CN103724126A - Multielement high-efficiency active organic liquid fertilizer and preparation method thereof - Google Patents

Multielement high-efficiency active organic liquid fertilizer and preparation method thereof Download PDF

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Publication number
CN103724126A
CN103724126A CN201310722180.XA CN201310722180A CN103724126A CN 103724126 A CN103724126 A CN 103724126A CN 201310722180 A CN201310722180 A CN 201310722180A CN 103724126 A CN103724126 A CN 103724126A
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fertilizer
vinasse
enzymolysis
organic liquid
liquid
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CN103724126B (en
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张彩年
岳万华
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Haimen Yue Yue Textile Co Ltd
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Abstract

The invention discloses a multielement high-efficiency active organic liquid fertilizer and a preparation method thereof. The multielement high-efficiency active organic liquid fertilizer is prepared from a vinasse enzymolysis clear solution, chitosan, a nitrogen fertilizer, a phosphate fertilizer, a potash fertilizer, a minor element mixture and a natural surfactant. The vinasse enzymolysis clear solution, which is prepared by carrying out pretreatment, primary enzymolysis, secondary fermentation, centrifugation and the like, is used as the main raw material, and thus, the waste is fully utilized. The liquid fertilizer has the advantages of high nutrient content and comprehensive nutrients, can be subjected to surface spraying or used as a water flush fertilizer, and has favorable yield increase effect.

