CN109267359A - A kind of preparation method of anti-mosquito net - Google Patents
A kind of preparation method of anti-mosquito net Download PDFInfo
- Publication number
- CN109267359A CN109267359A CN201811129471.7A CN201811129471A CN109267359A CN 109267359 A CN109267359 A CN 109267359A CN 201811129471 A CN201811129471 A CN 201811129471A CN 109267359 A CN109267359 A CN 109267359A
- Authority
- CN
- China
- Prior art keywords
- mosquito net
- mosquito
- folium artemisiae
- preparation
- artemisiae argyi
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
- D06M13/51—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond
- D06M13/513—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond with at least one carbon-silicon bond
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/564—Polyureas, polyurethanes or other polymers having ureide or urethane links; Precondensation products forming them
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention relates to a kind of preparation methods of anti-mosquito net, belong to textile material technical field.The present invention is by peppermint extracting solution, finishing fluid of the mixed liquor of Folium Artemisiae Argyi extractive liquid and the fermentation liquid of bacillus thuringiensis as mosquito net, by treated, mosquito net is immersed in finishing fluid, the surface of mosquito net is fixed on by polyurethane adhesive, prepare a kind of anti-mosquito net with long-acting mosquito-driving, first pass through one layer of coupling agent in physical absorption on mosquito net, after rapid curing, then with the processing of the mixed solution of polyurethane adhesive and finishing agent, so that the adsorbance of finishing agent rises, polyurethane adhesive and finishing agent are uniformly dispersed in aqueous solution, coupled action also adheres to finishing agent, so that the amount of finishing agent also increases on terylene mosquito net, since polyurethane adhesive makes what finishing agent consolidated by compared with to be adsorbed on mosquito net with the adhesive attraction of mosquito net, so that its water-wash resistance improves, and the auxiliary agent added will not be shown Write the pliability for changing mosquito net.
Description
Technical field
The present invention relates to a kind of preparation methods of anti-mosquito net, belong to textile material technical field.
Background technique
Mosquito net is essential mosquito-proof daily necessity in daily life, but traditional mosquito net can only be from spatially by mosquito
It is limited in outside mosquito net, itself does not have mosquito and insect expelling effect, and mosquito proof effect is bad.
Mosquito proof arrangement is to carry out special processing to textile using antimosquito finishing agent (such as mosquito repellent agent or insecticide).
With the compound of efficiency and mosquitocide efficiency is walked quickly and kept away, there are many kinds, but difference on effect is larger.Ideal anophelifuge should meet: anti-
Mosquito effect durability is good, safe and harmless, is not likely to produce drug resistance, and does not influence the original various performances of fabric.
With insecticide Impregnated Mosquito Nets, to prevent mosquito invasion.However, when being maintained using the fabric insecticidal effect that infusion method is handled
Between shorter, drug effect sharp fall after washing, it is necessary to impregnate again.Not only troublesome in this way but also consuming medicament, low efficiency are easy to pollute
Environment.In order to overcome this disadvantage, researcher considers to wrap up Compositional type insecticide with capsule, then makes its suction by finishing technique
It is attached on fabric fibre, insecticide slow release can be made in this way, extend fabric drug effect, also have its washing fastness and preferably mention
It is high.
Microcapsules technology be coated with the thin layer of kind of natural or synthetic material from tens nanometers to the gas of hundreds of microns,
A kind of new technology of liquid and solia particle.Microcapsules are divided into semiclosed microcapsules and totally-enclosed microcapsules, are also classified into common micro-
Capsule and capsule of nano.Representative microcapsules production method has interfacial polymerization, on-site polymerization, hardens cladding process in liquid
(nozzle hair), the phase separation method of water solution system and intra-liquid desiccation method etc..
Anti-mosquito net is widely used in the prevention and treatment of mosquito and walks quickly and keeps away.The preparation of anti-mosquito net is exactly to use to contain various mosquitoes
Solution of repellent agent and insecticide etc. handles fabric, forms not soluble in water and common organic solvents anophelifuges in fiber surface
Film.This medicine film can give out the smell that mosquitos and flies etc. is detested, make mosquitos and flies etc. be reluctant to stop on the fabric containing anophelifuge and
Escape, as soon as while mosquitos and flies contact fabric, go down or kill immediately.
