CN108117372A - A kind of production method of porcelain product compound material and porcelain product - Google Patents

A kind of production method of porcelain product compound material and porcelain product Download PDF

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Publication number
CN108117372A
CN108117372A CN201810020030.7A CN201810020030A CN108117372A CN 108117372 A CN108117372 A CN 108117372A CN 201810020030 A CN201810020030 A CN 201810020030A CN 108117372 A CN108117372 A CN 108117372A
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mud
porcelain product
porcelain
oxide
iron
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滕召华
肖永红
易刚丽
肖滕
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Hunan Great Qiu Nici Skill Co Ltd
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Hunan Great Qiu Nici Skill Co Ltd
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    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00—Clay-wares
    • C04B33/02—Preparing or treating the raw materials individually or as batches
    • C04B33/04—Clay; Kaolin
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00—Clay-wares
    • C04B33/02—Preparing or treating the raw materials individually or as batches
    • C04B33/13—Compounding ingredients
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00—Clay-wares
    • C04B33/24—Manufacture of porcelain or white ware
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3201—Alkali metal oxides or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
    • C04B2235/3206—Magnesium oxides or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
    • C04B2235/3208—Calcium oxide or oxide-forming salts thereof, e.g. lime
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3217—Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3232—Titanium oxides or titanates, e.g. rutile or anatase
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/327—Iron group oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3272—Iron oxides or oxide forming salts thereof, e.g. hematite, magnetite
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3418—Silicon oxide, silicic acids, or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Dispersion Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Compositions Of Oxide Ceramics (AREA)

Abstract

The present invention provides a kind of porcelain product compound material, the composition material formula of composite fluxing agent is formed with potassium feldspar and talcum, especially two kinds of high quality kaolin, potassium feldspar, the combination for burning talcum and quartz and crucial proportioning, it is unstable to not only solve the quality brought with single potassium feldspar composition of raw materials, it also widened firing range, reduced deformation of products probability, make whiteness, the humidity of porcelain, the regularity of product, transparency have obtained significantly being promoted, so as to substantially increase product quality.The present invention also provides a kind of method for being made porcelain product of compound material of above-mentioned porcelain product, manufacture craft is simplified, and technological parameter is easy to control, convenient for large-scale production.

