CN103553772B - Compound preparation for nursing tapping panel dryness and strip ulcer of rubber trees, as well as preparation method and application thereof - Google Patents
Compound preparation for nursing tapping panel dryness and strip ulcer of rubber trees, as well as preparation method and application thereof Download PDFInfo
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Abstract
The invention relates to a compound preparation for nursing tapping panel dryness and strip ulcer of rubber trees. The preparation is prepared from the following components in percentage by weight: 1-50 percent of calcium peroxide, 10-70 percent of hydrogen peroxide, 1-10 percent of monopotassium phosphate, 4-10 percent of citric acid, 1-3 percent of diethyl aminoethyl hexanoate, 1-2 percent of glacial acetic acid, 1-3 percent of prochloraz, 2-4 percent of tween 80, 0.3-2 percent of copper sulfate, 0.3-2 percent of zinc sulfate, 0.3-2 percent of magnesium sulfate, 0.5-4 percent of ammonium molybdate, 0.1-2 percent of chitosan, 0.5-2 percent of polyvinyl alcohol, 0.5-2 percent of sodium lignin sulfonate, 0.5-4 percent of boric acid, 1-2 percent of moroxydine, and the balance of pharmaceutically acceptable carriers. The invention also relates to a preparation method and an application of the compound preparation. The compound preparation is easy to prepare, the tapping panel dryness and strip ulcer of rubber trees can be effectively treated.
Description
Technical field
The present invention relates to bamboo grows cultivation and extermination of disease and insect pest field, specifically, the present invention relates to compound formulation of a kind of dead skin disease for taking good care of bamboo grows and face Phytophthora spp and its preparation method and application.
Background technology
China's natural rubber place of production is mainly distributed in Hainan Province and Yunnan Province, due to factors such as weather, geographical conditions, rubber tapping technology, the 20%-30% of China's bamboo grows total amount is caused to be in dead skin state, can not normal binder removal, Rubber Yield declines year by year, has had a strong impact on the development of China's caoutchouc industry.
The same iron and steel of natural rubber, oil, coal together and be called the four large raw materials of industry, are the basic industry and strategic materials that involve the interests of the state and the people.As one of large raw material of industry in the world four, natural rubber is widely used in aspects such as industry, agricultural, national defence, communications and transportation, machine-building, medical and health and daily lifes because having very strong elasticity, good insulating properties, plasticity, wearability, resistance to drawing property, water proof gas barrier properties etc., becomes one of indispensable material in national defence and industry.Lactiferous plant in the world has kind more than 2000, but is become natural rubber unique commercial source by establishing in large scale at present, is Para rubber tree.But the harm that bamboo grows " dead skin disease " is caused to ruber plantation is extremely serious, it is one of main limiting factor of natural rubber per unit area yield raising.According to latest survey, no matter Hainan Land Reclamation region, or reclamation area, Yunnan, rubber tree dead skin rate average out to about 25%.More seriously, in recent years Dry bark tree also with 1% speed cumulative year after year.
Bamboo grows " dead skin disease " (sometimes also referred to as face Phytophthora spp) is divided into two types (Jacob JL, Prevot JC, Lacrotte is panel dryness in Hevea brasiliensis.Plantations R.1994.Tapping, Recherche, Development, 1 (3): 15-24.): gangrenosum acne " dead skin disease " and non-gangrenosum acne " dead skin disease ".Gangrenosum acne " dead skin disease " is also called " trunk phloem necorsis " (Trunk Phloem Necrosis, TPN), it is characterized in that latex dust and surrounding tissue aging thereof, endothelium brownization, this symptom can rapid spread to whole face, extend to the non-face on opposite time serious.In the treelet of just tapping rubber soon, just there will be gangrenosum acne " dead skin disease ", even in the treelet of not tapping rubber, also have generation.This dead skin is irreversible, because the bark of regeneration is ill too.Someone thinks, gangrenosum acne " dead skin disease " poisoningly to be caused (Fan Siwei, the few cause of disease of fine jade .1994. rubber tree dead skin of poplar and the hypothesis about dead skin, tropical crop research, (4): 43-48) by pathogen or cyanogen.The type " dead skin disease " occurs seldom, not constitute a threat to production.Non-gangrenosum acne " dead skin disease " is also called " face dry sick " (Tapeing Panel Dryness, TPD), a kind of that stimulate (well stimulation that existing production generally adopts) to cause by injury (rubber tapping) and ethene, complicated physiology syndrome has now been acknowledged as.The feature of non-gangrenosum acne TPD is that the histology of bark, cell suspending line are less, but latex dust metabolic disorder is serious, and sick when sending out, bamboo grows secant local or all blocking of mammary tube, binder removal amount greatly reduces not even binder removal.This TPD is reversible, as long as allow bamboo grows rest and reorganize about 1 year, bamboo grows just can rehabilitation.But the generation of this dead skin is very general, and constitute a serious threat to production, rubber tree dead skin carried in the industry just refers to this dead skin.Just hold a dead skin symposium every the international rubber research and development committee (IRRDB) of 2-3, that focus on is just non-gangrenosum acne TPD.
