CN103610821A - Production method of longan seed extract oral liquid - Google Patents

Production method of longan seed extract oral liquid Download PDF

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Publication number
CN103610821A
CN103610821A CN201310620682.1A CN201310620682A CN103610821A CN 103610821 A CN103610821 A CN 103610821A CN 201310620682 A CN201310620682 A CN 201310620682A CN 103610821 A CN103610821 A CN 103610821A
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CN
China
Prior art keywords
seed
arillus longan
oral liquid
extract oral
seed extract
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Pending
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CN201310620682.1A
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Chinese (zh)
Inventor
邹步珍
龙泽云
钟旭倩
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NANNING BAIJI BIOENGINEERING CO Ltd
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NANNING BAIJI BIOENGINEERING CO Ltd
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Priority to CN201310620682.1A priority Critical patent/CN103610821A/en
Publication of CN103610821A publication Critical patent/CN103610821A/en
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/70Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in livestock or poultry

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Abstract

The invention discloses a production method of a longan seed extract oral liquid and a use method thereof. By taking longan seeds as main raw materials, the production method comprises the following steps: cleaning, drying and crushing the longan seeds to 40-60 meshes; adding pure water or an alcohol and water mixture and carrying out ultrasonic extraction, clarification, filtration and concentration; adding 0.1-0.3% sodium benzoate; and carrying out technical processes such as sterilization, packaging and the like to obtain the longan seed extract oral liquid. Drinking water for poultry and the longan seed extract oral liquid are uniformly mixed and stirred according to a proportion of adding 50-200ml of the longan seed extract oral liquid into the drinking water for poultry to drink. The longan seed extract oral liquid contains abundant amino acids, proteins, vitamins and antibacterial substances, and can be used for preventing and treating diseases of various livestock, and particularly non-reactive pig production. The oral liquid is remarkable in disease preventing and treating effects, simple in preparation process, energy- and time-saving and easy to realize industrialized production.

