CN103351953A - Additive for vanilla cigarettes and preparation method thereof - Google Patents
Additive for vanilla cigarettes and preparation method thereof Download PDFInfo
- Publication number
- CN103351953A CN103351953A CN2013102708871A CN201310270887A CN103351953A CN 103351953 A CN103351953 A CN 103351953A CN 2013102708871 A CN2013102708871 A CN 2013102708871A CN 201310270887 A CN201310270887 A CN 201310270887A CN 103351953 A CN103351953 A CN 103351953A
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- China
- Prior art keywords
- vanilla
- weight
- add
- extracting solution
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000009499 Vanilla fragrans Nutrition 0.000 title claims abstract description 68
- 235000012036 Vanilla tahitensis Nutrition 0.000 title claims abstract description 68
- 244000263375 Vanilla tahitensis Species 0.000 title claims abstract description 67
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 24
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 239000000654 additive Substances 0.000 title claims description 17
- 230000000996 additive effect Effects 0.000 title claims description 17
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000006228 supernatant Substances 0.000 claims abstract description 16
- 239000012467 final product Substances 0.000 claims abstract description 8
- 239000011435 rock Substances 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 102000011759 adducin Human genes 0.000 claims description 7
- 108010076723 adducin Proteins 0.000 claims description 7
- 235000020415 coconut juice Nutrition 0.000 claims description 7
- 239000003205 fragrance Substances 0.000 abstract description 6
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 238000000034 method Methods 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 abstract description 2
- 239000001644 vanilla aromatica fruit extract Substances 0.000 abstract 2
- 235000020197 coconut milk Nutrition 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000002386 leaching Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 230000000638 stimulation Effects 0.000 abstract 1
- 239000000779 smoke Substances 0.000 description 5
- 244000061176 Nicotiana tabacum Species 0.000 description 2
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 235000019633 pungent taste Nutrition 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- 241000722824 Ardisia crenata Species 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 241000732800 Cymbidium Species 0.000 description 1
- 206010013911 Dysgeusia Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241000233855 Orchidaceae Species 0.000 description 1
- 244000290333 Vanilla fragrans Species 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
- Seasonings (AREA)
Abstract
The invention discloses a preparation method of addictive for vanilla cigarettes. The preparation method comprises following steps: 1) putting vanilla into coconut milk and adding rock sugar, immersing for 3 to 5 days; 2) adding water into the soaked vanilla and leaching for 1 to 3 hours, filtering and obtaining vanilla extract; 3) vacuum condensing the vanilla extract until the weight is 5 to 50% of original weight, and obtaining the vanilla concentrate; 4) adding 95% alcohol into the vanilla concentrate, making the mixture standing for 24 hours, then taking out the supernatant and subjecting the supernatant to a vacuum condensing process until the weight is 5 to 30% of the original weight, and obtaining the final product. The addictive for vanilla cigarettes has the advantages of rich fragrances, good taste, and prominent reduction on stimulation, at the same time, the raw materials are cheap and easy to get, and the production technology is simple.
Description
Technical field
The present invention relates to a kind of cigarette additive, specifically a kind of vanilla cigarette additive and preparation method thereof.
Background technology
Vanilla originates in African Madagascar tropical rain forest, until 18th century were were just discovered and used, it has another name called vanilla, Herba vanillae Planifoliae, vanilla, chinese cymbidium, is a kind of large-scale the orchid family spice berry in the typical tropical rain forest, and the good reputation of " king of food spice " is arranged.The vanilla of China is to introduce a fine variety from Indonesia nineteen sixty, and is succeeded indoor planting experimentally by Fujian Institute of Subtroical Plant.At present, China has classified vanilla as emphasis and has introduced brainstorm project, and has been introduced a fine variety the provinces such as Hainan, Yunnan, Guangxi, Guangdong.
The fragrance of vanilla is fresh and sweet creamy, makes the people comfortable, joyful, gives off a strong fragrance, enriches, lasting is lasting, long times of aftertaste.The vanilla cigarette additive is applied on the cigarette, plays and enriches cigarette perfume (or spice), the effect of soft, fine and smooth flue gas.But the rich deficiency of its fragrance, pungency is larger.
Summary of the invention
The purpose of this invention is to provide a kind of vanilla cigarette additive and preparation method thereof, the fragrance of this vanilla cigarette additive is abundant, and pungency is little.
