CN113862819A - Polyester fiber containing folium Artemisiae Argyi component and folium Artemisiae Argyi fragrance, and its preparation method - Google Patents
Polyester fiber containing folium Artemisiae Argyi component and folium Artemisiae Argyi fragrance, and its preparation method Download PDFInfo
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- CN113862819A CN113862819A CN202111147739.1A CN202111147739A CN113862819A CN 113862819 A CN113862819 A CN 113862819A CN 202111147739 A CN202111147739 A CN 202111147739A CN 113862819 A CN113862819 A CN 113862819A
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/92—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Medicines Containing Plant Substances (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention provides a polyester fiber containing wormwood components and wormwood fragrance and a preparation method thereof, and relates to the technical field of textile fibers. The polyester fiber containing the wormwood components and the wormwood fragrance comprises the following materials in parts by weight: 8-11 parts of radix stemonae, 6-9 parts of clove, 6-9 parts of dandelion, 8-11 parts of rheum officinale, 6-9 parts of gardenia, 2-3 parts of coptis chinensis, 30-35 parts of wormwood, 5-7 parts of cellulase, 50-55 parts of polyester, 15-18 parts of lignan, 16-19 parts of nano titanium dioxide and 25-28 parts of fiber forming polymer. Through the addition of the wormwood powder mixture and the wormwood extract, the smell of industrial additives is effectively removed, meanwhile, the wormwood has the mosquito and insect repelling effect, and secondly, the fragrance generated by the wormwood acts on nasal mucosa, so that the content of antibody secretory immunoglobulin S (SlGA) on the nasal mucosa is increased, and the virus is not easy to survive on the nasal mucosa and respiratory tract mucosa due to the increase of the content.
Description
Technical Field
The invention relates to the technical field of textile fibers, in particular to a polyester fiber containing wormwood components and wormwood fragrance and a preparation method thereof.
Background
Polyester fiber, commonly known as "dacron", is a synthetic fiber obtained by spinning polyester formed by polycondensation of organic dibasic acid and dihydric alcohol, called PET fiber for short, and belongs to a high molecular compound, and the polyester fiber is invented in 1941 and is the first major variety of the current synthetic fiber, and the polyester fiber has the greatest advantages of good crease resistance and shape retention, high strength and elastic recovery capability, firmness and durability, crease resistance, easy ironing and hair sticking.
Polyester fiber is deeply loved by consumers due to the strong and durable performance, but in the existing polyester fiber, the problem of peculiar smell caused by the use of process additives exists after the production of the polyester fiber is finished, meanwhile, most polyester fibers have no mosquito-proof function, and secondly, in the long-term use process of the polyester fiber, bacteria and mites are easy to breed on the surface of the polyester fiber, so that the health of users is harmed.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides the polyester fiber containing the wormwood component and the wormwood fragrance and the preparation method thereof, and solves the problems of peculiar smell, mosquito prevention, bacteria and mite breeding.
(II) technical scheme
In order to achieve the purpose, the invention is realized by the following technical scheme: a polyester fiber containing wormwood components and wormwood fragrance comprises the following materials in parts by weight: 8-11 parts of radix stemonae, 6-9 parts of clove, 6-9 parts of dandelion, 8-11 parts of rheum officinale, 6-9 parts of gardenia, 2-3 parts of coptis chinensis, 30-35 parts of wormwood, 5-7 parts of cellulase, 50-55 parts of polyester, 15-18 parts of lignan, 16-19 parts of nano titanium dioxide and 25-28 parts of fiber forming polymer.
