CN108265343A - A kind of method and its textile fabric for preparing fragrant long-acting mosquito-driving fiber - Google Patents
A kind of method and its textile fabric for preparing fragrant long-acting mosquito-driving fiber Download PDFInfo
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- CN108265343A CN108265343A CN201611255217.2A CN201611255217A CN108265343A CN 108265343 A CN108265343 A CN 108265343A CN 201611255217 A CN201611255217 A CN 201611255217A CN 108265343 A CN108265343 A CN 108265343A
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- Prior art keywords
- mosquito
- mosquito repellent
- fragrant
- fragrance
- long
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Classifications
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/92—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/44—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds as major constituent with other polymers or low-molecular-weight compounds
- D01F6/54—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds as major constituent with other polymers or low-molecular-weight compounds of polymers of unsaturated nitriles
Abstract
The invention discloses a kind of methods and its textile fabric for preparing fragrant long-acting mosquito-driving fiber, using first obtained fragrant culicifuge, then fragrant mosquito repellent master batch is made, and then fragrant long-acting mosquito-driving fiber is made by the fibers blend spinning such as fragrant mosquito repellent master batch and terylene, acrylic fibers, polyamide fibre, finally go out required textile fabric using the fibrous woven, such as mosquito repellent fragrance mosquito net, mosquito repellent fragrance tent, mosquito repellent fragrance charge garment, mosquito repellent fragrance footwear, mosquito repellent fragrance socks, mosquito repellent fragrance waterproof garment and mosquito repellent fragrance gloves;Mosquito repellent fiber obtained in this way has effects that long-acting slow-release mosquito repellent, and it is long to extend its usage time, due to anophelifuge substance and fiber are co-melting blended rather than coated in fiber surface therefore washing fastness it is good, preferable repelling effect can be still kept after washing;In addition the textile fabric has the experience that fragrance improves user.
Description
Technical field
It is specifically a kind of to prepare fragrant long-acting mosquito-driving fiber the present invention relates to a kind of method and its textile fabric for preparing fiber
Method and its textile fabric.
Background technology
With the development of science and technology the raising of living standards of the people, also accordingly improves the Functional Requirement of textile fabric.Mosquito
It bites and annoyings summer people’s lives always, the production for mosquitocidals mosquito eradications such as the invention various insecticides, anti-mosquito incense sheet, insecticidal solutions
Product.However, since the drug concentration for killing mosquito is higher, injury can more or less be generated to human body;And agrochemical kills
Worm tool belongs to passive type mosquitocidal pattern, and mosquito is there is also after having killed, can not it is long-acting holding mosquito repellent mosquitocidal the effect of, therefore
Also it can not just be truly realized from source and expel mosquito.Therefore, develop that a kind of dosage is few, it can be with the product of mosquito repellent, to from source
Upper repelling mosquitoes and preventing insects are of great significance to.
With being constantly progressive for textile technology, textile product of the design production with function of driving mosquitoes, such as clothes, on bed
Quilt blanket etc. can meet people and achieve the effect that mosquito repellent under the premise of without using insecticide and mosquito-repellent incense floral water.Outdoor production
After product increase function of driving mosquitoes, it can significantly avoid outdoor sports people that family can be substantially improved by the probability of bite by mosquitos
The outdoor experience of outer sports fan.Mosquito dispersing type textile fabric is also prevented from due to disease caused by bite by mosquitos.Therefore, it opens
Hair and manufacture mosquito dispersing type textile fabric, such as outerwear trousers, article, tent, not only there is considerable market prospects, can also be pre-
Such as zika virus disease that mosquito repellent sting generates is reduced because of disease caused by the summer disaster relief.
The technical foundation of textile product is exactly fibre technology, therefore produces a kind of fiber with mosquito repellent function and spun to improving
The mosquito repellent function tool for knitting product plays a very important role.Mosquito repellent fibre technology traditional at present will be driven in fiber manufacturing process
Mosquito agent is coated in the surface of fiber, although there is repelling effect in this way, persistence is poor, is easily washed with water, while is driven preparing
Exhaust gas and waste water can be generated during mosquito fiber;And due to being coated in fiber surface, skin is easily contacted, leads to user's meeting
Generate allergic phenomena.In addition chemical culicifuge is with certain pesticide taste, and then make the textile fabric of addition culicifuge
Used time can influence the experience of user.
Invention content
In view of the above existing problems in the prior art, the present invention provides a kind of method for preparing fragrant long-acting mosquito-driving fiber and
Its textile fabric has effects that long-acting slow-release mosquito repellent, and it is long to extend its usage time, and washing fastness is good;In addition there is fragrant gas
Taste improves the experience of user.