Description

A kind of production method of porcelain product compound material and porcelain product
Technical field
The present invention relates to porcelain product technical fields, particularly, are related to a kind of porcelain product compound material and porcelain system The production method of product.
Background technology
Porcelain product is made in the prior art uses potassium feldspar as flux raw material.
With the variation of current mineral resources, the quality of feldspar worse and worse, high-end porcelain making mineral resources it is fewer and fewer, and using single One potassium feldspar is big for the made product variations of the composition of raw materials of flux, and quality is extremely unstable.
Also there are some disclosed ceramic products in the prior art, it is as follows：
The patent of invention of Application No. 200910190071.1 discloses a kind of ceramic, and manufacturing raw material includes base Material, the chemical composition of blank include：SiO266%~72%, Al2O317%~23%, Fe2O32.5%~4.5%, CaO 0.4%~0.5%, MgO 1%~2%, Na2O 0.18%~0.22%, K2O 2.0%~3.5%, TiO20.75%~ 0.92%, it is described to be weight percentage.The ceramic of the present invention has the excellent energy of resistance to thermal denaturation, after testing, of the invention Ceramic thermal shock resistance is used up to 500 DEG C~550 DEG C so as to be adapted as the heating inner liner of electric soup cooker, electric cooker.
The patent application of Application No. 201210539844.4 discloses a kind of transparent ceramic articles, wherein, ceramic Chemistry composition by weight percent be：SiO2：65~71 parts, A12O3：8~12 parts, Fe2O3：0.05~0.3 part, CaO：6~8 Part, K2O+Na2O：1.5~3 parts, MgF：0.5~1 part, Li2O：0.01~0.5 part, P2O5：1~2 part, GaAs：5~6 parts.
In addition, there are other ceramic porcelains, these ceramics can not meet in actual life to porcelain product Deformation rate, the humidity of porcelain, the demand of the regularity of product and transparency etc..
Therefore, a kind of formula is developed to simplify, the firing range of product can be widened and the porcelain product of product quality can be improved It is of great significance with the production method of compound material and porcelain product.
The content of the invention
It is simplified it is an object of the invention to provide a kind of formula, the firing range of product can be widened and product quality can be improved Porcelain product compound material, specific technical solution is as follows：
A kind of porcelain product compound material, by the first kaolin 35-45%, the second kaolin 20- in terms of mass fraction 35%th, mud is made in potassium feldspar 8-15%, burning talcum 5-10% and quartz 20-25%；
Being calculated in mass percent first kaolin includes following components：Silica 55.5%, alundum (Al2O3) 32.12%th, di-iron trioxide 0.11%, calcium oxide 0.86%, magnesia 0.5%, potassium oxide 1.5%, sodium oxide molybdena 0.42% with And titanium oxide 0.04%, burning decrement 8.95%；
Being calculated in mass percent second kaolin includes following components：Silica 69.5%, alundum (Al2O3) 21%th, di-iron trioxide 0.09%, calcium oxide 0.9%, magnesia 0.5%, potassium oxide 1.5%, sodium oxide molybdena 1.42% and oxygen Change titanium 0.04%, burning decrement 5.05%.
Preferred in above technical scheme, being calculated in mass percent mud includes following components：Silica 54.5%, three Al 2 O 33%, di-iron trioxide 0.09%, calcium oxide 0.86%, magnesia 1.5%, potassium oxide 1.5%, sodium oxide molybdena 0.42% and titanium oxide 0.04%, burning decrement 8.09%.
Using the porcelain product compound material of the present invention, with potassium feldspar and the composition material of talcum formation composite fluxing agent Formula, especially two kinds of high quality kaolin, potassium feldspar, the combination for burning talcum and quartz and crucial proportioning, not only solves The quality brought with single potassium feldspar composition of raw materials is unstable, has also widened firing range, has reduced deformation of products probability, has made The whiteness of porcelain, humidity, the regularity of product, transparency have obtained significantly being promoted, so as to substantially increase product quality.
The second object of the present invention discloses a kind of side that porcelain product is made of above-mentioned porcelain product compound material Method specifically includes following steps：
The first step, ore dressing remove the impurity being made in the raw material of mud；
Talcum is fired to 1320 DEG C by second step, is ground to 320 mesh sieve margins less than 0.5%, is obtained talcum powder；
3rd step uses the ratio of pellet water as 1:2:1.0-2.0:1 ratio carries out ball milling, Ball-milling Time 25-40 Hour, mud is obtained, mud crosses 325 mesh sieve margins as 0.75%-0.8%；
The mud that Baume concentration is 38-42 Baume degrees is made in 4th step；
5th step sieves mud, except obtaining mud cake after iron and press filt；
6th step obtains porcelain product by the thick pugging of vacuum, aging and vacuum fine pugging successively.
It is preferred in above technical scheme, in the 5th step：It was three-deck vibrating screen to sieve, and sieving order is mistake successively 220 mesh sieves cross 220 mesh sieves and cross 250 mesh sieves；It is described except iron using magnetic separator de-ironing carry out, except the iron time be 2.0-5.0 it is small when； The press filt is carried out using slip drying press, and slip drying press pressure is 0.8-1.0MPa；
