CN103717299B - 可变压降上流预聚合器(ufpp)系统和方法 - Google Patents

可变压降上流预聚合器(ufpp)系统和方法 Download PDF

Info

Publication number
CN103717299B
CN103717299B CN201280039048.2A CN201280039048A CN103717299B CN 103717299 B CN103717299 B CN 103717299B CN 201280039048 A CN201280039048 A CN 201280039048A CN 103717299 B CN103717299 B CN 103717299B
Authority
CN
China
Prior art keywords
reaction zone
tray
pressure
riser
vapor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201280039048.2A
Other languages
English (en)
Chinese (zh)
Other versions
CN103717299A (zh
Inventor
C.A.哈米尔顿
R.E.尼特
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Invista Technologies SARL Switzerland
Original Assignee
Invista Technologies SARL Switzerland
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Invista Technologies SARL Switzerland filed Critical Invista Technologies SARL Switzerland
Publication of CN103717299A publication Critical patent/CN103717299A/zh
Application granted granted Critical
Publication of CN103717299B publication Critical patent/CN103717299B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/006Baffles
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/02Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
    • C08G63/12Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
    • C08G63/16Dicarboxylic acids and dihydroxy compounds
    • C08G63/18Dicarboxylic acids and dihydroxy compounds the acids or hydroxy compounds containing carbocyclic rings
    • C08G63/181Acids containing aromatic rings
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78Preparation processes
    • C08G63/785Preparation processes characterised by the apparatus used
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094Jackets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00162Controlling or regulating processes controlling the pressure
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00765Baffles attached to the reactor wall
    • B01J2219/00777Baffles attached to the reactor wall horizontal

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polymerisation Methods In General (AREA)
CN201280039048.2A 2011-06-10 2012-06-04 可变压降上流预聚合器(ufpp)系统和方法 Expired - Fee Related CN103717299B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201161495690P 2011-06-10 2011-06-10
US61/495690 2011-06-10
PCT/US2012/040745 WO2012170351A2 (en) 2011-06-10 2012-06-04 Variable pressure drop up flow-pre-polymerizer (ufpp) systems and methods

Publications (2)

Publication Number Publication Date
CN103717299A CN103717299A (zh) 2014-04-09
CN103717299B true CN103717299B (zh) 2015-12-23

Family

ID=47296692

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201280039048.2A Expired - Fee Related CN103717299B (zh) 2011-06-10 2012-06-04 可变压降上流预聚合器(ufpp)系统和方法

Country Status (8)

Country Link
US (1) US20150051367A1 (enExample)
EP (1) EP2718002A4 (enExample)
CN (1) CN103717299B (enExample)
BR (1) BR112013031805A2 (enExample)
IN (1) IN2014MN00006A (enExample)
MX (1) MX2013014483A (enExample)
WO (1) WO2012170351A2 (enExample)
ZA (1) ZA201309231B (enExample)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107469736A (zh) * 2017-10-12 2017-12-15 重庆农药化工(集团)有限公司 可调节反应压力的反应釜及可调压反应釜系统
CN114534624B (zh) * 2020-11-11 2024-04-19 中国石油化工股份有限公司 一种塔式预缩聚反应器
NL2034182B1 (en) * 2023-02-20 2024-09-03 Cure Tech Bv A method to recycle a stream of polyester waste material and a system for applying the method

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1204347A (zh) * 1995-12-14 1999-01-06 纳幕尔杜邦公司 制造聚酯预聚物的方法
US6353062B1 (en) * 2000-02-11 2002-03-05 E. I. Du Pont De Nemours And Company Continuous process for producing poly(trimethylene terephthalate)
WO2005042615A1 (de) * 2003-10-31 2005-05-12 Uhde Inventa-Fischer Gmbh & Co. Kg Turmreaktor sowie dessen verwendung zur kontinuierlichen herstellung von hochmolekularem polyester
CN2767447Y (zh) * 2005-02-05 2006-03-29 中国纺织工业设计院 生产聚对苯二甲酸乙二醇酯的高效简化装置
CN1867606A (zh) * 2003-10-10 2006-11-22 旭化成化学株式会社 生产聚对苯二甲酸烷基二醇酯的方法、生产聚对苯二甲酸烷基二醇酯成型制品的方法以及聚对苯二甲酸烷基二醇酯成型制品
US20090117013A1 (en) * 2006-06-02 2009-05-07 Eike Schulz Van Endert Process for continuous preparation of high molecular weight polyesters by esterification of dicarboxylic acids and/or transesterification of dicarboxylic acids with diols and/or mixtures thereof and an apparatus therefor
CN101612544A (zh) * 2009-05-27 2009-12-30 中国纺织工业设计院 预缩聚反应器装置
WO2010015810A1 (en) * 2008-08-07 2010-02-11 Invista Technologies S.A.R.L. Process for production of polyesters

