CN106821903A - Low alcohol mosquito repellent combination liquid of folium artemisiae argyi and preparation method thereof - Google Patents
Low alcohol mosquito repellent combination liquid of folium artemisiae argyi and preparation method thereof Download PDFInfo
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- CN106821903A CN106821903A CN201611269238.XA CN201611269238A CN106821903A CN 106821903 A CN106821903 A CN 106821903A CN 201611269238 A CN201611269238 A CN 201611269238A CN 106821903 A CN106821903 A CN 106821903A
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- folium artemisiae
- artemisiae argyi
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- repellent
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/02—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings containing insect repellants
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
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- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
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- Pest Control & Pesticides (AREA)
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Abstract
The invention discloses the low alcohol mosquito repellent combination liquid of folium artemisiae argyi, it is characterised in that be made up of following raw material:Octyl methoxycinnamate, plant extraction liquid, mint extract, natural borneol, solubilizer, ethanol, water surplus.The plant extraction liquid includes folium artemisiae argyi, lemon-grass, three kinds of extract solutions of natural plants of rose.Solubilizer used is that the rilanit specials of PEG 40 are formed with sodium cocoyl methyl sodium taurocholate compounding.The dimethyl phthalate of safety is used in mosquito-repellent liquid as effective mosquito component, and is equipped with the active principle of folium artemisiae argyi, lemon-grass, rose extract as antipruritic strong skin, make product while having special fragrant.Product ethanol content is below 15%, and the excitant to skin, mucous membrane is low, flammable also to reduce simultaneously, is conducive to ensureing the personal safety of user.
Description
Technical field
The present invention relates to low alcohol mosquito repellent combination liquid of folium artemisiae argyi and preparation method thereof, belong to daily chemical article preparation field.
Background technology
Folium artemisiae argyi, perennial herb is high 45~120 centimetres.Stem is upright, circular, and matter is hard, and base portion lignifying is soft by canescence
Hair, from middle part above branch.Dan Ye, alternate;The leaf of the lower portion of the stem is withered when blooming;Middle leaf has short handle, and blade ovate is ellipse
Circle, pinniform drastic crack, sliver ellipticity lanceolar, edge tool rough sawn tooth, above dirty-green, it is dilute by white fur, and gather gland
Point, below celadon, it is close by canescence fine hair;The leaf stockless on nearly stem top, full edge does not divide blade completely sometimes, lanceolar or
Wire lanceolar.The total shape of inflorescence, basidixed is formed by most capitulum set;4~5 layers of involucral bract, outer layer is smaller, ovate
Lanceolar, middle level and internal layer are larger, oval, edge film quality, close by wool;Holder is flat, hemispherical, upper raw female flower and two
Property spends more than 10;Female flower is not very developed, and is about 1 centimetre, without obvious corolla;Hermaphrodite flower is isometric with female flower, corolla tubular, red
Split on color, top 5;5 pieces of stamen, synandrium, filigree is short, is born in corolla base portion;Style is elongated, the bifurcated of top 2, and ovary is the next, and 1
Room.Achene Long Circle.7~October of florescence.
Mosquito repellent product currently on the market is generally mosquito-repellent perfume, and general concentration of alcohol is 70%~75%, to groups of people
Especially infant's skin has certain stimulation to group, and ethanol belongs to inflammable thing, and fire is susceptible to during production and use,
European Union in 2006 takes the lead in giving ethanol content in human body ethanol formulation product strict regulation limitation.
Dimethyl phthalate compares as wide spectrum, efficient insect repellent with standard mosquito-repellent, lower with toxicity, thorn
Sharp property is smaller, and the distinguishing feature such as the repellent time is longer, is the preferable regeneration product of standard mosquito-repellent.Natural mint extract
It is with quick refrigerant antipruritic effect but relatively violent and very brief, and menthyl lactate has gentle long-acting cooling effect, effectively
The refrigerant time, up to more than 1 hour, with mint extract with the use of that can make product both effects with Quick itch stopping, has again
There is long-acting refreshing effect.Sodium cocoyl methyl sodium taurocholate is the gentle amino acid type surfactant of green, compounding
Excitant of the other surfaces activating agent to skin can be effectively reduced afterwards, solubilizing effect can be more effectively improved, while improving polyethers
Class surfactant causes the soapy feeling of skin, soaks nourishes rough skin, strengthens the pleasant sensation of skin.