Chinese patent ZL93107276.X discloses a kind of manufacture method for the treatment of vegetable rubber tree dead skin revivifier, by multiple Chinese herbal medicine process, dry, grind and part liquor, mix and blend, propagandize (burying) hotly after to sieve quantitative package.Brown type, outer brown type, stable type, Phytophthora spp, mycosis, lines parasitosis, virus disease (containing diseases such as class gram Ci Shi bodies) in medicinal powder treatment intractable rubber tree dead skin, 1-15 is prolonged stops cutting the diseases such as the rubber tree dead skin of not producing glue special curative effect, coat medicinal powder of the present invention once, just can open after 3-12 month to cut and bring back to life bamboo grows production glue.
Application number be 97121908.7 Chinese patent application disclose a kind of preventing and treating chemical for brown spot of rubber tree, it is mainly made up of tetracyclines (chloramphenicol), methylcellulose, xanthans etc.Be suitable for painting to impose on the disease tree face of brown spot of rubber tree, effectively can prevent and treat brown spot of rubber tree, and bamboo grows dry incineration method can be made to increase production 14.27%, Cost and benefit ratio is 1:4.53-6.23.
Summary of the invention
The object of the present invention is to provide the compound formulation of a kind of dead skin disease for taking good care of bamboo grows and face Phytophthora spp.
The present invention also aims to provide the preparation method of this compound formulation to apply.
In order to realize object of the present invention, the invention provides the compound formulation of a kind of dead skin disease for taking good care of bamboo grows and face Phytophthora spp, comprise the material of following weight percentage: the calper calcium peroxide of 1%-50%, the hydrogen peroxide of 10-70%, the potassium dihydrogen phosphate of 1-10%, the citric acid of 4-10%, the diethyl aminoethyl hexanoate of 1-3%, the glacial acetic acid of 1-2%, the Prochloraz of 1-3%, the Tween 80 of 2-4%, the copper sulphate of 0.3%-2%, the zinc sulphate of 0.3%-2%, the magnesium sulfate of 0.3%-2%, the ammonium molybdate of 0.5%-4%, the shitosan of 0.1%-2%, the polyvinyl alcohol of 0.5%-2%, the sodium lignin sulfonate of 0.5%-2%, the boric acid of 0.5%-4%, the moroxydine of 1%-2%, surplus is pharmaceutically acceptable carrier.
Preferably, the compound formulation of dead skin disease for taking good care of bamboo grows of the present invention and face Phytophthora spp comprises the material of following weight percentage: the calper calcium peroxide of 1%-50%, the hydrogen peroxide of 10-80%, the potassium dihydrogen phosphate of 1-10%, the citric acid of 4-10%, the diethyl aminoethyl hexanoate of 1-3%, the glacial acetic acid of 1-2%, the Prochloraz of 1-3%, the Tween 80 of 2-4%, the copper sulphate of 0.3%-2%, the zinc sulphate of 0.3%-2%, the magnesium sulfate of 0.3%-2%, the ammonium molybdate of 0.5%-4%, the shitosan of 0.1%-2%, the polyvinyl alcohol of 0.5%-2%, the sodium lignin sulfonate of 0.5%-2%, the boric acid of 0.5%-4%, the moroxydine of 1%-2%, surplus is pharmaceutically acceptable carrier.
