CN111109307A - Preparation method of botanical drug mosquito-repellent textile and pharmaceutical composition thereof - Google Patents
Preparation method of botanical drug mosquito-repellent textile and pharmaceutical composition thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/34—Shaped forms, e.g. sheets, not provided for in any other sub-group of this main group
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention discloses a mosquito-repellent botanical drug composition which comprises mint, clove, perilla leaf, grassleaf sweelflag rhizome, Chinese mugwort leaf, dried orange peel, thin evodia herb, Anoectochilus roxburghii, heartleaf houttuynia herb and lavender. The invention also discloses a preparation method of the three botanical drug mosquito-repellent textiles. The effective mosquito repelling component in the preparation method of the botanical drug mosquito repelling textile provided by the invention is a pure traditional Chinese medicine formula, has no adverse effect on the health of a user, has no pollution to the environment, and has the advantages of simple and easy combination mode of the mosquito repelling drug and the textile, strong operability and low cost. The fabric treated by the medicine and the method has good mosquito repelling performance of Aedes albopictus, and the repelling rate is about 60 percent.
Description
Technical Field
The invention relates to the technical field of special textile preparation, in particular to a preparation method of a botanical drug mosquito-repellent textile and a pharmaceutical composition thereof.
Background
In summer and autumn, mosquitoes suck human blood, which brings great trouble to life of people, and meanwhile, mosquitoes can also transmit epidemic diseases such as epidemic encephalitis B, filariasis, malaria and the like. People use various methods to kill mosquitoes. Especially the use of chemical agents is more common, but excessive exposure to chemical agents can pose a potential threat to health, especially in infants. With the social progress, people's conception is changing, and more pay more attention to life in a green, safe, environment-friendly and ecological manner. The method for killing the mosquitoes by using the botanical drugs is environment-friendly, safe and high in social acceptance. The mosquito repellent effect of the botanical drug is transferred to the clothes, which is a very practical approach. Chinese patent CN109418331A discloses a mosquito-repellent traditional Chinese medicine bag, which is composed of 9 kinds of herbs such as folium artemisiae argyi, folium perillae, agastache rugosus, dried orange peel, clove and the like, and although the traditional Chinese medicine formula is provided in the traditional Chinese medicine bag, the formula utilizes the odor of the traditional Chinese medicine to repel mosquitoes, and the effect is not obvious. Chinese patent CN104195816A discloses a preparation process of a textile with mosquito repelling function, which obtains the mosquito repelling characteristic by soaking the textile with traditional Chinese medicines, but the preparation process is also simple to soak, and the mosquito repelling effect is not ideal.
Mosquito repellent products on the market are various at present, chemical agents are not good for the health of users, the environment is damaged, and the repelling effect and the maintaining time of botanical drugs are difficult to carry out scientific statistics. Moreover, according to the abundance of the substance level of people, the requirement for refining the textile market is more and more urgent aiming at the condition that mosquito repellent textiles are lacked in the market.
Disclosure of Invention
The invention aims to provide a mosquito-repellent botanical pharmaceutical composition in order to meet market demands and achieve effective mosquito-repellent effect on textiles.
The invention also aims to provide a preparation method of the botanical drug mosquito-repellent textile.
The invention provides a mosquito-repellent botanical drug composition, which comprises the following medicinal materials in parts by weight: 10-15 parts of mint, 8-12 parts of clove, 12-15 parts of perilla leaf, 10-12 parts of rhizoma acori graminei, 15-18 parts of folium artemisiae argyi, 12-15 parts of dried orange peel, 10-12 parts of evodia lepta, 10-15 parts of anoectochilus formosanus, 15-18 parts of herba houttuyniae and 15-18 parts of lavender.
Preferably, the mosquito-repellent botanical pharmaceutical composition comprises the following medicinal materials in parts by weight: 10 parts of mint, 8 parts of clove, 12 parts of perilla leaf, 10 parts of rhizoma acori graminei, 15 parts of folium artemisiae argyi, 12 parts of dried orange peel, 10 parts of thin evodia, 10 parts of herba Anoectochili Roxburghii, 15 parts of herba houttuyniae and 15 parts of lavender.
The mint is an aromatic traditional Chinese medicine with special economic value, mainly contains volatile oil such as menthol and the like, has pungent and cool sweating and fever relieving effects when being taken orally, can treat symptoms such as neuralgia, skin itch and the like when being taken externally, and has double functions of medical use and eating.