Existing simple use plant extraction liquid is in the floral water of culicifuge, product is also more because active ingredient antidecomposition is poor
And make mosquito repellent timeliness limited.Chemical repellents have carrying for the natural plants such as long-acting repelling effect, folium artemisiae argyi, peppermint and lavender
Taking liquid has comparatively ideal anti-inflammation, the antipruritic effect of miliaria is gone, while having the effects such as refreshing the mind.In existing commercially available floral water
Substantially also not by the product of its complex configuration.To make product that there is bactericidal effect, the floral water of chemical culicifuge its second
Alcohol content is more 75% or so.But if after this bactericidal effect is replaced by natural botanical extraction liquid, and in product component
Under being mutually dissolved property and stability obtain effectively solving, the ethanol content in product can significantly be cut down, while it also avoid perfume (or spice)
Gas effect is destroyed.
Folium artemisiae argyi has very good mosquito repellent function, therefore can be added in mosquito-driving liquid as natural additive.
The content of the invention
For the problem proposed in above-mentioned background technology, the invention provides the folium artemisiae argyi low combination of alcohol mosquito repellent liquid and its preparation
Method.
The low alcohol mosquito repellent combination liquid of folium artemisiae argyi, is made up of following raw material:Octyl methoxycinnamate, plant extraction liquid, peppermint carry
Take thing, natural borneol, solubilizer, ethanol, water surplus.
Specifically, the above-mentioned low alcohol mosquito repellent combination liquid of folium artemisiae argyi is made up of following raw material and its parts by weight:Methoxy cinnamic acid
Monooctyl ester 5-20%, plant extraction liquid 5-10%, mint extract 0.2-1.0%, natural borneol 0.2-1.0%, solubilizer 0.5-3%, second
Alcohol 5-15%, water surplus.
The plant extraction liquid includes folium artemisiae argyi, lemon-grass, three kinds of extract solutions of natural plants of rose, three kinds of plant extracts
Liquid is commercially available, and Folium Artemisiae Argyi extractive liquid accounts for 20-80% by weight in the mixed extract, and peppermint extract solution accounts for 10-40%, and rose carries
Take liquid and account for 10-40%.Remaining each raw material is easily purchase marketable material, all should meet cosmetic material production specification requirement.
The solubilizer is polyether surfactant Cremophor RH40 and N- acyl amino acid type surface-actives
The mixture of agent sodium cocoyl methyl sodium taurocholate by weight 1: 0.1-1.
The acid-base modifier is selected from:In sodium acid carbonate, sodium carbonate, potassium hydroxide.
The antioxidant BHT of no more than 0.1wt% can be also added in formula.
The preparation method of described argy wormwood leaf low-alcohol mosquito-repellent liquid, comprises the following steps:
(1) ethanol will be dissolved in by the natural borneol of proportioning, mint extract;
(2) ethanol will be scattered in by the octyl methoxycinnamate of proportioning, plant extraction liquid, solubilizer, step (1) resulting solution
In, it is well mixed;Octyl methoxycinnamate can be combined with the composition such as folium artemisiae argyi, lemon-grass, produce repelling effect;
(3) by acid-base modifier addition deionized water, it is made into the aqueous solution;
(4) step (2) resulting solution is well mixed with step (3) obtained aqueous solution;Obtain final product.
Step (4) gained mixture is aged 48 hours in aging tank, cold filtration is then carried out, by mosquito repellent after filtering
It is exposed in storage tank and stores 12-24 hours, gets product.
The present invention is produced to the compound of steady quality on the basis of substantial amounts of experimental study by method simple and easy to apply
Argy wormwood leaf low-alcohol mosquito-repellent liquid, with advantages below:
1st, the solubilising of Surfactant PEG -40HCO and sodium cocoyl methyl taurine acid sodium compounding is added in mosquito-repellent liquid
Agent.The use of the solubilizer substantially increases the emulsifying capacity of water solution system, can be reduced to the content of ethanol in mosquito-repellent liquid
Less than 25% will not also cause oil soluble material dimethyl phthalate therein, menthyl lactate etc. to separate out and be layered or precipitate, and be made
Mosquito-repellent liquid can keep clear in -10-45 DEG C, and stabilization can be also kept under centrifugal condition.Meanwhile, the skin sense effect of product is also bright
It is aobvious to improve.
2nd, folium artemisiae argyi, lemon-grass, rose extract are with the addition of in mosquito-repellent liquid, such extract has good antipruritic strong skin work(
Effect, itself has special natural faint scent, also there is certain repellent effect, and such material good water solubility, Ke Yijin to mosquito
The content of ethanol in one step reduction product.
