CN103435336A - Self-forming glaze white jade porcelain pug and manufacturing method of porcelain pug product - Google Patents
Self-forming glaze white jade porcelain pug and manufacturing method of porcelain pug product Download PDFInfo
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Abstract
The invention relates to self-forming glaze white jade porcelain pug and a manufacturing method of a porcelain pug product. The self-forming glaze white jade porcelain pug comprises the followings in percentage by weight: 13 to 21 percent of kaoline, 14 to 20 percent of feldspar, 2 to 7 percent of bentonite, 38 to 47 percent of quartz, 11 to 16 percent of wollostonite and 7 to 11 percent of calcite power. The manufacturing method provided by the invention comprises the steps of sparring, slurrying and the like. The method has the benefits as follows: traditional two-step firing is changed to be one-step firing, energy consumption is lowered, carbon discharge capacity is reduced, processes of glaze making and glazing are removed, the discharge capacity of three wastes is reduced, human resources are saved, the dissolving-out amount of heavy metals such as lead and cadmium and the like carried into glaze is reduced, the porcelain pug is glittering and translucent, like jade, and the section of the porcelain pug has no arrises and is shell-shaped. The porcelain pug product prepared by the invention is green, environmental-friendly and safe, can be used as dishware porcelain, daily porcelain, art porcelain, decorative porcelain, porcelain for lighting tools and the like in the ceramic industry.
Description
Technical field
The present invention relates to ceramic manufacture field, be specifically related to a kind of manufacture method that has glaze white jade porcelain pug and porcelain pug goods of one's own.
Background technology
From ancient times to the present, in the Ceramic Production process, after formed product, through biscuiting, pick, polishing, washing, drying, glazing, the multiple tracks technical process sides such as glaze firing become ceramic product.Wherein, biscuiting, enamel frit makeing, glazing is requisite technical process together especially.Kaolin accounts for 40-55%, consumes high-quality resource many, and the twice firing energy consumption is large, environmental pollution in the enamel frit makeing process " three wastes are high ", and the leaching ability of heavy metal amounts such as plumbous cadmium are wayward, and its production process is many, energy consumption is high.
The Patent Application Publication that application number is 200910111290.6 novel transparent high-grade ceramic pug and ceramic thereof, adopt base, glaze raw material to be mixed into the new ceramics pug of one, the formula of pug consists of: kaolin: 20-30%; Feldspar (potassium, albite): 10-15%; Quartzy: 35-45%; Calcium phosphate powder: 10-20%; Triphane: 2-3%; Talcum: 1-3%.In formula, adopt calcium phosphate powder to replace traditional ox bone ash.
The Patent Application Publication that application number is 201310104867.7 a kind of ceramic, make by the following method: the pug of following weight proportion is added to water and make slurry: kaolin 48-55%, feldspar 36-42%, aluminum oxide 2-4%, talcum 3-5% and quartzy 3-6%, add the water glass that accounts for this slurry 0.5-0.6% weight ratio and the U.S. Xian Shui that accounts for this slurry 0.1-0.2% weight ratio in the slurry made, then make base substrate, obtain finished product after biscuiting, glazing glaze firing.The temperature of described biscuiting is 780-820 ℃; The firing temperature of described glaze firing is 1280-1320 ℃, and wherein 960 ℃ keep 2h, and 1280-1320 ℃ keeps 1.5h.
In above-mentioned application documents, ceramic material is used the kaolin ratio large, causes the ceramic manufacturing cost high, and complex process, the production process complexity.Therefore the present invention proposes a kind of manufacture method that has glaze white jade porcelain pug and porcelain pug goods of one's own.
Summary of the invention
In order to overcome defect of the prior art, the purpose of this invention is to provide a kind of without glazing, ooze the glaze flame polish once firing middle transmutation, porcelain pug goods surfaces externally and internally self-assembling formation glaze layer, and production technique is simplified, less energy-consumption, high benefit, the sparkling and crystal-clear manufacture method that has glaze white jade porcelain pug and porcelain pug goods of one's own as white jade of lead and cadmium free leaching ability of heavy metal and porcelain pug goods.
The present invention is achieved through the following technical solutions:
The invention provides and have glaze white jade porcelain pug of one's own, its porcelain pug formula is by weight percentage: kaolin 13-21%, feldspar 14-20%, wilkinite 2-7%, quartzy 38-47%, wollastonite 11-16%, calcite powder 7-11%.