Description

A kind of production method of seed of Arillus Longan extract oral liquid
Technical field
The present invention relates to a kind of production method of seed of Arillus Longan extract oral liquid, especially take natural agricultural byproducts seed of Arillus Longan as main poultry extract oral liquid production method and using method thereof.
Background technology
Its mildly bitter flavor of seed of Arillus Longan, puckery is flat; Interior for stomachache, colicky; External controls traumatic hemorrhage, hemorrhage etc. for hemostasis and pain-relieving, burn and scald, knife injury.Seed of Arillus Longan is the seed of sapindaceous plant Arillus Longan.Core is containing saporin and fat.Seed is containing three seed amino acids: 2-amino-4-methyl-5--acetylenic acid (2-amino-4 methyl hex-5-ynoic acid), 2-amino-4-methylol-5-hexynic acid (2-amino-4-hydroxymethyl hex-5-ynoic acid) and 2-amino-4-hydroxy-6-heptynoic acid (2-amino-4-hydroxy hept-6-ynoic acid).In seed oil, contain dihydrosterculic acid (dihydroxterculic acids).
At present, the research of the extraction aspect of seed of Arillus Longan is as patent CN201210570380.3, and a kind of extracting method of seed of Arillus Longan polyphenol, dries clean seed of Arillus Longan; Raw material seed of Arillus Longan is pulverized, obtained seed of Arillus Longan powder; In seed of Arillus Longan powder, add sodium phosphate buffer, obtain leachate; Leachate is inclined to, filter, remove and soak slag, reclaim immersion; The filtrate obtaining is concentrated, obtain concentrated solution; In concentrated solution, add hydrochloric acid, after stirring, staticly settle, obtain precipitated liquid; Precipitated liquid is centrifugal, abandoning supernatant, precipitation, with after salt acid elution, is dried to seed of Arillus Longan polyphenol fine powder.
Patent CN201210426447.6, a kind of oral liquid for the treatment of poultry respiratory tract diseases and preparation method thereof, discloses a kind of oral liquid for the treatment of poultry respiratory tract diseases and preparation method thereof.Crude drug by following mass fraction is made: 10 ~ 40 parts, Herba Ephedrae, 100 ~ 200 parts, Gypsum Fibrosum, 10 ~ 50 parts of Semen Lepidii (Semen Descurainiae)s, 15 ~ 55 parts of Radix Scutellariaes, 25 ~ 65 parts, Semen Armeniacae Amarum, 15 ~ 45 parts of Pericarpium Citri Reticulataes, 15 ~ 45 parts of Radix Platycodoniss, 25 ~ 75 parts, Radix Glycyrrhizae.First Semen Armeniacae Amarum is squeezed out to fatty oil and leave and take recipe quantity, the Semen Armeniacae Amarum medicine cake again squeezing being deoiled and the surplus stock medicine of recipe quantity, twice of decocting, collect the distillate while decocting for the first time, merge filtrate twice, when concentrated filtrate to every 1 parts by volume medicinal liquid is equivalent to crude drug in whole 1.7 ~ 2.3 mass parts, let cool, adding ethanol is 60 ~ 70% to containing alcohol amount, stir evenly, standing rear filtration, be evaporated to extractum shape, with 500 ~ 600 parts by volume water dilutions, cold preservation, filter, add distillate, antiseptic, add water to again 1200 parts by volume, cold preservation, filter, encapsulation, sterilizing obtains oral liquid.
Seed of Arillus Longan is made to relevant poultry oral liquid, there are no relevant report; And existing disclosed poultry by the problem that oral liquid exists is: 1, fail to make full use of the large agricultural product seed of Arillus Longan of Guangxi real estate, wasted valuable crop resource; 2, main component is used the product of chemical element or processing of crude drugs, and Financial cost is high, and product curative effect is not remarkable.
Summary of the invention
The object of the invention is to the deficiency existing with oral liquid for poultry in prior art, provide a kind of and take natural agricultural byproducts seed of Arillus Longan as main poultry extract oral liquid production method and using method thereof, this additive improved agricultural byproducts value, reduced production cost, energy savings, reduce oral liquid taking medical material.
To achieve these goals, the present invention has adopted following technical scheme:
A production method for seed of Arillus Longan extract oral liquid, method step comprises: a. pulverizes dry seed of Arillus Longan raw material, then crosses 40-60 mesh sieve, obtains seed of Arillus Longan powder; B. the seed of Arillus Longan powder after pulverizing and sieving is put into tank, add the extractant of 5~10 times of seed of Arillus Longan powder raw material weight, be uniformly mixed and obtain seed of Arillus Longan serosity; C. use ultrasound wave to extract 20~120 minutes seed of Arillus Longan serosity, standing extracting solution 10-30 minute clarifies rear filtration again, in filtrate, add 0.1-0.3% sodium benzoate, filtrate obtains seed of Arillus Longan extract oral liquid with membrance concentration to 10~50% rear sterilizings of virgin pulp liquid.
As further restriction of the present invention: described extractant is any in ultra-pure water, 40 ~ 100% ethanol waters, 50 ~ 100% methanol aqueous solutions.
A using method for above-mentioned seed of Arillus Longan extract oral liquid, in the ratio that adds 50 ~ 200ml seed of Arillus Longan extract oral liquid in every liter of fowl drinking water, quotes water and seed of Arillus Longan extract oral liquid mixing and stirring by poultry, can be used for poultry and feeds drink.
