CN103550275B - A kind of extracting method of Herba Saussureae Involueratae essence substance - Google Patents
A kind of extracting method of Herba Saussureae Involueratae essence substance Download PDFInfo
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Abstract
The present invention discloses a kind of extracting method of Herba Saussureae Involueratae essence substance, comprises the steps: pretreatment and the purified water of (1) Herba Saussureae Involueratae; (2) Herba Saussureae Involueratae pretreatment obtained and pure water extract; (3) be separated carrying out precision after the coarse filtration of cooled Herba Saussureae Involueratae soup; (4) be 0.25-0.45um micro-pore-film filtration with aperture again by secondary filter liquid; (5) polishing purification liquid reverse osmosis membrane is concentrated at normal temperatures; (6) the Herba Saussureae Involueratae soup concentrated through reverse osmosis membrane is carried out concentrating under reduced pressure again; (7) elite extract is finally obtained.Compared with prior art, the extracting method of Herba Saussureae Involueratae essence substance provided by the invention, extract the elite of Herba Saussureae Involueratae, greatly promote nutrition absorption rate, there is high efficiency, environmental protection, safety and guarantee the advantages such as effective ingredient activity, both maintained taste and the nutrient of Herba Saussureae Involueratae, be easy to carry again, famous and precious Herba Saussureae Involueratae efficacy effect can have been brought into play completely.
Description
Technical field
The present invention relates to field of health care products, exactly refer to a kind of extracting method of Herba Saussureae Involueratae essence substance.
Background technology
Herba Saussureae Involueratae is the herbaceous plant of Compositae phoenix hair Chrysanthemum Herba Saussureae Involueratae subgenus.Its growth is between the rubble near the rock flowing hillside of high mountains and snow line of height above sea level 4800-5800 meters.The plant of this subgenus has more than 20 to plant, and the overwhelming majority originates in Chinese Tibetan Plateau and its adjacent regions.Herba Saussureae Involueratae is the rare famous and precious medicinal plants of a kind of high mountain, therefore protects Herba Saussureae Involueratae germ plasm resource, in science, pharmaceutically or from viewing and admiring all significant.
Herba Saussureae Involueratae grows usually below high mountain snow line.Climate variability, cold and hot impermanence, alternately, the highest monthly average temperature 3--5 DEG C, minimum monthly average temperature-19 ~ 21 DEG C, annual precipitation about 800 millimeters, frost-free period only has about 50 days to sleet.Soil is based on alpine meadow soil, and the content of organic matter is 8.5--11%, nitrogen content 4.5--10%.Due to harsh environmental conditions, general plant is difficult to growth, only has minority to resist cold, low temperature resistant Carex Carexspp, and high grass belongs to Kobresiaspp. and the association with it of various high mountain herbaceos perennials.Herba Saussureae Involueratae is under this high mountain rigor condition, and poor growth, at least just can yield positive results after 4--5.But because trophophase is short, it can germinate rapidly in the short period of time, grow, Flowering and fruiting.July at florescence, really August phase.Growing environment lower altitude limit 2400 meters of altitude limit 4000 meters.
Herba Saussureae Involueratae has the biological characteristics adapting to Alpine environment, the extremely close shape of its leaf is as white long draft hair, as if silk tops, MIAOMAO interweaves, the gas defined in countless " cell " rooms is difficult to exchange with the external world, daytime, the heat that it absorbs than soil and the air of surrounding was large under the direct irradiation of sunlight; And MIAOMAO layer can make body exempt from the injury of intense radiation.In addition, intensive in the head inflorescence on stem top, normal mend two sides close encapsulate by the blade of long draft hair, just as having put on white sweater, connect generation to ensure to propagate under the Alpine environment of cold.The characteristic of this adaptation Alpine environment of Herba Saussureae Involueratae is formed under its condition cold and arid at high mountain for a long time.Due to the thin intracellular accumulation materials such as a large amount of soluble sugars, protein and lipid of Herba Saussureae Involueratae, the apparent freezing point of cellular plasm liquid can be made to reduce, when temperature drop to paraplasm below freezing time, intraprotoplasmic moisture just penetrate in intercellular substance and plasmolytic space freeze.And protoplast reduces gradually, can not suffer damage.When the same day, cyclostrophic warmed up, ice melting, moisture again absorb by protoplast, cell returns to again the peculiar acrophyta of normality---Herba Saussureae Involueratae is exactly by this cold-resistant characteristic, survives in high and cold mountain.