To achieve these goals, the technical solution adopted by the present invention is:This kind prepares the side of fragrant long-acting mosquito-driving fiber
Method, the specific steps are:
(1) by water, Ludox, surfactant, oil soluble perfume, mosquito and insect expelling agent, paraffin wax according to mass fraction
Proportioning is respectively:100 parts of water, surfactant are 0.1~10 part, and oil soluble perfume is 0.1~30 part, and mosquito and insect expelling agent is
0.1~30 part, Ludox ratio is 10~90 parts, the paraffin wax, oil soluble perfume and mosquito and insect expelling agent mass fraction
Ratio is 0.1:1~10:1;
(2) and then by said components it mixes in the following order, specially:It will slice first at a temperature of 60~100 DEG C
It is paraffin melting;Oil soluble perfume, mosquito and insect expelling agent are dissolved in liquid paraffin wax at this temperature, it is co-melting to form uniform liquid phase
Body;In addition water is heated to while agitating after 80 DEG C that surfactant is soluble in water, then will be cut under stirring
Piece paraffin, essence, the co-melting body of mosquito and insect expelling agent liquid phase are poured into the water dissolved with surfactant, form oil-in-water emulsion;Stirring 5
After minute, Ludox is added in into oil-in-water emulsion and is stopped after being stirred continuously until Ludox addition;By above-mentioned product
It is filtered at normal temperatures after being cooled to room temperature and obtains wet-milling;Wet-milling is 48 hours dry in 40 DEG C of baking oven, and last ball milling is made
Fragrant culicifuge;
(3) by fragrant culicifuge obtained above and textile fabric particle according to mass ratio 0.01~0.2:After 1 mixing
And it adds in additive and fragrant mosquito repellent master batch is made;
(4) by after one or more slices in terylene, acrylic fibers, PET with fragrant mosquito repellent master batch example 1 in mass ratio:0.01
Then~0.2 mixing carries out melt blending spinning and fragrant long-acting mosquito-driving fiber is made.
Further, the ball milling of the fragrant culicifuge is until 5000 mesh stop.
Further, the textile fabric particle is one or more combinations in polyamide fibre, terylene, polyamide.
Further, the mosquito and insect expelling agent is either mosquito repellent esters or the production of mosquito repellent amine of the Chinese herbal medicine with mosquito repellent function
Product.
Further, the additive is one or more combinations in PE waxes, antioxidant, light stabilizer.
Further, the Chinese herbal medicine with mosquito repellent function is one kind in folium artemisiae argyi, purple perilla, cloves, peppermint.
A kind of textile fabric of fragrance mosquito repellent, the textile fabric using long-acting mosquito-driving fibrous woven fragrant made from the above method and
Into.
Further, it is fragrant to include mosquito repellent fragrance mosquito net, mosquito repellent fragrance tent, mosquito repellent fragrance charge garment, mosquito repellent for the textile fabric
Fragrant footwear, mosquito repellent fragrance socks, mosquito repellent fragrance waterproof garment and mosquito repellent fragrance gloves.
Compared with prior art, then fragrant mosquito repellent master batch, Jin Ertong is made using fragrant culicifuge is first made in the present invention
It crosses the fragrant fibers blend spinning such as mosquito repellent master batch and terylene, acrylic fibers, polyamide fibre and fragrant long-acting mosquito-driving fiber is made, finally utilize the fibre
Required textile fabric of weaving out is tieed up, such as mosquito repellent fragrance mosquito net, mosquito repellent fragrance tent, mosquito repellent fragrance charge garment, mosquito repellent fragrance footwear, is driven
Mosquito fragrance socks, mosquito repellent fragrance waterproof garment and mosquito repellent fragrance gloves;Fragrant culicifuge process sequence is made using the present invention, is had
Following characteristics:1st, whole process is without exhaust gas discharge of wastewater;2nd, liquid essence and mosquito repellent are driven with high-melting-point paraffin wax (58 DEG C of fusing point)
It is dissolved under worm agent high temperature, it is at normal temperatures solid to make it, reaches and is sustained to obtain effect;3rd, oil-in-water emulsion is formed in the hot water, is made
Ludox is in the surface for hydrolyzing to be directly wrapped in oiliness droplet in the process, the slice stone of formation Silica-coated after cooling
Wax liquor is dripped, and the medium oil droplet diameter of emulsion method, at 200 nanometers, the single silica dioxide granule of Ludox is 20 nanometers;4th, it is fragrant
Fragrant mosquito repellent fiber obtains simultaneously in mosquito repellent, can cover the taste of culicifuge by discharging fragrance, can also increase fragrance in air,
Make one pleasant;6th, Ludox not only has good compatibility with textile, can also control as main additive and coating agent
The release of fragrance and anophelifuge reaches sustained release effect.Mosquito repellent fiber obtained in this way has effects that long-acting slow-release mosquito repellent, extends
Its usage time is long, since anophelifuge substance and fiber are co-melting blended rather than therefore washing fastness is good coated in fiber surface, passes through
Preferable repelling effect can be still kept after washing;In addition the textile fabric has the experience that fragrance improves user.