Anti-mosquito net is just being paid more and more attention as a kind of new mosquito-proof mode, and compared with common mosquito net, it is because by killing
Worm agent processing is provided with mosquito repellent and mosquitocide effect, therefore anti-mosquito net aperture can be done greatly, so that its ventilation effect is good.Separately
Although outer anti-mosquito net is same as mosquito-repellent incense and aerosol to use the cruel insecticides of pyrethroid, because anti-mosquito net is by medicament
It is attached on mosquito net, mosquito net is touched by mosquito and is worked, belong to contact killing type anophelifuge substance, so than disperse mosquito-repellent incense and aerosol
Agent toxicity is greatly reduced, relatively safer to children and pregnant woman, while this mosquito netting for preventing mosquito lasting medicine, cheap, is easy
By big well-established.
Summary of the invention
The technical problems to be solved by the invention: bad for anti-mosquito net washing-resistant effect, drug is easy washed
It falls off in journey, so that the problem of repelling effect of mosquito net reduces, provides a kind of preparation method of anti-mosquito net.
In order to solve the above technical problems, the technical solution adopted by the present invention is that:
(1) bacillus thuringiensis is seeded in complex medium, obtains blended liquid, be centrifuged and filtered, obtain ferment filtrate；
(2) according to parts by weight, 20~30 parts of ferment filtrates, 10~20 parts of peppermint extracting solutions, 8~15 portions of folium artemisiae argyis are weighed respectively to mention
Liquid, 10~18 parts of polyurethane adhesives are taken, ferment filtrate, peppermint extracting solution, Folium Artemisiae Argyi extractive liquid and polyurethane adhesive are mixed,
10~15min of ultrasonic disperse at room temperature obtains finishing agent；Mosquito net is soaked in the aminopropyl triethoxy that mass fraction is 0.5%
1~3min in the aqueous solution of silane coupling agent takes out, and naturally dry is at room temperature to get pretreatment mosquito net, by pretreatment mosquito net leaching
1~3min in finishing agent is steeped, processing is padded in padding machine, is dried to constant weight in 70~80 DEG C of baking oven to get mosquito repellent mosquito
Account.
Complex medium described in step (1) is to take peptone 10g, sodium chloride 5g, beef extract 3g, with 1mol/L hydroxide
It is 7.0~7.2 that sodium solution, which adjusts pH, is settled to 1000mL with deionized water, obtains fluid nutrient medium, and the agar of 10~20g is added
Powder stirs evenly.
Condition of culture described in step (1) is that temperature is 25~35 DEG C, and mixing speed is 60~80r/min, and inoculum concentration is
3%, it cultivates 1~2 day.
Centrifugation described in step (1) is simultaneously filtered at 5000~7000r/min 5~10min of centrifugation, and with 0.2~0.3
μm bacterial filter filtering.
Peppermint extracting solution described in step (2) is in mass ratio 1: 5 by peppermint fresh leaf and deionized water mixing, in temperature
Be that water-bath is heated to reflux 6~8h of extraction at 70~80 DEG C, obtain phegma, revolving speed be 2000~4000r/min under centrifugation 3~
5min takes supernatant liquor and filters to get peppermint extracting solution.
Folium Artemisiae Argyi extractive liquid described in step (2) is in mass ratio 1: 3 by fresh folium artemisiae argyi and deionized water mixing, is in temperature
1~2h is boiled at 100~110 DEG C, is cooled to room temperature, pulls folium artemisiae argyi out, filters to obtain Folium Artemisiae Argyi extractive liquid.
Processing is padded described in step (2) for the second dipping and rolling in padding machine, pick-up is 60%~70%.