Herba Saussureae Involueratae, except product Tibet, also has distribution in the Xinjiang of China, Qinghai, Sichuan, Yunnan.Various places are among the people by Herba Saussureae Involueratae all herbal medicine, cure mainly snow the region between the heart and the diaphragm, toothache, rheumatic arthritis, sexual impotence, menoxenia, redly to collapse, the disease such as leucorrhea.India is among the people also treats many chronics with Herba Saussureae Involueratae.As diseases such as gastric ulcer, hemorrhoid, bronchitis, heart disease, epistaxis and venom.On Tibetan medicine, Herba Saussureae Involueratae has long history as medicine.All on the books on Tibetanmedicine document " moon king medicine precious " and the Four-Volume Medical Code.
Herba Saussureae Involueratae has physiologically active effective ingredient.Wherein umbelliferone have significantly antibacterial, blood pressure lowering is calm, spasmolysis; Scopoletin has and dispels the wind, antiinflammatory, pain relieving, to eliminate the phlegm and antitumor action, and clinical treatment dyspnea with rapid respiration chronic bronchitis effective percentage is that 96.6% apigenin has smooth muscle spasmolysis and anti-ulcer effect; Obvious choleretic effect is had to antelope base benzophenone.Full of interest is especially colchicine contained in Herba Saussureae Involueratae, this composition is a Typical Representative of cell mitogen, the growth of energy anticancer, clinical in Therapeutic cancer, there is certain curative effect with breast carcinoma especially, also have certain effect to skin carcinoma, leukemia and what king's evil etc.To the special effect of gout acute attack, reduce inflammation in 12-24 hours and pain relieving rapidly, life-time service can reduce attack times.
There is estrogen-like effects activity in addition, energy prolong rats rutting period and metoestrus, and shorten dioestrus and proestrus.But the toxicity of colchicine is comparatively large, can cause nausea, loss of appetite, abdominal distention, and severe patient there will be enteroparalysis and the side effect such as constipation, extremities aching pain.Due to the colchicine that in Herba Saussureae Involueratae, toxicity is larger containing good effect, can't take so among the people when steeping in wine cure mainly rheumatic arthritis and gynaecopathia with Herba Saussureae Involueratae more.
At present, the eating method of most Herba Saussureae Involueratae is for cooking on the market, steeps in wine or fricassee, but above directly eating method can only absorb 20 to four ten of hundred parts of Herba Saussureae Involueratae nutrition, central hundred parts 60 to eight ten will therefore to waste.
Summary of the invention
For above-mentioned defect, the technical problem that the present invention solves is the extracting method providing a kind of Herba Saussureae Involueratae essence substance, extract the elite of Herba Saussureae Involueratae, greatly promote nutrition absorption rate, there is high efficiency, environmental protection, safety and guarantee the advantages such as effective ingredient activity, both maintained taste and the nutrient of Herba Saussureae Involueratae, be easy to carry again, famous and precious Herba Saussureae Involueratae efficacy effect can have been brought into play completely.
In order to solve above technical problem, the extracting method of Herba Saussureae Involueratae essence substance provided by the invention, comprises the steps:
(1) pretreatment of Herba Saussureae Involueratae, removes the impurity staff on Herba Saussureae Involueratae surface, and pulverize Herba Saussureae Involueratae at the temperature pulverizer lower than 60 DEG C, fineness requirement is at 8 orders or following, and particle diameter is the smaller the better; Extraction is processed with former water, uses the pure water removing ion;
(2) Herba Saussureae Involueratae pretreatment obtained and pure water are in the Herba Saussureae Involueratae of 1:8-1:15 weight portion and water ratio, water temperature extracts at 20 DEG C-50 DEG C, and extraction is carried out 2-4 time, each 10-60 minute, the Herba Saussureae Involueratae soup filtered out after extraction is several times merged, cools at ambient temperature;
(3) being separated carrying out precision after the coarse filtration of cooled Herba Saussureae Involueratae soup, by aperture at the accurate membrane filtration of 3-10um, obtaining the secondary filter liquid of Herba Saussureae Involueratae soup;
(4) be 0.25-0.45um micro-pore-film filtration with aperture again by secondary filter liquid, obtain the polishing purification liquid of Herba Saussureae Involueratae soup;
(5) polishing purification liquid reverse osmosis membrane is concentrated at normal temperatures, obtain the concentrated Herba Saussureae Involueratae soup that solid content is 8-15%;
(6) the Herba Saussureae Involueratae soup will concentrated through reverse osmosis membrane, then carry out concentrating under reduced pressure, adopt the low temperature of 40 DEG C-50 DEG C, Herba Saussureae Involueratae soup being concentrated to solid content is 50-70%;
(7) concentrated solution is carried out microwave vacuum low-temperature drying, vacuum lyophilization or spray-dired mode, finally obtain elite extract.
