CN106350191A - Mechanical cutting fluid high in stability - Google Patents

Mechanical cutting fluid high in stability Download PDF

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Publication number
CN106350191A
CN106350191A CN201610743536.1A CN201610743536A CN106350191A CN 106350191 A CN106350191 A CN 106350191A CN 201610743536 A CN201610743536 A CN 201610743536A CN 106350191 A CN106350191 A CN 106350191A
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China
Prior art keywords
cutting fluid
silica flour
stability
mechanical cutting
minute
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610743536.1A
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Chinese (zh)
Inventor
孟佩
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wide Auspicious Mechanical Co Ltd In Bengbu
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Wide Auspicious Mechanical Co Ltd In Bengbu
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Application filed by Wide Auspicious Mechanical Co Ltd In Bengbu filed Critical Wide Auspicious Mechanical Co Ltd In Bengbu
Priority to CN201610743536.1A priority Critical patent/CN106350191A/en
Publication of CN106350191A publication Critical patent/CN106350191A/en
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M173/00—Lubricating compositions containing more than 10% water
    • C10M173/02—Lubricating compositions containing more than 10% water not containing mineral or fatty oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M113/00—Lubricating compositions characterised by the thickening agent being an inorganic material
    • C10M113/12—Silica
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M159/00—Lubricating compositions characterised by the additive being of unknown or incompletely defined constitution
    • C10M159/12—Reaction products
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/10—Compounds containing silicon
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/06—Peroxides; Ozonides
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/128—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids containing hydroxy groups; Ethers thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/14—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to carbon atoms of six-membered aromatic rings
    • C10M2207/142—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to carbon atoms of six-membered aromatic rings polycarboxylic
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28—Esters
    • C10M2207/282—Esters of (cyclo)aliphatic oolycarboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2215/042—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/08—Amides
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2225/00—Organic macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2225/04—Organic macromolecular compounds containing phosphorus as ingredients in lubricant compositions obtained by phosphorisation of macromolecualr compounds not containing phosphorus in the monomers
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/02—Pour-point; Viscosity index
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling

Abstract

The invention belongs to the technical field of lubrication for mechanical processing, particularly relates to a mechanical cutting fluid high in stability. The mechanical cutting fluid comprises deionized water, petroleum sodium sulfonate, polyethylene glycol monoleate, cocamidopropyl betaine, triethanolamine oleate, sebacic dibutyl ester, peroxy diisopropyl benzene, alkylphenol polyoxyethylene ether phosphate, modified quartz powder, phthalandione and potassium sorbate. The mechanical cutting fluid has the advantages that by modifying quartz powder, a stable miniature emulsion structure is formed inside the cutting fluid, stable kinematic viscosity is kept, intermolecular friction force is decreased, good lubricity and good anti-rust property are achieved, and in a high-humidity condition, a cutting machine keeps a low surface tension to guarantee good permeability and cleaning ability of the mechanical cutting fluid, so that abrasions of cutters are reduced.

