CN103756773B - A kind of sewer oil micro-emulsion type cutting fluid and preparation method thereof - Google Patents
A kind of sewer oil micro-emulsion type cutting fluid and preparation method thereof Download PDFInfo
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- CN103756773B CN103756773B CN201310670824.5A CN201310670824A CN103756773B CN 103756773 B CN103756773 B CN 103756773B CN 201310670824 A CN201310670824 A CN 201310670824A CN 103756773 B CN103756773 B CN 103756773B
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- Prior art keywords
- sewer oil
- cutting fluid
- water
- emulsion type
- preparation
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- 239000002173 cutting fluid Substances 0.000 title claims abstract description 23
- 239000004530 micro-emulsion Substances 0.000 title claims abstract description 12
- 238000002360 preparation method Methods 0.000 title claims description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 21
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 9
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims abstract description 9
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims abstract description 8
- CRWNQZTZTZWPOF-UHFFFAOYSA-N 2-methyl-4-phenylpyridine Chemical compound C1=NC(C)=CC(C=2C=CC=CC=2)=C1 CRWNQZTZTZWPOF-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 7
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 229910052938 sodium sulfate Inorganic materials 0.000 claims abstract description 7
- 235000011152 sodium sulphate Nutrition 0.000 claims abstract description 7
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims abstract description 4
- -1 ethoxylated dodecyl alcohol sodium sulfate Chemical class 0.000 claims abstract description 4
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims abstract description 4
- 235000017557 sodium bicarbonate Nutrition 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 15
- 239000004160 Ammonium persulphate Substances 0.000 claims description 6
- YNAVUWVOSKDBBP-UHFFFAOYSA-N Morpholine Chemical compound C1COCCN1 YNAVUWVOSKDBBP-UHFFFAOYSA-N 0.000 claims description 6
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 claims description 6
- 235000019395 ammonium persulphate Nutrition 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- 229940058020 2-amino-2-methyl-1-propanol Drugs 0.000 claims description 3
- 235000006040 Prunus persica var persica Nutrition 0.000 claims description 3
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 3
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims description 3
- CBTVGIZVANVGBH-UHFFFAOYSA-N aminomethyl propanol Chemical compound CC(C)(N)CO CBTVGIZVANVGBH-UHFFFAOYSA-N 0.000 claims description 3
- 229910021538 borax Inorganic materials 0.000 claims description 3
- PMHQVHHXPFUNSP-UHFFFAOYSA-M copper(1+);methylsulfanylmethane;bromide Chemical compound Br[Cu].CSC PMHQVHHXPFUNSP-UHFFFAOYSA-M 0.000 claims description 3
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical class CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims description 3
- 239000000244 polyoxyethylene sorbitan monooleate Substances 0.000 claims description 3
- 229920000053 polysorbate 80 Polymers 0.000 claims description 3
- 235000019353 potassium silicate Nutrition 0.000 claims description 3
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 3
- 239000004328 sodium tetraborate Substances 0.000 claims description 3
- 235000010339 sodium tetraborate Nutrition 0.000 claims description 3
- 240000006413 Prunus persica var. persica Species 0.000 claims 1
- 150000001412 amines Chemical class 0.000 claims 1
- 238000001816 cooling Methods 0.000 abstract description 6
- 238000004140 cleaning Methods 0.000 abstract description 4
- 230000007613 environmental effect Effects 0.000 abstract description 3
- 239000002244 precipitate Substances 0.000 abstract description 2
- 244000144730 Amygdalus persica Species 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000005461 lubrication Methods 0.000 description 2
- 238000005555 metalworking Methods 0.000 description 2
- GSWAOPJLTADLTN-UHFFFAOYSA-N oxidanimine Chemical compound [O-][NH3+] GSWAOPJLTADLTN-UHFFFAOYSA-N 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000009972 noncorrosive effect Effects 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 235000020354 squash Nutrition 0.000 description 1
- 238000010186 staining Methods 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
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- Lubricants (AREA)
Abstract
A kind of sewer oil micro-emulsion type cutting fluid, is made up of the raw material of following weight part: diethanolamine 2-3, polyvinyl alcohol 6-8, sodium bicarbonate 1-2, ethoxylated dodecyl alcohol sodium sulfate 1-2, sodium hydroxide 1-2, sewer oil 20-23, diethylene glycol dibutyl ether 4-5, butyl (tetra) titanate 12-14, auxiliary agent 6-8, water 200; Cutting fluid of the present invention uses butyl (tetra) titanate, and stable viscosity, does not precipitate; By using sewer oil, not only oilness is good, and useful to environmental protection; The present invention is that water-base cutting fluid also has speed of cooling soon, and cleaning performance is good, has good economic benefit.