Advantage of the present invention: seed of Arillus Longan extract oral liquid contains abundant aminoacid, protein, vitamin and antibiotic substance, can be used for all kinds of domestic animals prevents and cures diseases, especially for nonreactive, raise pigs, diseases prevention and treatment effect is remarkable, manufacturing process is simple, energy savings and time, be easy to realize suitability for industrialized production.
The specific embodiment
Below in conjunction with embodiment, the present invention is further described, but protection scope of the present invention is not limited to these embodiment.
Embodiment 1:
Get dry seed of Arillus Longan 1kg, the preparation method of seed of Arillus Longan extract oral liquid is as follows:
A. dry seed of Arillus Longan raw material is pulverized, then crossed 60 mesh sieves, obtain seed of Arillus Longan powder; B. the seed of Arillus Longan powder after pulverizing and sieving is put into tank, add the extractant ultra-pure water of 5 times of seed of Arillus Longan powder raw material weight, be uniformly mixed and obtain seed of Arillus Longan serosity; C. use ultrasound wave to extract 50 minutes seed of Arillus Longan serosity, more standing extracting solution clarifies rear filtration in 20 minutes, add 0.15% sodium benzoate in filtrate, filtrate obtains seed of Arillus Longan extract oral liquid with membrance concentration to 50% rear sterilizing of virgin pulp liquid.
Embodiment 2:
Get dry seed of Arillus Longan 1kg, the preparation method of seed of Arillus Longan extract oral liquid is as follows:
A. dry seed of Arillus Longan raw material is pulverized, then crossed 40 mesh sieves, obtain seed of Arillus Longan powder; B. the seed of Arillus Longan powder after pulverizing and sieving is put into tank, add extractant 40% ethanol water of 10 times of seed of Arillus Longan powder raw material weight, be uniformly mixed and obtain seed of Arillus Longan serosity; C. use ultrasound wave to extract 120 minutes seed of Arillus Longan serosity, more standing extracting solution clarifies rear filtration in 30 minutes, add 0.3% sodium benzoate in filtrate, filtrate obtains seed of Arillus Longan extract oral liquid with membrance concentration to 20% rear sterilizing of virgin pulp liquid.
Embodiment 3:
Get dry seed of Arillus Longan 1kg, the preparation method of seed of Arillus Longan extract oral liquid is as follows:
A. dry seed of Arillus Longan raw material is pulverized, then crossed 50 mesh sieves, obtain seed of Arillus Longan powder; B. the seed of Arillus Longan powder after pulverizing and sieving is put into tank, add extractant 50% methanol aqueous solution of 8 times of seed of Arillus Longan powder raw material weight, be uniformly mixed and obtain seed of Arillus Longan serosity; C. use ultrasound wave to extract 20 minutes seed of Arillus Longan serosity, more standing extracting solution clarifies rear filtration in 10 minutes, add 0.1% sodium benzoate in filtrate, filtrate obtains seed of Arillus Longan extract oral liquid with membrance concentration to 10% rear sterilizing of virgin pulp liquid.
Embodiment 4:
Get dry seed of Arillus Longan 1kg, the preparation method of seed of Arillus Longan extract oral liquid is as follows:
A. dry seed of Arillus Longan raw material is pulverized, then crossed 40 mesh sieves, obtain seed of Arillus Longan powder; B. the seed of Arillus Longan powder after pulverizing and sieving is put into tank, add extractant 100% ethanol water of 10 times of seed of Arillus Longan powder raw material weight, be uniformly mixed and obtain seed of Arillus Longan serosity; C. use ultrasound wave to extract 70 minutes seed of Arillus Longan serosity, more standing extracting solution clarifies rear filtration in 15 minutes, add 0.2% sodium benzoate in filtrate, filtrate obtains seed of Arillus Longan extract oral liquid with membrance concentration to 30% rear sterilizing of virgin pulp liquid.
Embodiment 5:
Get dry seed of Arillus Longan 1kg, the preparation method of seed of Arillus Longan extract oral liquid is as follows:
A. dry seed of Arillus Longan raw material is pulverized, then crossed 60 mesh sieves, obtain seed of Arillus Longan powder; B. the seed of Arillus Longan powder after pulverizing and sieving is put into tank, add the extractant methanol aqueous solution of 5 times of seed of Arillus Longan powder raw material weight, be uniformly mixed and obtain seed of Arillus Longan serosity; C. use ultrasound wave to extract 60 minutes seed of Arillus Longan serosity, more standing extracting solution clarifies rear filtration in 20 minutes, add 0.25% sodium benzoate in filtrate, filtrate obtains seed of Arillus Longan extract oral liquid with membrance concentration to 40% rear sterilizing of virgin pulp liquid.
Application example: in August, 2012 Nanning City's Wuming County plant
This pig farm is individual plant, has 50 of sows, 240 of small weaning pigs.This pig farm small weaning pig various diseases is more before this, and particularly little diarrhea of pigs is more serious.It is object that 50 small weaning pigs are take in experiment, is divided into two groups of experimental group and matched groups, high spot reviews diarrhea rate and weightening finish.The ratio that adds 50 ~ 200ml seed of Arillus Longan extract oral liquid in every liter of fowl drinking water of experimental group, poultry is quoted to water and seed of Arillus Longan extract oral liquid mixing and stirring, can be used for feeding to small weaning pig, feed to 20 days continuously, matched group, according to daily management and forage feed, does not add Arillus Longan extract in drinking water.When experiment finishes, experimental group diarrhea rate on average reduces by 13.5% than matched group, and body weight increases by 5.5%, and effect is remarkable.