Specific embodiment
The invention will be further described below.
A kind of method for preparing fragrant long-acting mosquito-driving fiber, the specific steps are:
(1) by water, Ludox, surfactant, oil soluble perfume, mosquito and insect expelling agent, paraffin wax according to mass fraction
Proportioning is respectively:100 parts of water, surfactant are 0.1~10 part, and oil soluble perfume is 0.1~30 part, and mosquito and insect expelling agent is
0.1~30 part, Ludox ratio is 10~90 parts, the paraffin wax, oil soluble perfume and mosquito and insect expelling agent mass fraction
Ratio is 0.1:1~10:1;
(2) and then by said components it mixes in the following order, specially:It will slice first at a temperature of 60~100 DEG C
It is paraffin melting;Oil soluble perfume, mosquito and insect expelling agent are dissolved in liquid paraffin wax at this temperature, it is co-melting to form uniform liquid phase
Body;In addition water is heated to while agitating after 80 DEG C that surfactant is soluble in water, then will be cut under stirring
Piece paraffin, essence, the co-melting body of mosquito and insect expelling agent liquid phase are poured into the water dissolved with surfactant, form oil-in-water emulsion;Stirring 5
After minute, Ludox is added in into oil-in-water emulsion and is stopped after being stirred continuously until Ludox addition;By above-mentioned product
It is filtered at normal temperatures after being cooled to room temperature and obtains wet-milling;Wet-milling is 48 hours dry in 40 DEG C of baking oven, and last ball milling is made
Fragrant culicifuge;
(3) by fragrant culicifuge obtained above and textile fabric particle according to mass ratio 0.01~0.2:After 1 mixing
And it adds in additive and fragrant mosquito repellent master batch is made;
(4) matter will be pressed with fragrant mosquito repellent master batch after one or more slices in terylene, acrylic fibers, PET (i.e. polyester resin)
Amount ratio 1:Then 0.01~0.2 mixing carries out melt blending spinning and fragrant long-acting mosquito-driving fiber is made.
Further, the ball milling of the fragrant culicifuge is until 5000 mesh stop.
Further, the textile fabric particle is one or more combinations in polyamide fibre, terylene, polyamide.
Further, the mosquito and insect expelling agent is either mosquito repellent esters or the production of mosquito repellent amine of the Chinese herbal medicine with mosquito repellent function
Product.
Further, the additive is one or more combinations in PE waxes, antioxidant, light stabilizer.
Further, the Chinese herbal medicine with mosquito repellent function is one kind in folium artemisiae argyi, purple perilla, cloves, peppermint.
A kind of textile fabric of fragrance mosquito repellent, the textile fabric using long-acting mosquito-driving fibrous woven fragrant made from the above method and
Into.
Further, it is fragrant to include mosquito repellent fragrance mosquito net, mosquito repellent fragrance tent, mosquito repellent fragrance charge garment, mosquito repellent for the textile fabric
Fragrant footwear, mosquito repellent fragrance socks, mosquito repellent fragrance waterproof garment and mosquito repellent fragrance gloves.
Embodiment 1:
The weight percent of each ingredient is in fragrant mosquito repellent master batch:Fragrant culicifuge 20%, PE waxes 4%, antioxidant
MD697:0.5%th, light stabilizer 783:0.5%th, nylon fibre: 75%.The method for being prepared as described above fragrant mosquito repellent master batch is made
Fragrant mosquito repellent master batch carries out melt blending after then terylene chips are mixed with the fragrance mosquito repellent master batch according to 5: 1 weight ratio
Fragrant long-acting mosquito-driving fiber A is made in spinning.
Experimental verification:
Experiment 1:
Fragrant long-acting mosquito-driving fiber A is woven into cloth, then cloth made from fragrant long-acting mosquito-driving fiber A is cut out while incited somebody to action
It is cut out using the cloth of equal densities made from general fibre (no repelling effect), finally obtains the identical fragrance of two block sizes respectively
Long-acting mosquito-driving cloth and common cloth.
