CN103330670A - Ethanol-free perfume - Google Patents
Ethanol-free perfume Download PDFInfo
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- CN103330670A CN103330670A CN2013102260935A CN201310226093A CN103330670A CN 103330670 A CN103330670 A CN 103330670A CN 2013102260935 A CN2013102260935 A CN 2013102260935A CN 201310226093 A CN201310226093 A CN 201310226093A CN 103330670 A CN103330670 A CN 103330670A
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- ethanol
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- celsius
- ethyl acetate
- purified water
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Abstract
The invention relates to a perfume, and particularly relates to an ethanol-free perfume. The ethanol-free perfume comprises the following components in percentage by weight: 0.10%-0.50% of natural musk, 0.50%-1.50% of ethyl acetate, 10.00%-20.00% of rosebuds, 2.00%-8.00% of laurel flowers, 1.00%-3.00% of lavender, 4.00%-8.00% of polyethylene glycol 400 and the balance of purified water. The ethanol-free perfume disclosed by the invention overcomes the defect that ethanol as a solution medium is inflammable by combining the polyethylene glycol 400, ethyl acetate and the purified water as the solution medium, adopts the musk, roses, the laurel flowers and the lavender as the components of an aroma source, is reasonable in combination and prevents the component dissipation loss from being caused by high temperature by adopting a low-temperature operation mode in process production. The prepared perfume is pleasant in aroma, limpid in color, large in aroma diffusion radius and suitable for a human body or environment spraying.
Description
Technical field
The present invention relates to for daily use chemicals product field, refering in particular to is a kind of perfume that does not contain ethanol, is used for human body use or environment and sprays.
Background technology
The kind of perfume is many at present, and except the main component difference, most of perfume contains the alcohol type composition, and main cause is the ethanol low price, has good volatility, and is soluble in water, also is the best solvent of aromatics liposoluble substance simultaneously, is widely used.Adopt ethanol can promote the organic principle dissolving as solvent, that avoids occurring in the storage process separates out or layering.But the negative effect that ethanol brings as solvent also is very apparent.As inflammable problem, responsive colony allergic problem etc.For the purpose of safety, some travelling safety checks also require the quantity of these type of article is limited.For this reason, the perfume that proposes a kind of soft composition can carry out refinement with perfume market, agrees with the demand of different crowd, is conducive to strengthen competitiveness of product.For this reason, the present invention fully studies from composition combination and solvent composition aspect, proposes a kind of perfume of soft composition.
Summary of the invention
The present invention adopts PEG400, and ethyl acetate and purified water compatibility avoid using ethanol as the deficiency of solvent as solvent.Adopt Moschus, Flos Rosae Rugosae, month Flos Osmanthi Fragrantis and lavandula angustifolia are as the composition in fragrant source.Consider that mainly micro-Moschus becomes branch to discharge the gonadal hormone factor of trace, mainly transmit people's bio information when using as perfume, have the effect that the quickening of people's heart rate, blood pressure drops, respiratory frequency and the degree of depth are increased, user and contactee can produce comfortable joyful sense; Effect was clear and definite, also as safe as a house when trace used.Flos Rosae Rugosae as tradition, classical fragrant derived components considers that mainly the use crowd is more extensive, its abnormal smells from the patient fragrance, Hui Tian always as the main fragrant derived components of most of perfume, and stands long-term market test.Month Flos Osmanthi Fragrantis and lavandula angustifolia fragrance are dense, are easy to diffusion, except pleasant aroma own, can also improve the diffusion radius of perfume integral body as the carrier of Moschus and the diffusion of Flos Rosae Rugosae fragrance.A kind of perfume that does not contain ethanol of special proposition.It comprises following component by weight percentage: natural Moschus 0.10%-0.50%; Ethyl acetate 0.50%-1.50%; Rosebud 10.00%-20.00%; Moon Flos Osmanthi Fragrantis 2.00%-8.00%; Lavandula angustifolia 1.00%-3.00%; PEG400 4.00%-8.00%; Other is purified water.