Preferably, the preparation method of the polyester fiber containing the wormwood component and the wormwood fragrance comprises the following steps:
s1. auxiliary Material treatment
Firstly, spraying and cleaning radix stemonae, clove, dandelion, rheum officinale, gardenia, coptis and half of wormwood, then putting the mixture into a heat-preservation drying room, drying the mixture for 2-3 hours in an environment with the temperature set to 65-75 ℃, then reducing the temperature to 35-40 ℃, drying the mixture for 2-3 hours, setting the temperatures to 40-55 ℃ and 50-55 ℃ in sequence, drying the mixture for 8-9 hours, obtaining a dried mixture after the drying is finished, and crushing the dried mixture in a high-speed crusher to obtain a powder mixture;
placing the rest half of the wormwood into a heat-preservation drying room, drying for 5-6 h in an environment with the temperature set to be 50-55 ℃, then crushing the dried wormwood, placing the crushed wormwood into a stirrer, adding a proper amount of deionized water and cellulase, fully stirring, and finally filtering and distilling the mixture under reduced pressure to obtain the wormwood extract;
s2, main material treatment
Putting polyester into a grinder for grinding treatment to obtain polyester powder, putting the obtained polyester powder into a reaction kettle, sequentially adding lignans and nano-scale titanium dioxide, fully stirring the mixture, finally adding a fiber-forming polymer into the reaction kettle, and fully stirring to obtain a polyester mixture;
s3, mixing treatment
Putting the polyester mixture obtained in the step S2 into a reaction kettle, adding the powder mixture prepared in the step S1 into the reaction kettle, fully stirring the mixture in an environment with the temperature set to be 45-55 ℃, and gradually adding the wormwood extract into the reaction kettle at intervals of 30-35 min in the stirring process until the stirring is finished;
putting the mixture into a double-screw extruder for extrusion treatment, and cutting after cooling and forming to obtain polyester fiber granules;
and thirdly, granulating the polyester fiber, drying, performing melt spinning after drying, cooling, oiling and stretching the spun yarn, and finally performing cold setting and winding on the melt strand to obtain the polyester fiber containing the wormwood component and the wormwood fragrance.
Preferably, the ratio of the stemona root to the rhubarb by weight part is 1: 1, the ratio of parts by weight of clove, dandelion and gardenia is 1: 1: 1.
preferably, the mixture obtained in the step S1 is dried and then is put into a high-speed pulverizer for processing for 40-50 min, and the particle diameter of the powder mixture is 100-150 nm.
Preferably, the time for crushing the dried wormwood in the step S1 is 30-35 min, and the time for fully stirring after adding a proper amount of deionized water and cellulase in the step S1 is 1.1-1.5 h.
Preferably, the time for grinding the polyester in the S2 is 45-50 min, and the diameter of the polyester particle after grinding in the S2 is 120-160 nm.
Preferably, the time for fully stirring after the powder mixture is added into the S3 is 1.5-1.8 h.
(III) advantageous effects
The invention provides a polyester fiber containing wormwood components and wormwood fragrance. The method has the following beneficial effects:
1. the invention dries and crushes half of the wormwood and mixes the dried and crushed wormwood with the main material, so that the polyester fiber contains wormwood components, the other half of the wormwood is processed into wormwood extract and mixed with the main material, so that the polyester fiber contains wormwood fragrance, the smell of industrial additives is effectively removed through the wormwood fragrance, the wormwood has the functions of repelling mosquitoes and insects, and the wormwood fragrance acts on nasal mucosa, so that the content of antibody secretion immunoglobulin S (SlGA) on the nasal mucosa is increased, and the virus is not easy to survive on the nasal mucosa and respiratory tract mucosa.
2. According to the invention, the stemona root, the clove, the dandelion, the rheum officinale, the gardenia and the coptis are added, so that the breeding of bacteria and mites is effectively inhibited, meanwhile, the functions of the polyester fiber are effectively enriched by adding various traditional Chinese medicinal materials and matching with the wormwood, and then, the antibacterial capacity of the polyester fiber is enhanced by adding the lignan and the nano titanium dioxide.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows:
the embodiment of the invention provides a polyester fiber containing a wormwood component and wormwood fragrance, which comprises the following materials in parts by weight: 8 parts of radix stemonae, 6 parts of clove, 6 parts of dandelion, 8 parts of rhubarb, 6 parts of gardenia, 2 parts of coptis, 30 parts of wormwood, 5 parts of cellulase, 50 parts of polyester, 15 parts of lignan, 16 parts of nano-titanium dioxide and 25 parts of fiber-forming polymer.