The present invention also provides and has used the above-mentioned manufacture method that has the porcelain pug goods of glaze white jade porcelain pug of one's own, and its manufacture method at least comprises the following steps:
S110: blanking, choose soft material kaolin;
S111: air exercise, described kaolin is put in the male and female mold that waddy is housed and fought each other, described kaolin fragmentation, granularity are diminished;
S112: change slurry, in changing stock tank, add water, will, through in the kaolin inputization stock tank of fighting each other, stir standby simultaneously;
S113: blanking, choose the hard material, described hard material comprises potassium felspar sand, albite, wilkinite, quartz, wollastonite, calcite powder;
S114: ball milling, described hard material is put into to ball milling in ball mill, add high aluminium ball, water simultaneously;
S115: sieve, the hard material after ball milling in S114 is sieved;
S116: mix, the soft material after above-mentionedization slurry, hard material after ball milling are mixed and put into stirrer and fully stirs, the formation mixture, enter S117;
S117: impurity elimination, it is 300 purpose vibration screening machines that the mixture formed in S116 is put into to fineness, removes foreign material, enters S118;
S118: deironing, said mixture is put into to Gauss's magnetic magnetic separator de-ironing and rushed magnetic, mixture is carried out to deironing, enter S119;
S119: press filtration, the mixture after deironing is dropped in suction pit, squeeze into the filter pressing machine through the mud ram pump, become the mud cake that water content is 25% after pressing dry moisture, enter S120;
S120: a pugging, the mud cake that is 25% by above-mentioned water content is put into vacuum deairing machine, the air in mud cake is taken away, to improve the quality of mud cake;
S121: old, the mud cake after the pugging of above-mentioned S120 step is packed in plastics bag and placed 7-15 days, make pug fully react and mix, to improve its processability, improve plasticity-;
S122: secondary pugging, the same S120 of its operation steps;
S123: moulding, make base substrate;
S124: drying, by the body drying of making;
S125: loading of kiln is fired, and the base substrate after moulding is put in kiln, in kiln, once forms by a firing;
S126: finished product.
Be preferably, in described S111 air exercise step, the described waddy diameter that the male and female mold of waddy is housed is 25-45 centimetre.
Be preferably, in described S112ization slurry step, the part by weight of described soft material and water is 1: 2.5.
Be preferably, in described S111 air exercise step, it is 24-36 hour that described kaolin is put into the time of fighting each other in the male and female mold that waddy is housed.
Be preferably, in described S114 ball milling step, the part by weight of described hard material, high aluminium ball, water is 1: 1.5: 0.5.
Be preferably, described S115 sieves in step, and described hard material can be all 250 purpose sieves by fineness, and while by fineness, being 300 purpose sieve, percent of pass is not 1%.
Be preferably, in described S118 deironing step, the magneticstrength of described Gauss's magnetic magnetic separator de-ironing is 20000-30000 Gauss.
Be preferably, described S125 loading of kiln is fired in step, and the firing temperature of described kiln is at 1260 ℃-1310 ℃.
The chemical composition of porcelain pug goods of the present invention is by weight percentage: SiO
268-75%; Al
2o
37.8-11%; Fe
2o
30.07-0.20%; CaO8-11.5%; MgO0.6-1.2%; K
2o+Na
2o1.6-2.5%; Loss on ignition 6-8%.
Compared with prior art, the superior effect that has the manufacture method of glaze white jade porcelain pug and porcelain pug goods of one's own of the present invention is: the manufacture method of porcelain pug goods of the present invention is fired traditional secondary to change into once and is fired, reduced energy consumption, reduced the quantity discharged of carbon, and removed the processing sequence of enamel frit makeing, glazing, reduced the quantity discharged of " three wastes ", manpower have been saved, the leaching ability of heavy metal amounts such as plumbous cadmium of bringing into have been reduced in glaze, its porcelain pug goods are sparkling and crystal-clear as beautiful, and section is conchoidal without the cutting edge of a knife or a sword mouth.Porcelain pug goods of the present invention have green, environmental protection, and safety, can be applicable to tableware porcelain, household china, artistic porcelain, decorative ceramics, the ceramic industries such as lighting apparatus porcelain.
The accompanying drawing explanation
Be the manufacturing approach craft schema of porcelain pug goods of the present invention as shown in drawings.
Embodiment
Below in conjunction with accompanying drawing, the specific embodiment of the invention is described in further detail.
The invention provides and have glaze white jade porcelain pug of one's own, its porcelain pug formula is by weight percentage: kaolin 13-21%, feldspar 14-20%, wilkinite 2-7%, quartzy 38-47%, wollastonite 11-16%, calcite powder 7-11%.