The present invention is achieved in that
1, by weight percentage with natural Moschus 0.10%-0.50%; Ethyl acetate 0.50%-1.50% precision is weighed, and after refrigerator and cooled Celsius about 10 ℃ is hidden half an hour, Moschus is placed on the ethyl acetate that glass mortar adds half grinds, after five minutes, with liquid filtering.Residue adds remaining half ethyl acetate to be continued to grind, after three minutes, and liquid filtering, with last time liquid merging, standby as liquid 1.
2, by weight percentage with rosebud 10.00%-20.00%; Moon Flos Osmanthi Fragrantis 2.00%-8.00%; Lavandula angustifolia 1.00%-3.00%; Cold preservation under 10 ℃ of conditions Celsius after the pulverizer of employing band cold water circulation is pulverized, adds multi-function extractor, 50 ℃-65 ℃ insulations Celsius 24 hours, keep vacuum 0.3-0.5MPa, 7 ℃ of recirculated waters cooling Celsius, in collecting tank, collect fraction, standby as liquid 2.
3, PEG400 4.00%-8.00% that will be by weight percentage, liquid 1, liquid 2 join in the residue purified water, stir under 10 ℃ of conditions, filter with the filter in suitable aperture, namely.
Concrete embodiment:
Embodiment 1
1, by weight percentage with natural Moschus 0.20%; Ethyl acetate 0.50% precision is weighed, and after refrigerator and cooled Celsius about 10 ℃ is hidden half an hour, Moschus is placed on glass mortar adding ethyl acetate 0.25% grinds, after five minutes, with liquid filtering.Residue adds remaining ethyl acetate 0.25% to be continued to grind, after three minutes, and liquid filtering, with last time liquid merging, standby as liquid 1.
2, by weight percentage with rosebud 20.00%; Month Flos Osmanthi Fragrantis 5.00%; Lavandula angustifolia 3.00%; Cold preservation under 10 ℃ of conditions Celsius after the pulverizer of employing band cold water circulation is pulverized, adds multi-function extractor, 50 ℃-65 ℃ insulations Celsius 24 hours, keep vacuum 0.3-0.5MPa, 7 ℃ of recirculated waters cooling Celsius, in collecting tank, collect fraction, standby as liquid 2.
3, PEG400 7.00% that will be by weight percentage, liquid 1, liquid 2 join in the residue purified water, in 10 ℃ of insulations jar, stir, and be the filter filtration of 0.5um with the aperture, be filled into suitable container.
Embodiment 2
1, by weight percentage with natural Moschus 0.50%; Ethyl acetate 1.50% precision is weighed, and after refrigerator and cooled Celsius about 10 ℃ is hidden half an hour, Moschus is placed on the ethyl acetate that glass mortar adds half grinds, after five minutes, with liquid filtering.Residue adds remaining half ethyl acetate to be continued to grind, after three minutes, and liquid filtering, with last time liquid merging, standby as liquid 1.
2, by weight percentage with rosebud 18.00%; Month Flos Osmanthi Fragrantis 6.00%; Lavandula angustifolia 2.00%; Cold preservation under 10 ℃ of conditions Celsius after the pulverizer of employing band cold water circulation is pulverized, adds multi-function extractor, 50 ℃-65 ℃ insulations Celsius 24 hours, keep vacuum 0.3-0.5MPa, 7 ℃ of recirculated waters cooling Celsius, in collecting tank, collect fraction, standby as liquid 2.
3, general's PEG400 4.00% by weight percentage, liquid 1, liquid 2 join in the residue purified water, under 10 ℃ of conditions, stirs, be the filter filtration of 0.22um with the aperture, fill gets final product.
The present invention adopts PEG400, ethyl acetate and purified water compatibility be as solvent, has avoided the deficiency of ethanol and sensitization inflammable as solvent.Moschus, Flos Rosae Rugosae, month Flos Osmanthi Fragrantis and lavandula angustifolia are as the composition in fragrant source, and prescription compatibility of medicines is reasonable.In the explained hereafter, adopt the low-temperature operation mode, prevent that high temperature from causing the loss of composition loss.The perfume pleasant aroma who makes, limpid in sight, under the combined effect of multiple composition, fragrance diffusion radius is big, and lasting fragrance is applicable to that human body uses or environment sprays.
