CN106234471A - A kind of Folium Artemisiae Argyi anophelifuge pastil and preparation method thereof - Google Patents
A kind of Folium Artemisiae Argyi anophelifuge pastil and preparation method thereof Download PDFInfo
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- CN106234471A CN106234471A CN201610603892.3A CN201610603892A CN106234471A CN 106234471 A CN106234471 A CN 106234471A CN 201610603892 A CN201610603892 A CN 201610603892A CN 106234471 A CN106234471 A CN 106234471A
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- folium artemisiae
- artemisiae argyi
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/20—Combustible or heat-generating compositions
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/44—Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- General Health & Medical Sciences (AREA)
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- Agronomy & Crop Science (AREA)
- Environmental Sciences (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Mycology (AREA)
- Biotechnology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Microbiology (AREA)
- Pest Control & Pesticides (AREA)
- Toxicology (AREA)
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of Folium Artemisiae Argyi anophelifuge pastil and preparation method thereof, be made up of the raw material of following weight portion: wormwood extract 10 25 parts, bagasse 20 40 parts, Eucalyptus corium farinosum 8 15 parts and carbon dust 3 10 parts;Preparation method is as follows: one, produce wormwood extract;Two, by bagasse, 400 mesh it are crushed to by bark powder;Three, required each component is put into agitator, mix homogeneously in proportion;Mosquito incense pressing machine extrudes the material into type;Four, dehydrate in exsiccator, controls water content 3 7%, subpackage, to obtain final product;Obtained Folium Artemisiae Argyi culicifuge incense have natural, pollution-free, mosquito is walked quickly and kept away the feature that effect is good.
Description
Technical field
The present invention relates to a kind of culicifuge incense, be specially a kind of Folium Artemisiae Argyi anophelifuge pastil and preparation method thereof.
Background technology
Sanitary insect pest insecticide is at present based on chemical composition, and mosquito is as one of " four pests ", to daily life
Bring the biggest puzzlement, the not only normal rest of harassing and wrecking people, some mosquito or malaria, filaricide, epidemic encephalitis type B
Disseminator with dengue fever.Mosquito incense is dependent on effective ingredient and forms cigarette shape granule in a heated state to the mosquito that tags, relative to
It is wide that spray agent has distribution, low toxin.But effective ingredient is mainly chrysanthemum lactone component in current mosquito incense, such as allyl chrysanthemum
Ester, alphamethrin etc., chrysanthemum ester insecticide has quickly knocks down the effect killing insect, but human body is still had not by it
Little injury effect, especially infant and anemia of pregnant woman etc..Along with people's enhancing to environmental consciousness, natural, pollution-free, noresidue
Anophelifuge more favored by people, the plant source anophelifuge that research is popular especially at present.
Folium Artemisiae Argyi (Artemisia argyi H. L é v. Vaniot), another name: Xiao Mao, ice platform, hold back grass, Artemisia argyi, Artemisia argyi Levl. et Van. var. argyi cv. Qiai,
Ai Xiao, Radix Artemisia ordosicae, Radix Artemisia ordosicae, fluffy ligusticumic, moxa-moxibustion herbalist's straw colour grass Folium Artemisiae Argyi etc..Perennial herb or slightly become suffruticose.Modern medicine
Haircut is existing, and Folium Artemisiae Argyi volatile oil content is many, and 1.8-cineole (accounts for more than 50%), other have α-absinthol, sesquiterpene alcohols and
Ester.Air dried leaves contains mineral 10.13%, fat 2.59%, protein 25.85%, and vitamin A, B1, B2, C etc..Herb enters
Medicine, have warming the meridian, dry, cold expelling, hemostasis, antiinflammatory, relieving asthma, cough-relieving, the effect such as antiabortive, antiallergic.Folium Artemisiae Argyi nature and flavor are bitter, pungent, warm, enter
Spleen, liver, kidney.Compendium of Material Medica is recorded: Ai Yiye is used as medicine, warm in nature, bitter in the mouth, the property of sun nontoxic, pure, logical 12 through, tool recuperating depleted YANG, reason
QI and blood, by effects such as raw, arresting bleeding and miscarriage preventions, be also commonly used for acupuncture.It addition, the multiple volatile oil component contained in Folium Artemisiae Argyi is to mosquito