The present invention also provides and has used the above-mentioned manufacture method that has the porcelain pug goods of glaze white jade porcelain pug of one's own, and its manufacture method comprises the following steps:
S110: blanking, choose soft material kaolin 140kg;
S111: air exercise, described kaolin is put in the male and female mold that waddy is housed and fought each other, described kaolin fragmentation, granularity are diminished; The described waddy diameter that the male and female mold of waddy is housed is 25-45 centimetre, and it is 24-36 hour that described kaolin is put into the time of fighting each other in the male and female mold that waddy is housed; The described male and female mold that waddy is housed is driven by motor;
S112: change slurry, in changing stock tank, add water 350kg, will, through in the kaolin 140kg inputization stock tank of fighting each other, stir standby simultaneously; The part by weight of described soft material and water is 1: 2.5;
S113: blanking, choose the hard material, described hard material comprises potassium felspar sand 30kg, albite 140kg, wilkinite 50kg, quartzy 440kg, wollastonite 120kg, calcite powder 80kg;
S114: ball milling, described hard material is put into to ball milling in ball mill, add high aluminium ball, water simultaneously; The part by weight of described hard material, high aluminium ball, water is 1: 1.5: 0.5; The aluminium content of described high aluminium ball is 92%; Described ball mill is driven by motor, and described high aluminium ball is grinding medium, drives described high aluminium ball during described ball mill work and rotates in ball mill, and described high aluminium ball and described hard material push mutually, grind, thereby described hard material is ground; Described high aluminium ball and the extruding of hard material, the time of grinding are 24-36 hour;
S115: sieve, above-mentioned hard material after ball milling is sieved, described hard material can be all 250 purpose sieves by fineness after described ball mill grinding, and while by fineness, being 300 purpose sieve, percent of pass is not 1%;
S116: mix, the soft material after above-mentionedization slurry, hard material after ball milling are mixed and put into stirrer and fully stirs, the formation mixture, enter S117;
S117: impurity elimination, it is 300 purpose vibration screening machines that said mixture is put into to fineness, removes foreign material, enters S118;
S118: deironing, mixture in S117 is put into to Gauss's magnetic magnetic separator de-ironing that magneticstrength is 20000-30000 Gauss and rushed magnetic, and mixture is carried out to deironing, enter S119;
S119: press filtration, the mixture after deironing is dropped in suction pit, squeeze into the filter pressing machine through the mud ram pump, become the mud cake that water content is 25% after pressing dry moisture, enter S120;
S120 a: pugging; The mud cake that is 25% by above-mentioned water content is put into vacuum deairing machine, and the air in mud cake is taken away, to improve the quality of pug, strengthens the plasticity of pug;
S121: old; Mud cake after the pugging of above-mentioned S120 step is packed in plastics bag and placed 7-15 days, make pug fully react and mix, to improve its processability, improve plasticity-;
S122: secondary pugging; The same S120 of its operation steps, its purpose is in order further to improve pug plasticity-equally;
S123: moulding, make base substrate;
S124: drying, by the body drying of making;
S125: loading of kiln is fired, and the base substrate after moulding is put in kiln to once-firing type in the kiln of 1260 ℃-1310 ℃;
S126: finished product.
The pug made with the composition of raw materials that has glaze white jade porcelain pug of one's own of the present invention, can carry out easily the plastotype moulding and become base substrate, described base substrate has good slip casting, roll extrusion, the plastic pressure forming performance, described base substrate can be in 1260 ℃ of-1310 ℃ of scopes be fired into the porcelain pug goods under oxidizing atmosphere and/or reducing atmosphere, is specially the implicit light green in pure white position of porcelain pug goods in oxidizing atmosphere, the implicit nattierblue in the pure white position of porcelain pug goods in reducing atmosphere.
The chemical composition of porcelain pug goods of the present invention is by weight percentage: SiO
268-75%; Al
2o
37.8-11%; Fe
2o
30.07-0.20%; CaO8-11.5%; MgO0.6-1.2%; K
2o+Na
2o1.6-2.5%; Loss on ignition 6-8%.
The mechanical means related in the manufacture method of porcelain pug goods of the present invention is equipment of the prior art, as mechanical means such as male and female mold, ball mill, stirrer, vibration screening machine, Gauss's magnetic magnetic separator de-ironing, mud ram pump, filter pressing machine, vacuum deairing machines, for example application number is 201020246015.3 to disclose a kind of domestic ceramics vacuum deairing machine.
Adopt cheap wollastonite in the formula that has glaze white jade porcelain pug of one's own of the present invention, calcite powder, quartzy part has substituted rare high grade kaolinite resource, has reduced production cost; The manufacture method of porcelain pug goods of the present invention is reduced to " once firing " by original " secondary is fired " simultaneously, has simplified production technique, and the lead and cadmium free leaching ability of heavy metal, energy-saving and environmental protection, efficient.
The present invention is not limited to above-mentioned embodiment, in the situation that do not deviate from flesh and blood of the present invention, any distortion it may occur to persons skilled in the art that, improvement, replacement all fall into scope of the present invention.