Fragrant long-acting mosquito-driving cloth is individually positioned in the bottom of two identical glass containers of shape, institute with common cloth
State two glass container insole portions not She You equal-wattage LED light, and the middle part of glass container be equipped with markings;It marks respectively
It is denoted as glass container A and glass container B;Then 50 laboratories are respectively placed into two glass containers respectively with batch cultivation mosquito
Son finally opens each LED light and each glass container black-out cloth is completely obscured;Black-out cloth sight is raised in waiting after ten minutes
Mosquito distribution situation (i.e. mosquito is in the quantity over and under of markings) in glass container is examined, such as the following table 1:
Table 1
Quantity (only) above markings | Quantity (only) below markings | |
Glass container A | 47 | 3 |
Glass container B | 0 | 50 |
As seen from the above table, due to the phototaxis of mosquito, in the case of only single light source, mosquito can be close to single light source,
LED light i.e. in this experiment is close, because LED light is placed on glass container bottom, therefore mosquito can be distributed under normal circumstances
It below markings, therefore places mosquito in the glass container B of common cloth and is distributed in below markings, and place the long-acting drive of fragrance
Mosquito is largely distributed in above markings in the glass container A of mosquito cloth, is only distributed on a small quantity below markings;Therefore
Going out the present invention has mosquito preferable expeling effect.
Experiment 2:Above-mentioned fragrant long-acting mosquito-driving cloth is placed in washing machine and carries out washing 1 hour and dries, repeats 3
It is secondary;The fragrance long-acting mosquito-driving cloth is repeated to the process of experiment 1 after the completion, observes mosquito distribution situation in glass container, such as
The following table 2;
Table 2
Quantity (only) above markings | Quantity (only) below markings | |
Glass container A | 40 | 10 |
Glass container B | 0 | 50 |
As can be known from the above table, though after repeatedly washing fragrant long-acting mosquito-driving cloth compared with the cloth before not washing,
Repelling effect decreases, but it is less to reduce situation;Remain to keep preferable repelling effect, therefore it is with stronger washability
Energy.
Claims (8)
- A kind of 1. method for preparing fragrant long-acting mosquito-driving fiber, which is characterized in that this method the specific steps are:(1) water, Ludox, surfactant, oil soluble perfume, mosquito and insect expelling agent, paraffin wax are distinguished according to mass fraction It matches and is:100 parts of water, surfactant are 0.1~10 part, and oil soluble perfume is 0.1~30 part, mosquito and insect expelling agent for 0.1~ 30 parts, Ludox ratio is 10~90 parts, and the ratio of the paraffin wax, oil soluble perfume and mosquito and insect expelling agent mass fraction is 0.1:1~10:1;(2) and then by said components it mixes in the following order, specially:First by paraffin wax at a temperature of 60~100 DEG C Melt;Oil soluble perfume, mosquito and insect expelling agent are dissolved in liquid paraffin wax at this temperature, form the co-melting body of uniform liquid phase; In addition water is heated to while agitating after 80 DEG C that surfactant is soluble in water, stone then will be sliced under stirring Wax, essence, the co-melting body of mosquito and insect expelling agent liquid phase are poured into the water dissolved with surfactant, form oil-in-water emulsion;Stirring 5 minutes Afterwards, Ludox is added in into oil-in-water emulsion and is stopped after being stirred continuously until Ludox addition;Above-mentioned product is cooled down It is filtered at normal temperatures after to room temperature and obtains wet-milling;Wet-milling is 48 hours dry in 40 DEG C of baking oven, and fragrance is made in last ball milling Culicifuge;(3) by fragrant culicifuge obtained above and textile fabric particle according to mass ratio 0.01~0.2:After 1 mixing and add Enter additive and fragrant mosquito repellent master batch is made;(4) by after one or more slices in terylene, acrylic fibers, PET with fragrant mosquito repellent master batch example 1 in mass ratio:0.01~0.2 Then mixing carries out melt blending spinning and fragrant long-acting mosquito-driving fiber is made.
- 2. a kind of method for preparing fragrant long-acting mosquito-driving fiber according to claim 1, which is characterized in that the fragrance drives The ball milling of mosquito agent is until 5000 mesh stop.
- 3. a kind of method for preparing fragrant long-acting mosquito-driving fiber according to claim 1, which is characterized in that the weaving is fine Dimension particle is polyamide fibre, one or more combinations in terylene, polyamide.
