CN103583573B - Crop growth accelerant and preparation method thereof - Google Patents
Crop growth accelerant and preparation method thereof Download PDFInfo
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- CN103583573B CN103583573B CN201310576846.5A CN201310576846A CN103583573B CN 103583573 B CN103583573 B CN 103583573B CN 201310576846 A CN201310576846 A CN 201310576846A CN 103583573 B CN103583573 B CN 103583573B
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Abstract
The invention provides a crop growth accelerant suitable for a water and fertilizer integration system and a preparation method of the crop growth accelerant. The crop growth accelerant is mainly prepared from potassium tripolyphosphate, glycosaminoglycan, maltose oligosaccharide, ammonium tartrate, indole-3-butyric acid potassium, methyl alcohol and water. The crop growth accelerant provided by the invention is water soluble liquid, can be directly applied in a drop irrigation system, a spray irrigation system or a microspray irrigation system, is added into water according to certain proportion, and is applied to the crop along with the system. The crop growth accelerant takes the methyl alcohol as a solvent and substances like potassium tripolyphosphate as an organic solute, and the crop growth accelerant suitable for the water and fertilizer integration system is prepared through the steps of pH regulating, heating and the like. Tests show that the crop growth accelerant has an excellent accelerating effect on the crop growth, the root activity is improved, the utilization ratio of water and fertilizer and the crop yield are remarkably increased, and secondary pollution is avoided.
Description
Technical field
The invention belongs to technical field of agriculture science, be specifically related to a kind of crop growth accelerant, Preparation Method And The Use.
Background technology
The chemical fertilizer utilization ratio of China is general lower, and nitrogenous fertilizer average utilization is about 30%, and phosphate fertilizer this season availability is about 25%, and potassium utilization rate is about 50%, and China is the country of a water resource famine simultaneously.The scientific worker of China has carried out large quantity research to the methods improving water and fertilizer utilization, achieves good effect.Particularly in recent years, along with the deep development of land transformation, Labor Transfer, agriculture industrialization, the Ministry of Agriculture widelys popularize the Integration of Water into Fertilizer, has promoted the raising of water and utilization rate of fertilizer, save labour and production cost, and promote the raising of China's crop yield.But; only rely on water and fertilizer to use and still can not reach best effect of increasing production; also need the productive potential fully excavating and play crop itself; namely crop growth accelerant is the production capacity that can promote crop itself; realize moisture, nutrient supply is coordinated mutually with plant growth; not only can improve crop yield, also can increase substantially liquid manure utilization ratio, protection of the environment.
Abroad, particularly the water soluble fertilizer effect of Israel, Norway is very outstanding, its technological core is just the use of crop growth accelerant, the second largest Agro-chemistry service company HELENA of Japanese MARUBENI, Zhong Hua company, the U.S. all has a large amount of crop growth accelerant technology, but need information disclosure because enterprise applies for a patent, enterprise scarcely applies for a patent, and only uses these technology in inside.The research and development of China to crop growth accelerant are still in the starting stage, with the development of the intensive management on land transformation and farm, water-fertilizer integral is inexorable trend, crop growth accelerant will be used widely safely and efficiently, but the crop growth accelerant also not matching with the Integration of Water into Fertilizer, be connected mutually in the market.
Summary of the invention
The object of this invention is to provide and be a kind ofly applicable to crop growth accelerant of water-fertilizer integral system and preparation method thereof.
Crop growth accelerant of the present invention, is prepared from by weight the ratio of 10:1-5:2-4:5-10:2-4:5-16.5:50-82.5 primarily of PTPP, glycosaminoglycan, oligomeric maltose, ammonium tartrate, butyric acid potassium, first alcohol and water.
Preferably, crop growth accelerant of the present invention, is prepared from by weight the ratio of 10:2-4:2.5-3.5:6-8:2.5-3.5:7-12:60-75 primarily of PTPP, glycosaminoglycan, oligomeric maltose, ammonium tartrate, butyric acid potassium, first alcohol and water.