Description

The active organic liquid fertilizer of a kind of multielement high-efficiency and preparation method
Technical field
The present invention relates to a kind of agricultural fertilizer, relate in particular to the active organic liquid fertilizer of a kind of multielement high-efficiency and preparation method.
Background technology
At present, international fertilizer is consumed the future development to high density, Composite, fluidization, slow.Owing to having, productive expense is low, nutrient content is high, it is compound to be easy to for liquid fertilizer, can be directly by farm crop, absorbed, be convenient to the plurality of advantages such as rational application of fertilizers (balance fertilizing) and mechanized application, is more and more subject to the common concern of various countries.
Along with the quickening of global economic integration progress, developing country, in order to promote national agricultural development, reduces agriculture production cost, improves agricultural-food competitive power in the international market, start to adopt a series of measures to carry out agricultural restructuring, improve intensive agriculture and industrialization level.Mechanized application condition progressively improves, and the demand of dedicated fertilizer is constantly increased, and then provide more wide space for the development of liquid fertilizer.
For improving utilization rate of fertilizer, alleviate chemical fertilizer to the particularly impact of soil of environment, improve the nutrition absorption rate of crop, reduce peasant's production cost, middle peasant Shun sky Eco-fertilizer industry company limited is devoted to the research of new-type fertilizer always, the scientific and technical personnel of company are in conjunction with agricultural state and the in the future development trend of fertilizer both at home and abroad, through feasibility study repeatedly, Development and Production represent middle peasant Shun sky multifunctional ecological organic liquid fertilizer of China's new-type fertilizer advanced level, this organic liquid fertilizer improves the yield and quality of kind of plant, and fertilizer can increase the content of soil with organic matter.This fertilizer application is in extensive range, adapt to various soil.Have antibacterial disease-resistant deinsectization, improve the effect of crop anti-adversity, long-term application can play the effect that prevents and reduce environmental pollution.
Summary of the invention
The object of this invention is to provide a kind of nutrient comprehensive, and the polynary efficient organic Liquid Fertilizer that contains biological activity.
Another object of the present invention is to provide the preparation method of the active organic liquid fertilizer of a kind of multielement high-efficiency.
The object of the invention is to be achieved through the following technical solutions, the weight part proportioning of active its raw material of organic liquid fertilizer of this multielement high-efficiency is: vinasse enzymolysis clear liquid 600-700 part, chitosan 6-9 part, nitrogenous fertilizer 50-100 part, phosphate fertilizer 40-50 part, potash fertilizer 50-100 part, trace element mixture 15-30 part, natural surface active agent 1-2 part.
Preferably, the weight part proportioning of active its raw material of organic liquid fertilizer of this multielement high-efficiency is: 650 parts of vinasse enzymolysis clear liquids, 7 parts of chitosans, 75 parts, nitrogenous fertilizer, 45 parts, phosphate fertilizer, 75 parts, potash fertilizer, 22 parts of trace element mixtures, 1.5 parts of natural surface active agents.
The preparation technology of described vinasse enzymolysis clear liquid is:
1. vinasse pre-treatment: the vinasse that will wet are dry, controlling water content is 25%, and is crushed to 80 objects sieves excessively, obtains vinasse powder.
2. primary enzymolysis: after above-mentioned vinasse powder is mixed with the weight ratio of 1: 6 with water, first regulate P hbe worth to 8-10, then need the ratio interpolation Sumizyme MP of 12 grams of Sumizyme MPs to carry out enzyme digestion reaction according to per kilogram vinasse powder; Reaction times is 50 minutes, and temperature of reaction is 45 degree, obtains elementary enzymolysis solution;
3. Secondary Fermentation: add Semen Maydis powder, bean cake powder in enzymolysis solution, its add-on accounts for respectively 10% and 15% of enzymolysis solution gross weight, add again subtilis, viride, milk-acid bacteria, yeast, its add-on is according to the ratio of 10 grams of per kilogram enzymolysis solutions, fully stir, reaction times is 90 minutes, and temperature of reaction is 55 degree, obtains level enzymolysis solution eventually.
4. centrifugal: level enzymolysis solution is centrifugal eventually, obtains liquid phase A and deposit A;
5. washing: deposit A is mixed with the weight ratio of 1: 4 with water, obtain washings after stirring;
6. centrifugal: by centrifugal above-mentioned washings liquid phase B and the precipitate B of obtaining;
7. after above-mentioned liquid phase A being mixed with liquid phase B, be adjusted to neutrality, obtain vinasse enzymolysis clear liquid.