Clove is pungent in taste, slightly warm and nontoxic, can warm the middle-jiao, descend the adverse qi, tonify the kidney and strengthen yang, has the functions of resisting bacteria, relieving pain, expelling parasites and the like, and is described as killing insects, removing evil and eliminating evil in a compendium of materia Medica.
The perilla leaves have strong fragrance and strong qi, so as to open skin and hair, release lung qi and open striae; on the upper part, the medicine is used for treating wind-cold exogenous disease by dredging nasal obstruction and clearing head and eyes; in the middle, it opens the chest and diaphragm, activates the spleen and stomach, disperses phlegm and fluid, relieves stagnation and promotes qi stagnation.
Rhizoma Acori Graminei has effects of inducing resuscitation, eliminating phlegm, refreshing mind, improving intelligence, eliminating dampness and promoting appetite.
The folium Artemisiae Argyi contains volatile oil such as eucalyptol and myrcene, and has effects of eliminating dampness and relieving itching. Ancient people often hang wormwood before the door, so that one is used for avoiding evil and the other is used for expelling mosquitoes.
Dry orange peel is warm in nature, pungent and bitter in taste. Regulate qi-flowing for strengthening spleen, regulate middle energizer, dry dampness and resolve phlegm.
Bitter taste and cold nature of trigeminal, clearing away heat and toxic material, dispelling wind and removing dampness.
Herba Antenoronis Neofiliformis has effects of clearing away heat and toxic materials, dispelling pathogenic wind, and relieving pain.
The houttuynia cordata mainly contains volatile oil, flavonoids and the like, and has the effects of bacteriostasis, heat clearing and detoxifying.
Lavender contains volatile oil such as linalool and cineole, and has tranquilizing, hypnotic, and antibacterial effects.
The traditional Chinese medicines are applied in a combined way to play a synergistic role, so that the traditional Chinese medicines are fragrant and have the effects of removing dirt, regulating the middle warmer and consolidating the exterior, clearing away heat and toxic materials and expelling mosquitoes.
Furthermore, the invention also provides application of the mosquito-repellent botanical drug composition in preparation of mosquito-repellent products.
Preferably, the mosquito repelling product comprises mosquito repelling liquid, a mosquito repelling bracelet, a mosquito repelling product and the like.
Furthermore, in a preferred embodiment, the invention provides a preparation method of the botanical drug mosquito-repellent textile 1: which comprises the following steps:
(1) weighing the mosquito-repellent botanical drug composition according to the proportion;
(2) weighing raw traditional Chinese medicinal materials, drying and crushing the traditional Chinese medicinal materials for later use;
(3) taking the Chinese medicine powder in the step (2) according to the proportion of 1: adding water at a ratio of 10-30, mixing, heating to 80 deg.C for 10min, filtering with 280 mesh steel sieve to remove residue, and filtering to obtain medicinal liquid;
(4) soaking the textile in the liquid medicine in the step (3), soaking and rolling the textile by a JX macrohair dyeing and finishing padding machine for two times, then drying the textile for later use at 80-100 ℃ for 3-10min to obtain the botanical drug mosquito-repellent textile raw material.
Preferably, the weight ratio of the textile raw materials to the traditional Chinese medicine powder in the step (4) is 1: 1 to 2.0.
The effective components of the traditional Chinese medicine and the extraction and separation method thereof are inseparable, and the scheme provided by the embodiment extracts the effective components of the traditional Chinese medicine by a decoction method and leads the effective components to be fully fused on the textile by an impregnation method so as to achieve the effect of mosquito repelling.
Still further, in a preferred embodiment, the method of the present invention may further adopt a sealed aromatherapy preparation method 2, specifically including the steps of:
(1) weighing the mosquito-repellent botanical drug composition according to the proportion;
(2) weighing raw traditional Chinese medicinal materials, drying the traditional Chinese medicinal materials, pulverizing into fine powder, and sieving for later use;
(3) and (3) wrapping the traditional Chinese medicine powder in the step (2) by using cotton cloth to form a small bag, putting the small bag and the textile raw materials into a sealed plastic bag, and sealing and placing the bag at normal temperature for 12-72 hours to obtain the botanical drug mosquito-repellent textile raw material.