Preferred, crop growth accelerant of the present invention, is prepared from by weight the ratio of 10:3:3:7:3:8-10:65-70 primarily of PTPP, glycosaminoglycan, oligomeric maltose, ammonium tartrate, butyric acid potassium, first alcohol and water.
The preparation method of crop growth accelerant of the present invention, mainly comprises the steps:
The preparation of A, solvent: compound concentration is the methanol aqueous solution of 10%-20%;
The preparation of B, organic solute: get PTPP, glycosaminoglycan, oligomeric maltose, ammonium tartrate and butyric acid potassium in proportion, after mixing, obtains organic solute;
The preparation of C, crop growth accelerant: solvent described in 100 weight portion steps A is joined in reactor, organic solute described in the step B slowly adding 20-33 weight portion while stirring, after continuous stirring 10-15min, be that the inorganic acid of 0.5%-1% or inorganic base regulate pH to be 6-8 by concentration, continue to stir 5-10min, then after being slowly heated to 50 DEG C-60 DEG C while stirring, continue 1-3 hour, then the liquid reactor is released from discharge port, to be cooled to room temperature, obtain described crop growth accelerant.
Preferably, described inorganic acid is selected from the one in hydrochloric acid, sulfuric acid, nitric acid, phosphoric acid.
Preferably, described inorganic base is selected from the one in sodium hydroxide, potassium hydroxide, sodium carbonate, potash, saleratus, sodium bicarbonate.
Present invention also offers the application of described crop growth accelerant in water-fertilizer integral system.
According to above-mentioned application, in described crop growth accelerant and water-fertilizer integral system, the part by weight of water is 0.5-1:1000.
Crop growth accelerant of the present invention is water-soluble liquid, can directly apply in drip irrigation and spray irrigation, micro-sprinkler irrigation system, add to by a certain percentage in water, with systemic application in crop, during use, in this crop growth accelerant and system, the part by weight of water is 0.5-1:1000, and before using, this crop growth accelerant should seal preservation.
The present invention is solvent with methanol solution, with materials such as PTPPs for organic solute, is applicable to the crop growth accelerant of water-fertilizer integral system through step preparations such as pH adjustment and heating.Production process is without the need to special solvent, and temperature required gentleness, energy consumption is low, good stability, safety and environmental protection.Test shows, crop growth accelerant of the present invention has good facilitation to plant growth, can improve improving activity of root system, significantly improves water and fertilizer utilization and crop yield, avoids secondary pollution.
Embodiment
The present invention can be understood better by following embodiment and test example.
embodiment 1
Implementation step is as follows:
The preparation of A, solvent
Compound concentration is the methanol aqueous solution of 10%.
The preparation of B, organic solute
After PTPP, glycosaminoglycan, oligomeric maltose, ammonium tartrate and butyric acid potassium being mixed by weight the ratio of 10:1:2:5:2, obtain organic solute.
The preparation of C, crop growth accelerant
Solvent prepared by 100 weight portion steps A is joined in reactor, slowly add the organic solute of 20 weight portions while stirring, after continuous stirring 10min, be 6 with the sulphur acid for adjusting pH that concentration is 0.5%, continue to stir 5min, after being then slowly heated to 50 DEG C while stirring, continue 1 hour, then the liquid reactor is released from discharge port, to be cooled to room temperature, obtain described crop growth accelerant.
embodiment 2
Implementation step is as follows:
The preparation of A, solvent
Compound concentration is the methanol aqueous solution of 20%.
The preparation of B, organic solute
After PTPP, glycosaminoglycan, oligomeric maltose, ammonium tartrate and butyric acid potassium being mixed by weight the ratio of 10:5:4:10:4, obtain organic solute.