Having stronger avoidance effect, at present, the patent of research Folium Artemisiae Argyi mosquito-repelling function is many, such as: Chinese patent: Authorization Notice No. CN
The invention of 101564049 B: a kind of pure natural mosquito-repellent perfume and preparation method, this perfume is by culicifuge incense grass juice factor, Folium Artemisiae Argyi juice, Cacumen Platycladi
Juice, Herba Rosmarini Officinalis juice, Herba thymi vulgaris, Herba Menthae juice, remaining be distilled water.The also invention of grant number CN 102429840 B: mosquito-driving liquid
And preparation method thereof, its formula is consisting of: lavandula angustifolia, lemon grass (Cymbopogon citratus), Aloe, Flos Inulae, Flos Matricariae chamomillae, Flos Jasmini Sambac, Flos Rosae Rugosae
Flower, Radix Oenotherae erythrosepalae, mentha leave, Folium cinnamomi camphorae, Folium Artemisiae Argyi, eucalyptus leaves, anise, fly expelling plum 20, Mozzie buster, Salvia japonica Thunb., Origanum majorana L., fan are repeatedly
Fragrant.The invention also having granted patent number to be CN 102835428B: a kind of essential mosquito repellent, composed of the following components: citronella oil,
Fructus Citri Limoniae oil, Oleum lavandula angustifolia, Oleum menthae, mugwort oil, surplus is food stage 95% ethanol.In addition, also patent application publication number
Patent for CN101433195A: Thyme mosquito-repellent incense, it is made up of Herba thymi vulgaris, Radix Artemisia ordosicae, Pericarpium Zanthoxyli and starch;Application publication number is:
The patent of CN1806556A: a kind of mosquitos and flies incense prescription, it is by Radix Artemisia ordosicae, HUANGSONG, Rhizoma Atractylodis, Realgar, the Radix Angelicae Dahuricae and the group such as Radix Et Rhizoma Nardostachyos, Rhizoma Kaempferiae
Become.
Visible, the report using Folium Artemisiae Argyi to develop mosquito incense or other dosage form anophelifuge as composition is much, but, mostly
Number all has the composition of more than 3 kinds to combine, and most plants extracts through ethanol equal solvent or slightly carries with water, its composition
Complicated various, and for preventing and treating the composition of mosquito, to only have volatile oil etc. several, therefore, combine other botanical components the most not
Foot is for strange.Even so, exploitation Folium Artemisiae Argyi prevents and treats the effective ingredient of mosquito to greatest extent, increases operation rate, the most favorably
In the protection of species resource rare to China, the most beneficially industrialized production.
Summary of the invention
Present invention aim at the above-mentioned deficiency for prior art, it is provided that a kind of Folium Artemisiae Argyi anophelifuge pastil and preparation side thereof
Method, this culicifuge incense is with wormwood extract as main component, and relative to tradition culicifuge incense, noresidue, to people's safety, relative to market
Plant source culicifuge incense, not only repelling effect is good, and poisons composition without to human body, and low cost of manufacture, technique is simple.
Folium Artemisiae Argyi anophelifuge pastil of the present invention and preparation method thereof is achieved by the following technical solution:
The Folium Artemisiae Argyi anophelifuge pastil of the present invention, is made up of the raw material of following weight portion: wormwood extract 10-25 part, bagasse 20-40
Part, Eucalyptus corium farinosum 8-15 part and carbon dust 3-10 part.
Volatile oil component in Folium Artemisiae Argyi has a stronger avoidance effect to mosquito, but much tens kinds of the composition in Folium Artemisiae Argyi,
Great majority are the best to repelling effect, if do not extracted the effective ingredient in Folium Artemisiae Argyi, only prepare as main material with Folium Artemisiae Argyi
Culicifuge incense, can largely effect on repelling effect, and inventor is found by research, uses technical solution of the present invention to prepare Folium Artemisiae Argyi extraction
Thing, improves more than 30% than simple with Folium Artemisiae Argyi repelling effect.
Bagasse is sugaring waste material, and in Guangxi province, sugarcane acreage reaches 16,000,000 mu, annual bagasse major part quilt
As waste disposal, time-consuming, pollute environment.After the drying, moisture controls below 3% bagasse, easy firing, no
Producing toxic gas, be combustible material, inventor uses it for culicifuge incense filler, not only makes resource reutilization, decreases simultaneously
The use of powdered carbon, has saved cost.