Claims (9)
1. have glaze white jade porcelain pug of one's own, it is characterized in that, its porcelain pug formula is by weight percentage: kaolin 13-21%, feldspar 14-20%, wilkinite 2-7%, quartzy 38-47%, wollastonite 11-16%, calcite powder 7-11%.
2. the manufacture method of porcelain pug goods, adopted the glaze white jade porcelain pug that has of one's own claimed in claim 1, and described manufacture method at least comprises the following steps:
S110: blanking, choose soft material kaolin;
S111: air exercise, described kaolin is put in the male and female mold that waddy is housed and fought each other, described kaolin fragmentation, granularity are diminished;
S112: change slurry, in changing stock tank, add water, will, through in the kaolin inputization stock tank of fighting each other, stir standby simultaneously;
S113: blanking, choose the hard material, described hard material comprises potassium felspar sand, albite, wilkinite, quartz, wollastonite, calcite powder;
S114: ball milling, described hard material is put into to ball milling in ball mill, add high aluminium ball, water simultaneously;
S115: sieve, above-mentioned hard material after ball milling is sieved;
S116: mix, the soft material after above-mentionedization slurry, hard material after ball milling are mixed and put into stirrer and fully stirs, the formation mixture, enter S117;
S117: impurity elimination, it is 300 purpose vibration screening machines that said mixture is put into to fineness, removes foreign material, enters S118;
S118: deironing, will put into Gauss's magnetic magnetic separator de-ironing through the mixture of above-mentioned S117 step and be rushed magnetic, mixture is carried out to deironing, enter S119;
S119: press filtration, the mixture after deironing is dropped in suction pit, squeeze into the filter pressing machine through the mud ram pump, become the mud cake that water content is 25% after pressing dry moisture, enter S120;
S120: a pugging, the mud cake that is 25% by above-mentioned water content is put into vacuum deairing machine, and the air in mud cake is taken away;
S121: old, the mud cake after the pugging of above-mentioned S120 step is packed in plastics bag and placed 7-15 days, make pug fully react and mix;
S122: secondary pugging, the same S120 of its operation steps;
S123: moulding, make base substrate;
S124: drying, by the body drying of making;
S125: loading of kiln is fired, and the base substrate after moulding is put in kiln, in kiln, once forms by a firing;
S126: finished product.
3. the manufacture method of porcelain pug goods according to claim 2, is characterized in that, in described S111 air exercise step, the described waddy diameter that the male and female mold of waddy is housed is 25-45 centimetre.
4. the manufacture method of porcelain pug goods according to claim 2, is characterized in that, in described S112ization slurry step, the part by weight of described soft material and water is 1: 2.5.
5. the manufacture method of porcelain pug goods according to claim 2, is characterized in that, it is 24-36 hour that kaolin described in described S111 air exercise step is put into the time of fighting each other in the male and female mold that waddy is housed.
6. the manufacture method of porcelain pug goods according to claim 2, is characterized in that, described in described S114 ball milling step, the part by weight of hard material, high aluminium ball, water is 1: 1.5: 0.5.
7. the manufacture method of porcelain pug goods according to claim 2, it is characterized in that, the described S115 material of hard described in step that sieves can be all 250 purpose sieves by fineness after described ball mill grinding, and while by fineness, being 300 purpose sieve, percent of pass is not 1%.
8. the manufacture method of porcelain pug goods according to claim 2, is characterized in that, described in described S118 deironing step, the magneticstrength of Gauss's magnetic magnetic separator de-ironing is 20000-30000 Gauss.
9. the manufacture method of porcelain pug goods according to claim 2, is characterized in that, described S125 loading of kiln fire described in the firing temperature of kiln at 1260 ℃-1310 ℃.
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| CN105819844A (en) * | 2016-03-31 | 2016-08-03 | 谢敬裕 | Mutton-fat jade like spontaneous glaze ceramic, pug and once-firing production process |
| CN105859266A (en) * | 2016-03-31 | 2016-08-17 | 谢敬裕 | Kiln transmutation autogenous glaze Shandong celadon, mud material and method |
| CN105859328A (en) * | 2016-03-31 | 2016-08-17 | 谢敬裕 | Self-glazed ceramic-molded clay body blocking agent and method |
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| CN112408941A (en) * | 2020-11-20 | 2021-02-26 | 龙岩高岭土股份有限公司 | High-whiteness and high-light-transmittance petuntse and preparation method thereof |
| CN113149678A (en) * | 2021-02-21 | 2021-07-23 | 罗焕焕 | High-performance antibacterial domestic ceramic and preparation method thereof |
| CN114105623A (en) * | 2021-08-03 | 2022-03-01 | 湖南仙凤瓷业有限公司 | High-strength jade porcelain pug and preparation method thereof |
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