Description

A kind of preferable Mechanism cutting emulsification wastewater of stability
Technical field
The invention belongs to the lubrication technical field of machining is and in particular to a kind of preferable Mechanism cutting emulsification wastewater of stability.
Background technology
Cutting fluid is that one kind is used in metal cutting, grinds in the course of processing, for cooling down and lubricating the work of cutter and workpiece Industry liquid, cutting fluid is provided simultaneously with good cooling performance, greasy property, rustless property, oil removing cleaning function, anti-corrosion work( Energy, easily dilutable feature, but when the lubrication of cutting fluid, antirust function strengthen, cooling, cleaning performance will be deteriorated, and vice versa, In some areas due to working environment relative humidity, the antirust function of cutting fluid will be had higher requirements, but cutting fluid cooling The reduction of function, can increase the abrasion of cutter, reduce cutting-tool's used life, meanwhile, cutting fluid seal after opening bad, After placing a period of time, it is possible that cutting fluid kinematic viscosity raises, the situation that lubricating function weakens.
Content of the invention
The purpose of the present invention is for existing problem, there is provided a kind of preferable Mechanism cutting emulsification wastewater of stability.
The present invention is achieved by the following technical solutions: a kind of preferable Mechanism cutting emulsification wastewater of stability, by following weight The raw material of part is made: deionized water 20-40 part, petroleum sodium sulfonate 30-35 part, PEG400 monoleate 15-20 part, coconut palm Oleamide CAB 2-4 part, triethanolamine oleate 1-3 part, SA dibutyl ester 1-2 part, peroxide diisopropylbenzene (DIPB) 2-3 part, Alkylphenol polyoxyethylene phosphoesterase 30 .4-0.7 part, modified silica flour 0.8-1.5 part, phthalic acid 1-2 part, potassium sorbate 0.4-0.8 part.
As further improvement of these options, the fineness of described modification silica flour is 400 mesh.
As further improvement of these options, the method for modifying of described modification silica flour is: by vinyl trimethoxy Agent silane ph is 3.6 aqueous acetic acid hydrolysis, adds the ethylene after the hydrolysis being equivalent to its weight 1.42% in silica flour Base trimethoxy agent silane, makes it be uniformly dispersed with ultrasonic disperse device, reacts 4.5 hours, obtain modification in 120 DEG C of baking oven Silica flour.
A kind of preferable Mechanism cutting emulsification wastewater of stability, is made up of following steps:
(1) deionized water, petroleum sodium sulfonate and PEG400 monoleate are added in reaction pot, stir post-heating To 75-80 DEG C, add cocamido propyl betaine, SA dibutyl ester, alkylphenol polyoxyethylene phosphate ester and peroxide Diisopropylbenzene (DIPB) stirring reaction 10-15 minute；
(2) it is continuously heating to 110-115 DEG C, adds modified silica flour, stirring reaction 4-7 minute, near room temperature, add remaining former Material, after stirring 20-25 minute, obtains final product.
The present invention has the advantage that by being modified to silica flour in the present invention compared to existing technology, and gained cuts Liquid is internally formed stable microemulsion structure, keeps stable kinematic viscosity, reduces intermolecular frictional force, have excellent Lubricity and rust-preventing characteristic, under conditions of high humidity, this cutter keeps relatively low surface tension so as to ensure excellent permeability And cleaning, reduce the abrasion of cutter.
Specific embodiment
Embodiment 1
A kind of preferable Mechanism cutting emulsification wastewater of stability, is made up of the raw material of following weight portion: 20 parts of deionized water, petroleum sodium sulfonate 35 parts, 20 parts of PEG400 monoleate, 3 parts of cocamido propyl betaine, 2 parts of triethanolamine oleate, SA two fourth 2 parts of ester, 2 parts of peroxide diisopropylbenzene (DIPB), alkylphenol polyoxyethylene phosphoesterase 30 .5 part, 1 part of modified silica flour, phthalic acid 2 Part, 0.5 part of potassium sorbate.
Wherein, the fineness of described modification silica flour is 400 mesh；Method of modifying is: by vinyl trimethoxy agent silane ph Aqueous acetic acid hydrolysis for 3.6, adds the vinyl trimethoxy agent after the hydrolysis being equivalent to its weight 1.42% in silica flour Silane, makes it be uniformly dispersed with ultrasonic disperse device, reacts 4.5 hours, obtain modified silica flour in 120 DEG C of baking oven.
A kind of preferable Mechanism cutting emulsification wastewater of stability, is made up of following steps:
(1) deionized water, petroleum sodium sulfonate and PEG400 monoleate are added in reaction pot, stir post-heating To 75-80 DEG C, add cocamido propyl betaine, SA dibutyl ester, alkylphenol polyoxyethylene phosphate ester and peroxide Diisopropylbenzene (DIPB) stirring reaction 10-15 minute；
(2) it is continuously heating to 110-115 DEG C, adds modified silica flour, stirring reaction 4-7 minute, near room temperature, add remaining former Material, after stirring 20-25 minute, obtains final product.
Embodiment 2
A kind of preferable Mechanism cutting emulsification wastewater of stability, is made up of the raw material of following weight portion: 30 parts of deionized water, petroleum sodium sulfonate 32 parts, 16 parts of PEG400 monoleate, 3 parts of cocamido propyl betaine, 2 parts of triethanolamine oleate, SA two fourth 1 part of ester, 3 parts of peroxide diisopropylbenzene (DIPB), alkylphenol polyoxyethylene phosphoesterase 30 .4 part, 0.9 part of modified silica flour, phthalic acid 2 Part, 0.7 part of potassium sorbate.
Embodiment 3
A kind of preferable Mechanism cutting emulsification wastewater of stability, is made up of the raw material of following weight portion: 40 parts of deionized water, petroleum sodium sulfonate 30 parts, 15 parts of PEG400 monoleate, 3 parts of cocamido propyl betaine, 2 parts of triethanolamine oleate, SA two fourth 2 parts of ester, 2 parts of peroxide diisopropylbenzene (DIPB), alkylphenol polyoxyethylene phosphoesterase 30 .4 part, 1.2 parts of modified silica flour, phthalic acid 1 Part, 0.4 part of potassium sorbate.
By experiment test, the technology that in the present invention, embodiment 1-3 all meets required by gb/t6144-2010 standard refers to Mark, concrete test result is as follows:
Table 1
Can be seen that in the present invention, cutting fluid antirust function preferably, in real work, has and preferably oozes by data in table 1 Permeability and cleaning, the conventional viscosity of cutting fluid is 6.8mm/s, and after placing 15 days, cutting fluid increased 1.7mm/s, protects Hold preferable lubricity.

