CN103666731A - Mildew-resistant microemulsified cutting fluid and preparation method thereof - Google Patents
Mildew-resistant microemulsified cutting fluid and preparation method thereof Download PDFInfo
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- CN103666731A CN103666731A CN201310653446.XA CN201310653446A CN103666731A CN 103666731 A CN103666731 A CN 103666731A CN 201310653446 A CN201310653446 A CN 201310653446A CN 103666731 A CN103666731 A CN 103666731A
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Abstract
A mildew-resistant microemulsified cutting fluid is prepared from the following raw materials: by weight, 1-2 parts of petroleum sodium sulfonate, 4-5 parts of sorbitan oleate, 2-3 parts of fatty alcohol polyoxyethylene ether, 1-2 parts of coconut oil diethanolamide, 20-23 parts of butyl carbitol, 1-2 parts of triethanolamine, 1-2 parts of benzalkonium bromide amine, 1-2 parts of palmitoleic acid, 2-3 parts of dimethyl silicone oil, 11-13 parts of dimethyl fumarate, 6-8 parts of an additive and 200 parts of water; the mildew-resistant microemulsified cutting fluid, by using of a variety of surface active agents, is good in water solubility, free of condensation, agglomeration, precipitation and bubbling; the mildew-resistant microemulsified cutting fluid, by using of the dimethyl fumarate, is mildew-resistant and has good lubricity; the mildew-resistant microemulsified cutting fluid is good in cleaning and rust resistant properties and is an environmentally friendly multi-purpose cutting fluid.
Description
Technical field
The present invention relates to cutting fluid technical field, relate in particular to a kind of mildew-resistant micro-emulsion cutting fluid and preparation method thereof.
Background technology
Cutting fluid should possess good cooling performance, lubricity, rustless property, oil removing cleaning function, anti-corrosion function, easily dilutable feature.Cutting fluid can be divided into two classes, oil soluble cutting fluid and water-soluble metalworking liquid at present.General oil soluble cutting fluid lubrication performance is good, but poor cooling performance, and contain large amount of organic, contaminate environment.Although some water-soluble metalworking liquid cooling performances are good, there is again the poor problem of oilness and rust-proof effect, therefore research and development have concurrently oilness, cooling, rust-preventing characteristic, easy cleaning, nontoxic, tasteless, non-corrosive to human body, to equipment not burn into the non-staining cutting fluid of environment is just seemed to very important.
Summary of the invention
The object of the present invention is to provide a kind of mildew-resistant micro-emulsion cutting fluid and preparation method thereof, this cutting fluid has good, the anti-feature of going mouldy of cleaning.
Technical scheme of the present invention is as follows:
A mildew-resistant micro-emulsion cutting fluid, is characterized in that being made by the raw material of following weight part: petroleum sodium sulfonate 1-2, sorbitan monooleate 4-5, fatty alcohol-polyoxyethylene ether 2-3, coconut oil diethanol amide 1-2, diethylene glycol monobutyl ether 20-23, trolamine 1-2, benzalkonium bromide 1-2, Zoomeric acid 1-2, dimethyl silicone oil 2-3, dimethyl fumarate 11-13, auxiliary agent 6-8, water 200; Described auxiliary agent is made by the raw material of following weight part: polyoxyethylene sorbitan monooleate 2-3, aluminum nitride powder 0.1-0.2, alcohol ester 12 1-2, tea-polyphenol 1-2, Kathon 1-2, Sodium orthomolybdate 2-3, Natvosol 5-8, peach gum 2-3, neopentyl glycol 3-4, ammonium persulphate 1-2, water 20-24; Preparation method be ammonium persulphate is water-soluble after, then add other leftover materials, stir 10-15 minute, be heated to 70-80 ℃, stirring reaction 1-2 hour, obtains.
The preparation method of described mildew-resistant micro-emulsion cutting fluid, is characterized in that comprising the following steps: water, petroleum sodium sulfonate, sorbitan monooleate, fatty alcohol-polyoxyethylene ether, coconut oil diethanol amide, benzalkonium bromide are mixed, be heated to 40-50 ℃; Under 3000-4000 rev/min of stirring, add diethylene glycol monobutyl ether, Zoomeric acid, dimethyl silicone oil, dimethyl fumarate, auxiliary agent, continue to be heated to 70-80 ℃, stir 10-15 minute; Add other remaining components, continue to stir 15-25 minute, obtain.
Beneficial effect of the present invention
Cutting fluid of the present invention is by being used kinds of surface promoting agent, and good water solubility, does not condense, does not lump, do not produce precipitation, non-foaming; By using dimethyl fumarate, anti-going mouldy, and oilness is better; Cutting fluid cleaning of the present invention is good, and rustless property is better, is a kind of multiduty cutting fluid of environmental protection.