Preferably, in step (1), with pulverizer, Herba Saussureae Involueratae is pulverized at the temperature of 20-50 DEG C.
Preferably, described elite extract makes electuary, tablet or capsule.
Preferably, the residue obtained after microwave vacuum low-temperature drying, vacuum lyophilization or spraying dry is made highland barley biscuit.
Compared with prior art, the extracting method of Herba Saussureae Involueratae essence substance provided by the invention, the elite using low-temperature extraction isolation technics to extract Herba Saussureae Involueratae can bring up to hundred parts 70%, low-temperature extraction isolation technics is by the low-temperature extraction technology in conjunction with shearing and vibration force effect, combined type microwave-assisted extraction technique and supercritical carbon dioxide extraction isolation technics three technology are integrated and are formed, this technology can carry out combination adjustment according to the characteristic of raw material and product demand, there is high efficiency, environmental protection, safety with guarantee the advantages such as effective ingredient is active, the scope of application is quite extensive, operative temperature is lower than 60 DEG C, the activity of effective ingredient in natural goods can be guaranteed, do not use the solvent of harmful human body, carry out extract and separate in an economical manner, can fully retain its effective ingredient and fragrance, equipment is easy to amplify, emphasizing the modern life that is healthy and health preserving, coordinate low-temperature extraction isolation technics the efficacy exertion of Herba Saussureae Involueratae to maximum, greatly promote nutrition absorption rate, there is high efficiency, environmental protection, safety with guarantee the advantages such as effective ingredient is active, both taste and the nutrient of Herba Saussureae Involueratae had been maintained, be easy to carry again, famous and precious Herba Saussureae Involueratae efficacy effect can be brought into play completely.
Accompanying drawing explanation
Fig. 1 is the flow chart of the extracting method of Herba Saussureae Involueratae essence substance in the present invention.
Detailed description of the invention
In order to those skilled in the art can understand technical scheme provided by the present invention better, set forth below in conjunction with specific embodiment.
Refer to Fig. 1, this figure is the structural representation of the extracting method of Herba Saussureae Involueratae essence substance in the present invention.
Embodiment 1
The extracting method of the Herba Saussureae Involueratae essence substance that the embodiment of the present invention provides, comprises the steps:
(1) pretreatment of Herba Saussureae Involueratae, removes the impurity staff on Herba Saussureae Involueratae surface, and pulverize Herba Saussureae Involueratae at the temperature pulverizer of 50 DEG C, fineness requirement is at 8 orders; Extraction is processed with former water, uses the pure water removing ion;
(2) Herba Saussureae Involueratae pretreatment obtained and pure water are in the Herba Saussureae Involueratae of 1:8 weight portion and water ratio, and water temperature extracts at 20 DEG C, and extraction carries out 3 times, each 30 minutes, and the Herba Saussureae Involueratae soup filtered out after extracting 4 times merges, and cools at ambient temperature;
(3) being separated carrying out precision after the coarse filtration of cooled Herba Saussureae Involueratae soup, by aperture at the accurate membrane filtration of 8um, obtaining the secondary filter liquid of Herba Saussureae Involueratae soup;
(4) be 0.25um micro-pore-film filtration with aperture again by secondary filter liquid, obtain the polishing purification liquid of Herba Saussureae Involueratae soup;
(5) polishing purification liquid reverse osmosis membrane is concentrated at normal temperatures, obtain the concentrated Herba Saussureae Involueratae soup that solid content is 10%;
(6) the Herba Saussureae Involueratae soup will concentrated through reverse osmosis membrane, then carry out concentrating under reduced pressure, adopt the low temperature of 50 DEG C, Herba Saussureae Involueratae soup being concentrated to solid content is 70%;
(7) concentrated solution is carried out microwave vacuum low-temperature drying, vacuum lyophilization or spray-dired mode, finally obtain elite extract, elite extract makes electuary; The residue obtained after microwave vacuum low-temperature drying, vacuum lyophilization or spraying dry is made highland barley biscuit.
For 10 grams of Herba Saussureae Involueratae, have 72% with the elite that low-temperature extraction isolation technics is extracted wherein, only remaining 28% residue.