The present invention is compared with other methods, and advantageous effects are:
(1) present invention is using the mixed liquor of peppermint extracting solution, Folium Artemisiae Argyi extractive liquid and the fermentation liquid of bacillus thuringiensis as mosquito net
Finishing fluid then will treated that mosquito net is immersed in arrangement using aminopropyltriethoxywerene werene coupling agent treatment mosquito net
In the cruel gluing agent emulsion of the poly- ammonia of liquid, it is fixed on the surface of mosquito net by polyurethane adhesive, prepares a kind of with long-acting mosquito-driving
Anti-mosquito net after rapid curing, then use polyurethane adhesive first on mosquito net through one layer of coupling agent in physical absorption
It is handled with the mixed solution of finishing agent, so that the adsorbance of finishing agent rises, this is because polyurethane adhesive and finishing agent are equal
In aqueous solution, the coupled action of coupling agent and polyurethane adhesive also adheres to finishing agent, so that washing for even dispersion
The amount of finishing agent also increases on synthetic fibre mosquito net, makes finishing agent steady by compared with the adhesive attraction of mosquito net due to polyurethane adhesive
Solid be adsorbed on mosquito net so that its water-wash resistance improves, and the auxiliary agent added will not significantly change the pliability of mosquito net；
(2) using bacillus thuringiensis as the main culicifuge in finishing agent, bacillus thuringiensis can be cooked micro- the present invention
Biological source low toxic pesticide, based on stomach poison function, which can produce two major classes toxin, i.e. endotoxin and exotoxin, make pest
Stop feeding, death due to hungry and cell wall rupture, blood are ruined with neurotoxic of last pest, its main active
It is one or several kinds of insecticidal crystal proteins, to insects such as Lepidoptera, coleoptera, Diptera, Hymenoptera, Homopteras, and dynamic plant
The arthropods such as object nematode, acarian have the cytotoxicity of specificity, and to nontarget organism safety, so the mosquito repellent mosquito of preparation
Account have many advantages, such as it is single-minded, efficiently and to safety of human and livestock.
Specific embodiment
Peptone 10g, sodium chloride 5g, beef extract 3g are taken, adjusting pH with 1mol/L sodium hydroxide solution is 7.0~7.2, is used
Deionized water is settled to 1000mL, obtains fluid nutrient medium, and the agar powder of 10~20g is added, stirs evenly to get compound criteria
Bacillus thuringiensis is seeded in complex medium by base, and temperature is 25~35 DEG C, and mixing speed is 60~80r/min, connects
Kind amount is 3%, cultivates 1~2 day, obtains blended liquid, 5~10min is centrifuged at 5000~7000r/min, and with 0.2~0.3um's
Bacterial filter filtering, obtains ferment filtrate；In mass ratio 1: 5 mixes peppermint fresh leaf and deionized water, is 70~80 in temperature
Water-bath is heated to reflux 6~8h of extraction at DEG C, obtains phegma, is centrifuged 3~5min in the case where revolving speed is 2000~4000r/min, takes
Layer clear liquid simultaneously filters to get peppermint extracting solution；In mass ratio 1: 3 mixes fresh folium artemisiae argyi and deionized water, temperature be 100~
1~2h is boiled at 110 DEG C, is cooled to room temperature, pulls folium artemisiae argyi out, filters to obtain Folium Artemisiae Argyi extractive liquid；According to parts by weight, 20 are weighed respectively
~30 parts of ferment filtrates, 10~20 parts of peppermint extracting solutions, 8~15 parts of Folium Artemisiae Argyi extractive liquids, 10~18 parts of polyurethane adhesives, will send out
Ferment filtrate, peppermint extracting solution, Folium Artemisiae Argyi extractive liquid and polyurethane adhesive mixing, 10~15min of ultrasonic disperse, must arrange at room temperature
Agent；Mosquito net is soaked in 1~3min in the aqueous solution for the aminopropyltriethoxywerene werene coupling agent that mass fraction is 0.5%, is taken
Out, pretreatment mosquito net is soaked in 1~3min in finishing agent, two in padding machine to get pretreatment mosquito net by naturally dry at room temperature
Leaching two is rolled, and pick-up is 60%~70%, is dried to constant weight in 70~80 DEG C of baking oven to get anti-mosquito net.