3rd, using octyl methoxycinnamate as effective mosquito component, octyl methoxycinnamate is wide spectrum, efficient
Insect repellent, the repellent time is long, and repellent effect is good, skin and mucous membrane is had no toxic side effect, without anaphylaxis and without Cutaneous permeation
The advantages of property, be the preferable regeneration product of standard mosquito-repellent using very safe.
4th, the mosquito-repellent liquid that this technology is prepared, below 15%, compared with traditional processing technology, this technology is significantly for concentration of alcohol
Degree reduces production cost, improves the aroma quality and security of mosquito-repellent liquid.
Specific embodiment
Further description is made to the present invention below according to embodiment.
Embodiment 1
The low alcohol mosquito repellent combination liquid of folium artemisiae argyi is made up of following raw material and its parts by weight:Octyl methoxycinnamate 6%, plant extract
Liquid 7%, mint extract 0.3%, natural borneol 1.0%, solubilizer 3%, ethanol 15%, water surplus.
The preparation method of described argy wormwood leaf low-alcohol mosquito-repellent liquid, comprises the following steps:
(1) ethanol will be dissolved in by the natural borneol of proportioning, mint extract;
(2) ethanol will be scattered in by the octyl methoxycinnamate of proportioning, plant extraction liquid, solubilizer, step (1) resulting solution
In, it is well mixed;
(3) by acid-base modifier addition deionized water, it is made into the aqueous solution;
(4) step (2) resulting solution is well mixed with step (3) obtained aqueous solution;Obtain final product.
Embodiment 2
The low alcohol mosquito repellent combination liquid of folium artemisiae argyi is made up of following raw material and its parts by weight:Octyl methoxycinnamate 7%, plant extract
Liquid 5%, mint extract 0.2%, natural borneol 0.2%, solubilizer 0.5%, ethanol 5%, water surplus.
The preparation method of described argy wormwood leaf low-alcohol mosquito-repellent liquid, comprises the following steps:
(1) ethanol will be dissolved in by the natural borneol of proportioning, mint extract;
(2) ethanol will be scattered in by the octyl methoxycinnamate of proportioning, plant extraction liquid, solubilizer, step (1) resulting solution
In, it is well mixed;
(3) by acid-base modifier addition deionized water, it is made into the aqueous solution;
(4) step (2) resulting solution is well mixed with step (3) obtained aqueous solution;Obtain final product.
Embodiment 3
The low alcohol mosquito repellent combination liquid of folium artemisiae argyi is made up of following raw material and its parts by weight:Octyl methoxycinnamate 17%, plant extract
Liquid 6%, mint extract 0.5%, natural borneol 0.6%, solubilizer 2.7%, ethanol 5%, water surplus.
The preparation method of described argy wormwood leaf low-alcohol mosquito-repellent liquid, comprises the following steps:
(1) ethanol will be dissolved in by the natural borneol of proportioning, mint extract;
(2) ethanol will be scattered in by the octyl methoxycinnamate of proportioning, plant extraction liquid, solubilizer, step (1) resulting solution
In, it is well mixed;
(3) by acid-base modifier addition deionized water, it is made into the aqueous solution;
(4) step (2) resulting solution is well mixed with step (3) obtained aqueous solution;Obtain final product.
Embodiment 4
The low alcohol mosquito repellent combination liquid of folium artemisiae argyi is made up of following raw material and its parts by weight:Octyl methoxycinnamate 18%, plant extract
Liquid 10%, mint extract 0.8%, natural borneol 0.9%, solubilizer 1.8%, ethanol 14%, water surplus.
The preparation method of described argy wormwood leaf low-alcohol mosquito-repellent liquid, comprises the following steps:
(1) ethanol will be dissolved in by the natural borneol of proportioning, mint extract;
(2) ethanol will be scattered in by the octyl methoxycinnamate of proportioning, plant extraction liquid, solubilizer, step (1) resulting solution
In, it is well mixed;
(3) by acid-base modifier addition deionized water, it is made into the aqueous solution;
(4) step (2) resulting solution is well mixed with step (3) obtained aqueous solution;Obtain final product.
Described above not limitation of the present invention, the present invention is also not limited to the example above.The art it is common
In essential scope of the invention, change, remodeling, addition or the replacement made should also belong to protection of the invention to technical staff
Scope.
