoo once a day, each 10ml.
Efficacy assessment standard:
Cure: alopecia transference cure, 70 examples.
Effective: alopecia symptom is obviously improved, 27 examples.
Invalid: alopecia symptom is not improved 3 examples.Total effective rate 97%.
Typical clinical case:
Wang, man, 28 years old, deskman, alopecia when washing hair of combing one's hair was a lot of, uses the present invention real After executing the anticreep shampoo 30 days of setting out again described in example 3, hair the most no longer comes off, the color development of hair and gloss Degree all has clear improvement.
Lu, female, 33 years old, certain enterprise personnel, alopecia was serious, and hair is sparse withered and yellow, uses the present invention real After executing the anticreep shampoo 40 days of setting out again described in example 4, alopecia phenomenon is obviously improved, and adheres to using 80 In the future, the most no longer alopecia, color development blackening, glossy.
Chen, man, 58 years old, peasant, alopecia was serious, and setting out again described in the use embodiment of the present invention 5 is anti- After de-shampoo 90 days, hair no longer comes off.
The present invention is not limited to above-mentioned preferred forms, and anyone can draw it under the enlightenment of the present invention His various forms of products, no matter but in its shape or structure, make any change, every have and the application Technical scheme as same or like, within all falling within protection scope of the present invention.

Claims (10)

1. an anticreep shampoo of setting out again, it is characterised in that raw material components includes:
Cacumen Platycladi, 0.5~3 weight portions;
Radix Polygoni Multiflori, 0.5~3 weight portions;
Angelica root, 0.5~3 weight portions;
Tea tree ethereal oil, 0.1~1 weight portion;
Sweet orange oil, 0.1~1 weight portion.
Anticreep shampoo of setting out again the most according to claim 1, it is characterised in that raw material components includes:
Cacumen Platycladi, 2 weight portions;
Radix Polygoni Multiflori, 2 weight portions;
Angelica root, 2 weight portions;
Tea tree ethereal oil, 0.5 weight portion;
Sweet orange oil, 0.5 weight portion.
Anticreep shampoo of setting out again the most according to claim 1 and 2, it is characterised in that raw material components is also Including 2~6 weight portion sodium lauryl sulfate, 12~18 weight portion sodium laureth sulfate, 2~6 Weight portion cocamido propyl betaine, 0.5~2 weight portion Ethylene Glycol Distearate, 0.1~1 weight portion Cetearyl alcohol, 0.1~0.6 weight portion Polyquaternium-10,0.1~0.6 weight portion guar gum, 0.1~0.6 Weight portion DMDM Hydantoin, 0.05~0.2 parts by weight of lemon acid, 0.05~0.2 weight portion EDTA- Disodium, 0.1~0.5 weight portion methyl hydroxybenzoate, 0.1~0.4 weight portion ethyl hydroxybenzoate.
4. the method for the anticreep shampoo of setting out again prepared described in claim 1, it is characterised in that include Following steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to described weight portion and be sufficiently mixed, Obtain compound;
(2) in gained compound, add deionized water to carry out boiling carrying, obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, add deionized water to carry out boiling again carrying, obtain the second medicine Liquid and the second medicinal residues;
(4) obtaining stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution is through for the first time Heating is concentrated under reduced pressure to give concentrated solution;
(5) ethanol adding 1~4 times of volume in step (4) described concentrated solution settles, and has settled Carry out after one-tenth filtering and collecting filtrate;
(6) step (5) described filtrate is carried out second time and heat concentrating under reduced pressure, whole ethanol is evaporated off, To Chinese medicine extraction liquid;
(7) in step (6) described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed Uniformly, obtain described in set out again anticreep shampoo.
5. the method for the anticreep shampoo of setting out again prepared described in claim 3, it is characterised in that include Following steps:
(1) weigh Cacumen Platycladi, Radix Polygoni Multiflori, angelica root successively according to described weight portion and be sufficiently mixed, Obtain compound;
(2) in gained compound, add deionized water to carry out boiling carrying, obtain the first medicinal liquid and the first medicinal residues;
(3) in step (2) gained the first medicinal residues, add deionized water to carry out boiling carrying, obtain the second medicinal liquid With the second medicinal residues;
(4) obtaining stock solution after described first medicinal liquid and the second medicinal liquid being sufficiently mixed, described stock solution is through for the first time Heating is concentrated under reduced pressure to give concentrated solution;
(5) ethanol adding 1~4 times of volume in step (4) described concentrated solution settles, and has settled Carry out after one-tenth filtering and collecting filtrate;
(6) step (5) described filtrate is carried out second time and heat concentrating under reduced pressure, whole ethanol is evaporated off, To Chinese medicine extraction liquid;
(7) in step (6) described Chinese medicine extraction liquid, add tea tree ethereal oil and sweet orange oil, be sufficiently mixed Uniformly, sodium lauryl sulfate, sodium laureth sulfate, cocamidopropyl propyl amide it are sequentially added into afterwards sweet Dish alkali, Ethylene Glycol Distearate, cetearyl alcohol, Polyquaternium-10, guar gum, DMDM second Interior uride, citric acid, EDTA-disodium, methyl hydroxybenzoate, ethyl hydroxybenzoate, be sufficiently mixed uniformly, obtain institute State anticreep shampoo of setting out again.
6. according to the method for the anticreep shampoo of setting out again described in claim 4 or 5, it is characterised in that step (2), in, the mass ratio of described compound and described deionized water is 1:6~1:9, described in boil to carry and enter for normal pressure OK, temperature is 95~100 DEG C, and extraction time is 0.5~3h.
7. according to the method for the anticreep shampoo of setting out again described in claim 4 or 5, it is characterised in that step (3), in, the mass ratio of described first medicinal residues and described deionized water is 1:6~1:9, described in boil and carry as normal pressure Carrying out, temperature is 95~100 DEG C, and extraction time is 0.5~3h.
8. according to the method for the anticreep shampoo of setting out again described in claim 4 or 5, it is characterised in that step (4) carry out in described first time heating concentrating under reduced pressure temperature be 63~68 DEG C, pressure be-0.04~ -0.07MPa, described concentrated solution is 1:2~1:4 with the mass ratio of described stock solution.
9. according to the method for the anticreep shampoo of setting out again described in claim 4 or 5, it is characterised in that step (5) volumetric concentration of ethanol described in is 60~80%, and the time carrying out described sedimentation is 12~36h.
10. according to the method for the anticreep shampoo of setting out again described in claim 4 or 5, it is characterised in that step Suddenly (6) are carried out described second time heating concentrating under reduced pressure temperature be 40~50 DEG C, pressure be-0.04~ -0.07MPa, the time carrying out described second time heating concentrating under reduced pressure is 2~5h.
CN201610482781.1A 2016-06-27 2016-06-27 Hair re-growing and hair loss preventing shampoo and preparation method thereof Pending CN105919900A (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108042403A (en) * 2018-02-05 2018-05-18 淮安智品企业管理有限公司 A kind of no silicone oil anticreep hair-care shampoo
CN108403607A (en) * 2018-05-31 2018-08-17 云南健牛生物科技有限公司 A kind of natural hair oil preparation method
CN110025510A (en) * 2019-05-29 2019-07-19 龙春艳 Essential oils of herbs shampoo and preparation method thereof
CN111714436A (en) * 2020-07-24 2020-09-29 南京佰宏卓越科技有限公司 Anti-hair loss shampoo and preparation method thereof
CN113069390A (en) * 2020-01-06 2021-07-06 广州樱奈儿化妆品有限公司 Anti-hair-loss hair-growing lotion and preparation method thereof
CN115836992A (en) * 2023-02-27 2023-03-24 北京普世安生物科技有限公司 Anti-hair loss shampoo and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101422528A (en) * 2007-11-02 2009-05-06 绿谷(集团)有限公司 Alopecia prevention composition and production method thereof
KR20100074880A (en) * 2008-12-24 2010-07-02 김석환 Shampoo composition for promoting restoring hair and preventing from losing hair
CN103550108A (en) * 2013-11-15 2014-02-05 广州好迪集团有限公司 Hair nourishing and damage repairing shampoo
CN104644483A (en) * 2013-11-23 2015-05-27 楚乐然 Alopecia prevention shampoo