Claims (3)

1. a production method for seed of Arillus Longan extract oral liquid, is characterized in that:
A. dry seed of Arillus Longan raw material is pulverized, then crossed 40-60 mesh sieve, obtain seed of Arillus Longan powder;
B. the seed of Arillus Longan powder after pulverizing and sieving is put into tank, add the extractant of 5~10 times of seed of Arillus Longan powder raw material weight, be uniformly mixed and obtain seed of Arillus Longan serosity;
C. use ultrasound wave to extract 20~120 minutes seed of Arillus Longan serosity, standing extracting solution 10-30 minute clarifies rear filtration again, in filtrate, add 0.1-0.3% sodium benzoate, filtrate obtains seed of Arillus Longan extract oral liquid with membrance concentration to 10~50% rear sterilizings of virgin pulp liquid.
2. the production method of seed of Arillus Longan extract oral liquid according to claim 1, is characterized in that: described extractant is any in ultra-pure water, 40 ~ 100% ethanol waters, 50 ~ 100% methanol aqueous solutions.
3. the using method of the seed of Arillus Longan extract oral liquid as described in as arbitrary in claim 1-2, it is characterized in that: in the ratio that adds 50 ~ 200ml seed of Arillus Longan extract oral liquid in every liter of fowl drinking water, poultry is quoted to water and seed of Arillus Longan extract oral liquid mixing and stirring, can be used for poultry and feed drink.
CN201310620682.1A 2013-11-29 2013-11-29 Production method of longan seed extract oral liquid Pending CN103610821A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103948805A (en) * 2014-05-19 2014-07-30 韦江南 Traditional Chinese medicinal preparation for treating stomachache
CN104288313A (en) * 2014-10-31 2015-01-21 于芳 Method for extracting flavone from longan seeds
CN104383078A (en) * 2014-12-15 2015-03-04 天津商业大学 Compound longan seed oral liquid, and preparation method and application thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101744928A (en) * 2008-12-12 2010-06-23 黄驰波 Method for extracting active substance in longan seeds
CN102920830A (en) * 2012-11-28 2013-02-13 华南师范大学 Method for effectively extracting polyphenol from Longan seed
CN102961486A (en) * 2012-12-24 2013-03-13 厦门大学 Extraction method of longan seed polyphenol

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101744928A (en) * 2008-12-12 2010-06-23 黄驰波 Method for extracting active substance in longan seeds
CN102920830A (en) * 2012-11-28 2013-02-13 华南师范大学 Method for effectively extracting polyphenol from Longan seed
CN102961486A (en) * 2012-12-24 2013-03-13 厦门大学 Extraction method of longan seed polyphenol

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103948805A (en) * 2014-05-19 2014-07-30 韦江南 Traditional Chinese medicinal preparation for treating stomachache
CN104288313A (en) * 2014-10-31 2015-01-21 于芳 Method for extracting flavone from longan seeds
CN104383078A (en) * 2014-12-15 2015-03-04 天津商业大学 Compound longan seed oral liquid, and preparation method and application thereof

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Application publication date: 20140305