Take peptone 10g, sodium chloride 5g, beef extract 3g, with 1mol/L sodium hydroxide solution adjust pH be 7.0, spend from
Sub- water is settled to 1000mL, obtains fluid nutrient medium, and the agar powder of 10g is added, and stirs evenly to get complex medium, by Su Yun
Golden bacillus is seeded in complex medium, and temperature is 25 DEG C, mixing speed 60r/min, and inoculum concentration 3% is cultivated 1 day,
Blended liquid is obtained, 5min is centrifuged at 5000r/min, and filtered with the bacterial filter of 0.2um, obtains ferment filtrate；In mass ratio 1: 5
Peppermint fresh leaf and deionized water are mixed, water-bath is heated to reflux extraction 6h at being 70 DEG C in temperature, obtains phegma, is in revolving speed
It is centrifuged 3min under 2000r/min, take supernatant liquor and is filtered to get peppermint extracting solution；In mass ratio 1: 3 fresh folium artemisiae argyi and will go
Ionized water mixing boils 1h at being 100 DEG C in temperature, is cooled to room temperature, pulls folium artemisiae argyi out, filter to obtain Folium Artemisiae Argyi extractive liquid；By weight
Number meter weighs 20 parts of ferment filtrates, 10 parts of peppermint extracting solutions, 8 parts of Folium Artemisiae Argyi extractive liquids, 10 parts of polyurethane adhesives respectively, will
Ferment filtrate, peppermint extracting solution, Folium Artemisiae Argyi extractive liquid and polyurethane adhesive mixing, ultrasonic disperse 10min, must arrange at room temperature
Agent；Mosquito net is soaked in 1min in the aqueous solution for the aminopropyltriethoxywerene werene coupling agent that mass fraction is 0.5%, is taken out,
Pretreatment mosquito net is soaked in 1min in finishing agent, two leaching two in padding machine to get pretreatment mosquito net by naturally dry at room temperature
It rolls, pick-up 60%, dries to constant weight in 70 DEG C of baking oven to get anti-mosquito net.
Take peptone 10g, sodium chloride 5g, beef extract 3g, with 1mol/L sodium hydroxide solution adjust pH be 7.1, spend from
Sub- water is settled to 1000mL, obtains fluid nutrient medium, and the agar powder of 15g is added, and stirs evenly to get complex medium, by Su Yun
Golden bacillus is seeded in complex medium, and temperature is 30 DEG C, mixing speed 70r/min, and inoculum concentration 3% is cultivated 1 day,
Blended liquid is obtained, 8min is centrifuged at 6000r/min, and filtered with the bacterial filter of 0.2um, obtains ferment filtrate；In mass ratio 1: 5
Peppermint fresh leaf and deionized water are mixed, water-bath is heated to reflux extraction 7h at being 75 DEG C in temperature, obtains phegma, is in revolving speed
It is centrifuged 4min under 3000r/min, take supernatant liquor and is filtered to get peppermint extracting solution；In mass ratio 1: 3 fresh folium artemisiae argyi and will go
Ionized water mixing boils 1h at being 105 DEG C in temperature, is cooled to room temperature, pulls folium artemisiae argyi out, filter to obtain Folium Artemisiae Argyi extractive liquid；By weight
Number meter weighs 25 parts of ferment filtrates, 15 parts of peppermint extracting solutions, 10 parts of Folium Artemisiae Argyi extractive liquids, 14 parts of polyurethane adhesives respectively, will
Ferment filtrate, peppermint extracting solution, Folium Artemisiae Argyi extractive liquid and polyurethane adhesive mixing, ultrasonic disperse 12min, must arrange at room temperature
Agent；Mosquito net is soaked in 2min in the aqueous solution for the aminopropyltriethoxywerene werene coupling agent that mass fraction is 0.5%, is taken out,
Pretreatment mosquito net is soaked in 2min in finishing agent, two leaching two in padding machine to get pretreatment mosquito net by naturally dry at room temperature
It rolls, pick-up 65%, dries to constant weight in 75 DEG C of baking oven to get anti-mosquito net.