Above-mentioned purpose is achieved through the following technical solutions:
A kind of preparation method of vanilla cigarette additive may further comprise the steps:
1) vanilla is cut into the segment of 1 ~ 2cm, puts into the Coconut Juice of 5 ~ 25 times of weight, and add the rock sugar of 0.2 ~ 1 times of weight, soak and took out afterwards in 3 ~ 5 days;
2) add the water of 30 ~ 100 times of weight in the vanilla after soak, lixiviate is 1 ~ 3 hour under 60 ~ 100 ℃ of conditions, filters, and gets the vanilla extracting solution;
3) the vanilla extracting solution is evaporated under 50 ~ 70 ℃ of conditions concentrated before extracting solution weight 5 ~ 50%, obtain the vanilla concentrated solution;
4) add 95% ethanol of 2 ~ 5 times of weight in the vanilla concentrated solution, leave standstill 24 hours after, get supernatant liquor under 40 ~ 60 ℃ of conditions, be evaporated to concentrated before supernatant liquor weight 5 ~ 30%, and get final product.
Preferably, the preparation method of described vanilla cigarette additive may further comprise the steps:
1) vanilla is cut into the segment of 1 ~ 2cm, puts into the Coconut Juice of 10 times of weight, and add the rock sugar of 0.5 times of weight, soak and took out afterwards in 4 days;
2) add the water of 50 times of weight in the vanilla after soak, lixiviate is 2 hours under 90 ℃ of conditions, filters, and gets the vanilla extracting solution;
3) the vanilla extracting solution is evaporated under 60 ℃ of conditions concentrated before extracting solution weight 20%, obtain the vanilla concentrated solution;
4) add 95% ethanol of 4 times of weight in the vanilla concentrated solution, leave standstill 24 hours after, get supernatant liquor under 50 ℃ condition, be evaporated to concentrated before supernatant liquor weight 10%, and get final product.
According to the character of extract, sample is used for cigarette as flavoring essence, 5606.4-1996 operates according to the cigarette standard GB/T.Get blank pipe tobacco, be balance after 48 hours under 60 ± 2% environment in 22 ± 1 ℃ of temperature, relative humidity, distinguish the additive of evenly sprinkling 0.02%, 0.04%, 0.06%, 0.08%, 0.1% on pipe tobacco with atomizer, roll into cigarette, select the cigarette of quality in 0.91 ± 0.02g scope, be that balance was done contrast with the blank cigarette that does not add additive and smoked panel test after 48 hours under 60 ± 2% environment in 22 ± 1 ℃ of temperature, relative humidity again.
Smoke panel test through the specialty personnel that smoke panel test, the result is as follows:
The fragrance of the vanilla cigarette additive that the present invention makes is abundant, and mouthfeel alcohol just stimulates obviously to reduce.The present invention also has raw material and is easy to get at a low price, the simple advantage of production technique.
Embodiment
The present invention will be further described below in conjunction with example:
Embodiment 1
The preparation method of vanilla cigarette additive may further comprise the steps:
1) vanilla is cut into the segment of 1 ~ 2cm, puts into the Coconut Juice of 10 times of weight, and add the rock sugar of 0.5 times of weight, soak and took out afterwards in 4 days;
2) add the water of 50 times of weight in the vanilla after soak, lixiviate is 2 hours under 90 ℃ of conditions, filters, and gets the vanilla extracting solution;
3) the vanilla extracting solution is evaporated under 60 ℃ of conditions concentrated before extracting solution weight 20%, obtain the vanilla concentrated solution;
4) add 95% ethanol of 4 times of weight in the vanilla concentrated solution, leave standstill 24 hours after, get supernatant liquor under 50 ℃ condition, be evaporated to concentrated before supernatant liquor weight 10%, and get final product.
Smoke panel test through specialty, the result is as follows:
Embodiment 2
A kind of preparation method of vanilla cigarette additive may further comprise the steps:
1) vanilla is cut into the segment of 1 ~ 2cm, puts into the Coconut Juice of 5 times of weight, and add the rock sugar of 0.2 times of weight, soak and took out afterwards in 5 days;
2) add the water of 30 times of weight in the vanilla after soak, lixiviate is 3 hours under 60 ℃ of conditions, filters, and gets the vanilla extracting solution;
3) the vanilla extracting solution is evaporated under 50 ℃ of conditions concentrated before extracting solution weight 50%, obtain the vanilla concentrated solution;
4) add 95% ethanol of 2 times of weight in the vanilla concentrated solution, leave standstill 24 hours after, get supernatant liquor under 40 ℃ of conditions, be evaporated to concentrated before supernatant liquor weight 30%, and get final product.