Claims (8)
1. the low alcohol mosquito repellent of folium artemisiae argyi combines liquid, it is characterised in that be made up of following raw material:Octyl methoxycinnamate, plant extract
Liquid, mint extract, natural borneol, solubilizer, ethanol, water surplus.
2. the low alcohol mosquito repellent of folium artemisiae argyi according to claim 1 combines liquid, it is characterised in that by following raw material and its parts by weight
Composition:Octyl methoxycinnamate 5-20%, plant extraction liquid 5-10%, mint extract 0.2-1.0%, natural borneol 0.2-
1.0%th, solubilizer 0.5-3%, ethanol 5-15%, water surplus.
3. folium artemisiae argyi according to claim 1 low alcohol mosquito repellent combination liquid, it is characterised in that the plant extraction liquid include folium artemisiae argyi,
Lemon-grass, three kinds of extract solutions of natural plants of rose, three Plant Extracts are commercially available, in the mixed extract by weight
Folium Artemisiae Argyi extractive liquid accounts for 20-80%, and peppermint extract solution accounts for 10-40%, and rose extract solution accounts for 10-40%.Remaining each raw material is easily
Purchase marketable material, all should meet cosmetic material production specification requirement.
4. the low alcohol mosquito repellent of folium artemisiae argyi according to claim 1 combines liquid, it is characterised in that the solubilizer is polyethers surface
Activating agent Cremophor RH40 is with N- acyl amino acid type surfactant sodium cocoyl methyls sodium taurocholate by weight 1
: the mixture of 0.1-1.
5. the low alcohol mosquito repellent of folium artemisiae argyi according to claim 1 combines liquid, it is characterised in that the acid-base modifier is selected from:Carbonic acid
In hydrogen sodium, sodium carbonate, potassium hydroxide.
6. the low alcohol mosquito repellent of folium artemisiae argyi according to claim 1 combines liquid, it is characterised in that can also be added no more than in formula
The antioxidant BHT of 0.1wt%.
7. the low alcohol mosquito repellent of folium artemisiae argyi according to claim 1 combines liquid, it is characterised in that described argy wormwood leaf low-alcohol mosquito-repellent liquid
Preparation method, comprises the following steps:
1) ethanol will be dissolved in by the natural borneol of proportioning, mint extract;
2) octyl methoxycinnamate, plant extraction liquid, solubilizer, the step 1 of proportioning will be pressed) resulting solution is scattered in ethanol
In, it is well mixed;
3) by acid-base modifier addition deionized water, it is made into the aqueous solution;
4) by step 2) resulting solution and step 3) obtained aqueous solution is well mixed;Obtain final product.
8. the low alcohol mosquito repellent of folium artemisiae argyi according to claim 1 combines liquid, it is characterised in that by step (4) gained mixture old
It is aged 48 hours in change tank, then carries out cold filtration, store mosquito-repellent liquid in storage tank 12-24 hours after filtering, is obtained final product into
Product.
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CN201611269238.XA CN106821903A (en) | 2016-12-31 | 2016-12-31 | Low alcohol mosquito repellent combination liquid of folium artemisiae argyi and preparation method thereof |
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CN201611269238.XA CN106821903A (en) | 2016-12-31 | 2016-12-31 | Low alcohol mosquito repellent combination liquid of folium artemisiae argyi and preparation method thereof |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109267359A (en) * | 2018-09-27 | 2019-01-25 | 佛山九陌科技信息咨询有限公司 | A kind of preparation method of anti-mosquito net |
CN111789795A (en) * | 2020-04-28 | 2020-10-20 | 广东分子态生物股份有限公司 | Hand sanitizer with liposome-encapsulated bactericidal component and preparation method thereof |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102349547A (en) * | 2011-08-15 | 2012-02-15 | 湖南轻工研究院有限责任公司 | Composite argy wormwood leaf low-alcohol mosquito-repellent liquid and preparation method thereof |
-
2016
- 2016-12-31 CN CN201611269238.XA patent/CN106821903A/en active Pending
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102349547A (en) * | 2011-08-15 | 2012-02-15 | 湖南轻工研究院有限责任公司 | Composite argy wormwood leaf low-alcohol mosquito-repellent liquid and preparation method thereof |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109267359A (en) * | 2018-09-27 | 2019-01-25 | 佛山九陌科技信息咨询有限公司 | A kind of preparation method of anti-mosquito net |
CN111789795A (en) * | 2020-04-28 | 2020-10-20 | 广东分子态生物股份有限公司 | Hand sanitizer with liposome-encapsulated bactericidal component and preparation method thereof |
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