More preferably, the compound formulation of dead skin disease for taking good care of bamboo grows of the present invention and face Phytophthora spp comprises the material of following weight percentage: the calper calcium peroxide of 20%, the hydrogen peroxide of 40%, the potassium dihydrogen phosphate of 5%, the citric acid of 5%, the diethyl aminoethyl hexanoate of 2%, the glacial acetic acid of 1%, the Prochloraz of 1%, the Tween 80 of 3%, the copper sulphate of 1%, the zinc sulphate of 1%, the magnesium sulfate of 1%, the ammonium molybdate of 2%, the shitosan of 1%, the polyvinyl alcohol of 1%, the sodium lignin sulfonate of 1%, the boric acid of 2%, the moroxydine of 1%, surplus is pharmaceutically acceptable carrier.
Most preferably, described compound formulation can be aqua, pulvis or spray.
The present invention also provides the preparation method of the compound formulation of a kind of dead skin disease for taking good care of bamboo grows and face Phytophthora spp, the method comprises the following steps: the calper calcium peroxide of 1%-50%, the hydrogen peroxide of 10-70%, the potassium dihydrogen phosphate of 1-10%, the citric acid of 4-10%, the diethyl aminoethyl hexanoate of 1-3%, the glacial acetic acid of 1-2%, the Prochloraz of 1-3%, the Tween 80 of 2-4%, the copper sulphate of 0.3%-2%, the zinc sulphate of 0.3%-2%, the magnesium sulfate of 0.3%-2%, the ammonium molybdate of 0.5%-4%, the shitosan of 0.1%-2%, the polyvinyl alcohol of 0.5%-2%, the sodium lignin sulfonate of 0.5%-2%, the boric acid of 0.5%-4%, the moroxydine of 1%-2% and the water of surplus add in reactor, stir, staticly settle, filling, bottling, encapsulate and get final product.
The present invention also provides the application of compound formulation in the preparation for the preparation of the dead skin disease and face Phytophthora spp of taking good care of bamboo grows, described compound formulation comprises the material of following weight percentage: the calper calcium peroxide of 1%-50%, the hydrogen peroxide of 10-70%, the potassium dihydrogen phosphate of 1-10%, the citric acid of 4-10%, the diethyl aminoethyl hexanoate of 1-3%, the glacial acetic acid of 1-2%, the Prochloraz of 1-3%, the Tween 80 of 2-4%, the copper sulphate of 0.3%-2%, the zinc sulphate of 0.3%-2%, the magnesium sulfate of 0.3%-2%, the ammonium molybdate of 0.5%-4%, the shitosan of 0.1%-2%, the polyvinyl alcohol of 0.5%-2%, the sodium lignin sulfonate of 0.5%-2%, the boric acid of 0.5%-4%, the moroxydine of 1%-2%, surplus is pharmaceutically acceptable carrier.
Preferably, described compound formulation comprises the material of following weight percentage: the calper calcium peroxide of 1%-50%, the hydrogen peroxide of 10-80%, the potassium dihydrogen phosphate of 1-10%, the citric acid of 4-10%, the diethyl aminoethyl hexanoate of 1-3%, the glacial acetic acid of 1-2%, the Prochloraz of 1-3%, the Tween 80 of 2-4%, the copper sulphate of 0.3%-2%, the zinc sulphate of 0.3%-2%, the magnesium sulfate of 0.3%-2%, the ammonium molybdate of 0.5%-4%, the shitosan of 0.1%-2%, the polyvinyl alcohol of 0.5%-2%, the sodium lignin sulfonate of 0.5%-2%, the boric acid of 0.5%-4%, the moroxydine of 1%-2%, surplus is pharmaceutically acceptable carrier.