Described nitrogenous fertilizer is that nitrogen content is 46% urea, and described phosphate fertilizer is that phosphorus content is 50% monoammonium phosphate or calcium superphosphate, and described potash fertilizer is that potassium content is 50% potassium sulfate;
Described natural surface active agent is sorbitol, mannitol, Saccharum lactis, and the ratio of its consumption is 2: 1: 2.
Described trace element comprises zinc sulfate, ferrous sulfate, manganous sulfate, copper sulfate, boric acid and ammonium molybdate, and the ratio of its consumption is 1: 3: 1: 1.5: 2: 1.
The preparation method of the active organic liquid fertilizer of this multielement high-efficiency comprises the following steps:
1, prepare vinasse enzymolysis clear liquid;
2, chitosan, trace element are joined in vinasse enzymolysis clear liquid in proportion, fully stir 5-10 minute;
3, nitrogenous fertilizer, phosphate fertilizer, potash fertilizer, natural surface active agent are joined in the solution that step 2 forms, in airflow stirring machine, continue to stir 10-15 minute.
4, the liquid stirring is carried out to biochemical investigation, packing, finished product.
Compare with prior art, product of the present invention not only nutrient content is high, and, both can spray comprehensively, also can rush and execute.Nontoxic, harmless, pollution-free, also there is the function of removing pesticide residue and soil disease, have that the farm crop of enhancing are cold-resistant, a drought resisting, the anti-several functions such as saline and alkaline, pest-resistant simultaneously.Through field test on field crop: make foliage-spray, 500 milliliters of every mu of consumptions, three days visible positive effects, fertilizer efficiency period can reach about 40 days; Do punching and use, 1500 milliliters of every mu of consumptions, four days visible positive effects, fertilizer efficiency period can reach about 50 days.Can reduce chemical fertilizer, agricultural chemicals 30% usage quantity, make that soil is more loose, agricultural product quality is safer, high-quality more.
Sci-tech model household Lee, one mu of planting greenhouse cucumber, wherein half mu of plastic tent cucumber sprays liquid fertilizer of the present invention, the water of another half mu of ground spray as much compares, in the result Sheng phase, spray, 300 milliliters of half mu of liquid fertilizer consumptions, add water and spray with atomizer after appropriate, and control group adopts the water spray with amount.Result shows, the cucumber leaves performance on half mu of ground that sprays liquid fertilizer is thicker, blade and fruit ageing green; Plant disease resistance is strong, can reduce pesticide number of times; Fruit quality is good.Spray half mu of ground of liquid fertilizer,
Within every two days, receive a cucumber and can receive 67.5 kilograms, control group is received a cucumber too for every two days can receive 50.6 kilograms, increases the yield per unit area more than 25%.
Embodiment
Embodiment mono-:
Take 650 kilograms of vinasse enzymolysis clear liquids, 7 kilograms of chitosans, 75 kilograms, nitrogenous fertilizer, 45 kilograms, phosphate fertilizer, 75 kilograms, potash fertilizer, 22 kilograms of trace element mixtures, 1.5 kilograms of natural surface active agents.Concrete preparation method is:
7 kilograms of chitosans, 22 kilograms of zinc sulfate, ferrous sulfate, manganous sulfate, copper sulfate, boric acid and ammonium molybdates are joined in 650 kilograms of vinasse enzymolysis clear liquids, fully stir 8 minutes; Again 75 kilograms of urea, 45 kilograms of monoammonium phosphates, 75 kilograms of potassium sulfate, 1.5 kilograms of sorbitols, mannitol, Saccharum lactiss are joined in solution, in airflow stirring machine, continue to stir 15 minutes; The liquid stirring is carried out to biochemical investigation, packing, finished product.The liquid fertilizer of preparation is containing living bacteria count 2,000,000,000/milliliter thus, nitrogenous 7%, phosphorus 4%, and potassium 7%, oligose 0.5%, 19 seed amino acid, boron, molybdenum, zinc total content do 0.3% greatly.
Embodiment bis-:
Take 700 kilograms of vinasse enzymolysis clear liquids, 9 kilograms of chitosans, 100 kilograms, nitrogenous fertilizer, 50 kilograms, phosphate fertilizer, 100 kilograms, potash fertilizer, 30 kilograms of trace element mixtures, 2 kilograms of natural surface active agents.Concrete preparation method is:
9 kilograms of chitosans, 30 kilograms of zinc sulfate, ferrous sulfate, manganous sulfate, copper sulfate, boric acid and ammonium molybdates are joined in 700 kilograms of vinasse enzymolysis clear liquids, fully stir 10 minutes; Again 100 kilograms of urea, 50 kilograms of calcium superphosphate, 100 kilograms of potassium sulfate, 2 kilograms of sorbitols, mannitol, Saccharum lactiss are joined in solution, in airflow stirring machine, continue to stir 15 minutes; The liquid stirring is carried out to biochemical investigation, packing, finished product.The liquid fertilizer of preparation is containing living bacteria count 2,000,000,000/milliliter thus, nitrogenous 7.5%, phosphorus 5.2%, and potassium 7.8%, oligose 0.6%, 19 seed amino acid, boron, molybdenum, zinc total content do 0.3% greatly.