Preferably, the total weight ratio of the textile raw materials to the traditional Chinese medicine powder is 1: 0.5 to 2.0.
The scheme provided by the embodiment makes full use of natural effective components of traditional Chinese medicines, particularly substances such as volatile oil and the like, and achieves the effects of removing dirt with fragrance, clearing away heat and toxic materials and avoiding mosquitoes. The scheme completely reserves the natural effective components of the traditional Chinese medicines, volatilizes and fuses the effective components to the pure cotton textile fabric, and enables the textile fabric to obtain the mosquito repelling effect.
Still further, in a preferred embodiment, the method of the present invention can also adopt a method 3 of preparing a mixture of the two, specifically comprising the following steps:
(1) weighing the mosquito-repellent botanical drug composition according to the proportion;
(2) weighing raw traditional Chinese medicinal materials, drying and crushing the traditional Chinese medicinal materials for later use;
(3) mixing the textile raw materials with the traditional Chinese medicine powder 1: 1-2.0, taking the Chinese medicinal powder (2) according to the weight ratio of 1: adding water at a ratio of 10-30, mixing, heating to 80 deg.C for 10min, filtering with 280 mesh steel sieve to remove residue, and filtering to obtain medicinal liquid;
(4) soaking the textile in the liquid medicine in the step (3), soaking and rolling the textile by a JX macro dyeing and finishing padding machine for two times, then drying the textile for later use at the temperature of 80-100 ℃ for 3-10 min;
(5) mixing the textile raw materials with the traditional Chinese medicine powder 1: and (3) taking the traditional Chinese medicine powder in the step (2) according to the weight ratio of 0.5-2.0, wrapping the traditional Chinese medicine powder in a small bag by using cotton cloth, putting the small bag and the textile dried in the step (4) into a sealed plastic bag, and sealing and placing the bag at normal temperature for 12-72 hours to obtain the botanical drug mosquito-repellent textile raw material.
Preferably, the weight ratio of the textile raw materials to the traditional Chinese medicine powder in the step (5) is 1: 1.5 to 3.0.
The scheme provided by the embodiment makes full use of natural active ingredients of the traditional Chinese medicine and active ingredients extracted by a solvent method, gives full play to the maximum medicinal value of the traditional Chinese medicine, makes the liquid medicine deeply enter the textile fiber, and has firm and lasting medicinal effect so as to achieve the effect of better repelling mosquitoes.
In the scheme, the textile used by the invention is the primary-color pure cotton knitted fabric, the fabric is not dyed and is knitted and woven by pure cotton, the fabric is soft and comfortable to wear, is skin-friendly and does not generate static electricity, and the fabric has the characteristics of moisture absorption, moisture retention, sanitation and the like.
The invention has the following beneficial effects:
the effective mosquito repelling component in the preparation method of the botanical drug mosquito repelling textile provided by the invention is a pure traditional Chinese medicine formula, has no adverse effect on the health of a user, has no pollution to the environment, and has the advantages of simple and easy combination mode of the mosquito repelling drug and the textile, strong operability and low cost. The fabric treated by the medicine and the method has good mosquito repelling performance of Aedes albopictus, and the repelling rate is about 60 percent.
Detailed Description
The following examples are intended to illustrate the invention but are not intended to limit the scope of the invention. Unless otherwise specified, the technical means used in the examples are conventional means well known to those skilled in the art, and the reagents used are commercially available.
However, it should be understood that these are exemplary only and not intended to limit the present invention, and that materials that are the same as or similar to the type, model, quality, nature, or function of the following reagents and instruments may be used in the practice of the present invention. The experimental procedures used in the following examples are all conventional procedures unless otherwise specified. Materials, reagents and the like used in the following examples are commercially available unless otherwise specified.
Example 1 preparation of mosquito repellent botanical pharmaceutical composition 1.1
1.1A mosquito-repellent botanical pharmaceutical composition, which comprises the following medicinal materials in parts by weight: 10 parts of mint, 8 parts of clove, 12 parts of perilla leaf, 10 parts of rhizoma acori graminei, 15 parts of folium artemisiae argyi, 12 parts of dried orange peel, 10 parts of thin evodia, 10 parts of herba Anoectochili Roxburghii, 15 parts of herba houttuyniae and 15 parts of lavender.