The preparation of C, crop growth accelerant
Solvent prepared by 100 weight portion steps A is joined in reactor, slowly add the organic solute of 33 weight portions while stirring, after continuous stirring 15min, regulate pH to be 8 with the sodium hydroxide that concentration is 1%, continue to stir 10min, after being then slowly heated to 60 DEG C while stirring, continue 3 hours, then the liquid reactor is released from discharge port, to be cooled to room temperature, obtain described crop growth accelerant.
embodiment 3
Implementation step is as follows:
The preparation of A, solvent
Compound concentration is the methanol aqueous solution of 12%.
The preparation of B, organic solute
After PTPP, glycosaminoglycan, oligomeric maltose, ammonium tartrate and butyric acid potassium being mixed by weight the ratio of 10:2:2.5:6:2.5, obtain organic solute.
The preparation of C, crop growth accelerant
Solvent prepared by 100 weight portion steps A is joined in reactor, slowly add the organic solute of 25 weight portions while stirring, after continuous stirring 12min, be 6.5 with the salt acid for adjusting pH that concentration is 0.6%, continue to stir 6min, after being then slowly heated to 52 DEG C while stirring, continue 1.5 hours, then the liquid reactor is released from discharge port, to be cooled to room temperature, obtain described crop growth accelerant.
embodiment 4
Implementation step is as follows:
The preparation of A, solvent
Compound concentration is the methanol aqueous solution of 18%.
The preparation of B, organic solute
After PTPP, glycosaminoglycan, oligomeric maltose, ammonium tartrate and butyric acid potassium being mixed by weight the ratio of 10:4:3.5:8:3.5, obtain organic solute.
The preparation of C, crop growth accelerant
Solvent prepared by 100 weight portion steps A is joined in reactor, slowly add the organic solute of 30 weight portions while stirring, after continuous stirring 14min, regulate pH to be 7.5 with the potassium hydroxide that concentration is 0.8%, continue to stir 8min, after being then slowly heated to 58 DEG C while stirring, continue 2.5 hours, then the liquid reactor is released from discharge port, to be cooled to room temperature, obtain described crop growth accelerant.
embodiment 5
Implementation step is as follows:
The preparation of A, solvent
Compound concentration is the methanol aqueous solution of 15%.
The preparation of B, organic solute
After PTPP, glycosaminoglycan, oligomeric maltose, ammonium tartrate and butyric acid potassium being mixed by weight the ratio of 10:3:3:7:3, obtain organic solute.
The preparation of C, crop growth accelerant
Solvent prepared by 100 weight portion steps A is joined in reactor, slowly add the organic solute of 28 weight portions while stirring, after continuous stirring 13min, be 6.8 with the phosphorus acid for adjusting pH that concentration is 0.75%, continue to stir 7.5min, after being then slowly heated to 55 DEG C while stirring, continue 2 hours, then the liquid reactor is released from discharge port, to be cooled to room temperature, obtain described crop growth accelerant.
embodiment 6
Implementation step is as follows:
The preparation of A, solvent
Compound concentration is the methanol aqueous solution of 17.5%.
The preparation of B, organic solute
After PTPP, glycosaminoglycan, oligomeric maltose, ammonium tartrate and butyric acid potassium being mixed by weight the ratio of 10:3.5:2.8:8.5:3.8, obtain organic solute.
The preparation of C, crop growth accelerant
Solvent prepared by 100 weight portion steps A is joined in reactor, slowly add the organic solute of 29.5 weight portions while stirring, after continuous stirring 13.5min, regulate pH to be 7.9 with the potash that concentration is 0.85%, continue to stir 9min, after being then slowly heated to 59 DEG C while stirring, continue 2.6 hours, then the liquid reactor is released from discharge port, to be cooled to room temperature, obtain described crop growth accelerant.
