CN103663441B - 一种固相裂解法制备氮杂石墨烯和纳米金属石墨烯的方法 - Google Patents

一种固相裂解法制备氮杂石墨烯和纳米金属石墨烯的方法 Download PDF

Info

Publication number
CN103663441B
CN103663441B CN201310652296.0A CN201310652296A CN103663441B CN 103663441 B CN103663441 B CN 103663441B CN 201310652296 A CN201310652296 A CN 201310652296A CN 103663441 B CN103663441 B CN 103663441B
Authority
CN
China
Prior art keywords
graphene
degree
cracking
phthalocyanine
raw material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201310652296.0A
Other languages
English (en)
Chinese (zh)
Other versions
CN103663441A (zh
Inventor
薛卫东
赵睿
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SICHUAN HUANTAN TECHNOLOGY CO., LTD.
Original Assignee
SICHUAN HUANTAN TECHNOLOGY Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SICHUAN HUANTAN TECHNOLOGY Co Ltd filed Critical SICHUAN HUANTAN TECHNOLOGY Co Ltd
Priority to CN201310652296.0A priority Critical patent/CN103663441B/zh
Publication of CN103663441A publication Critical patent/CN103663441A/zh
Priority to PCT/CN2014/077420 priority patent/WO2015081663A1/fr
Application granted granted Critical
Publication of CN103663441B publication Critical patent/CN103663441B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/182—Graphene
    • C01B32/184—Preparation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Nanotechnology (AREA)
  • Inorganic Chemistry (AREA)
  • Carbon And Carbon Compounds (AREA)
CN201310652296.0A 2013-12-04 2013-12-04 一种固相裂解法制备氮杂石墨烯和纳米金属石墨烯的方法 Active CN103663441B (zh)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CN201310652296.0A CN103663441B (zh) 2013-12-04 2013-12-04 一种固相裂解法制备氮杂石墨烯和纳米金属石墨烯的方法
PCT/CN2014/077420 WO2015081663A1 (fr) 2013-12-04 2014-05-14 Procédé de préparation d'un graphène aza et d'un métal-graphène nanométrique par utilisation d'un procédé de craquage en phase solide

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310652296.0A CN103663441B (zh) 2013-12-04 2013-12-04 一种固相裂解法制备氮杂石墨烯和纳米金属石墨烯的方法

Publications (2)

Publication Number Publication Date
CN103663441A CN103663441A (zh) 2014-03-26
CN103663441B true CN103663441B (zh) 2016-03-23

Family

ID=50302351

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201310652296.0A Active CN103663441B (zh) 2013-12-04 2013-12-04 一种固相裂解法制备氮杂石墨烯和纳米金属石墨烯的方法

Country Status (2)

Country Link
CN (1) CN103663441B (fr)
WO (1) WO2015081663A1 (fr)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103663441B (zh) * 2013-12-04 2016-03-23 四川环碳科技有限公司 一种固相裂解法制备氮杂石墨烯和纳米金属石墨烯的方法
US10392256B2 (en) * 2014-11-07 2019-08-27 Xuyang SUN Method for preparing graphene by using molten inorganic salt reaction bed
CN104445160B (zh) * 2014-11-07 2017-04-12 孙旭阳 一种熔融态无机盐反应床制备石墨烯的方法
CN104477889A (zh) * 2014-12-03 2015-04-01 连丽君 一种于硅基片上直接生长石墨烯膜的方法
CN104449239A (zh) * 2014-12-18 2015-03-25 四川环碳科技有限公司 一种氮杂石墨烯复合的电磁屏蔽导电底漆及其制备方法
CN104860298B (zh) * 2015-03-25 2018-02-16 孙旭阳 利用熔融态反应床制备石墨烯的方法
CN104777207B (zh) * 2015-04-10 2017-11-28 武汉大学 一种三维氮掺杂石墨烯复合材料及其制备方法和应用
CN104952631B (zh) * 2015-06-15 2017-10-17 四川环碳科技有限公司 采用固相裂解技术制备石墨烯/碳纳米管复合材料的方法
CN105810945A (zh) * 2016-05-26 2016-07-27 江苏深苏电子科技有限公司 锂离子电池负极材料氮掺杂三维多孔石墨烯的制备方法
CN108636438B (zh) * 2018-05-16 2021-10-26 成都理工大学 一种氧氮共掺杂石墨烯光催化剂及其制备方法和应用
CN109786698A (zh) * 2018-12-29 2019-05-21 湖南中科星城石墨有限公司 一种以无机可延展碳材料为壳包覆的核壳结构锂离子电池阴极材料及其制备方法
CN109755519A (zh) * 2018-12-29 2019-05-14 湖南中科星城石墨有限公司 一种以延展性碳材料包覆的锂电池阳极材料及其制备方法
CN111874888B (zh) * 2020-08-06 2021-09-14 电子科技大学 一种微米尺度方块状碳材料的超宽频吸波剂的制备方法
CN114733546A (zh) * 2022-03-28 2022-07-12 云南锡业集团（控股）有限责任公司研发中心 一种氮掺杂的碳负载铟纳米粒子的制备方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101289181A (zh) * 2008-05-29 2008-10-22 中国科学院化学研究所 掺杂石墨烯及其制备方法
CN102134067A (zh) * 2011-04-18 2011-07-27 北京大学 一种制备单层石墨烯的方法
CN102491315A (zh) * 2011-12-08 2012-06-13 中国科学院化学研究所 制备石墨烯的方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101285175B (zh) * 2008-05-29 2010-07-21 中国科学院化学研究所 化学气相沉积法制备石墨烯的方法
CN102092710B (zh) * 2010-12-17 2013-01-23 中国科学院化学研究所 一种规则石墨烯及其制备方法
CN102229426B (zh) * 2011-05-25 2012-12-05 中国科学院化学研究所 一种单层、有序排布的等角六边形石墨烯的制备方法
CN102344131B (zh) * 2011-07-06 2013-03-20 中国科学院上海微系统与信息技术研究所 一种在钼基衬底上制备石墨烯薄膜的方法
CN103663441B (zh) * 2013-12-04 2016-03-23 四川环碳科技有限公司 一种固相裂解法制备氮杂石墨烯和纳米金属石墨烯的方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101289181A (zh) * 2008-05-29 2008-10-22 中国科学院化学研究所 掺杂石墨烯及其制备方法
CN102134067A (zh) * 2011-04-18 2011-07-27 北京大学 一种制备单层石墨烯的方法
CN102491315A (zh) * 2011-12-08 2012-06-13 中国科学院化学研究所 制备石墨烯的方法