More preferably, described compound formulation comprises the material of following weight percentage: the calper calcium peroxide of 20%, the hydrogen peroxide of 40%, 5% potassium dihydrogen phosphate, the citric acid of 5%, diethyl aminoethyl hexanoate, the glacial acetic acid of 1%, Prochloraz, the Tween 80 of 3%, copper sulphate, the zinc sulphate of 1%, magnesium sulfate, the ammonium molybdate of 2%, shitosan, the polyvinyl alcohol of 1%, sodium lignin sulfonate, the boric acid of 2%, the moroxydine of 1% of 1% of 1% of 1% of 1% of 1% of 2%, surplus is pharmaceutically acceptable carrier.
It should be noted that unless otherwise indicated, otherwise hydrogen peroxide used herein all refer to that concentration is the aqueous hydrogen peroxide solution of 42 % by weight.
The present invention solves the technical barrier of the current Tapping Panel Dryness Symptom in Hevea of China and face Phytophthora spp well.The technical program, since Hainan Province and Yunnan Province implement, has reached promising result: the recovery rate of dead skin disease and Phytophthora spp tree reaches more than 90%, and by digital proof, the present invention is practical new technology more satisfactory both at home and abroad at present.Technique brings huge economic benefit by for Rubber Industry after popularizing in an all-round way.
Embodiment
Below by way of the description of embodiment, the invention will be further described, but this is not limitation of the present invention, those skilled in the art are according to basic thought of the present invention, various amendment or improvement can be made, but only otherwise depart from basic thought of the present invention, all within the scope of the present invention.
The preparation of embodiment 1 compound formulation of the present invention
The formula rate of the compound formulation in the present embodiment is as follows: the calper calcium peroxide of 20%, the hydrogen peroxide of 40%, 5% potassium dihydrogen phosphate, the citric acid of 5%, diethyl aminoethyl hexanoate (purchased from Shaanxi Kang Ze Chemical Industry Science Co., Ltd), the glacial acetic acid of 1%, Prochloraz, the Tween 80 of 3%, copper sulphate, the zinc sulphate of 1%, magnesium sulfate, the ammonium molybdate of 2%, shitosan, the polyvinyl alcohol of 1%, sodium lignin sulfonate, the boric acid of 2%, the moroxydine of 1% of 1% of 1% of 1% of 1% of 1% of 2%, surplus is water.
Take the calper calcium peroxide of 20 kilograms, and take other compositions according to aforementioned proportion, then add in reactor, stir, staticly settle, filling, bottling, encapsulates and get final product.
The preparation of embodiment 2 compound formulation of the present invention
Prepare compound formulation according to the mode identical with embodiment 1, difference is not use calper calcium peroxide.
The preparation of embodiment 3 compound formulation of the present invention
Prepare compound formulation according to the mode identical with embodiment 1, difference is not use hydrogen peroxide.
The preparation of embodiment 4 compound formulation of the present invention
Prepare compound formulation according to the mode identical with embodiment 1, difference is not use diethyl aminoethyl hexanoate.
The preparation of embodiment 5 compound formulation of the present invention
Prepare compound formulation according to the mode identical with embodiment 1, difference is not use sodium lignin sulfonate.
The preparation of embodiment 6 compound formulation of the present invention
Prepare compound formulation according to the mode identical with embodiment 1, difference is not use moroxydine.
The preparation of embodiment 7 compound formulation of the present invention
Prepare compound formulation according to the mode identical with embodiment 1, difference is not use citric acid.
The preparation of embodiment 8 compound formulation of the present invention
Prepare compound formulation according to the mode identical with embodiment 1, difference is to use the hydrogen peroxide of identical weight to replace calper calcium peroxide.
Experimental example 1
Judge dead skin disease by following standard: bamboo grows secant local or all not binder removal, time serious, bark produces the symptom of brown spot, speckle, bark explosion and face deformation.And typical case is attended by the appearance of brown spot and speckle.And the standard of curing using above-mentioned transference cure as dead skin disease.
Get the ill bamboo grows of 180 strain, be divided into 9 groups, often organize 20 strains.Control group uses brush to smear ethrel paste (2g/ strain) at gum face.Seven days once, smears 49 days continuously.