Eucalyptus corium farinosum, Eucalyptus (Eucalyptus) has another name called eucalyptus globolus tree, is one of three big quick growing species of treess, its strong adaptability,
Assortment is various, of many uses, and Eucalyptus economic worth is high, is the rareest short cycle industrial cut stock seeds, general 5 ~ 8 years can
Fell and utilize.After deliberation, artificial forest Eucalyptus bark chemical composition content is respectively as follows: holocellulose 79.35%, cellulose
46.81%, lignin 19.69%, 1%NaOH extract 19.83%, cold water extract 5.30%, hot-water extraction thing 8.11%,
Alcohol benzene extractive 2.63%, ash 2.82%.Inventor finds that alcohol benzene extractive therein has certain repelling effect, and cold
Water, hot water and sodium hydroxide extracting take and mosquito are had killing effect.In addition, Eucalyptus corium farinosum inherently a kind of well combustion
Material, the combustion heat value after its solidification is up to 3700-5000Kcal/kg.Its combustion characteristics is:
1. briquette-fuel density is big, thus limits volatile matter and overflow speed, extends the burning time of volatile matter, combustion reaction
Major part is only carried out on the surface of briquette-fuel, and combustion position belongs to static infiltration type diffusion combustion, is similar to burning of coal
Journey.
2. the good characteristic such as inflammable, pollution-free that briquette-fuel had both remained that primordial matter had, has again and resistance to burns spy
Point.
3. closely knit because of briquette-fuel quality, accumulation of energy, volatile matter has remained carbon structure also after overflowing in combustion
Relative close, is clearly visible in combustion, and blue flame wraps up in bright carbon block, and it is bright that furnace temperature is greatly improved burning time
Aobvious prolongation.
The oxygen demand of the most whole combustion process tends to balance, and combustion process is more stable.
Described wormwood extract preparation method is:
(1) pre-treatment: take the Folium Artemisiae Argyi Herb without infection process, goes root to clean, dries in the shade, pulverize, obtain Folium Artemisiae Argyi coarse powder A, standby.
(2) seepage pressure effects: put into by A in percolator, adds pure water, adds a cover percolation 5-7 days, and filtrate crosses 400 mesh sieves,
Filtrate;Filtering residue continues to add water percolation 2-3 time, after merging liquor B;Seepage pressure effects percolation material-water ratio for the first time is 1:5-8;The
Two, three percolation material-water ratios are 1:2-5.
(3) concentrate;Liquor B is concentrated in concentrator and makes wormwood extract;Concentration condition be thickening temperature be 65-70
DEG C, pressure is-0.01--0.04Mpa.
The 1.2-1.5g Han dry in described wormwood extract.
The preparation method of described Folium Artemisiae Argyi anophelifuge pastil, is carried out as follows:
One, wormwood extract is produced;
Two, by bagasse, 400 mesh it are crushed to by bark powder;
Three, required each component is put into agitator, mix homogeneously in proportion;Mosquito incense pressing machine extrudes the material into type;
Four, dehydrate in exsiccator, controls water content 3-7%, subpackage, to obtain final product.
Having the beneficial effect that of culicifuge incense of the present invention
1. the culicifuge incense that the present invention develops, with wormwood extract as main component, after reasonable drawing, the material obtained has
Excellent repelling effect, active effect improves more than 30% relative to Folium Artemisiae Argyi itself.
2. the culicifuge incense that the present invention develops, does not contains any chemical composition, during burning anophelifuge, does not produce poisonous
Material, to the respiratory tract of people without ill effect, and conventional mosquito incense effective ingredient major part pyrethrin pesticide composition, mosquito is
Having had stronger Drug resistance, effect is not as, can not use infant and anemia of pregnant woman in the past meanwhile, therefore, and Folium Artemisiae Argyi anophelifuge pastil
Succeed in developing and will have great promotional value.
3. the culicifuge incense that the present invention develops, uses by bark powder as adjuvant, and bagasse is as main stuffing, by bark powder
In containing certain mosquito component and mosquito killing composition, it is to beat powder drying after-combustion ability strong, it is adaptable to the processing of mosquito incense,
Range and the application purpose of both are widened.