Claims (4)

1. a kind of preferable Mechanism cutting emulsification wastewater of stability is it is characterised in that be made up of the raw material of following weight portion: deionized water 20-40 part, petroleum sodium sulfonate 30-35 part, PEG400 monoleate 15-20 part, cocamido propyl betaine 2-4 part, Triethanolamine oleate 1-3 part, SA dibutyl ester 1-2 part, peroxide diisopropylbenzene (DIPB) 2-3 part, alkylphenol polyoxyethylene phosphate ester 0.4-0.7 part, modified silica flour 0.8-1.5 part, phthalic acid 1-2 part, potassium sorbate 0.4-0.8 part.
2. as claimed in claim 1 a kind of preferable Mechanism cutting emulsification wastewater of stability it is characterised in that described modification silica flour thin Spend for 400 mesh.
3. as claimed in claim 2 a kind of preferable Mechanism cutting emulsification wastewater of stability it is characterised in that the changing of described modification silica flour Property method be: by vinyl trimethoxy agent silane ph be 3.6 aqueous acetic acid hydrolysis, in silica flour add be equivalent to it Vinyl trimethoxy agent silane after the hydrolysis of weight 1.42%, makes it be uniformly dispersed with ultrasonic disperse device, in 120 DEG C of baking React 4.5 hours in case, obtain modified silica flour.
4. as claimed in claim 3 a kind of preferable Mechanism cutting emulsification wastewater of stability it is characterised in that being made up of following steps:
(1) deionized water, petroleum sodium sulfonate and PEG400 monoleate are added in reaction pot, stir post-heating To 75-80 DEG C, add cocamido propyl betaine, SA dibutyl ester, alkylphenol polyoxyethylene phosphate ester and peroxide Diisopropylbenzene (DIPB) stirring reaction 10-15 minute；
(2) it is continuously heating to 110-115 DEG C, adds modified silica flour, stirring reaction 4-7 minute, near room temperature, add remaining former Material, after stirring 20-25 minute, obtains final product.
CN201610743536.1A 2016-08-27 2016-08-27 Mechanical cutting fluid high in stability Pending CN106350191A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610743536.1A CN106350191A (en) 2016-08-27 2016-08-27 Mechanical cutting fluid high in stability

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Application Number Priority Date Filing Date Title
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108998187A (en) * 2018-09-05 2018-12-14 罗粉继 A kind of cutting fluid
CN108998186A (en) * 2018-09-05 2018-12-14 罗粉继 A kind of aqueous composition cooling for metal working lubricant
CN108998185A (en) * 2018-09-05 2018-12-14 罗粉继 A kind of water based lubrication cooling compositions for intermetallic composite coating

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CN104120021A (en) * 2014-06-30 2014-10-29 安徽铖友汽车零部件制造有限公司 Environment-friendly cutting fluid suitable for multiple metals and preparation method thereof
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CN104560327A (en) * 2014-12-30 2015-04-29 芜湖市润雨精密机械有限公司 High-permeability metal cutting fluid with excellent corrosion resistance and preparation method of metal cutting fluid

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108998187A (en) * 2018-09-05 2018-12-14 罗粉继 A kind of cutting fluid
CN108998186A (en) * 2018-09-05 2018-12-14 罗粉继 A kind of aqueous composition cooling for metal working lubricant
CN108998185A (en) * 2018-09-05 2018-12-14 罗粉继 A kind of water based lubrication cooling compositions for intermetallic composite coating

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Application publication date: 20170125