Claims (7)

1. the active organic liquid fertilizer of multielement high-efficiency, is characterized in that the weight part proportioning of this its raw material of Liquid Fertilizer is: vinasse enzymolysis clear liquid 600-700 part, chitosan 6-9 part, nitrogenous fertilizer 50-100 part, phosphate fertilizer 40-50 part, potash fertilizer 50-100 part, trace element mixture 15-30 part, natural surface active agent 1-2 part.
2. the active organic liquid fertilizer of a kind of multielement high-efficiency according to claim 1, is characterized in that the weight part proportioning of this its raw material of Liquid Fertilizer is: 650 parts of vinasse enzymolysis clear liquids, 7 parts of chitosans, 75 parts, nitrogenous fertilizer, 45 parts, phosphate fertilizer, 75 parts, potash fertilizer, 22 parts of trace element mixtures, 1.5 parts of natural surface active agents.
3. the active organic liquid fertilizer of a kind of multielement high-efficiency according to claim 1, is characterized in that the preparation technology of described vinasse enzymolysis clear liquid is:
1. vinasse pre-treatment: the vinasse that will wet are dry, controlling water content is 25%, and is crushed to 80 objects sieves excessively, obtains vinasse powder;
2. primary enzymolysis: after above-mentioned vinasse powder is mixed with the weight ratio of 1: 6 with water, first regulate P hbe worth to 8-10, then need the ratio interpolation Sumizyme MP of 12 grams of Sumizyme MPs to carry out enzyme digestion reaction according to per kilogram vinasse powder; Reaction times is 50 minutes, and temperature of reaction is 45 degree, obtains elementary enzymolysis solution;
3. Secondary Fermentation: add Semen Maydis powder, bean cake powder in enzymolysis solution, its add-on accounts for respectively 10% and 15% of enzymolysis solution gross weight, add again subtilis, viride, milk-acid bacteria, yeast, its add-on is according to the ratio of 10 grams of per kilogram enzymolysis solutions, fully stir, reaction times is 90 minutes, and temperature of reaction is 55 degree, obtains level enzymolysis solution eventually.
4. centrifugal: level enzymolysis solution is centrifugal eventually, obtains liquid phase A and deposit A;
5. washing: deposit A is mixed with the weight ratio of 1: 4 with water, obtain washings after stirring;
6. centrifugal: by centrifugal above-mentioned washings liquid phase B and the precipitate B of obtaining;
7. after above-mentioned liquid phase A being mixed with liquid phase B, be adjusted to neutrality, obtain vinasse enzymolysis clear liquid.
4. the active organic liquid fertilizer of a kind of multielement high-efficiency according to claim 1, it is characterized in that described nitrogenous fertilizer is that nitrogen content is 46% urea, described phosphate fertilizer is that phosphorus content is 50% monoammonium phosphate or calcium superphosphate, and described potash fertilizer is that potassium content is 50% potassium sulfate.
5. the active organic liquid fertilizer of a kind of multielement high-efficiency according to claim 1, is characterized in that described natural surface active agent is sorbitol, mannitol, Saccharum lactis, and the ratio of its consumption is 2: 1: 2.
6. the active organic liquid fertilizer of a kind of multielement high-efficiency according to claim 1, is characterized in that described trace element comprises zinc sulfate, ferrous sulfate, manganous sulfate, copper sulfate, boric acid and ammonium molybdate, and the ratio of its consumption is 1: 3: 1: 1.5: 2: 1.
7. a preparation method for the active organic liquid fertilizer of multielement high-efficiency, is characterized in that comprising the following steps:
(1) prepare vinasse enzymolysis clear liquid;
(2) chitosan, trace element are joined in vinasse enzymolysis clear liquid in proportion, fully stir 5-10 minute;
(3) nitrogenous fertilizer, phosphate fertilizer, potash fertilizer, natural surface active agent are joined in the solution that step 2 forms, in airflow stirring machine, continue to stir 10-15 minute.
(4) liquid stirring is carried out to biochemical investigation, packing, finished product.
CN201310722180.XA 2013-12-15 2013-12-15 A kind of organic liquid fertilizer and preparation method Active CN103724126B (en)

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104817347A (en) * 2015-03-30 2015-08-05 苏州仁成生物科技有限公司 Preparation method of biological organic fertilizer for improving content of proteins in potato
CN105601405A (en) * 2015-10-23 2016-05-25 潘福忠 Microbial targeting flora liquid organic fertilizer
CN107399999A (en) * 2017-09-21 2017-11-28 阿米巴南京生物技术有限责任公司 A kind of preparation method of high nitrogen type water-soluble fertilizer
CN107986888A (en) * 2018-01-18 2018-05-04 湖南润兆达农业科技发展有限公司 A kind of organic liquid fertilizer based on Application to the Chinese medical herbs
CN108059543A (en) * 2018-01-12 2018-05-22 夏逸雨 Strong liquid fertilizer of a kind of blade face adhesive ability and preparation method thereof
CN108752128A (en) * 2018-05-07 2018-11-06 北京百丰天下生物科技有限公司 Quickly carry biofluid bacterial manure of robust seedling and preparation method thereof
CN109081737A (en) * 2018-10-18 2018-12-25 贵州省中国科学院天然产物化学重点实验室 A kind of bioactivity plant foliar fertilizer using traditional Chinese medicine extraction byproduct fermentation
CN111333469A (en) * 2019-09-20 2020-06-26 安徽金种子酒业股份有限公司 Organic fertilizer prepared by utilizing white spirit solid waste lees through two-step method and preparation method thereof
CN111848313A (en) * 2020-08-26 2020-10-30 宁夏大学 Carbon-based full-nutrient liquid water-soluble fertilizer and preparation method thereof