Claims (3)
1. a perfume that does not contain ethanol is characterized in that it comprises following component by weight percentage: natural Moschus 0.10%-0.50%; Ethyl acetate 0.50%-1.50%; Rosebud 10.00%-20.00%; Moon Flos Osmanthi Fragrantis 2.00%-8.00%; Lavandula angustifolia 1.00%-3.00%; PEG400 4.00%-8.00%; Other is purified water.
2. according to the described a kind of manufacture method that does not contain the perfume of ethanol of claim 1, it is characterized in that: by weight percentage natural Moschus, ethyl acetate precision are weighed, after refrigerator and cooled Celsius about 10 ℃ is hidden half an hour, grind at glass mortar.
3. according to the described a kind of manufacture method that does not contain the perfume of ethanol of claim 1, it is characterized in that: with rosebud, month Flos Osmanthi Fragrantis, lavandula angustifolia cold preservation under 10 ℃ of conditions Celsius, adopt the pulverizer of band cold water circulation to pulverize, add multi-function extractor, 50 ℃-65 ℃ insulations Celsius 24 hours, keep vacuum 0.3-0.5MPa, fraction is collected in 7 ℃ of recirculated waters cooling Celsius in collecting tank.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013102260935A CN103330670A (en) | 2013-06-08 | 2013-06-08 | Ethanol-free perfume |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013102260935A CN103330670A (en) | 2013-06-08 | 2013-06-08 | Ethanol-free perfume |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103330670A true CN103330670A (en) | 2013-10-02 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2013102260935A Pending CN103330670A (en) | 2013-06-08 | 2013-06-08 | Ethanol-free perfume |
Country Status (1)
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| CN (1) | CN103330670A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104173224A (en) * | 2013-12-13 | 2014-12-03 | 金玛瑙香水（明光）有限公司 | Ethanol-free perfume |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0195199A (en) * | 1987-10-06 | 1989-04-13 | Duskin Co Ltd | Deodorizing and stainproofing agent for flush toilet |
| JPH02242899A (en) * | 1989-03-15 | 1990-09-27 | Lion Corp | Aroma-retaining composition |
| WO2011029895A2 (en) * | 2009-09-11 | 2011-03-17 | Givaudan Sa | Odour compounds |
| CN102028646A (en) * | 2010-11-23 | 2011-04-27 | 陕西师范大学 | Thyme perfume |
| CN103054756A (en) * | 2012-12-31 | 2013-04-24 | 义乌市美之源化妆品有限公司 | Ethanol-free perfume |
-
2013
- 2013-06-08 CN CN2013102260935A patent/CN103330670A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0195199A (en) * | 1987-10-06 | 1989-04-13 | Duskin Co Ltd | Deodorizing and stainproofing agent for flush toilet |
| JPH02242899A (en) * | 1989-03-15 | 1990-09-27 | Lion Corp | Aroma-retaining composition |
| WO2011029895A2 (en) * | 2009-09-11 | 2011-03-17 | Givaudan Sa | Odour compounds |
| CN102028646A (en) * | 2010-11-23 | 2011-04-27 | 陕西师范大学 | Thyme perfume |
| CN103054756A (en) * | 2012-12-31 | 2013-04-24 | 义乌市美之源化妆品有限公司 | Ethanol-free perfume |
Non-Patent Citations (3)
| Title |
|---|
| JOHN M.BLAKEWAY: "水基香水", 《广西轻工业》, no. 2, 31 December 1994 (1994-12-31), pages 48 - 50 * |
| 冯兰宾等: "《化妆品工艺学》", 31 May 1993, article "乳化香水" * |
| 孙宝国等: "《香精概论--生产、配方与应用》", 31 March 2006, article "第三章 日用香精", pages: 156 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104173224A (en) * | 2013-12-13 | 2014-12-03 | 金玛瑙香水（明光）有限公司 | Ethanol-free perfume |
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Application publication date: 20131002 |