Description
Technical field
The present invention relates to cutting fluid field, particularly relate to a kind of sewer oil micro-emulsion type cutting fluid and preparation method thereof.
Background technology
Cutting fluid should possess good cooling performance, lubricity, rustless property, oil removing cleaning function, anti-corrosion function, easily dilutable feature.Current cutting fluid can be divided into two classes, oil soluble cutting fluid and water-soluble metalworking liquid.General oil soluble cutting fluid lubrication performance is good, but poor cooling performance, and containing large amount of organic, contaminate environment.Although some water-soluble metalworking liquid cooling performances are good, there is again the problem of oilness and rust-proof effect difference, therefore research and development have concurrently oilness, cooling, rust-preventing characteristic, easy cleaning, nontoxic, tasteless, non-corrosive to human body, to equipment not burn into the non-staining cutting fluid of environment is just seemed very important.
Summary of the invention
The object of the present invention is to provide a kind of sewer oil micro-emulsion type cutting fluid and preparation method thereof, this cutting fluid lubrication is good, good antirust property, environmental protection and energy saving.
Technical scheme of the present invention is as follows:
A kind of sewer oil micro-emulsion type cutting fluid, is characterized in that being made up of the raw material of following weight part: diethanolamine 2-3, polyvinyl alcohol 6-8, sodium bicarbonate 1-2, ethoxylated dodecyl alcohol sodium sulfate 1-2, sodium hydroxide 1-2, sewer oil 20-23, diethylene glycol dibutyl ether 4-5, butyl (tetra) titanate 12-14, auxiliary agent 6-8, water 200; Described auxiliary agent is made up of the raw material of following weight part: ammonium oxide 1-2, morpholine 2-3, nano aluminum nitride 0.1-0.2, water glass 1-2, borax 2-3,2-amino-2-methyl-1-propanol 1-2, polyoxyethylene sorbitan monooleate 2-3, peach gum 2-3, ammonium persulphate 1-2, water 20-24; Preparation method be ammonium persulphate is water-soluble after, then add other leftover materials, stir 10-15 minute, be heated to 70-80 DEG C, stirring reaction 1-2 hour, to obtain final product.
The preparation method of described sewer oil micro-emulsion type cutting fluid, is characterized in that comprising the following steps: by water, sodium bicarbonate, ethoxylated dodecyl alcohol sodium sulfate, sodium hydroxide mixing, be heated to 40-50 DEG C; Add polyvinyl alcohol, sewer oil, diethylene glycol dibutyl ether, butyl (tetra) titanate, auxiliary agent, continue to be heated to 70-80 DEG C under stirring at 1000-1200 rev/min, stir 10-15 minute; Add other remaining components, continue to stir 15-20 minute, to obtain final product.
Beneficial effect of the present invention
Cutting fluid of the present invention uses butyl (tetra) titanate, and stable viscosity, does not precipitate; By using sewer oil, not only oilness is good, and useful to environmental protection; The present invention is that water-base cutting fluid also has speed of cooling soon, and cleaning performance is good, has good economic benefit.
Embodiment
A kind of sewer oil micro-emulsion type cutting fluid, is made up of the raw material of following weight part (kilogram): diethanolamine 2.5, polyvinyl alcohol 7, sodium bicarbonate 1.5, ethoxylated dodecyl alcohol sodium sulfate 1.5, sodium hydroxide 1.5, sewer oil 22, diethylene glycol dibutyl ether 4.5, butyl (tetra) titanate 13, auxiliary agent 7, water 200; Described auxiliary agent is made up of the raw material of following weight part (kilogram): ammonium oxide 1, morpholine 2, nano aluminum nitride 0.1, water glass 1, borax 2,2-amino-2-methyl-1-propanol 2, polyoxyethylene sorbitan monooleate 3, peach gum 2, ammonium persulphate 1, water 20; Preparation method be ammonium persulphate is water-soluble after, then add other leftover materials, stir 10-15 minute, be heated to 70-80 DEG C, stirring reaction 1-2 hour, to obtain final product.
The preparation method of described sewer oil micro-emulsion type cutting fluid, comprises the following steps: by water, sodium bicarbonate, ethoxylated dodecyl alcohol sodium sulfate, sodium hydroxide mixing, be heated to 45 DEG C; Add polyvinyl alcohol, sewer oil, diethylene glycol dibutyl ether, butyl (tetra) titanate, auxiliary agent, continue to be heated to 75 DEG C under stirring at 1100 revs/min, stir 13 minutes; Add other remaining components, continue stirring 18 minutes, to obtain final product.