Mud is added in the mud of electrolyte additive formation 38-42 Baume degrees, electrolyte additive in the 4th step The electrolyte mixture with sodium carbonate is formed at least one of waterglass, sodium humate, roasting glue and water-reducing agent.
It is preferred in above technical scheme, in the 6th step：The thick pugging of vacuum and time of the vacuum fine pugging Number is 3-8 times；When the aging time is 24-30 small.
Using the production method of the present invention, effect is：Manufacture craft is simplified, and technological parameter is easy to control, convenient for large-scale Production.
In addition to objects, features and advantages described above, the present invention also has other objects, features and advantages. Below with reference to embodiment, the present invention is described in further detail.
Specific embodiment
The present invention is described in detail with reference to embodiments, but the present invention can limit and cover according to claim The multitude of different ways of lid is implemented.
Embodiment 1：
A kind of porcelain product, the mud used are calculated in mass percent including following components：Silica 54.5%, three Al 2 O 33%, di-iron trioxide 0.09%, calcium oxide 0.86%, magnesia 1.5%, potassium oxide 1.5%, sodium oxide molybdena 0.42% and titanium oxide 0.04%, burning decrement 8.09%.
Above-mentioned mud is made of following component：By the first kaolin 35%, the second kaolin 30%, potassium in terms of mass fraction Mud is made in feldspar 8%, burning talcum 5% and quartz 22%；Being calculated in mass percent first kaolin is included with the following group Point：Silica 55.5%, alundum (Al2O3) 32.12%, di-iron trioxide 0.11%, calcium oxide 0.86%, magnesia 0.5%th, potassium oxide 1.5%, sodium oxide molybdena 0.42% and titanium oxide 0.04%, burning decrement 8.95%；With mass percent Counting second kaolin includes following components：Silica 69.5%, alundum (Al2O3) 21%, di-iron trioxide 0.09%, Calcium oxide 0.9%, magnesia 0.5%, potassium oxide 1.5%, sodium oxide molybdena 1.42% and titanium oxide 0.04%, burning decrement are 5.05%.
The specific manufacturing process of above-mentioned porcelain product comprises the following steps：
The first step, ore dressing remove the impurity being made in the raw material of mud, and impurity is removed using existing method；
Talcum is fired to 1320 DEG C by second step, is ground to 320 mesh sieve margins less than 0.5%, is obtained talcum powder；
3rd step uses the ratio of pellet water as 1：2：1.0-2.0：1 ratio carries out ball milling, Ball-milling Time 25-40 Hour, mud is obtained, mud crosses 325 mesh sieve margins as 0.75%-0.8%；
The mud that Baume concentration is 38-42 Baume degrees is made in 4th step, is specifically：Mud is added in into electrolyte additive The mud of 38-42 Baume degrees is formed, electrolyte additive is at least one in waterglass, sodium humate, roasting glue and water-reducing agent Kind forms the electrolyte mixture with sodium carbonate；
5th step sieves mud, except mud cake is obtained after iron and press filt, is specifically：It was three-deck vibrating screen to sieve, mistake Sieve order is to cross 220 mesh sieves successively, cross 220 mesh sieves and cross 250 mesh sieves；It is described to be carried out except iron using magnetic separator de-ironing, except the iron time For 2.0-5.0 it is small when；The press filt is carried out using slip drying press, and slip drying press pressure is 0.8-1.0MPa；
6th step obtains porcelain product by the thick pugging of vacuum, aging and vacuum fine pugging successively, wherein：The vacuum The number of thick pugging and the vacuum fine pugging be 3-8 time (vacuum pugging and aging be the method for using the prior art)； When the aging time is 24-30 small.
Using the technical solution of the present embodiment, effect is：
1st, the present invention intends the composition of raw materials using potassium feldspar and talcum as complex composition of purport, is improving high-end serial porcelain While matter product property, more important is the selection markets for also having widened porcelain making.All kinds of porcelain making mineral resources is allowed to have obtained more rationally Utilization.
2nd, the formula and method of the present embodiment, the performance parameter of porcelain product are as follows：(1) quality has reached more than 80%； (2) products made thereby whiteness has reached 92%, and glossiness has reached 90%, and water absorption rate is less than 0.2%；(3) thermal stability：From 180 It DEG C does not split once to 20 DEG C of heat exchanges；(4) with the lead of food-contacting surface, quantity of cadmium release：Lead release is not more than 0.15mg/L, cadmium Stripping quantity is not more than 0.10mg/L；(5) highest will be burnt till into porcelain and has widened 30 DEG C or so with minimum temperature value range, will be solved It is problem using single potassium feldspar as the one of the made product of composition of raw materials, there is very high application value.
The foregoing is only a preferred embodiment of the present invention, is not intended to limit the invention, for the skill of this field For art personnel, the invention may be variously modified and varied.Within the spirit and principles of the invention, that is made any repaiies Change, equivalent substitution, improvement etc., should all be included in the protection scope of the present invention.