Take peptone 10g, sodium chloride 5g, beef extract 3g, with 1mol/L sodium hydroxide solution adjust pH be 7.2, spend from
Sub- water is settled to 1000mL, obtains fluid nutrient medium, and the agar powder of 20g is added, and stirs evenly to get complex medium, by Su Yun
Golden bacillus is seeded in complex medium, and temperature is 35 DEG C, mixing speed 80r/min, and inoculum concentration 3% is cultivated 2 days,
Blended liquid is obtained, 10min is centrifuged at 7000r/min, and filtered with the bacterial filter of 0.3um, obtains ferment filtrate；In mass ratio 1:
5 mix peppermint fresh leaf and deionized water, and water-bath is heated to reflux extraction 8h at being 80 DEG C in temperature, phegma are obtained, in revolving speed
To be centrifuged 5min under 4000r/min, taking supernatant liquor and filtering to get peppermint extracting solution；In mass ratio 1: 3 by fresh folium artemisiae argyi and
Deionized water mixing boils 2h at being 110 DEG C in temperature, is cooled to room temperature, pulls folium artemisiae argyi out, filter to obtain Folium Artemisiae Argyi extractive liquid；By weight
Number meter is measured, weighs 30 parts of ferment filtrates, 20 parts of peppermint extracting solutions, 15 parts of Folium Artemisiae Argyi extractive liquids, 18 parts of polyurethane adhesives respectively,
Ferment filtrate, peppermint extracting solution, Folium Artemisiae Argyi extractive liquid and polyurethane adhesive are mixed, ultrasonic disperse 15min, must arrange at room temperature
Agent；Mosquito net is soaked in 3min in the aqueous solution for the aminopropyltriethoxywerene werene coupling agent that mass fraction is 0.5%, is taken out,
Pretreatment mosquito net is soaked in 3min in finishing agent, two leaching two in padding machine to get pretreatment mosquito net by naturally dry at room temperature
It rolls, pick-up 70%, dries to constant weight in 80 DEG C of baking oven to get anti-mosquito net.
Reference examples: the anti-mosquito net of Dongguan company production.
The anti-mosquito net that example and reference examples are prepared is detected, specific detection is as follows:
Investigate three indexs: the content of insecticide in mosquito net before not washing, the content of insecticide and mosquito in mosquito net after 1 washing
1 washable rate of account.
Specific test result such as table 1.
1 performance characterization contrast table of table
| Detection project | Example 1 | Example 2 | Example 3 | Reference examples |
| 0 washing/g/kg | 1.99 | 1.92 | 1.94 | 1.68 |
| 1 washing/g/kg | 1.44 | 1.45 | 1.48 | 1.0 |
| 1 washable rate/% | 80.0 | 79.9 | 78.1 | 68.2 |
As shown in Table 1, anti-mosquito net prepared by the present invention has good washing fastness.
Claims (7)
1. a kind of preparation method of anti-mosquito net, it is characterised in that specific preparation step are as follows:
(1) bacillus thuringiensis is seeded in complex medium, obtains blended liquid, be centrifuged and filtered, obtain ferment filtrate；
(2) according to parts by weight, 20~30 parts of ferment filtrates, 10~20 parts of peppermint extracting solutions, 8~15 portions of folium artemisiae argyis are weighed respectively to mention
Liquid, 10~18 parts of polyurethane adhesives are taken, ferment filtrate, peppermint extracting solution, Folium Artemisiae Argyi extractive liquid and polyurethane adhesive are mixed,
10~15min of ultrasonic disperse at room temperature obtains finishing agent；Mosquito net is soaked in the aminopropyl triethoxy that mass fraction is 0.5%
1~3min in the aqueous solution of silane coupling agent takes out, and naturally dry is at room temperature to get pretreatment mosquito net, by pretreatment mosquito net leaching
1~3min in finishing agent is steeped, processing is padded in padding machine, is dried to constant weight in 70~80 DEG C of baking oven to get mosquito repellent mosquito
Account.