Embodiment 2
The extracting method of the Herba Saussureae Involueratae essence substance that the embodiment of the present invention provides, comprises the steps:
(1) pretreatment of Herba Saussureae Involueratae, removes the impurity staff on Herba Saussureae Involueratae surface, and pulverize Herba Saussureae Involueratae at the temperature pulverizer of 30 DEG C, fineness requirement is at 20 orders; Extraction is processed with former water, uses the pure water removing ion;
(2) Herba Saussureae Involueratae pretreatment obtained and pure water are in the Herba Saussureae Involueratae of 1:15 weight portion and water ratio, and water temperature extracts at 50 DEG C, and extraction carries out 4 times, each 60 minutes, and the Herba Saussureae Involueratae soup filtered out after extracting 4 times merges, and cools at ambient temperature;
(3) being separated carrying out precision after the coarse filtration of cooled Herba Saussureae Involueratae soup, by aperture at the accurate membrane filtration of 10um, obtaining the secondary filter liquid of Herba Saussureae Involueratae soup;
(4) be 0.45um micro-pore-film filtration with aperture again by secondary filter liquid, obtain the polishing purification liquid of Herba Saussureae Involueratae soup;
(5) polishing purification liquid reverse osmosis membrane is concentrated at normal temperatures, obtain the concentrated Herba Saussureae Involueratae soup that solid content is 15%;
(6) the Herba Saussureae Involueratae soup will concentrated through reverse osmosis membrane, then carry out concentrating under reduced pressure, adopt the low temperature of 50 DEG C, Herba Saussureae Involueratae soup being concentrated to solid content is 50%;
(7) concentrated solution is carried out microwave vacuum low-temperature drying, vacuum lyophilization or spray-dired mode, finally obtain elite extract, elite extract makes capsule; The residue obtained after microwave vacuum low-temperature drying, vacuum lyophilization or spraying dry is made highland barley biscuit.
For 10 grams of Herba Saussureae Involueratae, have 70% with the elite that low-temperature extraction isolation technics is extracted wherein, only remaining 30% residue.
Embodiment 3
The extracting method of the Herba Saussureae Involueratae essence substance that the embodiment of the present invention provides, comprises the steps:
(1) pretreatment of Herba Saussureae Involueratae, removes the impurity staff on Herba Saussureae Involueratae surface, and pulverize Herba Saussureae Involueratae at the temperature pulverizer of 20 DEG C, fineness requirement is at 100 orders; Extraction is processed with former water, uses the pure water removing ion;
(2) Herba Saussureae Involueratae pretreatment obtained and pure water are in the Herba Saussureae Involueratae of 1:12 weight portion and water ratio, and water temperature extracts at 40 DEG C, and extraction carries out 2 times, each 30 minutes, and the Herba Saussureae Involueratae soup filtered out after extracting 2 times merges, and cools at ambient temperature;
(3) being separated carrying out precision after the coarse filtration of cooled Herba Saussureae Involueratae soup, by aperture at the accurate membrane filtration of 5um, obtaining the secondary filter liquid of Herba Saussureae Involueratae soup;
(4) be 0.35um micro-pore-film filtration with aperture again by secondary filter liquid, obtain the polishing purification liquid of Herba Saussureae Involueratae soup;
(5) polishing purification liquid reverse osmosis membrane is concentrated at normal temperatures, obtain the concentrated Herba Saussureae Involueratae soup that solid content is 10%;
(6) the Herba Saussureae Involueratae soup will concentrated through reverse osmosis membrane, then carry out concentrating under reduced pressure, adopt the low temperature of 45 DEG C, Herba Saussureae Involueratae soup being concentrated to solid content is 60%;
(7) concentrated solution is carried out microwave vacuum low-temperature drying, vacuum lyophilization or spray-dired mode, finally obtain elite extract, elite extract makes tablet; The residue obtained after microwave vacuum low-temperature drying, vacuum lyophilization or spraying dry is made highland barley biscuit.
For 10 grams of Herba Saussureae Involueratae, have 75% with the elite that low-temperature extraction isolation technics is extracted wherein, only remaining 25% residue.
Compared with prior art, the extracting method of Herba Saussureae Involueratae essence substance provided by the invention, the elite using low-temperature extraction isolation technics to extract Herba Saussureae Involueratae can bring up to hundred parts 70%, low-temperature extraction isolation technics is by the low-temperature extraction technology in conjunction with shearing and vibration force effect, combined type microwave-assisted extraction technique and supercritical carbon dioxide extraction isolation technics three technology are integrated and are formed, this technology can carry out combination adjustment according to the characteristic of raw material and product demand, there is high efficiency, environmental protection, safety with guarantee the advantages such as effective ingredient is active, the scope of application is quite extensive, operative temperature is lower than 60 DEG C, the activity of effective ingredient in natural goods can be guaranteed, do not use the solvent of harmful human body, carry out extract and separate in an economical manner, can fully retain its effective ingredient and fragrance, equipment is easy to amplify, emphasizing the modern life that is healthy and health preserving, coordinate low-temperature extraction isolation technics the efficacy exertion of Herba Saussureae Involueratae to maximum, greatly promote nutrition absorption rate, there is high efficiency, environmental protection, safety with guarantee the advantages such as effective ingredient is active, both taste and the nutrient of Herba Saussureae Involueratae had been maintained, be easy to carry again, famous and precious Herba Saussureae Involueratae efficacy effect can be brought into play completely.