A method for preparing polyester fiber containing folium Artemisiae Argyi components and folium Artemisiae Argyi fragrance comprises the following steps:
s1. auxiliary Material treatment
Firstly, carrying out spray cleaning on stemona root, clove, dandelion, rheum officinale, gardenia, coptis and half of wormwood, then putting the stemona root, clove, dandelion, rheum officinale, gardenia, coptis and half of wormwood into a heat-preservation drying room, carrying out drying treatment for 2h in an environment with the temperature set to 65 ℃, then reducing the temperature to 35 ℃, carrying out drying treatment for 2h, then sequentially setting the temperature to 40 ℃ and 50 ℃, carrying out drying treatment for 8h, obtaining a dried mixture after the drying treatment is finished, putting the mixture into a high-speed crusher for crushing treatment, and obtaining a powder mixture The dandelion, the rheum officinale, the gardenia and the coptis are added into the polyester fibers, so that the effect of inhibiting the breeding of bacteria and viruses is effectively realized, meanwhile, the mite removing effect is good, the function of the polyester fibers is enriched, the wormwood is added, on one hand, the taste of an industrial additive can be removed through the fragrance of the wormwood, on the other hand, the fragrance generated by the wormwood acts on nasal mucosa, so that the content of antibody secretion immunoglobulin S (SlGA) on the nasal mucosa is increased, the virus is not easy to survive on the nasal mucosa and respiratory tract mucosa due to the increase of the content, meanwhile, the wormwood has good characteristics of repelling mosquitoes and preventing insects, and the effect of inhibiting the breeding of bacteria and viruses can be enhanced by matching with the stemona root, the clove, the dandelion, the rheum officinale, the gardenia and the coptis;
putting the rest half of the wormwood into a heat-preservation drying room, drying for 5 hours in an environment with the temperature set to be 50 ℃, then crushing the dried wormwood, putting the crushed wormwood into a stirrer, adding a proper amount of deionized water and cellulase, fully stirring, filtering and distilling the mixture under reduced pressure to obtain a wormwood extract, effectively prolonging the fragrance released by the wormwood by adding the wormwood powder mixture and the wormwood extract, and enabling the polyester fiber to have wormwood components and wormwood fragrance;
s2, main material treatment
Putting polyester into a grinder for grinding treatment to obtain polyester powder, putting the obtained polyester powder into a reaction kettle, sequentially adding lignan and nano-scale titanium dioxide, then fully stirring the mixture, finally adding a fiber-forming polymer into the reaction kettle, and fully stirring to obtain a polyester mixture, wherein the lignan has the functions of sterilization and insect prevention, and the nano-scale titanium dioxide has the functions of sterilization, pollution prevention and deodorization;
s3, mixing treatment
Putting the polyester mixture obtained in the step S2 into a reaction kettle, adding the powder mixture prepared in the step S1 into the reaction kettle, fully stirring the mixture in an environment with the temperature set to be 45 ℃, and simultaneously gradually adding the wormwood extract into the reaction kettle at intervals of 30min in the stirring process until the stirring is finished;
putting the mixture into a double-screw extruder for extrusion treatment, and cutting after cooling and forming to obtain polyester fiber granules;
and thirdly, granulating the polyester fiber, drying, performing melt spinning after drying, cooling, oiling and stretching the spun yarn, and finally performing cold setting and winding on the melt strand to obtain the polyester fiber containing the wormwood component and the wormwood fragrance.
The weight ratio of the stemona root to the rhubarb is 1: 1, the ratio of the clove, the dandelion and the gardenia by weight part is 1: 1: 1.
and (S1) drying the mixture, and then putting the dried mixture into a high-speed pulverizer to process for 40min, wherein the particle diameter of the powder mixture is 100 nm.
The time for crushing the dried wormwood in the S1 is 30min, and the time for fully stirring the wormwood after adding a proper amount of deionized water and cellulose in the S1 is 1.1 h.
The time for grinding the polyester in S2 was 45min, and the diameter of the polyester particles after grinding in S2 was 120 nm.
The time for stirring the powder mixture after addition to S3 was 1.5 h.
Example two:
the embodiment of the invention provides a polyester fiber containing a wormwood component and wormwood fragrance, which comprises the following materials in parts by weight: 11 parts of radix stemonae root, 9 parts of clove, 9 parts of dandelion, 11 parts of rhubarb, 9 parts of gardenia, 3 parts of coptis, 35 parts of wormwood, 7 parts of cellulase, 55 parts of polyester, 18 parts of lignan, 19 parts of nano-titanium dioxide and 28 parts of fiber-forming polymer.