- 4. a kind of method for preparing fragrant long-acting mosquito-driving fiber according to claim 1, which is characterized in that the mosquito repellent drives Worm agent is either mosquito repellent esters or the mosquito repellent amine product of the Chinese herbal medicine with mosquito repellent function.
- A kind of 5. method for preparing fragrant long-acting mosquito-driving fiber according to claim 1, which is characterized in that the additive For one or more combinations in PE waxes, antioxidant, light stabilizer.
- 6. a kind of method for preparing fragrant long-acting mosquito-driving fiber according to claim 6, which is characterized in that described that there is drive The Chinese herbal medicine of mosquito effect is one kind in folium artemisiae argyi, purple perilla, cloves, peppermint.
- 7. a kind of textile fabric of fragrance mosquito repellent, which is characterized in that the textile fabric is long using fragrance made from method of claim 1 Effect mosquito repellent fibrous woven forms.
- 8. the textile fabric of a kind of fragrant mosquito repellent according to claim 8, which is characterized in that it is fragrant that the textile fabric includes mosquito repellent Fragrant mosquito net, mosquito repellent fragrance tent, mosquito repellent fragrance charge garment, mosquito repellent fragrance footwear, mosquito repellent fragrance socks, mosquito repellent fragrance waterproof garment and drive Mosquito fragrance gloves.
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110055614A (en) * | 2019-04-19 | 2019-07-26 | 中科纺织研究院(青岛)有限公司 | A kind of Yunnan Baiyao micro mist composite terylene slice macromolecular fibre and preparation method thereof |
CN111172613A (en) * | 2020-03-03 | 2020-05-19 | 百事基材料(青岛)股份有限公司 | Terylene staple fiber containing mint extract and preparation method thereof |
CN111234270A (en) * | 2020-03-18 | 2020-06-05 | 百事基材料(青岛)股份有限公司 | Mint terylene master batch and preparation method thereof |
CN113445153A (en) * | 2021-07-05 | 2021-09-28 | 苏州乾冠新纺织科技有限公司 | Long-acting mosquito-repelling pure cotton fabric and preparation method thereof |
CN113445151A (en) * | 2021-07-05 | 2021-09-28 | 苏州乾冠新纺织科技有限公司 | Washable mosquito-proof polyester fabric and preparation method thereof |
CN113774531A (en) * | 2021-08-19 | 2021-12-10 | 苏州中纺学面料产业研究院 | Preparation method of anti-mosquito polyester yarn, anti-mosquito fabric and garment |
CN113862871A (en) * | 2021-07-05 | 2021-12-31 | 苏州乾冠新纺织科技有限公司 | Long-acting mosquito-repelling polyester fabric and preparation method thereof |
CN114438613A (en) * | 2020-11-02 | 2022-05-06 | 嘉兴中科奥度新材料有限公司 | Preparation method and product of persistent mosquito and insect repelling silk thread |
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CN106245148A (en) * | 2016-08-20 | 2016-12-21 | 福建经纬新纤科技实业有限公司 | A kind of original liquid coloring anophelifuge polyester fiber |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110055614A (en) * | 2019-04-19 | 2019-07-26 | 中科纺织研究院(青岛)有限公司 | A kind of Yunnan Baiyao micro mist composite terylene slice macromolecular fibre and preparation method thereof |
CN111172613A (en) * | 2020-03-03 | 2020-05-19 | 百事基材料(青岛)股份有限公司 | Terylene staple fiber containing mint extract and preparation method thereof |
CN111234270A (en) * | 2020-03-18 | 2020-06-05 | 百事基材料(青岛)股份有限公司 | Mint terylene master batch and preparation method thereof |
CN114438613A (en) * | 2020-11-02 | 2022-05-06 | 嘉兴中科奥度新材料有限公司 | Preparation method and product of persistent mosquito and insect repelling silk thread |
CN113445153A (en) * | 2021-07-05 | 2021-09-28 | 苏州乾冠新纺织科技有限公司 | Long-acting mosquito-repelling pure cotton fabric and preparation method thereof |
CN113445151A (en) * | 2021-07-05 | 2021-09-28 | 苏州乾冠新纺织科技有限公司 | Washable mosquito-proof polyester fabric and preparation method thereof |
CN113862871A (en) * | 2021-07-05 | 2021-12-31 | 苏州乾冠新纺织科技有限公司 | Long-acting mosquito-repelling polyester fabric and preparation method thereof |
CN113774531A (en) * | 2021-08-19 | 2021-12-10 | 苏州中纺学面料产业研究院 | Preparation method of anti-mosquito polyester yarn, anti-mosquito fabric and garment |
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