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101422528A (en) * 2007-11-02 2009-05-06 绿谷(集团)有限公司 Alopecia prevention composition and production method thereof
KR20100074880A (en) * 2008-12-24 2010-07-02 김석환 Shampoo composition for promoting restoring hair and preventing from losing hair
CN103550108A (en) * 2013-11-15 2014-02-05 广州好迪集团有限公司 Hair nourishing and damage repairing shampoo
CN104644483A (en) * 2013-11-23 2015-05-27 楚乐然 Alopecia prevention shampoo

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
刘莹莹等: "《淑女美发宝典》", 31 January 2010, 经济管理出版社 *

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108042403A (en) * 2018-02-05 2018-05-18 淮安智品企业管理有限公司 A kind of no silicone oil anticreep hair-care shampoo
CN108403607A (en) * 2018-05-31 2018-08-17 云南健牛生物科技有限公司 A kind of natural hair oil preparation method
CN110025510A (en) * 2019-05-29 2019-07-19 龙春艳 Essential oils of herbs shampoo and preparation method thereof
CN113069390A (en) * 2020-01-06 2021-07-06 广州樱奈儿化妆品有限公司 Anti-hair-loss hair-growing lotion and preparation method thereof
CN111714436A (en) * 2020-07-24 2020-09-29 南京佰宏卓越科技有限公司 Anti-hair loss shampoo and preparation method thereof
CN111714436B (en) * 2020-07-24 2021-05-07 佛山市百分之秀化妆品有限公司 Anti-hair loss shampoo and preparation method thereof
CN115836992A (en) * 2023-02-27 2023-03-24 北京普世安生物科技有限公司 Anti-hair loss shampoo and preparation method thereof

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