2. a kind of preparation method of anti-mosquito net according to claim 1, it is characterised in that: compound described in step (1)
Culture medium is to take peptone 10g, sodium chloride 5g, beef extract 3g, and adjusting pH with 1mol/L sodium hydroxide solution is 7.0~7.2, is used
Deionized water is settled to 1000mL, obtains fluid nutrient medium, and the agar powder of 10~20g is added, stirs evenly.
3. a kind of preparation method of anti-mosquito net according to claim 1, it is characterised in that: culture described in step (1)
Condition is that temperature is 25~35 DEG C, and mixing speed is 60~80r/min, and inoculum concentration 3% is cultivated 1~2 day.
4. a kind of preparation method of anti-mosquito net according to claim 1, it is characterised in that: centrifugation described in step (1)
And it is filtered into 5~10min of centrifugation at 5000~7000r/min, and filtered with 0.2~0.3 μm of bacterial filter.
5. a kind of preparation method of anti-mosquito net according to claim 1, it is characterised in that: peppermint described in step (2)
Extracting solution is in mass ratio 1: 5 by peppermint fresh leaf and deionized water mixing, and water-bath is heated to reflux at being 70~80 DEG C in temperature
Extract 6~8h, obtain phegma, revolving speed be 2000~4000r/min under be centrifuged 3~5min, take supernatant liquor and filter to get
Peppermint extracting solution.
6. a kind of preparation method of anti-mosquito net according to claim 1, it is characterised in that: folium artemisiae argyi described in step (2)
Extracting solution is in mass ratio 1: 3 by fresh folium artemisiae argyi and deionized water mixing, boils 1~2h at being 100~110 DEG C in temperature, cold
But it to room temperature, pulls folium artemisiae argyi out, filters to obtain Folium Artemisiae Argyi extractive liquid.
7. a kind of preparation method of anti-mosquito net according to claim 1, it is characterised in that: step is padded described in (2)
Processing is the second dipping and rolling in padding machine, and pick-up is 60%~70%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811129471.7A CN109267359A (en) | 2018-09-27 | 2018-09-27 | A kind of preparation method of anti-mosquito net |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811129471.7A CN109267359A (en) | 2018-09-27 | 2018-09-27 | A kind of preparation method of anti-mosquito net |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109267359A true CN109267359A (en) | 2019-01-25 |
Family
ID=65198976
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811129471.7A Pending CN109267359A (en) | 2018-09-27 | 2018-09-27 | A kind of preparation method of anti-mosquito net |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109267359A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110670357A (en) * | 2019-09-24 | 2020-01-10 | 江苏烨天羊绒科技有限公司 | Manufacturing method of mothproof anti-static pure cashmere fabric and obtained fabric product |
| CN114381939A (en) * | 2022-01-17 | 2022-04-22 | 沧州永阔隆化工有限公司 | PE/PET mixed long-acting insecticidal mosquito net and preparation method thereof |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101129141A (en) * | 2006-08-24 | 2008-02-27 | 彭明 | Process for preparing biological culicide |
| CN101347129A (en) * | 2008-09-01 | 2009-01-21 | 佛山市正典生物技术有限公司 | Bacillus thuringiensis suspending agent for killing mosquito |
| US20110104224A1 (en) * | 2009-11-05 | 2011-05-05 | Cognis Ip Management Gmbh | Textile Finishing For Insect Repellency |
| CN104947435A (en) * | 2015-04-08 | 2015-09-30 | 江苏工程职业技术学院 | Preparation method of intelligent surface mosquito-repellent polyester fiber for mosquito net |
| CN106821903A (en) * | 2016-12-31 | 2017-06-13 | 新昌县迪斯曼科技有限公司 | Low alcohol mosquito repellent combination liquid of folium artemisiae argyi and preparation method thereof |
| CN107087645A (en) * | 2017-04-01 | 2017-08-25 | 杨飞 | A kind of biological mixed pesticide of pest control, preparation method and application |
| CN108552229A (en) * | 2018-05-31 | 2018-09-21 | 佛山市陵谐环保科技有限公司 | One kind catching mosquito liquid |
-
2018