Formulation Example
The preparation method of embodiment 1 wormwood extract
Gather or buy the Folium Artemisiae Argyi Herb without pest and disease damage infringement, as follows to the extracts active ingredients in Folium Artemisiae Argyi:
(1) pre-treatment: take the Folium Artemisiae Argyi Herb without infection process, goes root to clean, dries in the shade, pulverize, obtain Folium Artemisiae Argyi coarse powder A, standby;
(2) seepage pressure effects: put into by A in percolator, adds pure water, adds a cover percolation 5-7 days, and filtrate crosses 400 mesh sieves, obtains filter
Liquid;Filtering residue continues to add water percolation 2-3 time, after merging liquor B;Seepage pressure effects percolation material-water ratio for the first time is 1:5-8;The second,
Three percolation material-water ratios are 1:2-5.
(3) concentrate;Liquor B is concentrated in concentrator and makes wormwood extract;Concentration condition be thickening temperature be 65-70
DEG C, pressure is-0.01--0.04Mpa.The 1.2-1.5g Han dry in gained wormwood extract.
Embodiment 2 Folium Artemisiae Argyi anophelifuge pastil 1
The wormwood extract that Example obtains 10 parts, bagasse 20 parts, Eucalyptus corium farinosum 8 parts and carbon dust 3 parts.
The preparation method of Folium Artemisiae Argyi anophelifuge pastil, is carried out as follows:
One, wormwood extract is produced;
Two, by bagasse, 400 mesh it are crushed to by bark powder;
Three, required each component is put into agitator, mix homogeneously in proportion;Mosquito incense pressing machine extrudes the material into dish-type;
Four, dehydrate in exsiccator, controls water content 3%, uses carton subpackage, to obtain final product.
Embodiment 3 Folium Artemisiae Argyi anophelifuge pastil 2
The wormwood extract that Example obtains 25 parts, bagasse 40 parts, Eucalyptus corium farinosum 15 parts and carbon dust 10 parts.
The preparation method of Folium Artemisiae Argyi anophelifuge pastil, is carried out as follows:
One, wormwood extract is produced;
Two, by bagasse, 400 mesh it are crushed to by bark powder;
Three, required each component is put into agitator, mix homogeneously in proportion;Mosquito incense pressing machine extrude the material into tapered;
Four, dehydrate in exsiccator, controls water content 5%, uses carton subpackage, to obtain final product.
Embodiment 4 Folium Artemisiae Argyi anophelifuge pastil 3
The wormwood extract that Example obtains 15 parts, bagasse 30 parts, Eucalyptus corium farinosum 10 parts and carbon dust 8 parts.
The preparation method of Folium Artemisiae Argyi anophelifuge pastil, is carried out as follows:
One, wormwood extract is produced;
Two, by bagasse, 400 mesh it are crushed to by bark powder;
Three, required each component is put into agitator, mix homogeneously in proportion;Mosquito incense pressing machine extrudes the material into line style;
Four, dehydrate in exsiccator, controls water content 7%, uses carton subpackage, to obtain final product.
Embodiment 5 Folium Artemisiae Argyi anophelifuge pastil 4
The wormwood extract that Example obtains 20 parts, bagasse 20 parts, Eucalyptus corium farinosum 10 parts and carbon dust 7 parts.
The preparation method of Folium Artemisiae Argyi anophelifuge pastil, is carried out as follows:
One, wormwood extract is produced;
Two, by bagasse, 400 mesh it are crushed to by bark powder;
Three, required each component is put into agitator, mix homogeneously in proportion;Mosquito incense pressing machine extrudes the material into dish-type;
Four, dehydrate in exsiccator, controls water content 3%, uses carton subpackage, to obtain final product.
Application Example
For showing the effect of Folium Artemisiae Argyi anophelifuge pastil of the present invention, by Application Example, the invention will be further described
Detection environmental condition: temperature: 24 ± 1 DEG C;
Relative humidity 85%;
Square chest model: 0.5m × 0.5m × 0.5m;
1. square box device test method: glass square chest one jiao put into by the medicine taking experimental pharmacy, puts equipped with clearly in the middle of glass square chest
The glass dish of clean water.100 culex pipiens pallens are put in glass square chest, lights culicifuge incense, and timing, 5min, 10min, 20min
Observing examination worm death quantity, calculate mortality rate, test is repeated 3 times.