test example 1:crop growth accelerant of the present invention is on the impact of Maize Seedling improving activity of root system
Sand culture test is utilized to study the impact of described crop growth accelerant on Seedling Root Systems In Maize vigor.Routine control (CK) and crop growth accelerant of the present invention (C-1, C-2, C-3) 4 process are established in test, and C-1, C-2, C-3 are the crop growth accelerant being applicable to water-fertilizer integral system prepared by embodiment 1,2,3 respectively, repeat 6 times.First quartz sand clear water is cleaned, put into stainless steel pallet, keep certain humidity, corn kernel is put into dish, cover on it with wet cloth, under the condition of temperature 25 DEG C, carry out nursery.When corn sprout grow to 3-5cm time, by corn take out put into the cultivation cup filling with quartz sand, water every day concentration be 0.2% crop growth accelerant 25 mL or CK water 25 mL water.When corn grows to about 20 cm, take out root system, clean with clear water, and employing TTC method (bibliography: Zhang Xiong. vigor and the application [J] thereof of wheat root and pollen is measured by " TTC " method (red tetrazolium), Plant Physiology Communications, phase nineteen eighty-two the 3rd.) measure the improving activity of root system of corn.
Its result of the test is listed in the table below in 1.
Table 1: Root Activity in Maize (mg/gh, TTC method)
Process | Improving activity of root system |
CK | 0.942 |
C-1 | 1.330 |
C-2 | 1.374 |
C-3 | 1.351 |
Above-mentioned result of the test shows, compared with Routine control, crop growth accelerant of the present invention can significantly improve the improving activity of root system of Maize Seedling, and C-1, C-2, C-3 exceed 41.2%, 45.8% and 43.4% than contrast respectively.
test example 2: add the impact of described crop growth accelerant on corn yield and yield component
Test arranges 4 process (process 1: conventional Capsicum yield; Process 2: conventional liquid manure+C-1; Process 3: conventional liquid manure+C-2; Process 4: conventional liquid manure+C-3.The ratio of crop growth accelerant and irrigation amount is 1:1500), plot area 50m
2.Each process irrigation quantity is 3.6 tons/community, and fertilizing amount is 12kgN, 4kgP
2o
5, 8kgK
2o, fertilizer variety is urea, diammonium phosphate and potassium chloride.Each process is microspray irrigation (oblique 5 holes), and water and fertilizer use 50% respectively at Maize at Seedling Stage and typhon mouth phase.
Table 2: corn yield and constituent element
Process | Grain yield (kg/ mu) | Grain number per spike | 100-grain weight (g) |
CK | 522.4 | 338 | 18.60 |
Process 1 | 578.6 | 252 | 18.84 |
Process 2 | 610.1 | 277 | 19.05 |
Process 3 | 591.7 | 263 | 18.82 |
Above-mentioned result of the test: compared with conventional treatment, using crop growth accelerant of the present invention significantly can increase the grain number per spike of corn, 100-grain weight and grain yield.The corn yield of process 1,2,3 comparatively contrasts increase by 10.8%, 16.8% and 13.3% respectively.
test example 3: add the impact of described crop growth accelerant on Ginger Yield
This test is carried out in Qingzhou City Dong Xia town, and test arranges 4 process (process 1: conventional Capsicum yield; Process 2: conventional liquid manure+C-1; Process 3: conventional liquid manure+C-2; Process 4: conventional liquid manure+C-3.The ratio of crop growth accelerant and irrigation amount is 1:1000), each process 3 row (line width: 0.75m × row is long: 20 meters) ginger, repeats 3 times.The irrigation quantity of often going is 1 ton/time, and liquid manure is together used, and uses 3 times altogether, and each fertilizing amount is 8kgN, 4kgP
2o
5, 4kgK
2o, fertilizer variety is urea, diammonium phosphate and potassium chloride.