To the above-mentioned explanation of the disclosed embodiments, professional and technical personnel in the field are realized or uses the present invention.To be apparent for those skilled in the art to the multiple amendment of these embodiments, General Principle as defined herein can without departing from the spirit or scope of the present invention, realize in other embodiments.Therefore, the present invention can not be restricted to these embodiments shown in this article, but will meet the widest scope consistent with principle disclosed herein and features of novelty.
Claims (3)
1. an extracting method for Herba Saussureae Involueratae essence substance, is characterized in that, comprises the steps:
(1) pretreatment of Herba Saussureae Involueratae, removes the impurity staff on Herba Saussureae Involueratae surface, and pulverize Herba Saussureae Involueratae with pulverizer at the temperature of 20-50 DEG C, fineness requirement is at 8 orders or following; Extraction is processed with former water, uses the pure water removing ion;
(2) Herba Saussureae Involueratae pretreatment obtained and pure water are in the Herba Saussureae Involueratae of 1:8-1:15 weight portion and water ratio, water temperature extracts at 20 DEG C-50 DEG C, and extraction is carried out 2-4 time, each 10-60 minute, the Herba Saussureae Involueratae soup filtered out after extraction is several times merged, cools at ambient temperature;
(3) being separated carrying out precision after the coarse filtration of cooled Herba Saussureae Involueratae soup, by aperture at 3-10 μm of accurate membrane filtration, obtaining the secondary filter liquid of Herba Saussureae Involueratae soup;
(4) be 0.25-0.45 μm of micro-pore-film filtration with aperture again by secondary filter liquid, obtain the polishing purification liquid of Herba Saussureae Involueratae soup;
(5) polishing purification liquid reverse osmosis membrane is concentrated at normal temperatures, obtain the concentrated Herba Saussureae Involueratae soup that solid content is 8-15%;
(6) the Herba Saussureae Involueratae soup will concentrated through reverse osmosis membrane, then carry out concentrating under reduced pressure, adopt the low temperature of 40 DEG C-50 DEG C, Herba Saussureae Involueratae soup being concentrated to solid content is 50-70%;
(7) concentrated solution is carried out microwave vacuum low-temperature drying, vacuum lyophilization or spraying dry, finally obtain elite extract.
2. electuary, tablet or capsule that the Herba Saussureae Involueratae essence substance obtained by extracting method according to claim 1 is made.
3. a highland barley biscuit, is characterized in that, is made by the elite extract obtained after microwave vacuum low-temperature drying according to claim 1, vacuum lyophilization or spraying dry.
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| CN104397683B (en) * | 2014-10-31 | 2017-01-11 | 广州巴宝莉化妆品有限公司 | Method for extracting Saussurea medusa essence materials |
| CN108553498A (en) * | 2018-04-24 | 2018-09-21 | 烟台金蕊女性用品有限公司 | A kind of saussurea involucrata essence extraction process |
| CN115028751B (en) * | 2022-06-15 | 2023-05-16 | 中国科学院新疆理化技术研究所 | Preparation method and application of saussurea involucrata polysaccharide |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1759710A (en) * | 2005-11-09 | 2006-04-19 | 云南省农业机械研究所 | 'Puer' caffeine and processing method |
| CN102106889A (en) * | 2011-02-21 | 2011-06-29 | 贾正平 | Application of snow saussurea and snow saussurea extract in preparation of anti-hypoxia medicaments and method for preparing snow saussurea extract |
| CN103191166A (en) * | 2013-03-25 | 2013-07-10 | 西藏藏真堂藏药产业有限公司 | Method for increasing yield of saussurea obvallata, extract of saussurea obvallata and application of extract |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1759710A (en) * | 2005-11-09 | 2006-04-19 | 云南省农业机械研究所 | 'Puer' caffeine and processing method |
| CN102106889A (en) * | 2011-02-21 | 2011-06-29 | 贾正平 | Application of snow saussurea and snow saussurea extract in preparation of anti-hypoxia medicaments and method for preparing snow saussurea extract |
| CN103191166A (en) * | 2013-03-25 | 2013-07-10 | 西藏藏真堂藏药产业有限公司 | Method for increasing yield of saussurea obvallata, extract of saussurea obvallata and application of extract |
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