Weighing the following raw material medicines: 10g of mint, 8g of clove, 12g of perilla leaf, 10g of rhizoma acori graminei, 15g of folium artemisiae argyi, 12g of dried orange peel, 10g of thin evodia leaf, 10g of herba oectochili roxburghii, 15g of herba houttuyniae and 15g of lavender, and the traditional Chinese medicinal materials are dried, crushed into fine powder and uniformly mixed for later use.
1.2 taking primary color pure cotton knitted fabric (the gram weight is about 147 g/m)2) The weight was about 93.6 g.
2 methods and results
2.1 taking 1.1 of the traditional Chinese medicine powder, mixing the powder with 1: 20, adding water, mixing, heating to 80 deg.C for 10min, filtering with a 280-mesh steel sieve to remove residue, and filtering to obtain medicinal liquid.
2.2 soaking 1.2 cloth sample in 2.1 medicinal liquid, soaking and rolling with JX macrohair dyeing and finishing padding machine, and drying at 100 deg.C for 5 min.
2.3 reference GB/T13917.9-2009 "pesticide registration sanitary insecticide indoor efficacy test and evaluation part 9: and a repellent and GB/T30126 and 2013 detection and evaluation of mosquito prevention performance of textiles, wherein the fabric sample in 2.2 is subjected to mosquito prevention performance detection to obtain a good mosquito repellent effect of aedes albopictus. The specific operation is as follows:
providing a test insect: aedes albopictus (Aedes albopictus), uninoculated female adults 4-7 days after emergence;
the test conditions are as follows: the temperature was 26.2 ℃ and the relative humidity was 61.7%.
And (4) calculating a result: calculating the repellent rate of the finished fabric to mosquitoes, wherein R ═ B1-T1)/B1 x 100% (1) is shown in the formula: r is the repelling rate,%; b1 represents the average of control mosquito retentions, only; t1 represents the average of mosquito retentions of the samples to be tested. The test results are shown in Table 1.
TABLE 1 repellent Effect of the mosquito repellent samples on Aedes albopictus
3. Conclusion of the experiment
The repellent rate of the mosquito repellent sample to aedes albopictus is 66.34%, the evaluation is carried out according to GB/T30126 plus 2013 detection and evaluation of textile mosquito repellent performance, the inspected sample has good repellent effect, and the mosquito repellent rating is B level.
Example 2 preparation of mosquito repellent botanical pharmaceutical composition 1.2
1.1A mosquito-repellent botanical pharmaceutical composition, which comprises the following medicinal materials in parts by weight: 10 parts of mint, 10 parts of clove, 13 parts of perilla leaf, 10 parts of rhizoma acori graminei, 16 parts of folium artemisiae argyi, 13 parts of dried orange peel, 10 parts of thin evodia leaf, 10 parts of herba Anoectochili Roxburghii, 16 parts of herba houttuyniae and 16 parts of lavender.
Weighing the following raw material medicines: 10g of mint, 10g of clove, 13g of perilla leaf, 10g of rhizoma acori graminei, 16g of folium artemisiae argyi, 13g of dried orange peel, 10g of thin evodia leaf, 10g of herba oectochili roxburghii, 16g of herba houttuyniae and 16g of lavender, and the traditional Chinese medicinal materials are dried, crushed into fine powder and uniformly mixed for later use.
1.2 taking primary color pure cotton knitted fabric (the gram weight is about 147 g/m)2) The weight was about 99.2 g.
2 methods and results
2.1 taking 1.1 of the traditional Chinese medicine powder, mixing the powder with 1: 20, adding water, mixing, heating to 80 deg.C for 10min, filtering with a 280-mesh steel sieve to remove residue, and filtering to obtain medicinal liquid.
2.2 soaking 1.2 cloth sample in 2.1 medicinal liquid, soaking and rolling with JX macrohair dyeing and finishing padding machine, and drying at 100 deg.C for 5 min.
2.3 reference GB/T13917.9-2009 "pesticide registration sanitary insecticide indoor efficacy test and evaluation part 9: and a repellent and GB/T30126 and 2013 detection and evaluation of mosquito prevention performance of textiles, wherein the fabric sample in 2.2 is subjected to mosquito prevention performance detection to obtain a good mosquito repellent effect of aedes albopictus. The specific operation is as follows:
providing a test insect: aedes albopictus (Aedes albopictus), uninoculated female adults 4-7 days after emergence;
the test conditions are as follows: the temperature was 26.2 ℃ and the relative humidity was 61.7%.
And (4) calculating a result: calculating the repellent rate of the finished fabric to mosquitoes, wherein R ═ B1-T1)/B1 x 100% (1) is shown in the formula: r is the repelling rate,%; b1 represents the average of control mosquito retentions, only; t1 represents the average of mosquito retentions of the samples to be tested. The test results are shown in Table 2.
TABLE 2 repellent Effect of the mosquito repellent samples on Aedes albopictus
3. Conclusion of the experiment
The repellent rate of the mosquito repellent sample to aedes albopictus is 63.64%, the evaluation is carried out according to GB/T30126 plus 2013 detection and evaluation of textile mosquito repellent performance, the inspected sample has good repellent effect, and the mosquito repellent rating is B level.
Example 3 preparation of mosquito repellent botanical pharmaceutical composition 1.3
1.1A mosquito-repellent botanical pharmaceutical composition, which comprises the following medicinal materials in parts by weight: 15 parts of mint, 12 parts of clove, 15 parts of perilla leaf, 12 parts of rhizoma acori graminei, 18 parts of folium artemisiae argyi, 15 parts of dried orange peel, 12 parts of thin evodia, 15 parts of herba Anoectochili Roxburghii, 18 parts of herba houttuyniae and 18 parts of lavender.
Weighing the following raw material medicines: 15g of mint, 12g of clove, 15g of perilla leaf, 12g of rhizoma acori graminei, 18g of folium artemisiae argyi, 15g of dried orange peel, 12g of thin evodia leaf, 15g of herba oectochili roxburghii, 18g of herba houttuyniae and 18g of lavender, drying the traditional Chinese medicinal materials, crushing the traditional Chinese medicinal materials into fine powder, and uniformly mixing the fine powder for later use.
1.2 taking primary color pure cotton knitted fabric (the gram weight is about 147 g/m)2) The weight was about 120.0 g.
2 methods and results
2.1 taking 1.1 of the traditional Chinese medicine powder, mixing the powder with 1: 20, adding water, mixing, heating to 80 deg.C for 10min, filtering with a 280-mesh steel sieve to remove residue, and filtering to obtain medicinal liquid.
2.2 soaking 1.2 cloth sample in 2.1 medicinal liquid, soaking and rolling with JX macrohair dyeing and finishing padding machine, and drying at 100 deg.C for 5 min.
2.3 reference GB/T13917.9-2009 "pesticide registration sanitary insecticide indoor efficacy test and evaluation part 9: and a repellent and GB/T30126 and 2013 detection and evaluation of mosquito prevention performance of textiles, wherein the fabric sample in 2.2 is subjected to mosquito prevention performance detection to obtain a good mosquito repellent effect of aedes albopictus. The specific operation is as follows:
providing a test insect: aedes albopictus (Aedes albopictus), uninoculated female adults 4-7 days after emergence;
the test conditions are as follows: the temperature was 26.2 ℃ and the relative humidity was 61.7%.
And (4) calculating a result: calculating the repellent rate of the finished fabric to mosquitoes, wherein R ═ B1-T1)/B1 x 100% (1) is shown in the formula: r is the repelling rate,%; b1 represents the average of control mosquito retentions, only; t1 represents the average of mosquito retentions of the samples to be tested. The test results are shown in Table 3.
TABLE 3 repellent Effect of the mosquito repellent samples on Aedes albopictus
3. Conclusion of the experiment
The repellent rate of the mosquito repellent sample to aedes albopictus is 57.14%, the evaluation is carried out according to GB/T30126 plus 2013 detection and evaluation of textile mosquito repellent performance, the inspected sample has good repellent effect, and the mosquito repellent rating is B level.
Example 4 preparation of mosquito repellent botanical pharmaceutical composition 1.4
1.1A mosquito-repellent botanical pharmaceutical composition, which comprises the following medicinal materials in parts by weight: 10 parts of mint, 8 parts of clove, 12 parts of perilla leaf, 10 parts of rhizoma acori graminei, 15 parts of folium artemisiae argyi, 12 parts of dried orange peel, 10 parts of thin evodia, 10 parts of herba Anoectochili Roxburghii, 15 parts of herba houttuyniae and 15 parts of lavender.
Weighing the following raw material medicines: 10g of mint, 8g of clove, 12g of perilla leaf, 10g of rhizoma acori graminei, 15g of folium artemisiae argyi, 12g of dried orange peel, 10g of thin evodia leaf, 10g of herba oectochili roxburghii, 15g of herba houttuyniae and 15g of lavender, and the traditional Chinese medicinal materials are dried, crushed into fine powder and uniformly mixed for later use.
1.2 taking primary color pure cotton knitted fabric (the gram weight is about 147 g/m)2) The weight was about 117 g.
2 methods and results
2.1 taking 1.1 of the traditional Chinese medicine powder, mixing the powder with 1: 20, adding water, mixing, heating to 80 deg.C for 10min, filtering with a 280-mesh steel sieve to remove residue, and filtering to obtain medicinal liquid.
2.2 soaking 1.2 cloth sample in 2.1 medicinal liquid, soaking and rolling with JX macrohair dyeing and finishing padding machine, and drying at 100 deg.C for 5 min.
2.3 reference GB/T13917.9-2009 "pesticide registration sanitary insecticide indoor efficacy test and evaluation part 9: and a repellent and GB/T30126 and 2013 detection and evaluation of mosquito prevention performance of textiles, wherein the fabric sample in 2.2 is subjected to mosquito prevention performance detection to obtain a good mosquito repellent effect of aedes albopictus. The specific operation is as follows:
providing a test insect: aedes albopictus (Aedes albopictus), uninoculated female adults 4-7 days after emergence;
the test conditions are as follows: the temperature was 26.2 ℃ and the relative humidity was 61.7%.
And (4) calculating a result: calculating the repellent rate of the finished fabric to mosquitoes, wherein R ═ B1-T1)/B1 x 100% (1) is shown in the formula: r is the repelling rate,%; b1 represents the average of control mosquito retentions, only; t1 represents the average of mosquito retentions of the samples to be tested. The test results are shown in Table 4.
TABLE 4 repellent Effect of the mosquito repellent samples on Aedes albopictus
3. Conclusion of the experiment
The repellent rate of the mosquito repellent sample to aedes albopictus is 60.00%, the evaluation is carried out according to GB/T30126 plus 2013 detection and evaluation of textile mosquito repellent performance, the inspected sample has good repellent effect, and the mosquito repellent rating is B level.
According to the analysis of the cases of the examples 1 to 4, the mosquito-repellent botanical pharmaceutical composition comprises the following components in parts by weight: 10 parts of mint, 8 parts of clove, 12 parts of perilla leaf, 10 parts of rhizoma acori graminei, 15 parts of folium artemisiae argyi, 12 parts of dried orange peel, 10 parts of thin evodia, 10 parts of anoectochilus roxburghii, 15 parts of herba houttuyniae and 15 parts of lavender, wherein the mosquito repelling effect of the mosquito repelling textile is better than that of other proportions; and when the weight ratio of the textile raw materials to the traditional Chinese medicine powder in the step (4) is 1: 1.25-2.0, the obtained textile has the best avoidance effect, and the medicine is effectively utilized to the maximum extent in the proportion, for example, the medicine component is insufficient below the proportion, and the medicine is too concentrated above the proportion to achieve the maximum utilization effect.
Example 5 preparation of botanical drug mosquito repellent textile 2
1 Material
1.1 weighing the following raw material medicines: 10g of mint, 8g of clove, 12g of perilla leaf, 10g of rhizoma acori graminei, 15g of folium artemisiae argyi, 12g of dried orange peel, 10g of thin evodia leaf, 10g of herba oectochili roxburghii, 15g of herba houttuyniae and 15g of lavender, and the traditional Chinese medicinal materials are dried, crushed into fine powder and uniformly mixed for later use.
1.2 taking primary color pure cotton knitted fabric (the gram weight is about 147 g/m)2) The weights were about 234g, 117g, 78g, 58.5g, respectively.
2 methods and results
2.1 taking 1.1 Chinese medicinal powder, wrapping into small bag with cotton cloth, placing into sealed plastic bag together with 1.2 cloth sample, and keeping sealed state for more than 12 h.
2.2 reference GB/T13917.9-2009 "pesticide registration sanitary insecticide indoor efficacy test and evaluation part 9: and a repellent and GB/T30126 and 2013 detection and evaluation of mosquito prevention performance of textiles, wherein the fabric sample in 2.2 is subjected to mosquito prevention performance detection to obtain a good mosquito repellent effect of aedes albopictus. The specific operation is as follows:
providing a test insect: aedes albopictus (Aedes albopictus), uninoculated female adults 4-7 days after emergence;
the test conditions are as follows: the temperature was 26.2 ℃ and the relative humidity was 61.7%.
And (4) calculating a result: calculating the repellent rate of the finished fabric to mosquitoes, wherein R ═ B1-T1)/B1 x 100% (1) is shown in the formula: r is the repelling rate,%; b1 represents the average of control mosquito retentions, only; t1 represents the average of mosquito retentions of the samples to be tested. The test results are shown in Table 5.
TABLE 5 repellent Effect of the mosquito repellent samples on Aedes albopictus
3 conclusion of the test
The repellent rate of the mosquito repellent sample to aedes albopictus is 57.27-60.00%, and the inspection sample has good repellent effect according to GB/T30126 plus 2013 detection and evaluation of anti-mosquito performance of textiles, and the anti-mosquito rating is B level.
Example 6 preparation of botanical drug mosquito repellent textile 3
1 Material
1.1 weighing the following raw material medicines: the traditional Chinese medicine composition is prepared by drying and crushing the traditional Chinese medicinal materials into fine powder, and uniformly mixing the fine powder for later use, wherein the fine powder comprises 14g of mint, 11.2g of clove, 16.8g of perilla leaf, 14g of rhizoma acori graminei, 21g of folium artemisiae argyi, 16.8g of dried orange peel, 14g of thin evodia leaf, 14g of herba oectochili, 21g of herba houttuyniae and 21g of lavender. Divided into two parts on average.
1.2 taking primary color pure cotton knitted fabric (the gram weight is about 147 g/m)2) The weight was about 93.6 g.
2 methods and results
2.1 taking 117g of 1.1 Chinese medicinal powder, mixing the raw materials in a ratio of 1: 20 portions of water are added, the mixture is evenly mixed, heated to 80 ℃ for 10min, the residue is filtered by a 280-mesh steel sieve, and the liquid medicine is filtered. Soaking 1.2 cloth sample in the filtrate, soaking and rolling with JX macrodyeing and finishing padding machine, and drying at 100 deg.C for 5 min.
2.2 taking 46.8g of 1.1 traditional Chinese medicine powder, wrapping the powder into small bags by cotton cloth, putting the small bags and the cloth sample obtained in 2.1 into a sealed plastic bag, and keeping the sealed state for more than 12 hours for later use.
2.3 reference GB/T13917.9-2009 "pesticide registration sanitary insecticide indoor efficacy test and evaluation part 9: and a repellent and GB/T30126 and 2013 detection and evaluation of mosquito prevention performance of textiles, wherein the fabric sample in 2.2 is subjected to mosquito prevention performance detection to obtain a good mosquito repellent effect of aedes albopictus. The specific operation is as follows:
providing a test insect: aedes albopictus (Aedes albopictus), uninoculated female adults 4-7 days after emergence;
the test conditions are as follows: the temperature was 26.2 ℃ and the relative humidity was 61.7%.
And (4) calculating a result: calculating the repellent rate of the finished fabric to mosquitoes, wherein R ═ B1-T1)/B1 x 100% (1) is shown in the formula: r is the repelling rate,%; b1 represents the average of control mosquito retentions, only; t1 represents the average of mosquito retentions of the samples to be tested. The test results are shown in Table 6.
TABLE 6 repellent Effect of the mosquito repellent samples on Aedes albopictus
3 conclusion of the test
The repellent rate of the mosquito repellent sample to aedes albopictus is 67.62%, the evaluation is carried out according to GB/T30126 plus 2013 detection and evaluation of textile mosquito repellent performance, the inspected sample has good repellent effect, and the mosquito repellent rating is B level.
Although the invention has been described in detail hereinabove with respect to a general description and specific embodiments thereof, it will be apparent to those skilled in the art that modifications or improvements may be made thereto based on the invention. Accordingly, such modifications and improvements are intended to be within the scope of the invention as claimed.
Claims (10)
1. The mosquito-repellent botanical drug composition is characterized by comprising the following medicinal materials in parts by weight: 10-15 parts of mint, 8-12 parts of clove, 12-15 parts of perilla leaf, 10-12 parts of rhizoma acori graminei, 15-18 parts of folium artemisiae argyi, 12-15 parts of dried orange peel, 10-12 parts of evodia lepta, 10-15 parts of anoectochilus formosanus, 15-18 parts of herba houttuyniae and 15-18 parts of lavender.
2. The mosquito-repellent botanical pharmaceutical composition according to claim 1, which comprises the following medicinal materials in parts by weight: 10 parts of mint, 8 parts of clove, 12 parts of perilla leaf, 10 parts of rhizoma acori graminei, 15 parts of folium artemisiae argyi, 12 parts of dried orange peel, 10 parts of thin evodia, 10 parts of herba Anoectochili Roxburghii, 15 parts of herba houttuyniae and 15 parts of lavender.
3. The use of the mosquito repellent botanical pharmaceutical composition of claim 1 or 2 in the preparation of a mosquito repellent product.
4. The use of claim 3, wherein the mosquito repellent product comprises a mosquito repellent liquid, a mosquito repellent bracelet, and a mosquito repellent product.
5. A preparation method of a botanical drug mosquito-repellent textile is characterized by comprising the following steps:
(1) weighing the mosquito-repellent botanical drug composition of claim 1 or 2 in proportion;
(2) drying and pulverizing the Chinese medicinal materials into 50-100 mesh fine powder for later use;
(3) taking the Chinese medicine powder in the step (2) according to the proportion of 1: adding water at a ratio of 10-30, mixing, heating to 80 deg.C for 10min, filtering with 280 mesh steel sieve to remove residue, and filtering to obtain medicinal liquid;
(4) soaking the textile in the liquid medicine in the step (3), soaking and rolling the textile by a JX macrohair dyeing and finishing padding machine for two times, then drying the textile for later use at 80-100 ℃ for 3-10min to obtain the botanical drug mosquito-repellent textile raw material.
6. The preparation method according to claim 5, wherein the weight ratio of the textile raw materials to the traditional Chinese medicine powder in the step (4) is 1: 1 to 2.0.
7. A preparation method of a botanical drug mosquito-repellent textile is characterized by comprising the following steps:
(1) weighing the mosquito-repellent botanical drug composition of claim 1 or 2 in proportion;
(2) drying and pulverizing the Chinese medicinal materials into 50-100 mesh fine powder for later use;
(3) and (3) wrapping the traditional Chinese medicine powder in the step (2) by using cotton cloth to form a small bag, putting the small bag and the textile raw materials into a sealed plastic bag, and sealing and placing the bag at normal temperature for 12-72 hours to obtain the mosquito-repellent textile raw material.
8. The preparation method according to claim 7, wherein the weight ratio of the textile raw materials to the traditional Chinese medicine powder in the step (3) is 1: 0.5 to 2.0.
9. A preparation method of botanical drug mosquito-repellent textile is characterized in that,
(1) weighing the mosquito-repellent botanical drug composition of claim 1 or 2 in proportion;
(2) mixing the textile raw materials with the traditional Chinese medicine powder 1: weighing the raw traditional Chinese medicinal materials in a weight ratio of 1-2.0, drying the traditional Chinese medicinal materials, and crushing the dried traditional Chinese medicinal materials into 50-100 meshes of fine powder for later use;
(3) taking the Chinese medicine powder in the step (2) according to the proportion of 1: adding water at a ratio of 10-30, mixing, heating to 80 deg.C for 10min, filtering with 280 mesh steel sieve to remove residue, and filtering to obtain medicinal liquid;
(4) soaking the textile in the liquid medicine in the step (3), soaking and rolling the textile by a JX macro dyeing and finishing padding machine for two times, then drying the textile for later use at the temperature of 80-100 ℃ for 3-10 min;
(5) mixing the textile raw materials with the traditional Chinese medicine powder 1: and (3) wrapping the traditional Chinese medicine powder in the step (1) into a small bag by using cotton cloth according to the weight ratio of 0.5-2.0, putting the small bag and the textile dried in the step (4) into a sealed plastic bag, and sealing and placing the bag at normal temperature for 12-72 hours to obtain the botanical drug mosquito-repellent textile raw material.
10. The method of claim 9, wherein the total weight ratio of the textile raw materials to the traditional Chinese medicine powder is 1: 1.5 to 3.0.
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