Smoke panel test through specialty, the result is as follows:
Embodiment 3
A kind of preparation method of vanilla cigarette additive may further comprise the steps:
1) vanilla is cut into the segment of 1 ~ 2cm, puts into the Coconut Juice of 25 times of weight, and add the rock sugar of 1 times of weight, soak and took out afterwards in 3 days;
2) add the water of 100 times of weight in the vanilla after soak, lixiviate is 1 hour under 100 ℃ of conditions, filters, and gets the vanilla extracting solution;
3) the vanilla extracting solution is evaporated under 70 ℃ of conditions concentrated before extracting solution weight 5%, obtain the vanilla concentrated solution;
4) add 95% ethanol of 5 times of weight in the vanilla concentrated solution, leave standstill 24 hours after, get supernatant liquor under 60 ℃ of conditions, be evaporated to concentrated before supernatant liquor weight 5%, and get final product.
Smoke panel test through specialty, the result is as follows:
Claims (2)
1. the preparation method of a vanilla cigarette additive is characterized in that may further comprise the steps:
1) vanilla is cut into the segment of 1 ~ 2cm, puts into the Coconut Juice of 5 ~ 25 times of weight, and add the rock sugar of 0.2 ~ 1 times of weight, soak and took out afterwards in 3 ~ 5 days;
2) add the water of 30 ~ 100 times of weight in the vanilla after soak, lixiviate is 1 ~ 3 hour under 60 ~ 100 ℃ of conditions, filters, and gets the vanilla extracting solution;
3) the vanilla extracting solution is evaporated under 50 ~ 70 ℃ of conditions concentrated before extracting solution weight 5 ~ 50%, obtain the vanilla concentrated solution;
4) add 95% ethanol of 2 ~ 5 times of weight in the vanilla concentrated solution, leave standstill 24 hours after, get supernatant liquor under 40 ~ 60 ℃ of conditions, be evaporated to concentrated before supernatant liquor weight 5 ~ 30%, and get final product.
2. the preparation method of vanilla cigarette additive according to claim 1 is characterized in that may further comprise the steps:
1) vanilla is cut into the segment of 1 ~ 2cm, puts into the Coconut Juice of 10 times of weight, and add the rock sugar of 0.5 times of weight, soak and took out afterwards in 4 days;
2) add the water of 50 times of weight in the vanilla after soak, lixiviate is 2 hours under 90 ℃ of conditions, filters, and gets the vanilla extracting solution;
3) the vanilla extracting solution is evaporated under 60 ℃ of conditions concentrated before extracting solution weight 20%, obtain the vanilla concentrated solution;
4) add 95% ethanol of 4 times of weight in the vanilla concentrated solution, leave standstill 24 hours after, get supernatant liquor under 50 ℃ condition, be evaporated to concentrated before supernatant liquor weight 10%, and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310270887.1A CN103351953B (en) | 2013-06-28 | 2013-06-28 | Additive for vanilla cigarettes and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310270887.1A CN103351953B (en) | 2013-06-28 | 2013-06-28 | Additive for vanilla cigarettes and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103351953A true CN103351953A (en) | 2013-10-16 |
| CN103351953B CN103351953B (en) | 2014-11-26 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310270887.1A Active CN103351953B (en) | 2013-06-28 | 2013-06-28 | Additive for vanilla cigarettes and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN103351953B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104232313A (en) * | 2014-09-25 | 2014-12-24 | 秦富英 | Flowery extract |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102051266A (en) * | 2010-12-13 | 2011-05-11 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of vanilla perfume for cigarettes |
-
2013
- 2013-06-28 CN CN201310270887.1A patent/CN103351953B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102051266A (en) * | 2010-12-13 | 2011-05-11 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of vanilla perfume for cigarettes |
Non-Patent Citations (2)
| Title |
|---|
| 陈德新: "香荚兰豆专题系列之四———香荚兰豆初级与深度加工及其应用", 《香料香精化妆品》 * |
| 陈德新: "香荚兰豆专题系列之四———香荚兰豆在卷烟及食品中的应用", 《香料香精化妆品》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104232313A (en) * | 2014-09-25 | 2014-12-24 | 秦富英 | Flowery extract |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103351953B (en) | 2014-11-26 |
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