Table 3 crop growth accelerant is on the impact of Ginger Yield
Process | Output (kg/ mu) |
CK | 8047 |
Process 1 | 10190 |
Process 2 | 11508 |
Process 3 | 10924 |
Compared with conventional treatment, use the output that crop growth accelerant of the present invention significantly can increase ginger.The Ginger Yield of process 1,2,3 comparatively contrasts increase by 26.6%, 43.0% and 35.8% respectively.
As can be seen here, when fertilizer amount is identical, applying crop growth accelerant of the present invention can significantly increase maize grain yield and Ginger Yield.
Claims (8)
1. a crop growth accelerant, it is characterized in that, be prepared from by weight the ratio of 10:1-5:2-4:5-10:2-4:5-16.5:50-82.5 primarily of PTPP, glycosaminoglycan, oligomeric maltose, ammonium tartrate, butyric acid potassium, first alcohol and water.
2. crop growth accelerant as claimed in claim 1, it is characterized in that, be prepared from by weight the ratio of 10:2-4:2.5-3.5:6-8:2.5-3.5:7-12:60-75 primarily of PTPP, glycosaminoglycan, oligomeric maltose, ammonium tartrate, butyric acid potassium, first alcohol and water.
3. crop growth accelerant as claimed in claim 2, is characterized in that, is prepared from by weight the ratio of 10:3:3:7:3:8-10:65-70 primarily of PTPP, glycosaminoglycan, oligomeric maltose, ammonium tartrate, butyric acid potassium, first alcohol and water.
4. the preparation method of crop growth accelerant as described in any one of claim 1-3, is characterized in that, mainly comprise the steps:
The preparation of A, solvent: compound concentration is the methanol aqueous solution of 10%-20%;
The preparation of B, organic solute: get PTPP, glycosaminoglycan, oligomeric maltose, ammonium tartrate and butyric acid potassium in proportion, after mixing, obtains organic solute;
The preparation of C, crop growth accelerant: solvent described in steps A is joined in reactor, slowly add organic solute described in step B while stirring, after continuous stirring 10-15min, be that the inorganic acid of 0.5%-1% or inorganic base regulate pH to be 6-8 by concentration, continue to stir 5-10min, after being then slowly heated to 50 DEG C-60 DEG C while stirring, continue 1-3 hour, then the liquid reactor is released from discharge port, to be cooled to room temperature, obtain described crop growth accelerant.
5. the preparation method of crop growth accelerant as claimed in claim 4, it is characterized in that, described inorganic acid is selected from the one in hydrochloric acid, sulfuric acid, nitric acid, phosphoric acid.
6. the preparation method of crop growth accelerant as claimed in claim 4, it is characterized in that, described inorganic base is selected from the one in sodium hydroxide, potassium hydroxide, sodium carbonate, potash, saleratus, sodium bicarbonate.
7. the application of crop growth accelerant in water-fertilizer integral system as described in any one of claim 1-3.
8. apply as claimed in claim 7, it is characterized in that, in described crop growth accelerant and water-fertilizer integral system, the part by weight of water is 0.5-1:1000.
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CN107324878A (en) * | 2017-07-07 | 2017-11-07 | 安徽誉秀农业科技有限公司 | A kind of crop growth accelerant |
CN109169588A (en) * | 2018-08-28 | 2019-01-11 | 倪晓燕 | A kind of promotion crop growthing development method |
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CN102919247A (en) * | 2012-10-31 | 2013-02-13 | 四川国光农化股份有限公司 | Plant growth adjustment composition containing 6-benayl aminopurine |
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CN102850141A (en) * | 2012-10-19 | 2013-01-02 | 新疆农业科学院土壤肥料与农业节水研究所 | Multifunctional biogas slurry fertilizer for fruit trees |
CN102919247A (en) * | 2012-10-31 | 2013-02-13 | 四川国光农化股份有限公司 | Plant growth adjustment composition containing 6-benayl aminopurine |
CN102992902A (en) * | 2012-11-30 | 2013-03-27 | 王正泽 | Method for preparing plant growth promotor |
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