Before the sample using embodiment 1-8, remove the Lao Pi of bamboo grows, the trunk of ill bamboo grows is sprayed.For every strain bamboo grows, get 150 milliliters, corresponding sample, add 350 ml waters and dilute, then spray.Sample 1-8 sprays the ill bamboo grows of 20 strain respectively.Seven days once, smears 49 days continuously.It should be noted that, for convenience's sake, above-mentioned sample 1-8 directly prepares before use.
Above-mentioned all ill bamboo growss all grow in same rubber plantation.Result is as follows.
For the ill bamboo grows of smearing ethrel paste, cure rate only reaches 20%, and for using the situation of sample 1, ill bamboo grows is all cured, and this shows also can treat ill bamboo grows in the situation of the peroxide using low content.Therefore peroxide often has certain corrosivity, can damage operating personnel, and this is significant in actual applications.
For the sample of embodiment 2 and 3, cure rate reaches 71% and 74% respectively.For the sample of embodiment 4-6, cure rate reaches 84%, 88%, 91% respectively, and ironically, for the sample of embodiment 7, ill bamboo grows is also all cured unexpectedly.For the sample of embodiment 8, cure rate is 90%.
Claims (3)
1. the compound formulation for the dead skin disease and face Phytophthora spp of taking good care of bamboo grows, it is characterized in that, be made up of the material of following weight percentage: the calper calcium peroxide of 20%, the hydrogen peroxide of 40%, the potassium dihydrogen phosphate of 5%, diethyl aminoethyl hexanoate, the glacial acetic acid of 1%, Prochloraz, the Tween 80 of 3%, copper sulphate, the zinc sulphate of 1%, magnesium sulfate, the ammonium molybdate of 2%, shitosan, the polyvinyl alcohol of 1%, sodium lignin sulfonate, the boric acid of 2%, the moroxydine of 1% of 1% of 1% of 1% of 1% of 1% of 2%, surplus is water.
2. the preparation method for the compound formulation of the dead skin disease and face Phytophthora spp of taking good care of bamboo grows, the method comprises the following steps: the calper calcium peroxide of 20%, the hydrogen peroxide of 40%, the potassium dihydrogen phosphate of 5%, the diethyl aminoethyl hexanoate of 2%, the glacial acetic acid of 1%, the Prochloraz of 1%, the Tween 80 of 3%, the copper sulphate of 1%, the zinc sulphate of 1%, the magnesium sulfate of 1%, the ammonium molybdate of 2%, the shitosan of 1%, the polyvinyl alcohol of 1%, the sodium lignin sulfonate of 1%, the boric acid of 2%, the moroxydine of 1% and the water of surplus add in reactor, stir, staticly settle, filling, bottling, encapsulate and get final product.
3. the application of compound formulation in the preparation for the preparation of the dead skin disease and face Phytophthora spp of taking good care of bamboo grows, it is characterized in that, described compound formulation is made up of the material of following weight percentage: the calper calcium peroxide of 20%, the hydrogen peroxide of 40%, the potassium dihydrogen phosphate of 5%, the diethyl aminoethyl hexanoate of 2%, the glacial acetic acid of 1%, the Prochloraz of 1%, the Tween 80 of 3%, the copper sulphate of 1%, the zinc sulphate of 1%, the magnesium sulfate of 1%, the ammonium molybdate of 2%, the shitosan of 1%, the polyvinyl alcohol of 1%, the sodium lignin sulfonate of 1%, the boric acid of 2%, the moroxydine of 1%, surplus is water.
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| CN104003810B (en) * | 2014-03-28 | 2015-07-22 | 中国热带农业科学院橡胶研究所 | Rubber tree dead skin prevention and cure smearing agent and preparing method for rubber tree dead skin prevention and cure smearing agent |
| CN104430546B (en) * | 2014-12-09 | 2017-04-19 | 陈干忠 | High-yield disease-resistant and mothproof composite preparation for rubber trees as well as preparation method and application thereof |
| WO2022098227A1 (en) * | 2020-11-09 | 2022-05-12 | Palaniappan Kavitha | Compositions for treatment or rehabilitation of rubber trees |
| CN115281186B (en) * | 2022-08-06 | 2023-06-27 | 贵州大学 | Smearing preparation for preventing and treating kiwi fruit canker and preparation method thereof |
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