Embodiment
A mildew-resistant micro-emulsion cutting fluid, by following weight part (kilogram) raw material make: petroleum sodium sulfonate 1.5, sorbitan monooleate 4.5, fatty alcohol-polyoxyethylene ether 2.5, coconut oil diethanol amide 1.5, diethylene glycol monobutyl ether 21, trolamine 1.5, benzalkonium bromide 1.5, Zoomeric acid 1.5, dimethyl silicone oil 2.5, dimethyl fumarate 12, auxiliary agent 7, water 200; Described auxiliary agent by following weight part (kilogram) raw material make: polyoxyethylene sorbitan monooleate 2, aluminum nitride powder 0.1, alcohol ester 12, tea-polyphenol 1, Kathon 1, Sodium orthomolybdate 2, Natvosol 5, peach gum 3, neopentyl glycol 3, ammonium persulphate 1, water 20; Preparation method be ammonium persulphate is water-soluble after, then add other leftover materials, stir 10-15 minute, be heated to 70-80 ℃, stirring reaction 1-2 hour, obtains.
The preparation method of described mildew-resistant micro-emulsion cutting fluid, comprises the following steps: water, petroleum sodium sulfonate, sorbitan monooleate, fatty alcohol-polyoxyethylene ether, coconut oil diethanol amide, benzalkonium bromide are mixed, be heated to 45 ℃; Under 3500 revs/min of stirrings, add diethylene glycol monobutyl ether, Zoomeric acid, dimethyl silicone oil, dimethyl fumarate, auxiliary agent, continue to be heated to 75 ℃, stir 13 minutes; Add other remaining components, continue to stir 20 minutes, obtain.
The mildew-resistant micro-emulsion cutting fluid testing data that this embodiment obtains is as follows:
Claims (2)
1. a mildew-resistant micro-emulsion cutting fluid, is characterized in that being made by the raw material of following weight part: petroleum sodium sulfonate 1-2, sorbitan monooleate 4-5, fatty alcohol-polyoxyethylene ether 2-3, coconut oil diethanol amide 1-2, diethylene glycol monobutyl ether 20-23, trolamine 1-2, benzalkonium bromide 1-2, Zoomeric acid 1-2, dimethyl silicone oil 2-3, dimethyl fumarate 11-13, auxiliary agent 6-8, water 200; Described auxiliary agent is made by the raw material of following weight part: polyoxyethylene sorbitan monooleate 2-3, aluminum nitride powder 0.1-0.2, alcohol ester 12 1-2, tea-polyphenol 1-2,2-n-octyl-4-isothiazoline-3-ketone 1-2, Sodium orthomolybdate 2-3, Natvosol 5-8, peach gum 2-3, neopentyl glycol 3-4, ammonium persulphate 1-2, water 20-24; Preparation method be ammonium persulphate is water-soluble after, then add other leftover materials, stir 10-15 minute, be heated to 70-80 ℃, stirring reaction 1-2 hour, obtains.
2. the preparation method of mildew-resistant micro-emulsion cutting fluid according to claim 1, it is characterized in that comprising the following steps: water, petroleum sodium sulfonate, sorbitan monooleate, fatty alcohol-polyoxyethylene ether, coconut oil diethanol amide, benzalkonium bromide are mixed, be heated to 40-50 ℃; Under 3000-4000 rev/min of stirring, add diethylene glycol monobutyl ether, Zoomeric acid, dimethyl silicone oil, dimethyl fumarate, auxiliary agent, continue to be heated to 70-80 ℃, stir 10-15 minute; Add other remaining components, continue to stir 15-25 minute, obtain.
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CN201310653446.XA CN103666731A (en) | 2013-12-05 | 2013-12-05 | Mildew-resistant microemulsified cutting fluid and preparation method thereof |
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CN201310653446.XA CN103666731A (en) | 2013-12-05 | 2013-12-05 | Mildew-resistant microemulsified cutting fluid and preparation method thereof |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106350191A (en) * | 2016-08-27 | 2017-01-25 | 蚌埠市广瑞机械有限公司 | Mechanical cutting fluid high in stability |
CN106590902A (en) * | 2016-12-07 | 2017-04-26 | 德阳力久云智知识产权运营有限公司 | Anti-extreme pressure mould-proof cutting fluid and preparation method thereof |
-
2013
- 2013-12-05 CN CN201310653446.XA patent/CN103666731A/en active Pending
Non-Patent Citations (1)
Title |
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叶茂盛: "《金属切削液》", 31 December 1996 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106350191A (en) * | 2016-08-27 | 2017-01-25 | 蚌埠市广瑞机械有限公司 | Mechanical cutting fluid high in stability |
CN106590902A (en) * | 2016-12-07 | 2017-04-26 | 德阳力久云智知识产权运营有限公司 | Anti-extreme pressure mould-proof cutting fluid and preparation method thereof |
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