The sewer oil micro-emulsion type cutting fluid testing data that this embodiment obtains is as follows:
Claims (1)
1. a sewer oil micro-emulsion type cutting fluid, is characterized in that being made up of the raw material of following weight part: diethanolamine 2-3, polyvinyl alcohol 6-8, sodium bicarbonate 1-2, ethoxylated dodecyl alcohol sodium sulfate 1-2, sodium hydroxide 1-2, sewer oil 20-23, diethylene glycol dibutyl ether 4-5, butyl (tetra) titanate 12-14, auxiliary agent 6-8, water 200; Described auxiliary agent is made up of the raw material of following weight part: amine oxide 1-2, morpholine 2-3, nano aluminum nitride 0.1-0.2, water glass 1-2, borax 2-3,2-amino-2-methyl-1-propanol 1-2, polyoxyethylene sorbitan monooleate 2-3, peach gum 2-3, ammonium persulphate 1-2, water 20-24; Preparation method be ammonium persulphate is water-soluble after, then add other leftover materials, stir 10-15 minute, be heated to 70-80 DEG C, stirring reaction 1-2 hour, to obtain final product;
The preparation method of described sewer oil micro-emulsion type cutting fluid, comprises the following steps: by water, sodium bicarbonate, ethoxylated dodecyl alcohol sodium sulfate, sodium hydroxide mixing, be heated to 40-50 DEG C; Add polyvinyl alcohol, sewer oil, diethylene glycol dibutyl ether, butyl (tetra) titanate, auxiliary agent, continue to be heated to 70-80 DEG C under stirring at 1000-1200 rev/min, stir 10-15 minute; Add other remaining components, continue to stir 15-20 minute, to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310670824.5A CN103756773B (en) | 2013-12-07 | 2013-12-07 | A kind of sewer oil micro-emulsion type cutting fluid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310670824.5A CN103756773B (en) | 2013-12-07 | 2013-12-07 | A kind of sewer oil micro-emulsion type cutting fluid and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103756773A CN103756773A (en) | 2014-04-30 |
| CN103756773B true CN103756773B (en) | 2016-03-09 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201310670824.5A Active CN103756773B (en) | 2013-12-07 | 2013-12-07 | A kind of sewer oil micro-emulsion type cutting fluid and preparation method thereof |
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| CN (1) | CN103756773B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104450049A (en) * | 2014-11-10 | 2015-03-25 | 合肥宏图彩印有限公司 | Emulsion anti-rusting oil containing swill-cooked dirty oil |
| CN104560335A (en) * | 2014-12-30 | 2015-04-29 | 芜湖市润雨精密机械有限公司 | Semi-synthesis type rust preventive cutting fluid and preparation method thereof |
| CN106047451A (en) * | 2016-05-27 | 2016-10-26 | 安徽胜利精密制造科技有限公司 | Method for preparing ointment type cutting fluid matrix |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1174489A1 (en) * | 2000-07-21 | 2002-01-23 | Nueva Fl Ibérica, S.A. | Process for preparing cutting lubricant fluids |
| CN101240217A (en) * | 2008-02-29 | 2008-08-13 | 益田润石（北京）化工有限公司 | Micro-emulsion type metal cutting liquor composition |
-
2013
- 2013-12-07 CN CN201310670824.5A patent/CN103756773B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1174489A1 (en) * | 2000-07-21 | 2002-01-23 | Nueva Fl Ibérica, S.A. | Process for preparing cutting lubricant fluids |
| CN101240217A (en) * | 2008-02-29 | 2008-08-13 | 益田润石（北京）化工有限公司 | Micro-emulsion type metal cutting liquor composition |
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| Publication number | Publication date |
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| CN103756773A (en) | 2014-04-30 |
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Effective date of registration: 20160205 Address after: Baohe District of Hefei City, Anhui province 230001 East Road evergreen business center Applicant after: HEFEI JIEMING NEW MATERIAL TECHNOLOGY CO., LTD. Address before: Anhui province Ma'anshan City Xihuan Road 243173 Dangtu County Shiqiao Town No. 1 Applicant before: MAANSHAN LIXIN MACHINERY MANUFACTURING CO., LTD. |
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Effective date of registration: 20181229 Address after: 221000 Jiefangnan Road 310-11, Quanshan District, Xuzhou City, Jiangsu Province Patentee after: Xuzhou Zhi Ou mechanical and Electrical Equipment Co., Ltd. Address before: 230001 Dongliu Road Changqing Pioneering Center, Baohe District, Hefei City, Anhui Province Patentee before: HEFEI JIEMING NEW MATERIAL TECHNOLOGY CO., LTD. |
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Effective date of registration: 20190403 Address after: 610000 5th Floor, Xiongfei Center, No. 1 Tidu Street, Qingyang District, Chengdu City, Sichuan Province Patentee after: Wang Yajun Address before: 221000 Jiefangnan Road 310-11, Quanshan District, Xuzhou City, Jiangsu Province Patentee before: Xuzhou Zhi Ou mechanical and Electrical Equipment Co., Ltd. |