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JP2004147612A (en) * 2002-11-01 2004-05-27 Bio Giken:Kk Enzymatic composition having lactic acid fermentation and decomposition activity and method for producing lactic acid fermentation composition
CN1844054A (en) * 2006-05-18 2006-10-11 邹启吾 Method for preparing organic protein fertilizer by waste distiller's grains
CN101177360A (en) * 2007-11-23 2008-05-14 何章杰 Method for manufacturing amino acid active fertilizer
CN101885627A (en) * 2010-06-26 2010-11-17 甘肃省农业科学院生物技术研究所 Method for producing liquid bio-fertilizer from potato cell sap
CN102381905A (en) * 2011-07-22 2012-03-21 河北九派生物科技有限公司 Foliage fertilizer and application method thereof
CN102432378A (en) * 2011-09-19 2012-05-02 北京雷力农用化学有限公司 Foliar fertilizer and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004147612A (en) * 2002-11-01 2004-05-27 Bio Giken:Kk Enzymatic composition having lactic acid fermentation and decomposition activity and method for producing lactic acid fermentation composition
CN1844054A (en) * 2006-05-18 2006-10-11 邹启吾 Method for preparing organic protein fertilizer by waste distiller's grains
CN101177360A (en) * 2007-11-23 2008-05-14 何章杰 Method for manufacturing amino acid active fertilizer
CN101885627A (en) * 2010-06-26 2010-11-17 甘肃省农业科学院生物技术研究所 Method for producing liquid bio-fertilizer from potato cell sap
CN102381905A (en) * 2011-07-22 2012-03-21 河北九派生物科技有限公司 Foliage fertilizer and application method thereof
CN102432378A (en) * 2011-09-19 2012-05-02 北京雷力农用化学有限公司 Foliar fertilizer and preparation method thereof

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104817347A (en) * 2015-03-30 2015-08-05 苏州仁成生物科技有限公司 Preparation method of biological organic fertilizer for improving content of proteins in potato
CN105601405A (en) * 2015-10-23 2016-05-25 潘福忠 Microbial targeting flora liquid organic fertilizer
CN107399999A (en) * 2017-09-21 2017-11-28 阿米巴南京生物技术有限责任公司 A kind of preparation method of high nitrogen type water-soluble fertilizer
CN108059543A (en) * 2018-01-12 2018-05-22 夏逸雨 Strong liquid fertilizer of a kind of blade face adhesive ability and preparation method thereof
CN107986888A (en) * 2018-01-18 2018-05-04 湖南润兆达农业科技发展有限公司 A kind of organic liquid fertilizer based on Application to the Chinese medical herbs
CN108752128A (en) * 2018-05-07 2018-11-06 北京百丰天下生物科技有限公司 Quickly carry biofluid bacterial manure of robust seedling and preparation method thereof
CN109081737A (en) * 2018-10-18 2018-12-25 贵州省中国科学院天然产物化学重点实验室 A kind of bioactivity plant foliar fertilizer using traditional Chinese medicine extraction byproduct fermentation
CN111333469A (en) * 2019-09-20 2020-06-26 安徽金种子酒业股份有限公司 Organic fertilizer prepared by utilizing white spirit solid waste lees through two-step method and preparation method thereof
CN111848313A (en) * 2020-08-26 2020-10-30 宁夏大学 Carbon-based full-nutrient liquid water-soluble fertilizer and preparation method thereof

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Address after: 276300 Yinan County inspection center, AUCMA Road, Yinan County, Linyi, Shandong

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