A method for preparing polyester fiber containing folium Artemisiae Argyi components and folium Artemisiae Argyi fragrance comprises the following steps:
s1. auxiliary Material treatment
Firstly, carrying out spray cleaning on stemona root, clove, dandelion, rheum officinale, gardenia, coptis and half of wormwood, then putting the stemona root, clove, dandelion, rheum officinale, gardenia, coptis and half of wormwood into a heat-preservation drying room, carrying out drying treatment for 3h in an environment with the temperature set to be 75 ℃, then reducing the temperature to 40 ℃, carrying out drying treatment for 3h, then sequentially setting the temperature to be 55 ℃ and 55 ℃, carrying out drying treatment for 9h, obtaining a dried mixture after the drying treatment is finished, putting the mixture into a high-speed crusher for crushing treatment, and obtaining a powder mixture The dandelion, the rheum officinale, the gardenia and the coptis are added into the polyester fibers, so that the effect of inhibiting the breeding of bacteria and viruses is effectively realized, meanwhile, the mite removing effect is good, the function of the polyester fibers is enriched, the wormwood is added, on one hand, the taste of an industrial additive can be removed through the fragrance of the wormwood, on the other hand, the fragrance generated by the wormwood acts on nasal mucosa, so that the content of antibody secretion immunoglobulin S (SlGA) on the nasal mucosa is increased, the virus is not easy to survive on the nasal mucosa and respiratory tract mucosa due to the increase of the content, meanwhile, the wormwood has good characteristics of repelling mosquitoes and preventing insects, and the effect of inhibiting the breeding of bacteria and viruses can be enhanced by matching with the stemona root, the clove, the dandelion, the rheum officinale, the gardenia and the coptis;
secondly, putting the rest half of the wormwood into a heat-preservation drying room, drying for 6h in an environment with the temperature set to be 55 ℃, then crushing the dried wormwood, putting the crushed wormwood into a stirrer, adding a proper amount of deionized water and cellulase, fully stirring, filtering and distilling the mixture under reduced pressure to obtain a wormwood extract, effectively prolonging the fragrance released by the wormwood by adding the wormwood powder mixture and the wormwood extract, and enabling the polyester fiber to have wormwood components and wormwood fragrance;
s2, main material treatment
Putting polyester into a grinder for grinding treatment to obtain polyester powder, putting the obtained polyester powder into a reaction kettle, sequentially adding lignan and nano-scale titanium dioxide, then fully stirring the mixture, finally adding a fiber-forming polymer into the reaction kettle, and fully stirring to obtain a polyester mixture, wherein the lignan has the functions of sterilization and insect prevention, and the nano-scale titanium dioxide has the functions of sterilization, pollution prevention and deodorization;
s3, mixing treatment
Putting the polyester mixture obtained in the step S2 into a reaction kettle, adding the powder mixture prepared in the step S1 into the reaction kettle, fully stirring the mixture in an environment with the temperature set to be 55 ℃, and simultaneously gradually adding the wormwood extract into the reaction kettle at intervals of 35min in the stirring process until the stirring is finished;
putting the mixture into a double-screw extruder for extrusion treatment, and cutting after cooling and forming to obtain polyester fiber granules;
and thirdly, granulating the polyester fiber, drying, performing melt spinning after drying, cooling, oiling and stretching the spun yarn, and finally performing cold setting and winding on the melt strand to obtain the polyester fiber containing the wormwood component and the wormwood fragrance.
The weight ratio of the stemona root to the rhubarb is 1: 1, the ratio of the clove, the dandelion and the gardenia by weight part is 1: 1: 1.
and (S1) drying the mixture, and then putting the dried mixture into a high-speed pulverizer to treat for 50min, wherein the particle diameter of the powder mixture is 150 nm.
The time for crushing the dried wormwood in the S1 is 35min, and the time for fully stirring the wormwood after adding a proper amount of deionized water and cellulose in the S1 is 1.5 h.
The time for grinding the polyester in S2 was 50min, and the diameter of the polyester particles after grinding in S2 was 160 nm.
The time for stirring the powder mixture after addition to S3 was 1.8 h.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (7)
1. A polyester fiber containing a mugwort component and a mugwort fragrance, characterized in that: the material comprises the following materials in parts by weight: 8-11 parts of radix stemonae, 6-9 parts of clove, 6-9 parts of dandelion, 8-11 parts of rheum officinale, 6-9 parts of gardenia, 2-3 parts of coptis chinensis, 30-35 parts of wormwood, 5-7 parts of cellulase, 50-55 parts of polyester, 15-18 parts of lignan, 16-19 parts of nano titanium dioxide and 25-28 parts of fiber forming polymer.