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2504258A1 (de) * 1975-02-01 1976-08-05 Dynamit Nobel Ag Verfahren und apparatur zur herstellung von oligomeren alkylenterephthalaten
DZ3093A1 (fr) * 1999-09-21 2004-06-20 Du Pont Procédé pour ajuster les propriétés de post-chauffage de résines de polyester.
DE102005013764B3 (de) * 2005-03-22 2006-10-12 Epc Industrial Engineering Gmbh Modulare Vorrichtung zur kontinuierlichen Entgasung und Herstellung polymerer Vorkondensate, mit reaktionstechnisch hohem Verhältnis Produktoberfläche zu Volumen, bei schonender Behandlung der Reaktionsproduktmasse
US7718137B2 (en) * 2005-10-28 2010-05-18 Eastman Chemical Company Reactor with optimized internal tray design
US7892498B2 (en) * 2007-03-08 2011-02-22 Eastman Chemical Company Polyester production system employing an unagitated esterification reactor

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1204347A (zh) * 1995-12-14 1999-01-06 纳幕尔杜邦公司 制造聚酯预聚物的方法
US6353062B1 (en) * 2000-02-11 2002-03-05 E. I. Du Pont De Nemours And Company Continuous process for producing poly(trimethylene terephthalate)
CN1867606A (zh) * 2003-10-10 2006-11-22 旭化成化学株式会社 生产聚对苯二甲酸烷基二醇酯的方法、生产聚对苯二甲酸烷基二醇酯成型制品的方法以及聚对苯二甲酸烷基二醇酯成型制品
WO2005042615A1 (de) * 2003-10-31 2005-05-12 Uhde Inventa-Fischer Gmbh & Co. Kg Turmreaktor sowie dessen verwendung zur kontinuierlichen herstellung von hochmolekularem polyester
CN2767447Y (zh) * 2005-02-05 2006-03-29 中国纺织工业设计院 生产聚对苯二甲酸乙二醇酯的高效简化装置
US20090117013A1 (en) * 2006-06-02 2009-05-07 Eike Schulz Van Endert Process for continuous preparation of high molecular weight polyesters by esterification of dicarboxylic acids and/or transesterification of dicarboxylic acids with diols and/or mixtures thereof and an apparatus therefor
WO2010015810A1 (en) * 2008-08-07 2010-02-11 Invista Technologies S.A.R.L. Process for production of polyesters
CN101612544A (zh) * 2009-05-27 2009-12-30 中国纺织工业设计院 预缩聚反应器装置

Also Published As

Publication number Publication date
WO2012170351A3 (en) 2013-04-11
IN2014MN00006A (enExample) 2015-06-12
EP2718002A2 (en) 2014-04-16
ZA201309231B (en) 2015-12-23
BR112013031805A2 (pt) 2017-01-24
WO2012170351A2 (en) 2012-12-13
MX2013014483A (es) 2015-01-27
CN103717299A (zh) 2014-04-09
EP2718002A4 (en) 2015-03-18
US20150051367A1 (en) 2015-02-19

Similar Documents

Publication Publication Date Title
US7608225B2 (en) Tower reactor and use thereof for the continuous production of high molecular weight polyesters
US8252888B2 (en) Process for continuous preparation of high molecular weight polyesters by esterification of dicarboxylic acids and/or transesterification of dicarboxylic acids with diols and/or mixtures thereof and an apparatus therefor
US7179433B2 (en) Production process and production apparatus for polybutylene terephthalate
KR101496480B1 (ko) 비교반식 에스터화 반응기를 사용하는 폴리에스터 생산 시스템
CN107567470B (zh) 应用纯化的对苯二甲酸和1,4-丁二醇制备聚对苯二甲酸丁二醇酯的连续方法
JP2004502793A (ja) ポリ(トリメチレンテレフタレート)の連続的製造方法
CN103717299B (zh) 可变压降上流预聚合器(ufpp)系统和方法
CN102585216A (zh) 尼龙66短流程连续聚合的方法及设备
KR101955064B1 (ko) 방향족 폴리카보네이트의 제조 방법 및 제조 설비
KR101563755B1 (ko) 수직방향-이격된 구역을 갖는 다단계 관형 반응기
US20020137874A1 (en) Process for producing oligocarbonates
US10377854B2 (en) Continuous process for making polybutylene terephthalate
WO2007069463A1 (ja) 高品質芳香族ポリカーボネートを工業的に製造する方法
JP5344927B2 (ja) 高品質芳香族ポリカーボネートを工業的規模で製造する方法
CN105209409B (zh) 热虹吸酯化器蒸汽再利用
JP2011116915A (ja) ポリエステルの重合装置
TW201534636A (zh) 製備聚對苯二甲酸乙二酯之高固有黏度塔型反應器
JP3722138B2 (ja) 連続重縮合装置及び連続重縮合方法
US20160108173A1 (en) Thermosiphon esterifier
JP5938992B2 (ja) ポリカーボネート樹脂の製造方法
JP2015165011A (ja) ポリブチレンテレフタレートの製造方法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20151223

Termination date: 20200604