- 2018-09-27 CN CN201811129471.7A patent/CN109267359A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101129141A (en) * | 2006-08-24 | 2008-02-27 | 彭明 | Process for preparing biological culicide |
| CN101347129A (en) * | 2008-09-01 | 2009-01-21 | 佛山市正典生物技术有限公司 | Bacillus thuringiensis suspending agent for killing mosquito |
| US20110104224A1 (en) * | 2009-11-05 | 2011-05-05 | Cognis Ip Management Gmbh | Textile Finishing For Insect Repellency |
| CN104947435A (en) * | 2015-04-08 | 2015-09-30 | 江苏工程职业技术学院 | Preparation method of intelligent surface mosquito-repellent polyester fiber for mosquito net |
| CN106821903A (en) * | 2016-12-31 | 2017-06-13 | 新昌县迪斯曼科技有限公司 | Low alcohol mosquito repellent combination liquid of folium artemisiae argyi and preparation method thereof |
| CN107087645A (en) * | 2017-04-01 | 2017-08-25 | 杨飞 | A kind of biological mixed pesticide of pest control, preparation method and application |
| CN108552229A (en) * | 2018-05-31 | 2018-09-21 | 佛山市陵谐环保科技有限公司 | One kind catching mosquito liquid |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110670357A (en) * | 2019-09-24 | 2020-01-10 | 江苏烨天羊绒科技有限公司 | Manufacturing method of mothproof anti-static pure cashmere fabric and obtained fabric product |
| CN114381939A (en) * | 2022-01-17 | 2022-04-22 | 沧州永阔隆化工有限公司 | PE/PET mixed long-acting insecticidal mosquito net and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105594755B (en) | A kind of plant mosquito-repellent and the preparation method with repelling effect fabric | |
| CN100584817C (en) | Pyrethroid compound and uses | |
| CN100383335C (en) | Fabric finishing liquor for expelling and killing mosquitoes, method of use and products thereof | |
| DE3032616C2 (en) | ||
| CN107761374A (en) | A kind of antibacterial, the fabric/fiber dressing liquid of insecticidal medium and its application method and textile article/fibre/paper products | |
| CN107780210A (en) | A kind of mould proof, mosquito fiber/fabric/paper dressing liquid and its application method and product | |
| CN1851109A (en) | Fabric finishing liquid for insecticidal medium, and its use method and fabric product | |
| CN109267359A (en) | A kind of preparation method of anti-mosquito net | |
| CN104054758A (en) | Harmless plant insecticide | |
| CN102870771A (en) | Imidacloprid missible oil pesticide | |
| CN106942177A (en) | A kind of insect traps device, preparation method and application | |
| CN104938528B (en) | A kind of termite-killing trapping medicament and preparation method | |
| CN111109307A (en) | Preparation method of botanical drug mosquito-repellent textile and pharmaceutical composition thereof | |
| CN103749546B (en) | A kind of rose dark brown Isaria and beta-cypermethrin oil-suspending agent and application thereof | |
| CN109938047A (en) | Gelatin-gum arabic microcapsules of natural pyrethrin and preparation method thereof | |
| CN103374818B (en) | Biological source insect-preventing fabric and preparation method thereof | |
| CN103371169B (en) | Sophoramine insect-preventing missible oil, sophoramine insect-preventing fabric and preparation method of fabric | |
| CN105746584B (en) | A kind of Pesticidal combination and its preparation method and application containing Metarhizium anisopliae and cyromazine | |
| CN103651552A (en) | Ultra-low-volume liquor containing chlorfenapyr | |
| CN104068062B (en) | Chlorine tetramethrin aqueous emulsion of a kind of repelling and killing bugs and preparation method thereof | |
| DE69811993T2 (en) | Mosquito repellent and method for repelling mosquitoes | |
| CN101366395B (en) | Ectropis grisescens warreh nuclear polyhedrosis virus bakthane insect disinfestation suspension agent and preparation method thereof | |
| CN103397520B (en) | Fabric desinsection mosquito-repellent anti-static biologic product | |
| KR20130000105U (en) | Bedding for moustique extermination utiliser Natural plant extracts | |
| CN110301457A (en) | A method of striped rice borer is prevented and treated using entomopathogenic nematode |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20190125 |