2. The method for preparing the polyester fiber containing the moxa component and the moxa flavor according to claim 1, wherein: the method comprises the following steps:
s1. auxiliary Material treatment
Firstly, spraying and cleaning radix stemonae, clove, dandelion, rheum officinale, gardenia, coptis and half of wormwood, then putting the mixture into a heat-preservation drying room, drying the mixture for 2-3 hours in an environment with the temperature set to 65-75 ℃, then reducing the temperature to 35-40 ℃, drying the mixture for 2-3 hours, setting the temperatures to 40-55 ℃ and 50-55 ℃ in sequence, drying the mixture for 8-9 hours, obtaining a dried mixture after the drying is finished, and crushing the dried mixture in a high-speed crusher to obtain a powder mixture;
placing the rest half of the wormwood into a heat-preservation drying room, drying for 5-6 h in an environment with the temperature set to be 50-55 ℃, then crushing the dried wormwood, placing the crushed wormwood into a stirrer, adding a proper amount of deionized water and cellulase, fully stirring, and finally filtering and distilling the mixture under reduced pressure to obtain the wormwood extract;
s2, main material treatment
Putting polyester into a grinder for grinding treatment to obtain polyester powder, putting the obtained polyester powder into a reaction kettle, sequentially adding lignans and nano-scale titanium dioxide, fully stirring the mixture, finally adding a fiber-forming polymer into the reaction kettle, and fully stirring to obtain a polyester mixture;
s3, mixing treatment
Putting the polyester mixture obtained in the step S2 into a reaction kettle, adding the powder mixture prepared in the step S1 into the reaction kettle, fully stirring the mixture in an environment with the temperature set to be 45-55 ℃, and gradually adding the wormwood extract into the reaction kettle at intervals of 30-35 min in the stirring process until the stirring is finished;
putting the mixture into a double-screw extruder for extrusion treatment, and cutting after cooling and forming to obtain polyester fiber granules;
and thirdly, granulating the polyester fiber, drying, performing melt spinning after drying, cooling, oiling and stretching the spun yarn, and finally performing cold setting and winding on the melt strand to obtain the polyester fiber containing the wormwood component and the wormwood fragrance.
3. The polyester fiber containing moxa components and moxa flavor according to claim 1, wherein: the weight ratio of the stemona root to the rhubarb is 1: 1, the ratio of parts by weight of clove, dandelion and gardenia is 1: 1: 1.
4. the method for preparing the polyester fiber containing the moxa component and the moxa flavor according to claim 2, wherein: and drying the mixture obtained in the step S1, and then putting the dried mixture into a high-speed pulverizer for processing for 40-50 min, wherein the particle diameter of the powder mixture is 100-150 nm.
5. The method for preparing the polyester fiber containing the moxa component and the moxa flavor according to claim 2, wherein: the time for crushing the dried wormwood in the S1 is 30-35 min, and the time for fully stirring after adding a proper amount of deionized water and cellulase in the S1 is 1.1-1.5 h.
6. The method for preparing the polyester fiber containing the moxa component and the moxa flavor according to claim 2, wherein: the time for grinding the polyester in the S2 is 45-50 min, and the diameter of the ground polyester particles in the S2 is 120-160 nm.
7. The method for preparing the polyester fiber containing the moxa component and the moxa flavor according to claim 2, wherein: and the time for fully stirring the powder mixture added into the S3 is 1.5-1.8 h.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111147739.1A CN113862819A (en) | 2021-09-29 | 2021-09-29 | Polyester fiber containing folium Artemisiae Argyi component and folium Artemisiae Argyi fragrance, and its preparation method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202111147739.1A CN113862819A (en) | 2021-09-29 | 2021-09-29 | Polyester fiber containing folium Artemisiae Argyi component and folium Artemisiae Argyi fragrance, and its preparation method |
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| CN113862819A true CN113862819A (en) | 2021-12-31 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115182069A (en) * | 2022-08-16 | 2022-10-14 | 东莞市正盛无纺科技有限公司 | Functional wormwood polyester fiber and preparation method thereof |
| CN115216876A (en) * | 2022-08-29 | 2022-10-21 | 和也健康科技有限公司 | Preparation process of wormwood zinc jade fiber fabric |
-
2021
- 2021-09-29 CN CN202111147739.1A patent/CN113862819A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115182069A (en) * | 2022-08-16 | 2022-10-14 | 东莞市正盛无纺科技有限公司 | Functional wormwood polyester fiber and preparation method thereof |
| CN115216876A (en) * | 2022-08-29 | 2022-10-21 | 和也健康科技有限公司 | Preparation process of wormwood zinc jade fiber fabric |
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