Also Published As

Publication number Publication date
WO2015081663A1 (fr) 2015-06-11
CN103663441A (zh) 2014-03-26

Similar Documents

Publication Publication Date Title
CN103663441B (zh) 一种固相裂解法制备氮杂石墨烯和纳米金属石墨烯的方法
Liu et al. Intermediate-mediated strategy to horn-like hollow mesoporous ultrathin g-C3N4 tube with spatial anisotropic charge separation for superior photocatalytic H2 evolution
Kumar et al. A review on the current research on microwave processing techniques applied to graphene-based supercapacitor electrodes: An emerging approach beyond conventional heating
Chen et al. NiS and graphene as dual cocatalysts for the enhanced photocatalytic H2 production activity of g-C3N4
Yadav et al. Synthesis, characterization and prospective applications of nitrogen-doped graphene: A short review
Li et al. Templateless infrared heating process for fabricating carbon nitride nanorods with efficient photocatalytic H2 evolution
Cai et al. 3D graphene/ZnO composite with enhanced photocatalytic activity
Kong et al. Bridging the gap between reality and ideality of graphdiyne: the advances of synthetic methodology
Cheng et al. Facile synthesis of g-C3N4/BiVO4 heterojunctions with enhanced visible light photocatalytic performance
Qi et al. Ionic liquid-assisted synthesis of porous boron-doped graphitic carbon nitride for photocatalytic hydrogen production
CN104445160B (zh) 一种熔融态无机盐反应床制备石墨烯的方法
Luo et al. Preparation of 3D reticulated ZnO/CNF/NiO heteroarchitecture for high-performance photocatalysis
CN102176338B (zh) 一种石墨烯/铜纳米线复合导电材料与制备方法
Guan et al. Synthesis of sulfur doped g-C3N4 with enhanced photocatalytic activity in molten salt
Liu et al. Enhancement of heterogeneous photo-Fenton performance of core-shell structured boron-doped reduced graphene oxide wrapped magnetical Fe3O4 nanoparticles: Fe (II)/Fe (III) redox and mechanism
Zheng et al. A new carbon allotrope: graphdiyne
Wang et al. Preparation of Cu modified g-C3N4 nanorod bundles for efficiently photocatalytic CO2 reduction
CN103949234B (zh) 硼掺杂石墨烯/TiO2纳米棒光催化材料的制备方法
CN102225757B (zh) 一种石墨炔纳米薄膜及其制备方法
EP3216757B1 (fr) Procédé de préparation de graphène dans un lit réactionnel de sel inorganique à l'état fondu
CN103303912A (zh) 一种高比表面积多孔氮掺杂石墨化纳米碳材料的制备方法
CN107376976A (zh) 一种氧化铈/石墨烯量子点/类石墨烯相氮化碳复合光催化材料的制备方法
CN102320597B (zh) 一种石墨烯的制备方法
Cai et al. A green and facile route for constructing flower-shaped TiO2 nanocrystals assembled on graphene oxide sheets for enhanced photocatalytic activity
Jiao et al. Sulfur/phosphorus doping-mediated morphology transformation of carbon nitride from rods to porous microtubes with superior photocatalytic activity

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
ASS Succession or assignment of patent right

Free format text: FORMER OWNER: ZHAO RUI

Effective date: 20140425

Owner name: SICHUAN HUANTAN TECHNOLOGY CO., LTD.

Free format text: FORMER OWNER: XUE WEIDONG

Effective date: 20140425

C41 Transfer of patent application or patent right or utility model
COR Change of bibliographic data

Free format text: CORRECT: ADDRESS; FROM: 610212 CHENGDU, SICHUAN PROVINCE TO: 610000 CHENGDU, SICHUAN PROVINCE

TA01 Transfer of patent application right

Effective date of registration: 20140425

Address after: High tech Zone Gaopeng road in Chengdu city of Sichuan province 610000 5 Building No. 2 No. 102

Applicant after: SICHUAN HUANTAN TECHNOLOGY CO., LTD.

Address before: 610212, No. 90, middle and high road, hi tech Zone, Sichuan, Chengdu

Applicant before: Xue Weidong

Applicant before: Zhao Rui

C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant