CN113862871A - Long-acting mosquito-repelling polyester fabric and preparation method thereof - Google Patents
Long-acting mosquito-repelling polyester fabric and preparation method thereof Download PDFInfo
- Publication number
- CN113862871A CN113862871A CN202110755688.4A CN202110755688A CN113862871A CN 113862871 A CN113862871 A CN 113862871A CN 202110755688 A CN202110755688 A CN 202110755688A CN 113862871 A CN113862871 A CN 113862871A
- Authority
- CN
- China
- Prior art keywords
- parts
- mosquito
- repellent
- long
- repelling
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229920000728 polyester Polymers 0.000 title claims abstract description 43
- 239000004744 fabric Substances 0.000 title claims abstract description 40
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 238000004519 manufacturing process Methods 0.000 title description 3
- 239000000077 insect repellent Substances 0.000 claims abstract description 53
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 28
- 239000000835 fiber Substances 0.000 claims abstract description 23
- WOZVHXUHUFLZGK-UHFFFAOYSA-N dimethyl terephthalate Chemical compound COC(=O)C1=CC=C(C(=O)OC)C=C1 WOZVHXUHUFLZGK-UHFFFAOYSA-N 0.000 claims abstract description 22
- -1 polyethylene terephthalate Polymers 0.000 claims abstract description 18
- 239000005020 polyethylene terephthalate Substances 0.000 claims abstract description 15
- RLLPVAHGXHCWKJ-UHFFFAOYSA-N permethrin Chemical compound CC1(C)C(C=C(Cl)Cl)C1C(=O)OCC1=CC=CC(OC=2C=CC=CC=2)=C1 RLLPVAHGXHCWKJ-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229960000490 permethrin Drugs 0.000 claims abstract description 12
- CXBMCYHAMVGWJQ-CABCVRRESA-N (1,3-dioxo-4,5,6,7-tetrahydroisoindol-2-yl)methyl (1r,3r)-2,2-dimethyl-3-(2-methylprop-1-enyl)cyclopropane-1-carboxylate Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)OCN1C(=O)C(CCCC2)=C2C1=O CXBMCYHAMVGWJQ-CABCVRRESA-N 0.000 claims abstract description 11
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229920000139 polyethylene terephthalate Polymers 0.000 claims abstract description 11
- 229960005199 tetramethrin Drugs 0.000 claims abstract description 11
- 238000009987 spinning Methods 0.000 claims abstract description 10
- 239000012188 paraffin wax Substances 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 241001529821 Agastache Species 0.000 claims abstract description 6
- 241001162994 Rugosus Species 0.000 claims abstract description 6
- 230000032050 esterification Effects 0.000 claims abstract description 5
- 238000005886 esterification reaction Methods 0.000 claims abstract description 5
- 150000002148 esters Chemical group 0.000 claims abstract description 5
- 238000006068 polycondensation reaction Methods 0.000 claims abstract description 5
- BTVWZWFKMIUSGS-UHFFFAOYSA-N dimethylethyleneglycol Natural products CC(C)(O)CO BTVWZWFKMIUSGS-UHFFFAOYSA-N 0.000 claims abstract description 4
- 238000001035 drying Methods 0.000 claims description 18
- 238000002156 mixing Methods 0.000 claims description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 8
- 238000007667 floating Methods 0.000 claims description 5
- 238000009941 weaving Methods 0.000 claims description 5
- 238000004140 cleaning Methods 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 3
- 238000000643 oven drying Methods 0.000 claims description 2
- 238000010298 pulverizing process Methods 0.000 claims description 2
- 241000255925 Diptera Species 0.000 abstract description 10
- 230000000694 effects Effects 0.000 abstract description 6
- 230000001846 repelling effect Effects 0.000 abstract description 6
- 239000002202 Polyethylene glycol Substances 0.000 abstract description 3
- 229920001223 polyethylene glycol Polymers 0.000 abstract description 3
- KKEYFWRCBNTPAC-UHFFFAOYSA-L terephthalate(2-) Chemical compound [O-]C(=O)C1=CC=C(C([O-])=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-L 0.000 abstract description 3
- 239000007788 liquid Substances 0.000 abstract description 2
- 230000007774 longterm Effects 0.000 abstract description 2
- 229920001707 polybutylene terephthalate Polymers 0.000 description 5
- RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical compound COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 description 4
- 244000165852 Eucalyptus citriodora Species 0.000 description 3
- 235000004722 Eucalyptus citriodora Nutrition 0.000 description 3
- 239000004743 Polypropylene Substances 0.000 description 3
- 229920004933 Terylene® Polymers 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 229940092258 rosemary extract Drugs 0.000 description 3
- 235000020748 rosemary extract Nutrition 0.000 description 3
- 239000001233 rosmarinus officinalis l. extract Substances 0.000 description 3
- 239000004753 textile Substances 0.000 description 3
- 244000205574 Acorus calamus Species 0.000 description 2
- 229920002972 Acrylic fiber Polymers 0.000 description 2
- NPBVQXIMTZKSBA-UHFFFAOYSA-N Chavibetol Natural products COC1=CC=C(CC=C)C=C1O NPBVQXIMTZKSBA-UHFFFAOYSA-N 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 2
- 239000005770 Eugenol Substances 0.000 description 2
- 241000238631 Hexapoda Species 0.000 description 2
- UVMRYBDEERADNV-UHFFFAOYSA-N Pseudoeugenol Natural products COC1=CC(C(C)=C)=CC=C1O UVMRYBDEERADNV-UHFFFAOYSA-N 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000005038 ethylene vinyl acetate Substances 0.000 description 2
- 229960002217 eugenol Drugs 0.000 description 2
- 230000007794 irritation Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000011087 paperboard Substances 0.000 description 2
- 239000001331 rosmarinus officinalis leaf Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 241000238876 Acari Species 0.000 description 1
- 235000006480 Acorus calamus Nutrition 0.000 description 1
- 244000001632 Acorus gramineus Species 0.000 description 1
- 235000013073 Acorus gramineus Nutrition 0.000 description 1
- 235000011996 Calamus deerratus Nutrition 0.000 description 1
- 229920004934 Dacron® Polymers 0.000 description 1
- 201000004624 Dermatitis Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241000331598 Trombiculidae Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 238000010409 ironing Methods 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 229920001200 poly(ethylene-vinyl acetate) Polymers 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 239000012209 synthetic fiber Substances 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/20—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the material of the fibres or filaments constituting the yarns or threads
- D03D15/283—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the material of the fibres or filaments constituting the yarns or threads synthetic polymer-based, e.g. polyamide or polyester fibres
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/92—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
-
- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/50—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the properties of the yarns or threads
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
- D10B2331/04—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyesters, e.g. polyethylene terephthalate [PET]
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/13—Physical properties anti-allergenic or anti-bacterial
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a long-acting mosquito-repelling polyester fabric and a preparation method thereof, relates to the technical field of polyester fabrics, and aims at solving the problem that the existing mosquito-repelling polyester fabric in the background art cannot keep a long-term effective mosquito-repelling effect, the following scheme is proposed, wherein the scheme comprises the following raw materials in parts by mass: 200 parts of polyester fiber, 20-30 parts of poly terephthalic acid, 20-30 parts of dimethyl terephthalate, 15-25 parts of ethylene glycol, 10-20 parts of tetramethrin, 10-20 parts of paraffin, 10-15 parts of permethrin, 5-10 parts of agastache rugosus and 8-12 parts of rhizoma acori graminei extract solution. According to the invention, polyethylene glycol terephthalate is obtained by esterification or ester exchange and polycondensation of polyethylene terephthalate, dimethyl terephthalate and ethylene glycol, and is mixed with mosquito repellent liquid obtained from permethrin, tetramethrin and rhizoma acori graminei extract solution to form mosquito repellent fibers, so that the volatilization of the mosquito repellent in the spinning process can be reduced, and the volatilization speed of the mosquito repellent from the fibers can be slowed down, thereby achieving the effect of long-acting mosquito repelling.
Description
Technical Field
The invention relates to the technical field of polyester fabrics, in particular to a long-acting mosquito-repellent polyester fabric and a preparation method thereof.
Background
Terylene is also called polyester fiber, and is a textile formed by interweaving warp and weft yarns in a vertical and horizontal sinking and floating manner through a weaving machine. The terylene fabric has higher strength and elastic recovery capability, thus being firm and durable, and being crease-resistant and non-ironing. The polyester fabric has poor hygroscopicity, stuffy feeling when worn in summer, and easy electrostatic charge in winter, which affects comfort. But after washing, the fabric is extremely easy to dry, the wet strength is hardly reduced, the fabric is not deformed, and the fabric has good washing and wearing performance. The terylene is the fabric with the best heat resistance in the synthetic fiber fabric, has thermoplasticity, can be made into a pleated skirt, and has lasting pleating. The light resistance of the polyester fabric is better, and the sun-proof capability of the polyester fabric is better than that of a natural fiber fabric except that the polyester fabric is poorer than that of acrylic fiber. Especially, the sun-proof capability behind the glass is very good and almost the same as that of acrylic fiber. The polyester fabric has good resistance to various chemicals. The damage degree of acid and alkali is not large, and the product is not afraid of mould and worm damage.
The existing insect repellents are classified into anpolyester, permethrin, Ex-Calmette and Eucalyptus citriodora oil, the anpolyester is the most effective and thoroughly researched insect repellents in the market at present, the substance shows remarkable safety after being used for 40 years in the world, the plant-based insect repellents are generally not as effective as the deet, the deet is particularly effective to mosquitoes and can also repel other insects such as flies, chiggers and ticks, the deet can block the odor tracking capacity of the insects, compared with the ander polyester, the permethrin has the remarkable characteristics of lower toxicity, smaller irritation, longer repelling time and the like, but the mosquito repelling effect is not good enough, the irritation of the Ex-Calmette to the skin is equivalent to that of the deet, the mosquito repelling effect of the Eucalyptus citriodora is equivalent to that of the deet, but the Eucalyptus citriodora oil can irritate the eyes and easily cause skin allergy, and has strong smell.
Along with the progress of science and technology, the improvement of people's standard of living also corresponding improvement to the functional requirement of fabric, along with the continuous progress of textile technology, the textile product that design production has the mosquito repellent function, can satisfy people and reach the effect of mosquito repellent under the prerequisite that does not use insecticide and mosquito-repellent incense floral water like clothes etc. nevertheless, current mosquito repellent dacron can not keep long-term effectual mosquito repellent effect.
Disclosure of Invention
Based on the technical problems in the background art, the invention provides a long-acting mosquito-repellent polyester fabric and a preparation method thereof.
The invention provides a long-acting mosquito-repelling polyester fabric which comprises the following raw materials in parts by mass: 200 parts of polyester fiber, 20-30 parts of poly terephthalic acid, 20-30 parts of dimethyl terephthalate, 15-25 parts of ethylene glycol, 10-20 parts of tetramethrin, 10-20 parts of paraffin, 10-15 parts of chloranthester, 5-10 parts of agastache rugosus and 8-12 parts of rhizoma acori graminei extract solution.
Preferably, the feed comprises the following raw materials in parts by mass: 200 parts of polyester fiber, 30-40 parts of poly-terephthalic acid, 30-40 parts of dimethyl terephthalate, 25-35 parts of ethylene glycol, 20-30 parts of tetramethrin, 15-25 parts of paraffin, 15-20 parts of permethrin, 10-15 parts of agastache rugosus extract solution and 12-16 parts of rhizoma acori graminei extract solution.
The preparation method of the long-acting mosquito-repellent polyester fabric is characterized by comprising the following steps:
s1: taking proper amount of polyethylene terephthalate, dimethyl terephthalate and ethylene glycol, uniformly mixing, and carrying out esterification or ester exchange and polycondensation reaction to obtain polyethylene terephthalate;
s2: taking appropriate amount of permethrin, tetramethrin and rhizoma Acori Graminei extract solution, and stirring on a magnetic stirrer for 30-60min to obtain mosquito repellent;
s3: mixing polyethylene terephthalate slices with a mosquito repellent, standing for 1-2h at a constant temperature of 40 ℃, stirring by a stirrer, and mixing and granulating at 200 ℃ by a screw extruder to obtain mosquito repellent core slices;
s4: slicing the mosquito-repellent core, drying by a vacuum dryer, and putting into a spinning machine for spinning to obtain mosquito-repellent fiber;
s5: and (3) putting the mosquito-repellent fiber and the polyester fiber into a loom, and interweaving and weaving warp and weft yarns of the loom in a vertical and horizontal sinking and floating manner to obtain the long-acting mosquito-repellent polyester fabric.
Preferably, the method of the grassleaf sweelflag rhizome extract solution in step S2 is: cleaning rhizoma Acori Graminei leaf, oven drying, pulverizing, adding 20% ethanol solution, and standing for 5-10 hr.
Preferably, the drying conditions in step S4 are: the drying temperature is 90-100 ℃, the drying time is 6-7h, and the pressure in the vacuum dryer is-0.4 MPa to-0.6 MPa.
The invention has the beneficial effects that:
the invention obtains polyethylene glycol terephthalate by esterification or ester exchange and polycondensation reaction of polyethylene terephthalate, dimethyl terephthalate and glycol, and the polyethylene glycol terephthalate is mixed with mosquito repellent liquid obtained by permethrin, tetramethrin and acorus gramineus extract solution to form mosquito repellent fiber, so that the volatilization of the mosquito repellent agent in the spinning process can be reduced, and the volatilization speed of the mosquito repellent agent from the fiber can be slowed down, thereby achieving the effect of long-acting mosquito repelling.
Detailed Description
The technical solutions in the embodiments of the present invention will be described below clearly and completely in connection with the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments.
Example 1: the long-acting mosquito-repelling polyester fabric comprises the following raw materials in parts by weight: 200 parts of polyester fiber, 20 parts of poly terephthalic acid, 20 parts of dimethyl terephthalate, 15 parts of ethylene glycol, 10 parts of tetramethrin, 10 parts of paraffin, 10 parts of permethrin, 5 parts of agastache rugosus and 8 parts of calamus extract solution.
A preparation method of a long-acting mosquito-repellent polyester fabric comprises the following steps:
s1: taking proper amount of polyethylene terephthalate, dimethyl terephthalate and ethylene glycol, uniformly mixing, and carrying out esterification or ester exchange and polycondensation reaction to obtain polyethylene terephthalate;
s2: taking appropriate amount of Esquirrel, eugenol and rosemary extract solution, placing on a magnetic stirrer, stirring for 30-60min to obtain mosquito repellent, wherein the rosemary extract extraction method comprises: cleaning and drying rosemary leaf slices, crushing the rosemary leaf slices, adding a 20% ethanol solution, and standing for 5-10 h;
s3: mixing the PP mixture with a mosquito repellent, standing for 1-2h at a constant temperature of 40 ℃, stirring by a stirrer, and mixing and granulating by a screw extruder at 200 ℃ to obtain mosquito repellent core slices;
s4: the preparation method comprises the following steps of slicing polybutylene terephthalate, mixing the polybutylene terephthalate with the mosquito repellent core slices, drying the polybutylene terephthalate by using a vacuum dryer, and spinning the polybutylene terephthalate in a spinning machine to obtain mosquito repellent fibers, wherein the drying conditions are as follows: the drying temperature is 90-100 ℃, the drying time is 4-5h, and the internal pressure of the vacuum dryer is-0.4 MPa to-0.6 MPa;
s5: and (3) putting the mosquito-repellent fiber and the cotton fiber into a loom, and interweaving and weaving warp and weft yarns of the loom in a vertically and horizontally sinking and floating manner to obtain the long-acting mosquito-repellent polyester fabric.
Example 2: the long-acting mosquito-repelling polyester fabric comprises the following raw materials in parts by mass: 200 parts of cotton fiber, 40 parts of polybutylene terephthalate, 35 parts of polypropylene, 35 parts of ethylene-vinyl acetate copolymer, 20 parts of paraffin, 25 parts of escargin, 20 parts of eugenol and 16 parts of rosemary extract solution.
A preparation method of a long-acting mosquito-repellent polyester fabric comprises the following steps:
s1: taking a proper amount of polypropylene, ethylene-vinyl acetate copolymer and paraffin, uniformly mixing, and then mixing and granulating at 260 ℃ by using a screw extruder to obtain a PP mixture;
s2: taking appropriate amount of permethrin, tetramethrin and rhizoma Acori Graminei extract solution, placing on a magnetic stirrer, stirring for 30-60min to obtain mosquito repellent, the method for preparing rhizoma Acori Graminei extract solution is: cleaning and drying the leaves of the acorus calamus, crushing, adding a 20% ethanol solution, and standing for 5-10 h;
s3: mixing polyethylene terephthalate slices with a mosquito repellent, standing for 1-2h at a constant temperature of 40 ℃, stirring by a stirrer, and mixing and granulating at 200 ℃ by a screw extruder to obtain mosquito repellent core slices;
s4: slicing the mosquito-repellent core, drying by a vacuum dryer, and then putting into a spinning machine for spinning to obtain mosquito-repellent fibers, wherein the drying conditions are as follows: the drying temperature is 90-100 ℃, the drying time is 6-7h, and the pressure in the vacuum dryer is-0.4 MPa to-0.6 MPa;
s5: and (3) putting the mosquito-repellent fiber and the polyester fiber into a loom, and interweaving and weaving warp and weft yarns of the loom in a vertical and horizontal sinking and floating manner to obtain the long-acting mosquito-repellent polyester fabric.
Mosquito repelling experiment
Taking two glass boxes (50cm multiplied by 50cm), dividing the middle of the two glass boxes into A, B chambers by using paper boards, opening a hole in the middle of the paper boards to facilitate mosquitoes to pass through, putting the mosquito repellent polyester fabric in the embodiment 1 in the A1 chamber, putting the mosquito repellent polyester fabric in the embodiment 2 in the A2 chamber, putting the polyester fabric in the B1 chamber and the B2 chamber, putting warm sugar water in the A, B chamber, putting 50 mosquitoes in the A1 chamber, the B1 chamber, the A2 chamber and the B2 chamber, observing the number of mosquitoes in the A1 chamber, the B1 chamber, the A2 chamber and the B2 chamber after a certain time, and obtaining an experimental result shown in table 1.
TABLE 1 mosquito repellent Effect of polyester fabrics
In summary, the embodiment 2 is the best embodiment of the present invention.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and equivalent alternatives or modifications according to the technical solution and the inventive concept of the present invention should be covered by the scope of the present invention.
Claims (5)
1. The long-acting mosquito-repelling polyester fabric is characterized by comprising the following raw materials in parts by mass: 200 parts of polyester fiber, 20-30 parts of poly terephthalic acid, 20-30 parts of dimethyl terephthalate, 15-25 parts of ethylene glycol, 10-20 parts of tetramethrin, 10-20 parts of paraffin, 10-15 parts of permethrin, 5-10 parts of agastache rugosus and 8-12 parts of rhizoma acori graminei extract solution.
2. The long-acting mosquito-repelling polyester fabric according to claim 1 is characterized by comprising the following raw materials in parts by mass: 200 parts of polyester fiber, 30-40 parts of poly terephthalic acid, 30-40 parts of dimethyl terephthalate, 25-35 parts of ethylene glycol, 20-30 parts of tetramethrin, 15-25 parts of paraffin, 15-20 parts of permethrin, 10-15 parts of agastache rugosus extract solution and 12-16 parts of rhizoma acori graminei extract solution.
3. The preparation method of the long-acting mosquito-repelling polyester fabric according to claim 1, which is characterized by comprising the following steps of:
s1: taking proper amount of polyethylene terephthalate, dimethyl terephthalate and ethylene glycol, uniformly mixing, and carrying out esterification or ester exchange and polycondensation reaction to obtain polyethylene terephthalate;
s2: taking appropriate amount of permethrin, tetramethrin and rhizoma Acori Graminei extract solution, and stirring on a magnetic stirrer for 30-60min to obtain mosquito repellent;
s3: mixing polyethylene terephthalate slices with a mosquito repellent, standing for 1-2h at a constant temperature of 40 ℃, stirring by a stirrer, and mixing and granulating at 200 ℃ by a screw extruder to obtain mosquito repellent core slices;
s4: slicing the mosquito-repellent core, drying by a vacuum dryer, and spinning in a spinning machine to obtain mosquito-repellent fiber;
s5: and (3) putting the mosquito-repellent fiber and the polyester fiber into a loom, and interweaving and weaving warp and weft yarns of the loom in a vertically and horizontally sinking and floating manner to obtain the long-acting mosquito-repellent polyester fabric.
4. The preparation method of the long-acting mosquito-repellent polyester fabric according to claim 3, wherein the method of the rhizoma acori graminei extract solution in the step S2 is as follows: cleaning rhizoma Acori Graminei leaf, oven drying, pulverizing, adding 20% ethanol solution, and standing for 5-10 hr.
5. The preparation method of the long-acting mosquito-repelling polyester fabric according to claim 3, wherein the drying conditions in the step S4 are as follows: the drying temperature is 90-100 ℃, the drying time is 6-7h, and the pressure in the vacuum dryer is-0.4 MPa to-0.6 MPa.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110755688.4A CN113862871A (en) | 2021-07-05 | 2021-07-05 | Long-acting mosquito-repelling polyester fabric and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110755688.4A CN113862871A (en) | 2021-07-05 | 2021-07-05 | Long-acting mosquito-repelling polyester fabric and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN113862871A true CN113862871A (en) | 2021-12-31 |
Family
ID=78990137
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202110755688.4A Pending CN113862871A (en) | 2021-07-05 | 2021-07-05 | Long-acting mosquito-repelling polyester fabric and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN113862871A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115478336A (en) * | 2022-09-14 | 2022-12-16 | 福建凤竹纺织科技股份有限公司 | Production process of polyester insecticidal fabric |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1389490A (en) * | 2002-07-05 | 2003-01-08 | 孙启明 | Production process of polyethylene glycol terephthalate |
| CN106106562A (en) * | 2016-06-23 | 2016-11-16 | 江苏金典纺织有限公司 | A kind of preparation technology of function of driving mosquitoes textile |
| CN108265343A (en) * | 2016-12-30 | 2018-07-10 | 常州英中纳米科技有限公司 | A kind of method and its textile fabric for preparing fragrant long-acting mosquito-driving fiber |
| CN109418333A (en) * | 2017-08-30 | 2019-03-05 | 桂林市愚人服装有限公司 | It is a kind of can mosquito repellent fly bamboo charcoal fiber |
| CN111109307A (en) * | 2019-12-30 | 2020-05-08 | 河北省农林科学院棉花研究所（河北省农林科学院特种经济作物研究所） | Preparation method of botanical drug mosquito-repellent textile and pharmaceutical composition thereof |
| CN112663334A (en) * | 2020-12-23 | 2021-04-16 | 杭州宏达装饰布织造有限公司 | Mosquito-repelling sleep-aiding fabric and processing method thereof |
| CN112853575A (en) * | 2020-12-30 | 2021-05-28 | 南通海宇化纤有限公司 | Polyester fabric production process |
-
2021
- 2021-07-05 CN CN202110755688.4A patent/CN113862871A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1389490A (en) * | 2002-07-05 | 2003-01-08 | 孙启明 | Production process of polyethylene glycol terephthalate |
| CN106106562A (en) * | 2016-06-23 | 2016-11-16 | 江苏金典纺织有限公司 | A kind of preparation technology of function of driving mosquitoes textile |
| CN108265343A (en) * | 2016-12-30 | 2018-07-10 | 常州英中纳米科技有限公司 | A kind of method and its textile fabric for preparing fragrant long-acting mosquito-driving fiber |
| CN109418333A (en) * | 2017-08-30 | 2019-03-05 | 桂林市愚人服装有限公司 | It is a kind of can mosquito repellent fly bamboo charcoal fiber |
| CN111109307A (en) * | 2019-12-30 | 2020-05-08 | 河北省农林科学院棉花研究所（河北省农林科学院特种经济作物研究所） | Preparation method of botanical drug mosquito-repellent textile and pharmaceutical composition thereof |
| CN112663334A (en) * | 2020-12-23 | 2021-04-16 | 杭州宏达装饰布织造有限公司 | Mosquito-repelling sleep-aiding fabric and processing method thereof |
| CN112853575A (en) * | 2020-12-30 | 2021-05-28 | 南通海宇化纤有限公司 | Polyester fabric production process |
Non-Patent Citations (1)
| Title |
|---|
| 钱立军，王澜: "《高分子材料》", 31 August 2020, 中国轻工业出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115478336A (en) * | 2022-09-14 | 2022-12-16 | 福建凤竹纺织科技股份有限公司 | Production process of polyester insecticidal fabric |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103215751B (en) | Preparation method of long-acting insect prevention and mosquito repelling PP (Polypropylene) non-woven fabric | |
| CN106564222B (en) | A kind of multifunctional non-woven fabric | |
| CN103620097A (en) | Antibacterial synthetic fiber, and method for manufacturing same | |
| KR20090034202A (en) | Nanofibers comprising naturalplant extract or naturalplant essential oil and method for producing the same | |
| CN1821456A (en) | Novel fabric with skin-care function and its preparing method | |
| CN113862871A (en) | Long-acting mosquito-repelling polyester fabric and preparation method thereof | |
| EP2038474A2 (en) | Composition for impregnation of textiles | |
| CN108265343A (en) | A kind of method and its textile fabric for preparing fragrant long-acting mosquito-driving fiber | |
| CN102383258A (en) | Long-lasting insect repellent fabric and method for producing same | |
| CN107955995B (en) | A kind of multifunctional protein fiber | |
| CN112962168A (en) | Antibacterial and anti-mite functional fabric | |
| CN112251838A (en) | Lavender-containing polyester fiber and preparation method thereof | |
| CN101792939B (en) | Functional fiber | |
| US20130203919A1 (en) | Synthetic fiber containing plant fatty acids and method for manufacturing same | |
| Karthik et al. | Milkweed—A potential sustainable natural fibre crop | |
| US20060157882A1 (en) | Filled ultramicrocellular structures | |
| David et al. | Classification of textile fibres: production, structure, and properties | |
| KR102609179B1 (en) | Eco-friendly uniform using recycled polyester fabric and manufacturing method thereof | |
| CN109554929B (en) | Antibacterial functional fiber and processing technology thereof | |
| CN113862819A (en) | Polyester fiber containing folium Artemisiae Argyi component and folium Artemisiae Argyi fragrance, and its preparation method | |
| TW200845894A (en) | Process and composition for synergistically enhanced insecticidal impregnation of a fabric or netting or other kind of non-living material | |
| TW201210478A (en) | Biocidal acid-adjusted polymer with polypropylene | |
| CN105926114A (en) | Long-acting mosquito-repellent thermal-moisture comfortable hemp fabric and preparation method thereof | |
| CN113445153A (en) | Long-acting mosquito-repelling pure cotton fabric and preparation method thereof | |
| CN116219746A (en) | Bio-based mosquito-repellent finishing agent and preparation method and application thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20211231 |