2. experimental result
It can be seen that embodiment 1-5 that the present invention develops all has stronger killing effect to culex pipiens pallens, meanwhile, use Folium Artemisiae Argyi
For in the experiment of main material, there is certain repelling effect, but not as good as the present invention;Commercially available medicament be mainly composed of allethrin,
Effect is suitable with effect of the present invention, after 20 min, has serious pesticide taste, have the sense of dizziness headache in the square chest of commercially available mosquito incense
Feel, and embodiment 1-5 there is no bad smell, it is seen that the culicifuge incense that the present invention develops is safe and environment-friendly that there is the biggest market application
It is worth.
Claims (5)
1. a Folium Artemisiae Argyi anophelifuge pastil, it is characterised in that: it is made up of the raw material of following weight portion: wormwood extract 10-25 part, sweet
Bagasse 20-40 part, Eucalyptus corium farinosum 8-15 part and carbon dust 3-10 part.
Folium Artemisiae Argyi anophelifuge pastil the most according to claim 1, it is characterised in that: described wormwood extract preparation method is:
(1) pre-treatment: take the Folium Artemisiae Argyi Herb without infection process, goes root to clean, dries in the shade, pulverize, obtain Folium Artemisiae Argyi coarse powder A, standby;
(2) seepage pressure effects: put into by A in percolator, adds pure water, adds a cover percolation 5-7 days, and filtrate crosses 400 mesh sieves, obtains filter
Liquid;Filtering residue continues to add water percolation 2-3 time, after merging liquor B;
(3) concentrate: liquor B is concentrated in concentrator and makes wormwood extract;
The 1.2-1.5g Han dry in described wormwood extract.
Folium Artemisiae Argyi anophelifuge pastil the most according to claim 2, it is characterised in that: described (2) seepage pressure effects percolation material water for the first time
Ratio is 1:5-8;Second and third percolation material-water ratio is 1:2-5.
Folium Artemisiae Argyi anophelifuge pastil the most according to claim 2, it is characterised in that: described (3) concentration condition be thickening temperature be 65-
70 DEG C, pressure is-0.01--0.04Mpa.
5. the preparation method of Folium Artemisiae Argyi anophelifuge pastil described in claim 1, it is characterised in that: described preparation method is entered as follows
OK:
One, wormwood extract is produced;
Two, by bagasse, 400 mesh it are crushed to by bark powder;
Three, required each component is put into agitator, mix homogeneously in proportion;Mosquito incense pressing machine extrudes the material into type;
Four, dehydrate in exsiccator, controls water content 3-7%, subpackage, to obtain final product.
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Cited By (2)
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CN106822976A (en) * | 2017-03-28 | 2017-06-13 | 安徽中煦环保新材料科技有限公司 | A kind of natural environmental-protective material with fresh air and preparation method thereof |
CN113367163A (en) * | 2021-05-28 | 2021-09-10 | 天津科技大学 | Natural insect-expelling sterilizing incense and preparation method thereof |
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CN1784979A (en) * | 2004-12-10 | 2006-06-14 | 浙江黑猫神蚊香集团有限公司 | Foliu artemisiae argyi type mosquito-repellent incense and its prodn. method |
CN101156570A (en) * | 2007-08-13 | 2008-04-09 | 江西山峰日化有限公司 | Chinese mugwort leaves oil composite type disc type mosquito-repellent incense and method for making same |
CN101816314A (en) * | 2009-11-20 | 2010-09-01 | 于秉礼 | Argy wormwood smokeless ignition incense |
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Title |
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徐映明: "《农药施用技术》", 30 June 1999, 化学工业出版社 * |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106822976A (en) * | 2017-03-28 | 2017-06-13 | 安徽中煦环保新材料科技有限公司 | A kind of natural environmental-protective material with fresh air and preparation method thereof |
CN113367163A (en) * | 2021-05-28 | 2021-09-10 | 天津科技大学 | Natural insect-expelling sterilizing incense and preparation method thereof |
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Application publication date: 20161221 |