Claims (5)

1. a kind of porcelain product compound material, it is characterised in that：By the first kaolin 35-45%, second in terms of mass fraction Mud is made in kaolin 20-35%, potassium feldspar 8-15%, burning talcum 5-10% and quartz 20-25%；
Being calculated in mass percent first kaolin includes following components：Silica 55.5%, alundum (Al2O3) 32.12%th, di-iron trioxide 0.11%, calcium oxide 0.86%, magnesia 0.5%, potassium oxide 1.5%, sodium oxide molybdena 0.42% with And titanium oxide 0.04%, burning decrement 8.95%；
Being calculated in mass percent second kaolin includes following components：Silica 69.5%, alundum (Al2O3) 21%, three Aoxidize two iron 0.09%, calcium oxide 0.9%, magnesia 0.5%, potassium oxide 1.5%, sodium oxide molybdena 1.42% and titanium oxide 0.04%, burning decrement 5.05%.
2. porcelain product compound material according to claim 1, it is characterised in that：Being calculated in mass percent mud includes Following components：Silica 54.5%, alundum (Al2O3) 33%, di-iron trioxide 0.09%, calcium oxide 0.86%, magnesia 1.5%th, potassium oxide 1.5%, sodium oxide molybdena 0.42% and titanium oxide 0.04%, burning decrement 8.09%.
3. a kind of preparation method of porcelain product, it is characterised in that：Using the mud as described in claim 1-2 any one, Specifically include following steps：
The first step, ore dressing remove the impurity being made in the raw material of mud；
Talcum is fired to 1320 DEG C by second step, is ground to 320 mesh sieve margins less than 0.5%, is obtained talcum powder；
3rd step uses the ratio of pellet water as 1:2:1.0-2.0:1 ratio carries out ball milling, when Ball-milling Time is 25-40 small, Mud is obtained, mud crosses 325 mesh sieve margins as 0.75%-0.8%；
The mud that Baume concentration is 38-42 Baume degrees is made in 4th step；
5th step sieves mud, except obtaining mud cake after iron and press filt；
6th step obtains porcelain product by the thick pugging of vacuum, aging and vacuum fine pugging successively.
4. the preparation method of porcelain product according to claim 3, it is characterised in that：In 5th step：It sieves and was Three-deck vibrating screen, sieving order are to cross 220 mesh sieves successively, cross 220 mesh sieves and cross 250 mesh sieves；The iron that removes uses magnetic separator de-ironing Carry out, except the iron time for 2.0-5.0 it is small when；The press filt is carried out using slip drying press, and slip drying press pressure is 0.8-1.0MPa；
Mud is added in the mud of electrolyte additive formation 38-42 Baume degrees, electrolyte additive is water in the 4th step At least one of glass, sodium humate, roasting glue and water-reducing agent form the electrolyte mixture with sodium carbonate.
5. the preparation method of porcelain product according to claim 3, it is characterised in that：In 6th step：The vacuum The number of thick pugging and the vacuum fine pugging is 3-8 times；When the aging time is 24-30 small.
CN201810020030.7A 2018-01-09 2018-01-09 A kind of production method of porcelain product compound material and porcelain product Pending CN108117372A (en)

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Cited By (6)

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CN109320209A (en) * 2018-12-06 2019-02-12 湖南大球泥瓷艺有限公司 A kind of production method containing high-quality fine work pug
CN110467431A (en) * 2019-09-10 2019-11-19 恩平市金久圣陶瓷有限公司 A kind of white background ceramic tile
CN112250430A (en) * 2020-08-31 2021-01-22 杨纲雄 Porcelain clay, porcelain and preparation method thereof
CN113443895A (en) * 2020-03-27 2021-09-28 台宜陶瓷（宜兴）有限公司 Production process of open fire pizza tray
CN113501704A (en) * 2021-08-02 2021-10-15 景德镇陶瓷大学 Slurry for pile carving and preparation method and application thereof
CN113511814A (en) * 2020-04-10 2021-10-19 台宜陶瓷（宜兴）有限公司 Production process of gold-sprayed glaze for ceramic products

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CN103435336A (en) * 2013-08-15 2013-12-11 何晓洪 Self-forming glaze white jade porcelain pug and manufacturing method of porcelain pug product
CN103435329A (en) * 2013-08-19 2013-12-11 湖南华联瓷业股份有限公司 Low-water absorption stoneware and production method thereof
CN106316120A (en) * 2016-08-18 2017-01-11 湖南大球泥瓷艺有限公司 Manufacturing technology of large-ball mud high-end art porcelain feldspar glaze
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CN103159456A (en) * 2013-03-27 2013-06-19 福建省德化冠峰耐热瓷有限公司 Ceramic clay material and ceramic product thereof
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CN113501704A (en) * 2021-08-02 2021-10-15 景德镇陶瓷大学 Slurry for pile carving and preparation method and application thereof
CN113501704B (en) * 2021-08-02 2022-05-17 景德镇陶瓷大学 Slurry for pile carving and preparation method and application thereof

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